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    Tytuł:
    Effect Of The Desorption-Recombination Temperature On The Microstructure And Magnetic Properties Of HDDR Processed Nd-Fe-B Powders
    Wpływ temperatury desorpcji-rekombinacji na mikrostrukturę i właściwości magnetyczne proszków Nd-Fe-B przetwarzanych metodą HDDR
    Autorzy:
    Lee, J.-G.
    Cha, H.-R.
    Liu, S.
    Yu, J.-H.
    Baek, Y.-K.
    Kwon, H.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/353723.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B
    HDDR
    permanent magnet
    grain boundary
    metoda HDDR
    magnes trwały
    granica ziarna
    Opis:
    The effect of the desorption-recombination temperature on the microstructure and magnetic properties of hydrogenation-disproportionation-desorption-recombination (HDDR) processed Nd-Fe-B powders was studied. The NdxB6.4Ga0.3Nb20.2Febal (x=12.5-13.5, at.%) casting alloys were pulverized after homogenizing annealing, and then subjected to HDDR treatment. During the HDDR process, desorption-recombination (DR) reaction was induced at two different temperature, 810°C and 820°C. The higher Nd content resulted in enhanced coercivity of the HDDR powder, and which was attributed to the thicker and more uniform Nd-rich phase along grain boundaries. But this uniform Nd-rich phase induced faster grain growth. The remanence of the powder DR-treated at 820°C is higher than that DR-treated at 810°C. In addition, it was also confirmed that higher DR temperature is much more effective to improve squareness.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1499-1501
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Rapid Synthesis of Gold Nano-Particles Using Pulse Waved Potential in a Non-Aqueous Electrolyte
    Autorzy:
    Jang, J. G.
    Lee, J.-O.
    Lee, C. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/352529.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    gold
    nanoparticle
    nonaqueous electrolyte
    pulse wave
    catalyst
    Opis:
    Rapid synthesis of gold nanoparticles (AuNPs) by pulsed electrodeposition was investigated in the non-aqueous electrolyte, 1-ethyl-3-methyl-imidazoliumbis(trifluoro- methanesulfonyl)imide ([EMIM]TFSI) with gold trichloride (AuCl3). To aid the dissolution of AuCl3, 1-ethyl-3-methyl-imidazolium chloride ([EMIM]Cl) was used as a supporting electrolyte in [EMIM]TFSI. Cyclicvoltammetry experiments revealed a cathodic reaction corresponding to the reduction of gold at −0.4 V vs. Pt-QRE. To confirmthe electrodeposition process, potentiostatic electrodeposition of gold in the non-aqueous electrolyte was conducted at −0.4 V for 1 h at room temperature. To synthesize AuNPs, pulsed electrodeposition was conducted with controlled duty factor, pulse duration, and overpotential. The composition, particle-size distribution, and morphology of the AuNPs were confirmed by field-emission scanning electron microscopy (FE-SEM), energy-dispersive spectroscopy (EDS), and transmission electron microscopy (TEM). The electrodeposited AuNPs were uniformly distributed on the platinum electrode surface without any impurities arising from the non-aqueous electrolyte. The size distribution of AuNPs could be also controlled by the electrodeposition conditions.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1389-1392
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Valorization of Cobalt from Waste LIB Cathode through Cobalt Oxalate and Cobalt Oxide Synthesis by Leaching-Solvent Extract-Precipitation Stripping
    Autorzy:
    Swain, B.
    Lee, J.-C.
    Lee, C.-G.
    Powiązania:
    https://bibliotekanauki.pl/articles/352333.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    valorization of cobalt
    cobalt oxide powder
    rod-shaped cobalt oxalate
    precipitation stripping
    Opis:
    An ecoefficient, economical and sustainable valorization process for the synthesis of Co3O4 from waste lithium-ion battery (LIB) by leaching-solvent extract-scrubbing-precipitation stripping route has been developed. Through an optimization, the waste LIB cathode was leached using 2000 mole/m3 of H2SO4 and 5 Vol. % of the H2O2 at a pulp density of 100 kg/m3 under leaching time 60 minutes and temperature 75°C. From the separated leach liquor, cobalt was purified by saponified Cyanex 272. From cobalt, loaded Cyanex 272 impurities were scrubbed and the CoC2O4·2H2O was recovered through precipitation stripping. Finally, the precipitate was calcined to synthesize Co3O4, which is a precursor for LIB cathode materials manufacturing. From TGA-DTA, followed by XRD analysis it was confirmed that at 200°C the CoC2O4·2H2O can be converted to anhydrous CoC2O4 and at 350°C the anhydrous can be converted to Co3O4 and at 1100°C the Co3O4 can be converted to CoO. Through reported route waste LIB can back to LIB manufacturing process through a versatile and flexible industrial approach.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 2; 1037-1042
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Phase Transformation And Mechanical Properties Of Ti-12.1Mo-1Fe Alloy With Nano-Sized Precipitation
    Przemiany fazowe i właściwości mechaniczne stopu Ti-12.1Mo-1Fe z nanometrycznymi wydzieleniami
    Autorzy:
    Lee, D.-G.
    Seo, J.
    Li, Ch.
    Lee, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/352551.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    age hardening
    Omega phase
    Ti-Mo-Fe alloy
    precipitation
    hartowanie
    faza omega
    stop Ti-Mo-Fe
    wydzielenia
    Opis:
    Microstructural characterization and aging hardening behaviors of a new designed Ti-12.1Mo-1Fe alloy during solution treatment and aging were investigated in the present study. It is well known that when β-Ti alloys are generally under solution treatment or aging, α phases and ω phases appear or disappear dependent on heat treatment temperature and holding time. It is very necessary to understand the phase transformation phenomenon and to control the microstructure because these phases can control the drastic changes of the mechanical and physical properties of these alloys. According to the calculated [Mo]eq value and the microstructural observation, the β-transus temperature was about 780°. After the solution treatment, this alloy was composed of the β-phase and the microstructure mainly consisted of the equiaxed β grains with the average size of 25 μm. ω phases which were precipitated during aging process, played a more important role to the hardening effect than α phases. The highest hardness value of Ti-12.1Mo-1Fe alloy showed in the condition of the aging temperature of 450°. The hardening due to ω-phase precipitation can lead to a high hardness about 480 Hv but the coarse α-phase result in hardness below 300 Hv.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1393-1396
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Atomistic Analysis Of Radiation-Induced Segregation In Ion-Irradiated Stainless Steel 316
    Analiza w skali atomowej indukowanej promieniowaniem segregacji w stali nierdzewnej 316
    Autorzy:
    Lee, G.-G.
    Jin, H.-H.
    Chang, K.
    Lee, B. H.
    Kwon, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/354713.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    atom probe tomography (APT)
    radiation-induced segregation (RIS)
    ion irradiation
    irradiation defects
    stainless steel
    APT
    RIS
    stal nierdzewna
    segregacja
    Opis:
    Stainless steel (SS) is a well-known material for the internal parts of nuclear power plants. It is known that these alloys exhibit radiation-induced segregation (RIS) at point defect sinks at moderate temperature, while in service. The RIS behavior of SS can be a potential problem by increasing the susceptibility to irradiation-assisted stress corrosion cracking. In this work, the RIS behavior of solute atoms at sinks in SS 316 irradiated with Fe4+ ions were characterized by atom probe tomography (APT). There were torus-shaped defects along with a depletion of Cr and enrichment of Ni and Si. These clusters are believed to be dislocation loops resulting from irradiation. The segregation of solutes was also observed for various defect shapes. These observations are consistent with other APT results from the literature. The composition of the clusters was analyzed quantitatively almost at the atomic scale. Despite the limitations of the experiments, the APT analysis was well suited for discovering the structure of irradiation defects and performing a quantitative analysis of RIS in irradiated specimens.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1179-1184
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Study On Dispersion Stability Of Nickel Nanoparticles Synthesized By Wire Explosion In Liquid Media
    Badanie stabilności dyspersji nanocząstek niklu wytworzonych metodą WEP w ciekłym medium
    Autorzy:
    Kim, C. K.
    Lee, G.-J.
    Lee, M. K.
    Rhee, C. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/356909.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    nickel nanofluid
    pulsed wire evaporation
    surfactant
    zeta potential
    dispersion stability
    nanocząstka niklu
    środek powierzchniowo czynny
    stabilność dyspersji
    potencjał zeta
    dyspersja
    Opis:
    In this study, nickel nanoparticles were synthesized in ethanol using portable pulsed wire evaporation, which is a one-step physical method. From transmission electron microscopy images, it was found that the Ni nanoparticles exhibited a spherical shape with an average diameter of 7.3 nm. To prevent aggregation of the nickel nanoparticles, a polymer surfactant was added into the ethanol before the synthesis of nickel nanoparticles, and adsorbed on the freshly synthesized nickel nanoparticles during the wire explosion. The dispersion stability of the prepared nickel nanofluids was investigated by zeta-potential analyzer and Turbiscan optical analyzer. As a result, the optimum concentration of polymer surfactant to be added was suggested for the maximized dispersion stability of the nickel nanofluids.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1379-1382
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects of acute lipopolysaccharide-induced toxemia model on some neglected blood parameters
    Autorzy:
    Adam, G.O.
    Lee, H.R.
    Lee, S.J.
    Kim, S.J.
    Kim, G.B.
    Kang, H.S.
    Powiązania:
    https://bibliotekanauki.pl/articles/2087627.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Toxemia
    lipopolysaccharide
    base excess
    pH
    animal model
    Źródło:
    Polish Journal of Veterinary Sciences; 2018, 21, 4; 665-671
    1505-1773
    Pojawia się w:
    Polish Journal of Veterinary Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Extraction Factor Of Pure Ammonium Paratungstate From Tungsten Scraps
    Współczynnik ekstrakcji czystego parawolframianu amonu z odpadów wolframowych
    Autorzy:
    Pee, J-H.
    Kim, G. H.
    Lee, H. Y.
    Kim, Y. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/356567.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    raw material
    recycling
    ammonium paratungstate
    tungsten scraps
    extraction
    surowce
    recykling
    parawolfrawian amonu
    odpady wolframowe
    ekstrakcja
    Opis:
    Typical oxidation process of tungsten scraps was modified by the rotary kiln with oxygen burner to increase the oxidation rate of tungsten scraps. Also to accelerate the solubility of solid oxidized products, the hydrothermal reflux method was adapted. By heating tungsten scraps in rotary kiln with oxygen burner at around 900° for 2hrs, the scraps was oxidized completely. Then oxidized products (WO3 and CoWO4) was fully dissolved in the solution of NaOH by hydrothermal reflux method at 150° for 2hrs. The dissolution rate of oxidized products was increased with increasing the reaction temperature and concentration of NaOH. And then CaWO4 and H2WO4 could be generated from the aqueous sodium tungstate solution. Ammonium paratungstate (APT) also could be produced from tungstic acid using by aqueous ammonium solution. The morphologies (cubic and plate types) of APT was controlled by the stirring process of purified solution of ammonium paratungstate.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1403-1405
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Extraction Factor Of Tungsten Sources From Tungsten Scraps By Zinc Decomposition Process
    Współczynnik ekstrakcji związków wolframu z odpadów wolframowych w procesie rozkładu cynku
    Autorzy:
    Pee, J-H.
    Kim, G. H.
    Lee, H. Y.
    Kim, Y. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/354774.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    raw material
    recycling
    zinc decomposition process
    tungsten carbide
    tungstic acid
    surowce
    recykling
    proces rozkładu cynku
    węglik wolframu
    kwas wolframowy
    Opis:
    Decomposition promoting factors and extraction process of tungsten carbide and tungstic acid powders in the zinc decomposition process of tungsten scraps which are composed mostly of tungsten carbide and cobalt were evaluated. Zinc volatility was suppressed by the enclosed graphite crucible and zinc volatilization pressure was produced in the reaction graphite crucible inside an electric furnace for ZDP (Zinc Decomposition Process). Decomposition reaction was done for 2hours at 650°, which 100% decomposed the tungsten scraps that were over 30 mm thick. Decomposed scraps were pulverized under 75μm and were composed of tungsten carbide and cobalt identified by the XRD (X-ray Diffraction). To produce the WC(Tungsten Carbide) powder directly from decomposed scraps, pulverized powders were reacted with hydrochloric acid to remove the cobalt binder. Also to produce the tungstic acid, pulverized powders were reacted with aqua regia to remove the cobalt binder and oxidize the tungsten carbide. Tungsten carbide and tungstic acid powders were identified by XRD and chemical composition analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1311-1314
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Recovery Of Electrodic Powder From Spent Lithium Ion Batteries (LIBs)
    Odzysk proszku elektrodowego z zużytych akumulatorów litowo-jonowych
    Autorzy:
    Shin, S. M.
    Jung, G. J.
    Lee, W-J.
    Kang, C. Y.
    Wang, J. P.
    Powiązania:
    https://bibliotekanauki.pl/articles/354084.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    lithium ion battery
    electrodic powder
    cobalt
    lithium
    thermal treatment
    bateria litowo-jonowa
    proszek elektrodowy
    kobalt
    lit
    obróbka termiczna
    Opis:
    This study was focused on recycling process newly proposed to recover electrodic powder enriched in cobalt (Co) and lithium (Li) from spent lithium ion battery. In addition, this new process was designed to prevent explosion of batteries during thermal treatment under inert atmosphere. Spent lithium ion batteries (LIBs) were heated over the range of 300°C to 600°C for 2 hours and each component was completely separated inside reactor after experiment. Electrodic powder was successfully recovered from bulk components containing several pieces of metals through sieving operation. The electrodic powder obtained was examined by X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDS), and atomic absorption spectroscopy (AA) and furthermore image of the powder was taken by scanning electron microscopy (SEM). It was finally found that cobalt and lithium were mainly recovered to about 49 wt.% and 4 wt.% in electrodic powder, respectively.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1145-1149
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Evaluation of Surface Characteristics and Physical Properties on Biodegradable Magnesium-Calcium Alloys by Anodic Oxidation
    Autorzy:
    Kim, J.
    Lee, J.
    Yang, H.
    Park, S.
    Lim, H.
    Oh, G.
    Yun, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1191716.pdf
    Data publikacji:
    2016-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    87.85.jj
    87.85.jc
    Opis:
    The purpose of this study was to determine the effect of calcium (Ca) on the surface characteristics and physical properties of magnesium-calcium alloys after anodization. A novel binary alloy Mg-xCa (in which x=0.5, 1, or 5 wt.%) was cast by combining magnesium (99.9%) and calcium (99.9%) in an argon gas (99.99%) atmosphere. A magnesium alloy rod having a diameter of 15 mm was cut into discs, each 2 mm thick. The specimens were subjected to anodic oxidation at 120 V for 15 minutes at room temperature in an electrolyte solution consisting of calcium gluconate, sodium hexametaphosphate, and sodium hydroxide. Surface and cross-sectional morphological changes were observed using scanning electron microscopy, and the microstructures and phases were detected by means of X-ray diffraction. Hardness and surface roughness were assessed by means of a Vickers hardness tester and a surface roughness meter, respectively. The results show that the physical properties of these magnesium-calcium alloys have been improved, because it was possible to control the dissolution rate according to the amount of calcium added.
    Źródło:
    Acta Physica Polonica A; 2016, 129, 4; 736-741
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Compositional Dependence of Hardness of Ge-Sb-Se Glass for Molded Lens Applications
    Zależność stężeniowa twardości szkła Ge-Sb-Se do zastosowań na formowane soczewki
    Autorzy:
    Park, J. K.
    Lee, J. H.
    Shin, S. Y.
    Yi, J. H.
    Lee, W. H.
    Park, B. J.
    Choi, J. H.
    Kim, N. Y.
    Choi, Y. G.
    Powiązania:
    https://bibliotekanauki.pl/articles/352228.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    chalcogenide glasses
    Ge-Sb-Se glass
    infrared lens
    molded lens
    infrared camera
    szkło
    Ge-Sb-Se
    soczewki formowane
    twardość szkła
    kamera termowizyjna
    Opis:
    Chalcogenide glass in the ternary Ge-Sb-Se system is inherently moldable, thus being considered as a strong candidate material for use in infrared-transmitting lens applications from the viewpoint of thermal and mechanical stability. In an effort to experimentally determine compositional region suitable for the molded lens applications, we evaluate its compositional dependence of hardness. Among the constituent atoms, Ge content turns out to exert a most conspicuous correlation with hardness. This phenomenological behavior is then explained in connection with the structural evolution that Ge brings about.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1205-1208
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    High Temperature Oxidation Property of SiC Coating Layer Fabricated by Aerosol Deposition Process
    Autorzy:
    Ham, G.-S.
    Kim, S.-H.
    Park, J.-Y.
    Lee, K.-A.
    Powiązania:
    https://bibliotekanauki.pl/articles/352142.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    silicon carbide
    aerosol deposition
    coating
    high temperature oxidation
    Opis:
    This study investigated the high temperature oxidation property of SiC coated layer fabricated by aerosol deposition process. SiC coated layer could be successfully manufactured by using pure SiC powders and aerosol deposition on the Zr based alloy in an optimal process condition. The thickness of manufactured SiC coated layer was measured about 5 μm, and coating layer represented high density structure. SiC coated layer consisted of α-SiC and β-SiC phases, the same as the initial powder. The initial powder was shown to have been crushed to the extent and was deposited in the form of extremely fine particles. To examine the high temperature oxidation properties, oxidized weight gain was obtained for one hour at 1000°C by using TGA. The SiC coated layer showed superior oxidation resistance property than that of Zr alloy (substrate). The high temperature oxidation mechanism of SiC coated layer on Zr alloy was suggested. And then, the application of aerosol deposited SiC coated layer was also discussed.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1347-1351
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Evolution Of Precipitate Morphology During Extrusion In Mg ZK60A Alloy
    Ewolucja morfologii wydzieleń podczas wytłaczania stopu Mg ZK60A
    Autorzy:
    Park, J.
    Jung, K. H.
    Lee, G. A.
    Kawasaki, M.
    Ahn, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/356233.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    magnesium alloy
    ZK60A
    precipitation
    extrusion
    stopy magnezu
    wydzielenia
    wytłaczanie
    Opis:
    In this study, a continuously casted ZK60A magnesium alloy (Mg-Zn-Zr) was extruded in two different extrusion ratios, 6:1 and 10:1. The evolution of precipitates was investigated on the two extruded materials and compared with that of as-casted material. The microstructural analysis was performed by electron backscatter diffraction and transmission electron microscopy, and the compositional information was obtained using energy-dispersive X-ray spectroscopy. Several distinct morphologies of precipitates were observed, such as dot, rod, and disk shaped. The formation mechanisms of those precipitates were discussed with respect to the heat and strain during the extrusion process.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1423-1426
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal Conductivity and Microstructure of Copper Coated Graphite Composite by Spark Plasma Sintering Process
    Autorzy:
    Park, S. H.
    Kim, D. B.
    Lee, R. G.
    Son, I. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/355632.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    metal matrix composites
    thermal conductivity
    thermal expansion
    interfacial bonding
    spark plasma sintering
    Opis:
    This study focuses on the fabrication of thermal management material for power electronics applications using graphite flake reinforced copper composites. The manufacturing route involved electroless plating of copper in the graphite flake and sintering process are optimized. The microstructures, interface, thermal properties, and relative density of graphite/Cu composites are investigated. The relative density of the composites shows 99.5% after sintering. Thermal conductivities and coefficients of thermal expansion of this composites were 400-480 Wm-1K-1 and 8 to 5 ppm k-1, respectively. Obtained graphite nanoplatelets-reinforced composites exhibit excellent thermo-physical properties to meet the heat dispersion and matching requirements of power electronic devices to the packaging materials.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1303-1306
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Optical Properties of Multi-Stacked InAs Quantum Dots Embedded in GaAs/InGaAs Strained Layer and its Annealing Behaviors
    Autorzy:
    Kim, D.
    Kim, G.
    Jeon, S.
    Cho, M.
    Choi, H.
    Kim, M.
    Lee, D.
    Kim, J.
    Eom, G.
    Leem, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1537752.pdf
    Data publikacji:
    2010-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.67.Hc
    78.55.Cr
    81.05.Ea
    Opis:
    Multi-stacked InAs QDs embedded in ten periods of GaAs/$In_{0.1}Ga_{0.9}As$ strained layers were grown by MBE and their optical properties were investigated by using PL spectroscopy. For the QDs embedded in ten periods of GaAs/$In_{0.1}Ga_{0.9}As$ strained layers, the PL intensity is enhanced about 4.7 times and a narrower FWHM of 26 meV is observed compared to those of the conventional multi-stacked QDs. The PL spectra of the InAs QDs show blue-shifts of about 50 meV with increasing annealing temperature up to 850°C. At annealing temperature of 600°C, the FWHM of the PL peak is reduced to 16 meV and PL intensity is enhanced compared to those of the as-grown sample, which indicates improvement of size uniformity and crystal quality of the QDs.
    Źródło:
    Acta Physica Polonica A; 2010, 117, 6; 941-944
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Oxidation Behavior of Steel with Cr Content and Water Flow Rate
    Autorzy:
    Kim, D.-J.
    Kim, K. M.
    Shin, J. H.
    Cheong, Y. M.
    Lee, E. H.
    Lee, G. G.
    Kim, S. W.
    Kim, H. P.
    Choi, M. J.
    Lim, Y. S.
    Hwang, S. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/351548.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    steel
    flow accelerated corrosion
    Cr content
    flow rate
    surface oxides
    Opis:
    Fast water flow facilitates ferrous ion transport leading to flow accelerated corrosion (FAC) of carbon steel and the possibility of a large accident through a failure of a secondary pipe in a nuclear power plant. Ion transport is directly linked to oxide properties such as the thickness, chemical composition and porosity. This work deals with a precise observation of the cross section of the corroded specimen focusing on an oxide passivity and its thickness using SEM (scanning electron microscope) and TEM (transmission electron microscope) as well as an apparent weight loss and a surface observation for the specimens corroded using a rotating cylindrical electrode autoclave system in pure water of pH 7 at 150°C having dissolved oxygen below 1 ppb within a flow rate range of 0 to 10 m/s. The Cr content in steel was changed from 0.02 to 2.4 wt%. Increasing the Cr content in the alloy, the FAC rate and oxide thickness decreased. The oxide porosity tends to decrease with the Cr content and immersion time owing to the development of Cr containing oxide. The oxidation behavior is not changed with the immersion time.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1383-1387
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication and Characterization of CoCrFeNiMn High Entropy Alloy Powder Processed by Gas Atomization
    Autorzy:
    Park, T. G.
    Lee, S. H.
    Lee, B.
    Cho, H. M.
    Choi, W. J.
    Kim, B. S.
    Shin, K. S.
    Kim, T.-S.
    Powiązania:
    https://bibliotekanauki.pl/articles/353649.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    high entropy alloy
    gas atomization
    spark plasma sintering
    CoCrFeNiMn
    Opis:
    In this study, precisely controlled large scale gas atomization process was applied to produce spherical and uniform shaped high entropy alloy powder. The gas atomization process was carried out to fabricate CoCrFeNiMn alloy, which was studied for high ductility and mechanical properties at low temperatures. It was confirmed that the mass scale, single phase, equiatomic, and high purity spherical high entropy alloy powder was produced by gas atomization process. The powder was sintered by spark plasma sintering process with various sintering conditions, and mechanical properties were characterized. Through this research, we have developed a mass production process of high quality and spherical high entropy alloy powder, and it is expected to expand applications of this high entropy alloy into fields such as powder injection molding and 3D printing for complex shaped components.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 2; 1055-1059
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Growth and Characterization of Indium-Doped Zinc Oxide Thin Films Prepared by Sol-Gel Method
    Autorzy:
    Kim, M.
    Yim, K.
    Kim, S.
    Nam, G.
    Lee, D.
    Kim, Jin
    Kim, Jong
    Leem, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1491351.pdf
    Data publikacji:
    2012-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Dz
    81.20.Fw
    78.66.Hf
    Opis:
    Indium-doped ZnO thin films were deposited by sol-gel spin-coating method with various In content. The effects of In content on the structural and optical properties of the indium-doped ZnO thin films were investigated by scanning electron microscopy, X-ray diffraction, and UV-visible spectroscopy. The particle-like surface morphology and the crystallinity of the indium-doped ZnO thin films were affected by change in the In content, especially at the In content of 3 at.%. The values of direct band gap were decreased with increase in the In content. The width of localized states in the optical band gap of the indium-doped ZnO thin films were changed with In content and the Urbach energy $(E_{U})$ was changed inversely with optical band gap of the indium-doped ZnO thin films.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 1; 217-220
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Studies on the effect of coal particle size on biodepyritization of high sulfur coal in batch bioreactor
    Autorzy:
    Singh, S.
    Srichandan, H.
    Pathak, A.
    Gahan, Ch. S.
    Lee, S.
    Kim, D. J.
    Kim, B. G.
    Powiązania:
    https://bibliotekanauki.pl/articles/778523.pdf
    Data publikacji:
    2015
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    biodepyritization
    coal
    pyrite
    stirred tank bioreactor
    Opis:
    The moderate thermophilic mix culture bacteria were used to depyritize the Illinois coal of varying particle sizes (-100 μm, 100-200 μm, +200 μm). Mineral libration analysis showed the presence of pyrite along with other minerals in coal. Microbial depyritization of coal was carried out in stirred tank batch reactors in presence of an iron-free 9K medium. The results indicate that microbial depyritization of coal using moderate thermophiles is an efficient process. Moreover, particle size of coal is an important parameter which affects the efficiency of microbial depyritization process. At the end of the experiment, a maximum of 75% pyrite and 66% of pyritic sulphur were removed from the median particle size. The XRD analysis showed the absence of pyrite mineral in the treated coal sample. A good mass balance was also obtained with net loss of mass ranging from 5-9% showing the feasibility of the process for large scale applications.
    Źródło:
    Polish Journal of Chemical Technology; 2015, 17, 1; 97-102
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Self-Consolidation Mechanism Of Porous Ti-6Al-4V Implant Prototypes Produced By Electro-Discharge-Sintering Of Spherical Ti-6Al-4V Powders
    Mechanizm autokonsolidacji prototypów porowatych implantów wytworzonych przez spiekanie sferycznych proszków Ti-6Al-4V
    Autorzy:
    Lee, W. H.
    Jo, Y. J.
    Kim, Y. H.
    Jo, Y. H.
    Seong, J. G.
    Van Tyne, C. J.
    Chang, S. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/356277.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ti-6Al-4V
    implant
    porous
    sintering
    electrodischarge
    porowatość
    spiekanie
    proszki spiekane
    Opis:
    Electro-Discharge-Sintering (EDS) was employed to fabricate Ti-6Al-4V porous implant prototypes from atomized powders (100 – 150 μm), that were subjected to discharges of 0.75 to 2.0 kJ/0.7g-powder from 150, 300, and 450 μF capacitors. Both fully porous and porous-surfaced Ti-6Al-4V compacts with various solid core sizes were self-consolidated in less than 86 – 155 μsec. It is known that EDS can simultaneously produce the pinch pressure to squeeze and deform powder particles and the heat to weld them together. The formation of a solid core in these prototypes depends on the amounts of both the pinch pressure and heat generated during a discharge. The size of the solid core and the thickness of the porous layer can be successfully controlled by manipulating the discharge conditions such as input energy and capacitance.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1185-1189
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    ZnO Nanorods on Nanofibrous ZnO Seed Layers by Hydrothermal Method and Their Annealing Effects
    Autorzy:
    Yim, K.
    Jeon, S.
    Kim, M.
    Kim, S.
    Nam, G.
    Lee, D.
    Kim, Jin
    Kim, Jong
    Leem, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1491348.pdf
    Data publikacji:
    2012-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Dz
    81.15.Lm
    78.55.Et
    Opis:
    ZnO nanorods were grown by using the hydrothermal method on p-type Si (100) substrates with nanofibrous ZnO seed layers. Before the ZnO nanorods growth, nanofibrous ZnO seed layers were spin-coated onto the Si substrates. The structural and optical properties of ZnO nanorods were characterized by scanning electron microscopy, X-ray diffraction, and photoluminescence. The fibrous ZnO nanorods is possible due to the surface morphology of the nanofibrous ZnO seed layers. To investigate annealing effects of the ZnO nanorods, the post-annealing process was carried out at various temperatures ranging from 300 to 700C under argon conditions. The structural and optical properties of the ZnO nanorods were also affected by the post-annealing treatment.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 1; 214-216
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Carbon Co-Deposition During Gas Reduction of Water-Atomized Fe-Cr-Mo Powder
    Autorzy:
    Ali, B.
    Choi, S. H.
    Seo, S. J.
    Maeng, D. Y.
    Lee, C. G.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/352709.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    water atomization
    Fe-based powder
    oxide reduction
    powder metallurgy
    sinter-hardening alloys
    Opis:
    The water atomization of iron powder with a composition of Fe-3Cr-0.5Mo (wt.%) at 1600°C and 150 bar creates an oxide layer, which in this study was reduced using a mixture of methane (CH4) and argon (Ar) gas. The lowest oxygen content was achieved with a 100 cc/min flow rate of CH4, but this also resulted in a co-deposition of carbon due to the cracking of CH4. This carbon can be used directly to create high-quality, sinter hardenable steel, thereby eliminating the need for an additional mixing step prior to sintering. An exponential relationship was found to exist between the CH4 gas flow rate and carbon content of the powder, meaning that its composition can be easily controlled to suit a variety of different applications.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1119-1124
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication and Characterization of GaN/Polymer Composite p-n Junction with PEDOT Nanoparticle Interface Layer
    Autorzy:
    Kim, M.
    Jin, S.
    Choi, H.
    Kim, G.
    Yim, K.
    Kim, S.
    Nam, G.
    Yoon, H.
    Kim, Y.
    Lee, D.
    Kim, Jin
    Kim, Jong
    Leem, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1505152.pdf
    Data publikacji:
    2011-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    73.61.Ey
    81.15.Gh
    Opis:
    A heavily Si-doped GaN/polymer hybrid structure with p-type poly(3,4-ethylene-dioxythiophene):beta-1,3-glucan (PEDOT nanoparticle) interface layer has been fabricated. The Si-doped GaN thin film with carrier concentration of 1 × $10^{19} cm^{-3}$ was grown by metal-organic chemical vapor deposition. The PEDOT nanoparticle with various sizes ranging from 60 to 120 nm was synthesized via a miniemulsion polymerization process. The electrical conductivity of the PEDOT nanoparticle is less than 1.2 S/cm. The current-voltage (I-V) characteristic of the hybrid structure shows diode-like behavior. The I-V characteristic was examined in the framework of the thermionic emission model. The ideality factor of the structure without PEDOT nanoparticle interface layer is 12.9. However, the ideality factor of the hybrid structure with PEDOT nanoparticle interface layer is obtained as 1.9. The value of ideality factor is dramatically decreased by inserting the PEDOT nanoparticle interface layer.
    Źródło:
    Acta Physica Polonica A; 2011, 119, 6; 875-879
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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