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Tytuł:
Graphite Nanosheet Exfoliation From Graphite Flakes Through Functionalization Using Phthalic Acid
Złuszczanie nanoarkuszy grafitu z płatków grafitu przy użyciu kwasu ftalowego
Autorzy:
Kim, J. H.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/351457.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
exfoliation
graphite nanosheet
functionalization
grafting molecule
Friedel-Crafts acylation
złuszczanie
nanoarkusz grafitu
funkcjonalizacja
kwas ftalowy
acylowanie Friedela-Craftsa
Opis:
In order to fabricate graphite nanosheets from graphite flakes, edge-functionalized graphite nanosheets were prepared by a functionalization method using phthalic acid as the molecule to be grafted. A polyphosphoric acid/P2O5 solution containing graphite and phthalic acid were heated at different temperatures for 72 h in a nitrogen atmosphere. It was confirmed by transmission electron microscopy and atomic force microscopy that the resultant phthalic acid-functionalized graphite nanosheets had a large surface area of 20.69 μm2 in average and an average thickness of 1.39 nm. It was also found by X-ray diffractometry and Fourier transform infrared spectroscopy (FT-IR) analysis that the functionalization caused the formation of C=O bonds at the edges of the graphite nanosheets. The yield from this functionalization method was found to be dependent on the reaction temperature, only when it is between 70 and 130°C, because of the dehydration of phthalic acid at higher temperatures. This was confirmed by FT-IR analysis and the observation of low thermal energies at low temperatures.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1251-1255
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of Submicroscale Ag-Coated Cu Particles by Multi-Step Addition of Ag Plating Solution and Antioxidation Properties for Different Ag Shell Thicknesses
Autorzy:
Choi, E. B.
Lee, J.-H.
Powiązania:
https://bibliotekanauki.pl/articles/351202.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ag-coated Cu particle
submicrometer
Glycol-based Ag plating solution
mult-step addition
antioxidation
Opis:
For application as a low-cost conductive filler material, submicroscale Cu@Ag particles were fabricated at room temperature without any reductants by a multi-step addition method using an ethylene glycol-based Ag plating solution. Scanning electron microscopy images of the Ag-coated Cu particles demonstrated the formation of discrete Ag particles less than 100 nm in size as well as a thin Ag coating on Cu particles, during the early addition steps. However, as the thickness of the Ag coating increased, the small Ag particles agglomerated into Ag coatings with an increase in the number of Ag plating steps. Owing to the absence of additives such as surfactants, a comparison between the microstructural images and calculations indicated increased agglomeration between fabricated Ag-coated Cu particles with an increase in the number of Ag plating steps. However, thermogravimetric-differential scanning calorimetry of the agglomerated Ag-coated Cu particles after the fifth addition of the Ag plating solution demonstrated their antioxidation behavior even after 70 min in air at 150°C.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1137-1142
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects Of Process Parameters On Cu Powder Synthesis Yield And Particle Size In A Wet-Chemical Process
Wpływ parametrów procesu na wydajność syntezy proszku Cu i wielkości cząstek w procesie mokrym chemicznym
Autorzy:
Shin, Y. M.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/354168.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
wet-chemical process
micron-size Cu powder
Synthesis yield
particle size
gibbs free energy difference
proszek Cu
proces chemiczny mokry
wydajność syntezy
rozmiar cząsteczki
różnica energii swobodnej Gibbsa
Opis:
This study presents a simple wet-chemical process to prepare several micron-size Cu powders. Moreover, changes in powder synthesis yield and particle size are examined with different solvents, synthesis temperatures, and amounts of reducing agent during the synthesis. As a reducing agent and capping agent, L-ascorbic acid and polyvinyl pyrrolidone were used, respectively. The yields in distilled water or an ethylene glycol (EG)/distilled water mixture were higher than that in EG alone, and the yield increased with increasing temperature owing to a lower Δ Gred value. Increasing the L-ascorbic acid concentration also increased the yield. The Cu powder synthesized in 3 h at 90°C in distilled water with 272.8 mM of L-ascorbic acid showed the lowest average particle size of 2.52 μm, indicating mechanisms of short burst nucleation and reduced growth via the increased reduction rate of Cu ions. It is estimated that the nucleation step was nearly completed within 10 min in this system. The Cu powders synthesized in an ethylene glycol/distilled water mixture presented an average particle size of 3.76 μm and the highest yield of 87.9%.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1247-1250
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Transient Liquid Phase Behavior of Sn-Coated Cu Particles and Chip Bonding using Paste Containing the Particles
Autorzy:
Hwang, J. H.
Lee, J.-H.
Powiązania:
https://bibliotekanauki.pl/articles/353042.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Sn-coated Cu
immersion plating
chip bonding
intermetallic compounds (IMC)
transient liquid phase (TLP)
sintering
Opis:
Sn-coated Cu particles were prepared as a filler material for transient liquid phase (TLP) bonding. The thickness of Sn coating was controlled by controlling the number of plating cycles. The Sn-coated Cu particles best suited for TLP bonding were fabricated by Sn plating thrice, and the particles showed a pronounced endothermic peak at 232°C. The heating of the particles for just 10 s at 250°C destroyed the initial core-shell structure and encouraged the formation of Cu-Sn intermetallic compounds. Further, die bonding was also successfully performed at 250°C under a slight bonding pressure of around 0.1 MPa using a paste containing the particles. The bonding time of 30 s facilitated the bonding of Sn-coated Cu particles to the Au surface and also increased the probability of network formation between particles.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1143-1148
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Fatigue Fracture Study on TDCB Aluminum Foam Specimen of Type Mode III Bonded with Adhesive
Autorzy:
Lee, J. H.
Cho, J. U.
Powiązania:
https://bibliotekanauki.pl/articles/356731.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum foam
fatigue fracture
fatigue analysis
load
Mode III type
specimen thickness
Opis:
This paper studies the characteristics of junction structure of closed-cell type aluminum foam, which is generally used as a shock absorber. TDCB specimens were designed for mode III type with thickness as a variable and performed a fatigue experiment on them by thickness. As the result, the load value of all specimens peaks under 0 to 25 cycles and decreases as the cycles increase. As the specimen thickens by 10 mm, the maximum load value is 1.2 times. When the thickness increases by 20 mm, the maximum value increases by 1.5 times. This study result can be utilized by investigating the mechanical characteristics of TDCB specimens for mode III type under fatigue loading conditions systematically and efficiently.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1359-1362
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Compressive Deformation Behavior of Thick Micro-Alloyed HSLA Steel Plates at Elevated Temperatures
Autorzy:
Lee, J.-H.
Kim, D.-O.
Lee, K.
Powiązania:
https://bibliotekanauki.pl/articles/351774.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
alloys
rolling
strain rate
compression test
HSLA steel
Opis:
The hot deformation behavior of a heavy micro-alloyed high-strength low-alloy (HSLA) steel plate was studied by performing compression tests at elevated temperatures. The hot compression tests were carried out at temperatures from 923 K to 1,223 K with strain rates of 0.002 s-1 and 1.0 s-1. A long plateau region appeared for the 0.002 s-1 strain rate, and this was found to be an effect of the balancing between softening and hardening during deformation. For the 1.0 s-1 strain rate, the flow stress gradually increased after the yield point. The temperature and the strain rate-dependent parameters, such as the strain hardening coefficient (n), strength constant (K), and activation energy (Q), obtained from the flow stress curves were applied to the power law of plastic deformation. The constitutive model for flow stress can be expressed as σ = (39.8 ln (Z) – 716.6) · ε(−0.00955ln(Z) + 0.4930) for the 1.0 s-1 strain rate and σ = (19.9ln (Z) – 592.3) · ε(−0.00212ln(Z) + 0.1540) for the 0.002 s-1 strain rate.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1191-1196
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Towards Safe Navigation by Formalizing Navigation Rules
Autorzy:
Kreutzmann, A.
Wolter, D.
Dylla, F.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/117627.pdf
Data publikacji:
2013
Wydawca:
Uniwersytet Morski w Gdyni. Wydział Nawigacyjny
Tematy:
safety of navigation
Navigation Rules
artificial intelligence
Spatio-temporal Logics
Opis:
One crucial aspect of safe navigation is to obey all navigation regulations applicable, in particular the collision regulations issued by the International Maritime Organization (IMO Colregs). Therefore, decision support systems for navigation need to respect Colregs and this feature should be verifiably correct. We tackle compliancy of navigation regulations from a perspective of software verification. One common approach is to use formal logic, but it requires to bridge a wide gap between navigation concepts and simple logic. We introduce a novel domain specification language based on a spatio‐temporal logic that allows us to overcome this gap. We are able to capture complex navigation concepts in an easily comprehensible representation that can directly be utilized by various bridge systems and that allows for software verification.
Źródło:
TransNav : International Journal on Marine Navigation and Safety of Sea Transportation; 2013, 7, 2; 161-168
2083-6473
2083-6481
Pojawia się w:
TransNav : International Journal on Marine Navigation and Safety of Sea Transportation
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Quantitative Analysis of Cryomilled Nanocrystalline Ti-6Al-4V Alloy Powder by X-Ray Diffraction
Autorzy:
Oh, M.
Yu, H. K.
Lee, J.-H.
Oh, M. C.
Jung, S.-H.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/356265.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nanocrystalline
cryomilling
Ti alloy
X-ray diffraction
size-strain plot method
Opis:
A nanocrystalline Ti alloy powder was fabricated using cryomilling. The grain size and lattice strain evolution during cryomilling were quantitatively analyzed using X-ray diffraction (XRD) based on the Scherrer equation, Williamson-Hall (W-H) plotting method, and size-strain (S-S) method assuming uniform deformation. Other physical parameters including stress and strain have been calculated. The average crystallite size and the lattice strain evaluated from XRD analysis are in good agreement with the result of transmission electron microscopy (TEM).
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1439-1442
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology Change Of Si Deposit In Molten Salt Electrorefining
Zmiana morfologii osadu Si podczas elektrorafinacji w stopionych solach
Autorzy:
Ryu, H. Y.
Kwon, S. C.
Han, M. H.
An, Y. S.
Lee, J. S.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/354346.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
molten salt
silicon
morphology
electrorefining
current density
sól stopiona
krzem
morfologia
elektrorafinacja
gęstość prądu
Opis:
The effects of processing parameters on the morphology change in a Si deposit recovered by means of molten salt electrorefining are evaluated using electrochemical techniques such as cyclic voltammetry and chronopotentiometry at 800°C. It was found that concentration of K2SiF6 and current density were important parameters in determining deposit size. Higher concentrations of K2SiF6 were effective in coarsening the silicon deposit and decreasing the cell potential. Silicon nanofiber was recovered at 5 wt% of K2SiF6 whereas dense particles were prepared at 30 and 50 wt% of K2SiF6. The morphology of the Si deposit was determined by the concentration of Si in the electrolyte which is related to the formation of crystal and growth of Si. The formation mechanism of the Si deposit was interpreted by using high resolution TEM as well as electrochemical properties.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1491-1497
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Compositional Dependence of Hardness of Ge-Sb-Se Glass for Molded Lens Applications
Zależność stężeniowa twardości szkła Ge-Sb-Se do zastosowań na formowane soczewki
Autorzy:
Park, J. K.
Lee, J. H.
Shin, S. Y.
Yi, J. H.
Lee, W. H.
Park, B. J.
Choi, J. H.
Kim, N. Y.
Choi, Y. G.
Powiązania:
https://bibliotekanauki.pl/articles/352228.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chalcogenide glasses
Ge-Sb-Se glass
infrared lens
molded lens
infrared camera
szkło
Ge-Sb-Se
soczewki formowane
twardość szkła
kamera termowizyjna
Opis:
Chalcogenide glass in the ternary Ge-Sb-Se system is inherently moldable, thus being considered as a strong candidate material for use in infrared-transmitting lens applications from the viewpoint of thermal and mechanical stability. In an effort to experimentally determine compositional region suitable for the molded lens applications, we evaluate its compositional dependence of hardness. Among the constituent atoms, Ge content turns out to exert a most conspicuous correlation with hardness. This phenomenological behavior is then explained in connection with the structural evolution that Ge brings about.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1205-1208
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
$SiO_x$ Nanowires Produced on Molybdenum-Coated Si Substrates
Autorzy:
Kim, H.
Lee, J.
Yang, J.
Powiązania:
https://bibliotekanauki.pl/articles/1813396.pdf
Data publikacji:
2008-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
We synthesized $SiO_x$ nanowires with diameters of 30-140 nm, for the first time by the simple heating of the Mo-coated Si substrates. X-ray diffraction, selected area electron diffraction, and energy-dispersive X-ray spectroscopy indicated that the nanowires were in an amorphous state, comprising Si and O only. Fitting the photoluminescence spectrum with Gaussian functions revealed that the nanowires exhibited significant photoluminescence intensities near blue and green light regions. We extensively discussed the possible growth mechanism of $SiO_x$ nanowires.
Źródło:
Acta Physica Polonica A; 2008, 113, 3; 1017-1020
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Immobilization of rambutan (Nephelium lappaceum) peel as a sorbent for Basic Fuchsin removal
Autorzy:
Lee, H.-J.
Ong, S.-T.
Powiązania:
https://bibliotekanauki.pl/articles/207651.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
fuchsin
Fourier transform infrared spectrophotometry
FTIR
Nephelium lappaceum
fuksyna
spektroskopia w podczerwieni z transformatą Fouriera
Opis:
The potential of rambutan (Nephelium lappaceum) peel as a low-cost adsorbent in an immobilized condition to remove Basic Fuchsin from aqueous solution was studied. The effect of initial dye concentration, contact time, pH and adsorbent dosage for the dye removal was studied at room temperature (26±2 °C). Infrared spectrum of rambutan peel indicates the presence of C–O, –OH and C=C functional groups. The adsorption rate was found to be high at the first 30 min and the process reached equilibrium after 3 h with more than 80% of dye being removed. The uptake of Basic Fuchsin was more promising at pH slightly above 7. The study of sorption model and kinetic model showed that the adsorption of Basic Fuchsin on rambutan peel conformed to the Freundlich isotherm and pseudo-second order kinetics with a high correlation coefficient, R,sup>2 > 0.98. This indicates the Basic Fuchsin adsorbs chemically on the heterogeneous surface of rambutan peel. The maximum adsorption capacity determined from the Langmuir isotherm was 108.696 mg/g. It seems that rambutan peel has the potential to substitute activated carbon as an alternative low-cost adsorbent in the treatment of the dye effluent.
Źródło:
Environment Protection Engineering; 2017, 43, 1; 169-181
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development of Carbon Nanotube Based Reflection Type X-ray Source
Autorzy:
Choi, H.
Kim, J.
Lee, C.
Powiązania:
https://bibliotekanauki.pl/articles/1807922.pdf
Data publikacji:
2009-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.47.Lx
75.47.Gk
73.50.Fq
Opis:
X-ray imaging technology is a useful and leading medical diagnostic tool for health care professionals to diagnose disease in human body. Carbon nanotube based X-ray source, which we have developed in this study, could be also useful and supply integrated diagnostic X-ray imaging tool in diagnosis. Conventionally, thermionic type of tungsten filament X-ray tube is widely employed in the field of biomedical and industrial application fields. However, intrinsic problems, such as poor emission efficiency, low imaging resolution, and high electrical energy consumption etc., may cause the limitation of using the X-ray tube. To fulfill the current market requirement, specifically for medical diagnostic field, we have developed rather a portable and compact carbon nanotube based X-ray device in which microfocus high imaging resolution can be feasible.
Źródło:
Acta Physica Polonica A; 2009, 115, 6; 1078-1080
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of Porous Silica Fibers by Electrospinning for Sound Absorbing Materials
Autorzy:
Cho, Y.-S.
Lee, H. J.
Powiązania:
https://bibliotekanauki.pl/articles/353561.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrospinning
porous silica fiber
thermal insulator
sound absorption
Opis:
Macroporous silica fibers having spherical cavities were fabricated by electrospinning using the spinning solution prepared from the mixed dispersion of tetraethylorthosilicate (TEOS) and polystyrene nanospheres as precursor and sacrificial templates, respectively, by injection through metallic nozzle. By applying electric field, the electro-spun fibers obtained by evaporation-driven self-assembly were collected on flat substrate or rotating drum, followed by the removal of the templates by calcination. The sound absorption coefficient of the porous fibers was measured by impedance tube, and the measured value was larger than 0.9 at high frequency region of incident waves. The surface of the resulting fibers was modified using fluorine-containing silane coupling agent to produce superhydrophobic fibrous materials to prevent the infiltration of humidity.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1497-1502
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Atomistic Analysis Of Radiation-Induced Segregation In Ion-Irradiated Stainless Steel 316
Analiza w skali atomowej indukowanej promieniowaniem segregacji w stali nierdzewnej 316
Autorzy:
Lee, G.-G.
Jin, H.-H.
Chang, K.
Lee, B. H.
Kwon, J.
Powiązania:
https://bibliotekanauki.pl/articles/354713.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
atom probe tomography (APT)
radiation-induced segregation (RIS)
ion irradiation
irradiation defects
stainless steel
APT
RIS
stal nierdzewna
segregacja
Opis:
Stainless steel (SS) is a well-known material for the internal parts of nuclear power plants. It is known that these alloys exhibit radiation-induced segregation (RIS) at point defect sinks at moderate temperature, while in service. The RIS behavior of SS can be a potential problem by increasing the susceptibility to irradiation-assisted stress corrosion cracking. In this work, the RIS behavior of solute atoms at sinks in SS 316 irradiated with Fe4+ ions were characterized by atom probe tomography (APT). There were torus-shaped defects along with a depletion of Cr and enrichment of Ni and Si. These clusters are believed to be dislocation loops resulting from irradiation. The segregation of solutes was also observed for various defect shapes. These observations are consistent with other APT results from the literature. The composition of the clusters was analyzed quantitatively almost at the atomic scale. Despite the limitations of the experiments, the APT analysis was well suited for discovering the structure of irradiation defects and performing a quantitative analysis of RIS in irradiated specimens.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1179-1184
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Molding Condition on Waviness Profile of GFRP Composites in Compression Molding
Autorzy:
Kim, J.
Kim, H.
Lee, D.
Powiązania:
https://bibliotekanauki.pl/articles/1399878.pdf
Data publikacji:
2013-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Lg
81.05.Qk
88.30.mj
Opis:
During compression molding of glass fiber reinforced plastic composites, annealing and quenching experiment is conducted by changing pre-heating and cooling method. As results, major cause of unevenness that affects waviness profile (winding) is the shrinkage of matrix during holding and cooling process. Waviness profile of the surface on molding in glass fiber reinforced plastic composites will be lower when holding pressure load is higher, mold temperature is lower during demolding, and cooling rate is slower. In addition, surface roughness of moldings is depending on holding pressure load compared with mold temperature. According to molding condition of glass fiber reinforced plastic composites, waviness profile of surface can be quantitatively estimated using the proposed equation.
Źródło:
Acta Physica Polonica A; 2013, 123, 2; 337-340
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Availability analysis of series redundancy models with imperfect switchover and interrupted repairs
Analiza gotowości modeli redundancji kaskadowej uwzględniających niedoskonałe przełączanie oraz przerwane naprawy
Autorzy:
Shim, J.
Ryu, H.
Lee, Y.
Powiązania:
https://bibliotekanauki.pl/articles/302074.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Polskie Naukowo-Techniczne Towarzystwo Eksploatacyjne PAN
Tematy:
gotowość
redundancja kaskadowa
niedoskonałe przełączenie
naprawa przerwana
ogólny czas naprawy
availability
series redundancy
imperfect switchover
interrupted repair
general repair time
Opis:
This paper considers N + 1 series redundancy, where N components are active and 1 component is standby in normal state. The active components execute the service, while the standby component is ready to take over the active role if the active components fail. When an active component fails, the standby, if available, automatically takes over system operations. However, the automatic switchover of the standby component to active mode might not be possible due to hardware or software issues. When a component failure or an imperfect switchover occurs, it immediately begins to be repaired. However, the repair process is possible to be interrupted. The most existing literature of redundancy models has focused on Markovian systems with uninterrupted repairs. This paper considers a non-Markovian redundancy model with interrupted repairs, where the repair time, the non-automatic switchover time, and the interrupted time are generally distributed. Using supplementary variable method and integro-differential equations, we obtain the steady-state availability for the redundancy model.
W niniejszym artykule rozważano przypadek redundancji kaskadowej typu N + 1, w której liczba N elementów pozostaje aktywnych, a jeden komponent jest w trybie gotowości w stanie normalnym. Elementy aktywne wykonują usługę, podczas gdy składowa rezerwowa pozostaje w stanie gotowości do przejęcia roli aktywnej w przypadku, gdyby składniki aktywne uległy uszkodzeniu. Gdy element aktywny przestaje działać, element zastępczy, jeśli jest dostępny, automatycznie przejmuje operacje systemowe. Jednak automatyczne przełączenie komponentu zastępczego na tryb aktywny nie zawsze jest możliwe z powodu problemów ze sprzętem lub oprogramowaniem. Jeśli wystąpi awaria komponentu lub niedoskonałe przełączenie, natychmiast rozpoczyna się naprawa. Proces naprawy może jednak zostać przerwany. Większośćistniejącej literatury na temat modeli nadmiarowości koncentruje się na systemach Markowa, w których nie dochodzi do przerwania naprawy. W niniejszym artykule rozważano niemarkowowski model nadmiarowości uwzględniający możliwość przerwania naprawy, w którym czas naprawy, czas nieautomatycznego przełączenia oraz czas przerwany mają rozkład ogólny. Wykorzystując metodę dodatkowej zmiennej oraz równania całkowo-różniczkowe otrzymano gotowość stacjonarną dla omawianego modelu redundancji.
Źródło:
Eksploatacja i Niezawodność; 2017, 19, 4; 640-649
1507-2711
Pojawia się w:
Eksploatacja i Niezawodność
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Boundary element modelling of wave diffraction by interaction with wave-offshore structure and dredged region
Autorzy:
Kim, S. D.
Lee, H. J.
Powiązania:
https://bibliotekanauki.pl/articles/259525.pdf
Data publikacji:
2010
Wydawca:
Politechnika Gdańska. Wydział Inżynierii Mechanicznej i Okrętownictwa
Tematy:
Submarine pit
Green function
boundary integral approach
breakwater
Opis:
The purpose of this study is to estimate the wave height at the front face of breakwater (Refracted breakwater and Straight breakwater), when dredging like the submarine pit is performed in the distant offshore from outer breakwater. The wave field of the problem is considered to be two dimensional planes and the configuration of the pit region is designated by a single horizontal long-rectangular system. The numerical approach uses the Green function based on the boundary integral approach. The results of the present numerical works are illustrated by applying the normal and inclined incidence. It is shown that in the case of normal incidence, the ratio of wave height reduction at the front face of both types of breakwaters is approximately more than 20% due to the effect of the submarine pit on the sea bed. Furthermore, regardless of the type of breakwater and the difference in incident wave angles, the ratio of wave height was shown to be reduced.
Źródło:
Polish Maritime Research; 2010, 2; 67-71
1233-2585
Pojawia się w:
Polish Maritime Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, Structure, Photoluminescence, and Raman Spectrum of Indium Oxide Nanowires
Autorzy:
Kim, H.
Na, H.
Yang, J.
Lee,, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505485.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
Production of indium oxide $(In_2O_3)$ whiskers at a very low temperature of 650°C was reported. The synthetic route was comprised of a thermal heating process of a mixture of In and Mg powders. We have investigated the structural properties of the as-synthesized nanowires by using X-ray diffraction and scanning electron microscopy. The product consisted of one-dimensional nanowires, with a crystalline cubic structure of $In_2O_3$. The photoluminescence measurement with the Gaussian fitting exhibited visible light emission bands centered at 2.1 eV and 2.8 eV. The peaks of the Raman spectrum were indexed to the modes being associated with cubic $In_2O_3$.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 143-145
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Extraction Factor Of Pure Ammonium Paratungstate From Tungsten Scraps
Współczynnik ekstrakcji czystego parawolframianu amonu z odpadów wolframowych
Autorzy:
Pee, J-H.
Kim, G. H.
Lee, H. Y.
Kim, Y. J.
Powiązania:
https://bibliotekanauki.pl/articles/356567.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
raw material
recycling
ammonium paratungstate
tungsten scraps
extraction
surowce
recykling
parawolfrawian amonu
odpady wolframowe
ekstrakcja
Opis:
Typical oxidation process of tungsten scraps was modified by the rotary kiln with oxygen burner to increase the oxidation rate of tungsten scraps. Also to accelerate the solubility of solid oxidized products, the hydrothermal reflux method was adapted. By heating tungsten scraps in rotary kiln with oxygen burner at around 900° for 2hrs, the scraps was oxidized completely. Then oxidized products (WO3 and CoWO4) was fully dissolved in the solution of NaOH by hydrothermal reflux method at 150° for 2hrs. The dissolution rate of oxidized products was increased with increasing the reaction temperature and concentration of NaOH. And then CaWO4 and H2WO4 could be generated from the aqueous sodium tungstate solution. Ammonium paratungstate (APT) also could be produced from tungstic acid using by aqueous ammonium solution. The morphologies (cubic and plate types) of APT was controlled by the stirring process of purified solution of ammonium paratungstate.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1403-1405
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Incorporation of Resonators Into Plenum Window
Autorzy:
Lee, H. M.
Haris, A.
Lim, K. M.
Xie, J.
Lee, H. P.
Powiązania:
https://bibliotekanauki.pl/articles/176744.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
plenum window
Helmholtz resonators
noise pollution
ventilation
Opis:
A plenum window with incorporation of Helmholtz resonators in between two glass panes was tested in a reverberation room. The effects of jagged flap on reducing strength of diffracted sound was also investigated in the present studies where white, traffic and construction noises were examined Turing each set of experiment. When the noise source was located at the central line of the plenum window, the plenum window with Helmholtz resonators was able to mitigate 8.5 dBA, 8.9 dBA and 8.2 dBA of white, traffic and construction noises, respectively, compared with the case of without window. These amounts of noises that attenuated by the plenum window were slightly higher than the case where noise source was diverged 30° away from the plenum window. The effects of jagged flaps on the acoustical performance of the plenum window were negligible. The Helmholtz resonators had the best performance in the frequency region between 900 Hz to 1300 Hz where in this frequency range, the plenum window with Helmholtz resonators was able to attenuate additional 1.7 dBA, 1.9 dBA and 1.6 dBA of white, traffic and construction noises, respectively, compared with the case of without resonators.
Źródło:
Archives of Acoustics; 2018, 43, 4; 739-746
0137-5075
Pojawia się w:
Archives of Acoustics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Properties of Copper Doped Neodymium Nickelate Oxide as Cathode Material for Solid Oxide Fuel Cells
Autorzy:
Lee, K. J.
Choe, Y-J.
Hwang, H-J.
Powiązania:
https://bibliotekanauki.pl/articles/351292.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
solid oxide fuel cells
copper
electrical conductivity
excess oxygen
Opis:
Mixed ionic and electronic conducting K2NiF4-type oxide, Nd2Ni1-xCuxO4+δ (x=0~1) powders were synthesized by solid state reaction technique and solid oxide fuel cells consisting of a Nd2Ni1-xCuxO4+δ cathode, a Ni-YSZ anode and ScSZ as an electrolyte were fabricated. The effect of copper substitution for nickel on the electrical and electrochemical properties was examined. Small amount of copper doping (x=0.2) resulted in the increased electrical conductivity and decreased polarization resistance. It appears that this phenomenon was associated with the high mean valence of nickel and copper and the resulting excess oxygen (δ). It was found that power densities of the cell with the Nd2Ni1-xCuxO4+δ (x=0.1 and 0.2) cathode were higher than that of the cell with theNd2NiO4+δ cathode.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 625-628
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Implementation of a Novel Audio Network Protocol
Autorzy:
Lee, J.
Jeon, H.
Choi, P.
Kwon, S.
Lee, S.
Powiązania:
https://bibliotekanauki.pl/articles/178062.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
audio mixer
AoIP
audio over internet protocol
DANTE
SR System
Opis:
Recently, the rapid advancement of the IT industry has resulted in significant changes in audio-system configurations; particularly, the audio over internet protocol (AoIP) network-based audio-transmission technology has received favourable evaluations in this field. Applying the AoIP in a certain section of the multiple-cable zone is advantageous because the installation cost is lower than that for the existing systems, and the original sound is transmitted without any distortion. The existing AoIP-based technology, however, cannot control the audio-signal characteristics of every device and can only transmit multiple audio signals through a network. In this paper, the proposed Audio Network & Control Hierarchy Over peer-to-peer (Anchor) system enables all audio equipment to send and receive signals via a data network, and the receiving device can mix the signals of different IPs. Accordingly, it was possible to improve the system-application flexibility by simplifying the audio-system configuration. The research results confirmed that the received audio signals from different IPs were received, mixed, and output without errors. It is expected that Anchor will become a standard for audio-network protocols.
Źródło:
Archives of Acoustics; 2018, 43, 4; 637-645
0137-5075
Pojawia się w:
Archives of Acoustics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of Mo-Si-B Intermetallic Compound Powders Under Different Heat Treatment Conditions
Autorzy:
Park, J. H.
Lee, S.
Kim, D.
Kim, Y.
Yang, S. H.
Lee, S. H.
Powiązania:
https://bibliotekanauki.pl/articles/353369.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mo-Si-B alloys
intermetallic compounds
reitveld refinement
T2 phase
A15 phase
Opis:
In this research, we investigated the effects of reduction atmospheres on the creation of the Mo-Si-B intermetallic compounds (IMC) during the heat treatments. For outstanding anti-oxidation and elevated mechanical strength at the ultrahigh temperature, we fabricated the uniformly dispersed IMC powders such as Mo5SiB2 (T2) and Mo3Si (A15) phases using the two steps of chemical reactions. Especially, in the second procedure, we studied the influence of the atmospheres (e.g. vacuum, argon, and hydrogen) on the synthesis of IMCs during the reduction. Furthermore, the newly produced IMCs were observed by SEM, XRD, and EDS to identify the phase of the compounds. We also calculated an amount of IMCs in the reduced powders depending on the atmosphere using the Reitveld refinement method. Consequently, it is found that hydrogen atmosphere was suitable for fabrication of IMC without other IMC phases.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1509-1512
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Extraction Factor Of Tungsten Sources From Tungsten Scraps By Zinc Decomposition Process
Współczynnik ekstrakcji związków wolframu z odpadów wolframowych w procesie rozkładu cynku
Autorzy:
Pee, J-H.
Kim, G. H.
Lee, H. Y.
Kim, Y. J.
Powiązania:
https://bibliotekanauki.pl/articles/354774.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
raw material
recycling
zinc decomposition process
tungsten carbide
tungstic acid
surowce
recykling
proces rozkładu cynku
węglik wolframu
kwas wolframowy
Opis:
Decomposition promoting factors and extraction process of tungsten carbide and tungstic acid powders in the zinc decomposition process of tungsten scraps which are composed mostly of tungsten carbide and cobalt were evaluated. Zinc volatility was suppressed by the enclosed graphite crucible and zinc volatilization pressure was produced in the reaction graphite crucible inside an electric furnace for ZDP (Zinc Decomposition Process). Decomposition reaction was done for 2hours at 650°, which 100% decomposed the tungsten scraps that were over 30 mm thick. Decomposed scraps were pulverized under 75μm and were composed of tungsten carbide and cobalt identified by the XRD (X-ray Diffraction). To produce the WC(Tungsten Carbide) powder directly from decomposed scraps, pulverized powders were reacted with hydrochloric acid to remove the cobalt binder. Also to produce the tungstic acid, pulverized powders were reacted with aqua regia to remove the cobalt binder and oxidize the tungsten carbide. Tungsten carbide and tungstic acid powders were identified by XRD and chemical composition analysis.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1311-1314
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cr Poisoning On Nd2Ni0.95Cu0.05O4+δ Cathode for Solid Oxide Fuel Cells
Autorzy:
Choe, Y-J.
Lee, K. J.
Hwang, H-J.
Powiązania:
https://bibliotekanauki.pl/articles/354728.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chromium poisoning
Ruddlesden-Popper
layered perovskite
solid oxide fuel cells
Nd2NiO4
Opis:
In this study, Nd2Ni1-xCuxO4+δ (x=0, 0.05, 0.1, and 0.2) layered perovskite powders were synthesized by the glycine nitrate process (GNP) and the chromium poisoning effect on the electrochemical performance of the Nd2Ni0.95Cu0.05O4+δ and La0.6Sr0.4Co0.2Fe0.88O3-δ cathodes were investigated. In the case of the LSCF cathode, the strontium chromite phase formed after the exposure of the gaseous chromium species, while there was no additional phase in the Nd2Ni0.95Cu0.05O4+δ cathode. The area specific resistance (ASR) of the Nd2Ni0.95Cu0.05O4+δ cathode did not change significantly after the exposure of the gaseous chromium species at 800°C
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 629-634
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Properties and Mechanical Behavior of the 2 Step-Reinforced Al-Si/SiCp Metal Matrix Composite by Titanium-Fiber
Autorzy:
Oak, J.-J.
Lee, Y. C.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/356010.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metal matrix composite
sintering
Ti fiber
mechanical properties
diffusion
Opis:
In this study, the newly designed Al-9Si/SiC particles (SiCp) + Ti-fiber (2step-reinforced Al-9Si alloy matrix) metal matrix composites (MMCs) were fabricated by hot-pressing sintering at 560°C. 2step-reinforced Al-based MMCs were characterized by thermal shrinkage, phase transition, microstructure and tensile strength. The addition of Ti-fiber reduced thermal shrinkage was caused by temperature difference in sintering process as well as enhanced assistance for tensile strength and plastic deformation at room temperature. Experimental results reveal that the 2step-reinforcment sintering by ceramic and metal has a significant effect to increase interface bonding in boundary of each component material and the improved mechanical properties were due to the influence of interfacial product by diffusion. Tensile strength and elongation at room temperature by 2step-reinforcement were improved in 19.5% and 26.2% more than those of Al-9Si/SiCp, respectively. Especially, it reveals that diffusion direction may be varied by sintering methods at low temperature in this study.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1089-1097
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Aluminum Oxide Formation On Fecral Catalyst Support By Electro-Chemical Coating
Powstawanie tlenku glinu na nośniku katalizatora FeCrAl przez osadzanie elektrochemiczne
Autorzy:
Yang, H. S.
Jang, D. H.
Lee, K. J.
Powiązania:
https://bibliotekanauki.pl/articles/355942.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
FeCrAl
catalyst support
aluminum oxide formation
PEO
plasma electrolytic oxidation
electrochemical coating
nośnik katalizatora
tlenek glinu
plazmowe utlenianie elektrolityczne
elektrochemiczne osadzanie
Opis:
FeCrAl is comprised essentially of Fe, Cr, Al and generally considered as metallic substrates for catalyst support because of its advantage in the high-temperature corrosion resistance, high mechanical strength, and ductility. Oxidation film and its adhesion on FeCrAl surface with aluminum are important for catalyst life. Therefore various appropriate surface treatments such as thermal oxidation, Sol, PVD, CVD has studied. In this research, PEO (plasma electrolytic oxidation) process was applied to form the aluminum oxide on FeCrAl surface, and the formed oxide particle according to process conditions such as electric energy and oxidation time were investigated. Microstructure and aluminum oxide particle on FeCrAl surface after PEO process was observed by FE-SEM and EDS with element mapping analysis. The study presents possibility of aluminum oxide formation by electro-chemical coating process without any pretreatment of FeCrAl.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1503-1506
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of Cu and Ni Nano-Fluids Synthesized by Pulsed Wire Evaporation Method
Autorzy:
Kim, H.-S.
Yilmaz, F.
Dharmaiah, P.
Lee, D.-J
Lee, T.-H.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/356475.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
pulsed wire evaporation
nanofluid
Cu
Ni
suspension stability
dispersibility
Opis:
In the present work, Cu and Ni nanofluids were synthesized using the pulsed wire evaporation (PWE) method in the different aqueous medias, namely (ethanol and ethylene glycol), and the effects of the aqueous media on the dispersion state, stability, and particle size of nanoparticles were studied. The size and morphology of synthesized nano-particles were investigated by transmission electron microscopy (TEM). Also, the dispersion stability of the nanofluids was evaluated by turbiscan analysis. The TEM results showed that the nano-particles were spherical in shape, and the average particle size was below 100 nm. The average particle size of the Cu nano-particles was smaller than that of Ni, which was attributed to a difference in the specific sublimation energy of the elements. Moreover, ethylene glycol (EG) exhibited higher suspension stability than ethanol. Finally, the dispersion stability of Cu@EG displayed the highest value due to lower particle size and greater viscosity.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 999-1004
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Magnetic Properties of NdFeB Sintered Magnets Diffusion-Treated with Cu/Al Mixed Dyco Alloy-Powder
Autorzy:
Lee, M.-W.
Bae, K.-H.
Lee, S.-R.
Kim, H.-J.
Jang, T.-S.
Powiązania:
https://bibliotekanauki.pl/articles/353351.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd-Fe-B sintered magnets
grain boundary diffusion process
low melting point element
DyCo alloy-powder diffusion
Opis:
We investigated the microstructural and magnetic property changes of DyCo, Cu + DyCo, and Al + DyCo diffusion-treated NdFeB sintered magnets. The coercivity of all diffusion treated magnet was increased at 880ºC of 1st post annealing(PA), by 6.1 kOe in Cu and 7.0 kOe in Al mixed DyCo coated magnets, whereas this increment was found to be relatively low (3.9 kOe) in the magnet coated with DyCo only. The diffusivity and diffusion depth of Dy were increased in those magnets which were treated with Cu or Al mixed DyCo, mainly due to comparatively easy diffusion path provided by Cu and Al because of their solubility with Ndrich grain boundary phase. The formation of Cu/Al-rich grain boundary phase might have enhanced the diffusivity of Dy-atoms. Moreover, relatively a large number of Dy atoms reached into the magnet and mostly segregated at the interface of Nd2 Fe14 B and grain boundary phases covering Nd2 Fe14 B grains so that the core-shell type structures were developed. The formation of highly anisotropic (Nd, Dy)2Fe14B phase layer, which acted as the shell in the core-shell type structure so as to prevent the reverse domain movement, was the cause of enhancing the coercivity of diffusion treated NdFeB magnets. Segregation of cobalt in Nd-rich TJP followed by the formation of Co-rich phase was beneficial for the coercivity enhancement, resulting in the stabilization of the metastable c-Nd2O3 phase.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1263-1266
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of Single Crystalline Titanium Oxide and Sodium Titanate Nanorods via Salt-Assisted Ultrasonic Spray Pyrolysis
Autorzy:
Hwangbo, Y.
Yoo, J.-H.
Lee, Y.-I.
Powiązania:
https://bibliotekanauki.pl/articles/352337.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2
nanorods
salt
Ultrasonic Spray Pyrolysis
optical properties
Opis:
The simple and continuous synthesis of single crystalline anatase titanium dioxide and sodium titanate nanorods by a saltassisted ultrasonic spray pyrolysis method is demonstrated. This method does not require expensive precursors, long reaction time, and physical templates or surfactant. In addition, its continuous nature makes it a suitable method for the large-scale preparation. Moreover, the effect of a salt concentration in a starting solution on material properties, including morphology and phase of the synthesized products was systematically investigated. The synthesized nanorods had one-dimensionality, a single crystalline and the average diameter of 12.3 nm with dual phases of titanium dioxide and sodium titanate by FE-SEM, XRD, HR-TEM as well as FFT-converted SAED pattern analysis.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1411-1414
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on the Microstructure and Tensile Deformation Behavior of Oxide Dispersion Strengthened Alloys Manufactured by Complex Milling Process
Autorzy:
Kim, Y.-K.
Kim, J.-H.
Gwon, J.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352535.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
oxide dispersion strengthening
microstructure
tensile deformation behavior
Opis:
This study attempted to manufacture an ODS alloy by combining multiple milling processes in mechanical alloying stage to achieve high strength and fracture elongation. The complex milling process of this study conducted planetary ball milling, cryogenic ball milling and drum ball milling in sequential order, and then the microstructure and tensile deformation behavior were investigated after additional heat treatment. The oxide particles distributed within the microstructure were fine oxide particles of 5~20 nm and coarse oxide particles of 100~200 nm, and the oxide particles were confirmed to be composed of Cr, Ti, Y and O. Results of tensile tests at room temperature measured yield strength, tensile strength and elongation as 1320 MPa, 2245 MPa and 4.2%, respectively, before heat treatment, and 1161 MPa, 2020 MPa and 5.5% after heat treatment. This results indicate that the ODS alloy of this study gained very high strengths compared to other known ODS alloys, allowing greater plastic zones.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1335-1340
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron Annilation Lifetime and Glass Transition Temperatures in $CO_2$ Sorption Polystyrene
Autorzy:
Jean, Y.
Chen, H.
Lee, L.
Yang, J.
Powiązania:
https://bibliotekanauki.pl/articles/1812530.pdf
Data publikacji:
2008-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
78.66.Qn
71.60.+z
Opis:
Positron annihilation lifetime spectroscopy was used to measure the free-volume size and distributions as a function of temperature in polystyrene with and without 400 psi $CO_2$ sorption. The transition temperatures in the polystyrene with $CO_2$ sorption obtained from ortho-positronium lifetimes were found to depend on the thermal cycles and a meta-stable state showing a negative thermal expansion coefficient was observed between 53°C and 82°C during the first heating up experiment. The observed $T_g$ in polystyrene with, and without $CO_2$ sorption after annealing from ortho-positronium lifetimes were found to be 86°C and 91°C, which are 5°C higher, and 10°C lower than from the differential scanning calorimetry data, respectively. The observed free-volume variations are discussed in terms of hole expansion, creation, free-volume relaxation, plasticization, and hole filling in amorphous polymers.
Źródło:
Acta Physica Polonica A; 2008, 113, 5; 1385-1395
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Biological Evaluation of Anodized Biodegradable Magnesium-Calcium Alloys
Autorzy:
Kim, J.
Lee, J.
Lee, K.
Park, S.
Lim, H.
Park, C.
Bae, J.
Yun, K.
Powiązania:
https://bibliotekanauki.pl/articles/1398763.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.85.jj
87.85.J-
Opis:
The objective of this study was to evaluate the biocompatibility of studied binary magnesium-calcium (Mg-Ca) alloys for biodegradable intraosseous implants. Mg is necessary for health and is a non-toxic biodegradable material that decomposes naturally in the body. Nevertheless, Mg has been implicated in problems including diminished physical properties and corrosion resistance when degradation is too rapid prior to bone healing. This study has explored the effect of Ca on the corrosion resistance and biological evaluation after anodizing treatment with different contents of Ca alloy. Binary Mg-0.5Ca, Mg-1Ca and Mg-5Ca alloys were prepared by the casting method under an argon atmosphere and cut into disc-shaped pieces. Pure Mg alloy was used as the control. Anodic oxidation was performed for 15 minutes at a voltage of 120 V using an electrolyte solution containing Ca gluconate, sodium hexametaphosphate, and sodium hydroxide at room temperature. Corrosion resistance was analyzed using a corrosion tester. After a hydrogen evolution test, the surface pattern and phase changes were observed on a scanning electron microscop (SEM) and energy dispersive spectroscop (EDS). Microscopic evaluation of the adhesion and cell biological functions of Mg was conducted by observing the response of human fetal osteoblastic 1.19 cells with regard to changes in surface film properties, depending on the amount of Ca. Our results support the view that in Mg-xCa alloys (x=0.5, 1, 5 wt.%) treated using anodic oxidation, the increasing Ca content controls the rate of decomposition and improves corrosion resistance.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 728-735
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spontaneous Formation of Titanium Nitride on the Surface of a Ti Rod Induced by Electro-Discharge-Heat-Treatment in an N2 Atmosphere
Autorzy:
Lee, W. H.
Yoon, Y. H.
Kim, Y. H.
Lee, Y. K.
Kim, J. Y.
Chang, S. Y.
Powiązania:
https://bibliotekanauki.pl/articles/352477.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
surface modification
diffusion
heat treatment
XPS
Opis:
A single pulse of 2.0 to 3.5 kJ of input energy from a 450 mF capacitor was applied to a commercially pure Ti rod in a N2 atmosphere. The surface of the Ti rod transformed from TiO2 into titanium nitride in times as short as 159 msec, providing a bimodal morphology of the cross-section. A much higher value of hardness that was observed at the edge of the cross-section was attributed to nitrogen-induced solid-solution hardening that occurred during the electrical discharge process. The activation energy (Ea) for the diffusion process was estimated to be approximately 86.9 kJ/mol. Results show that the electrical discharge process is a possible potential method for the nitriding of Ti; advantages include a short processing time and control of the nitrided layer without dimensional changes.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1281-1285
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of acute lipopolysaccharide-induced toxemia model on some neglected blood parameters
Autorzy:
Adam, G.O.
Lee, H.R.
Lee, S.J.
Kim, S.J.
Kim, G.B.
Kang, H.S.
Powiązania:
https://bibliotekanauki.pl/articles/2087627.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Toxemia
lipopolysaccharide
base excess
pH
animal model
Źródło:
Polish Journal of Veterinary Sciences; 2018, 21, 4; 665-671
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High-temperature Oxidation Behavior and Kinetics of Forged 12Cr-MoVW Steel
Autorzy:
Kim, Y. H.
Oak, J.-J.
Bae, K.-C.
Lee, W-J.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/351450.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ferritic/martensitic stainless steels
forging
oxidation kinetics
oxide layer
Opis:
The oxidation kinetics of forged 12Cr-MoVW steel was investigated in an air (N2+O2) atmosphere at 873-1073 K (Δ50 K) using thermogravimetric analysis. The oxidized samples were characterized using X-ray diffraction, and the surface and cross-sectional morphologies were examined using scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy. The forged 12Cr-MoVW steel samples exhibited parabolic behavior and a low oxidation rate compared with their as-cast counterparts. A protective oxide layer was uniformly formed at relatively low temperature (≤973 K) for the forged samples, which thus exhibited better oxidation resistance than the as-cast ones. These oxides are considered solid-solution compounds such as (Fe, Cr)2O3.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1099-1104
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Variable-Focus Fluid Lens Using an Electromagnetic Actuator
Autorzy:
Lee, J.
Park, K.
Choi, J.
Kim, H.
Kong, S.
Powiązania:
https://bibliotekanauki.pl/articles/1399681.pdf
Data publikacji:
2013-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
85.85.+j
42.79.Bh
Opis:
A variable-focus fluid lens controlled by an electromagnetic actuator and its characteristics are presented in this paper. The repulsive force between an NdFeB magnet and a solenoid through electromagnetic induction causes deflections in the elastomeric membranes integrated in the lens resulting in a focal-length change. The controllability of the focal length of the fabricated lens with an aperture size of 2 mm was approximately from infinity to 15 mm (with input current of 100 mA). The actuator including the solenoid was carefully designed to avoid thermal crosstalk of the lens fluid and magnet from the electromagnetic induction of the solenoid. The settling time to form a convex shape of the lens membrane was approximately 2.5 ms at an input current of 20 mA.
Źródło:
Acta Physica Polonica A; 2013, 123, 2; 202-204
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Contamination of soil with heavy metals drained out from abandoned mines in the South-West region of Korea
Autorzy:
Kim, S.-D.
Dho, H.-S.
Lee, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/207493.pdf
Data publikacji:
2015
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
soil pollution
abandoned mines
arsenic
heavy metals
nickel
soils
zinc
contamination level
forest regions
surface soil
zanieczyszczenie gleby
zlikwidowane kopalnie
arsen
metale ciężkie
nikiel
gleby
cynk
poziom zanieczyszczeń
obszary leśne
powierzchniowe warstwy gleby
Opis:
Contamination of soil with heavy metals drained out from twenty eight abandoned mines in the southwest regions of Korea has been investigated. Utilizing various statistical techniques, the goal was to evaluate and analyze pH and the contamination with Arsenic, and the following six heavy metals: cadmium, hydrargyrum, lead, nickel, chromium, and zinc. Contamination levels of heavy metals were determined depending on the depth of the soil. Results indicated that the subsoil and the surface soil both were strongly contaminated with lead and arsenic. Furthermore, the subsoil also contained much nickel. In forest regions, high levels of lead and arsenic, whereas in all regions high levels of zinc have been detected.
Źródło:
Environment Protection Engineering; 2015, 41, 3; 61-72
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication Of Zn4Sb3 Alloys By A Combination Of Gas-Atomization And Spark Plasma Sintering Processes
Wytwarzanie i konsolidacja proszków stopowych zn4sb3 przez kombinację procesów atomizacji gazowej i spiekania
Autorzy:
Dharmaiah, P.
Kim, H.-S.
Lee, L. H.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/355894.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gas atomization
microstructure
spark plasma sintering (SPS)
X-ray diffraction
atomizacja gazowa
mikrostruktura
SPS
spiekanie plazmowe
analiza rentgenowska (XRD)
Opis:
In this study, single phase polycrystalline Zn4Sb3 as well as 11 at.% Zn-rich Zn4Sb3 alloy having ε-Zn4Sb3 (majority phase) and Zn (minority phase) phases bulk samples produced by gas-atomization and subsequently consolidated by spark plasma sintering (SPS) process. The crystal structures were analyzed by X-ray diffraction (XRD) and cross-sectional microstructure were observed by the scanning electron microscopy (SEM). The internal grain microstructure of 11at.% Zn-rich Zn4Sb3 powders shows lamellar structure. Relative density, Vickers hardness and crack lengths were measured to investigate the effect of sintering temperature of Zn4Sb3 samples which are sintered at 653, 673 and 693 K. Relative density of the single phase bulk Zn4Sb3 sample reached to 99.2% of its theoretical density. The micro Vickers hardness of three different sintering temperatures were found around 2.17 – 2.236 GPa.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1417-1421
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The effect of patterns on image-based modelling of texture-less objects
Autorzy:
Hafeez, J.
Jeon, H.-J.
Hamacher, A.
Kwon, S.-C.
Lee, S.-H.
Powiązania:
https://bibliotekanauki.pl/articles/221814.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
structure-from-motion
feature detection
patterns analysis
3D reconstruction
surface comparison
Opis:
The task of generating fast and accurate three-dimensional (3D) models of objects or scenes through a sequence of non-calibrated images is an active field of research. The recent development in algorithm optimization has resulted in many automatic solutions that can provide an accurate 3D model from texture-full objects. Structure-from-motion (SfM) is an image-based method that uses discriminative point-based feature identifier, such as SIFT, to locate feature points in the images. This method faces difficulties when presented with the objects made of homogenous or texture-less surfaces. To reconstruct such surfaces a well-known technique is to apply an artificial variety by covering the surface with a random texture pattern prior to the image capturing process. In this work, we designed three series of image patterns which are tested based on the contrast and density ratio which increases from the first to the last pattern within the same series. The performance of the patterns is evaluated by reconstructing the surface of a texture-less object and comparing it with the true data. Using the best-found patterns from the experiments, a 3D model of a Moai statue is reconstructed. The experimental results demonstrate that the density and structure of a pattern highly affects the quality of the reconstruction.
Źródło:
Metrology and Measurement Systems; 2018, 25, 4; 755-767
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evaluation of Surface Characteristics and Physical Properties on Biodegradable Magnesium-Calcium Alloys by Anodic Oxidation
Autorzy:
Kim, J.
Lee, J.
Yang, H.
Park, S.
Lim, H.
Oh, G.
Yun, K.
Powiązania:
https://bibliotekanauki.pl/articles/1191716.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.85.jj
87.85.jc
Opis:
The purpose of this study was to determine the effect of calcium (Ca) on the surface characteristics and physical properties of magnesium-calcium alloys after anodization. A novel binary alloy Mg-xCa (in which x=0.5, 1, or 5 wt.%) was cast by combining magnesium (99.9%) and calcium (99.9%) in an argon gas (99.99%) atmosphere. A magnesium alloy rod having a diameter of 15 mm was cut into discs, each 2 mm thick. The specimens were subjected to anodic oxidation at 120 V for 15 minutes at room temperature in an electrolyte solution consisting of calcium gluconate, sodium hexametaphosphate, and sodium hydroxide. Surface and cross-sectional morphological changes were observed using scanning electron microscopy, and the microstructures and phases were detected by means of X-ray diffraction. Hardness and surface roughness were assessed by means of a Vickers hardness tester and a surface roughness meter, respectively. The results show that the physical properties of these magnesium-calcium alloys have been improved, because it was possible to control the dissolution rate according to the amount of calcium added.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 736-741
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation and Surface Modification of Mechanical Alloyed Ti-25.0 at.% Al Powder Mixture by Using an Electro-Discharge Technique
Autorzy:
Chang, S. Y.
Jang, H. S.
Yoon, Y. H.
Kim, Y. H.
Kim, J. Y.
Lee, Y. K.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/354212.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintering
mechanical alloying
powder consolidation
intermetallic compounds
titanium aluminides
Opis:
Electrical discharges using a capacitance of 450 μF at 0.5, 1.0, and 1.5 kJ input energies were applied in a N2 atmosphere to obtain the mechanical alloyed Ti3Al powder without applying any external pressure. A solid bulk of nanostructured Ti3Al was obtained as short as 160 μsec by the Electrical discharge. At the same time, the surface has been modified into the form of Ti and Al nitrides due to the diffusion process of nitrogen to the surface. The input energy was found to be the most important parameter to affect the formation of a solid core and surface chemistry of the compact.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1293-1297
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Point-Contact Spectroscopy of Superconducting $MgCNi_3$ Single Crystals
Autorzy:
Pribulová, Z.
Szabó, P.
Kačmarčík, J.
Samuely, P.
Jang, D.
Lee, H.
Lee, S.
Powiązania:
https://bibliotekanauki.pl/articles/1813611.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
74.50.+r
Opis:
The first point-contact spectroscopy measurements on $MgCNi_3$ single crystals of very good quality are presented. The measurements have been performed in the temperature range from 1.5 K up to 10 K and at magnetic fields up to 6 T. The superconducting energy gap Δ of the system is found to be scattered between 1 and 1.2 meV which gives the 2Δ/k $T_c$ ratio between BCS weak-coupling value of ~3.5 and a strong coupling of about 4.2. The excess current evaluated in magnetic field indicates the presence of a single energy gap.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 215-218
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization Of The Graded Microstructure In Powder Sintered Porous Titanium
Charakterystyka gradientowej mikrostruktury porowatego tytanu spiekanego z proszku
Autorzy:
Oak, J.-J.
Bang, J. I.
Bae, K.-C.
Kim, Y. H.
Lee, Y. C.
Chun, H. H.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/356239.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
powder metallurgy
porous structure
sintering
biomaterial
tytan
metalurgia proszków
struktura porowata
spiekanie
biomateriał
Opis:
The proposed sintering process produce porosity and functional graded microstructure in the sinterd titanium powders. Titanium powders with different micro sizes were sintered at the proposed temperature region at 1200 and 1300°C for 2h. The apatite-forming on the graded microstructure is observed by immersion test in Hanks balanced salt soluion at 37°C. Sintering condition of titanium powders is estimated by thermogravitmetry-differential thermal analysis (TG-DTA). The synthersied surface structures and apatite-forming ability were characterized by a field emission scanning electron microscopy (FE-SEM) observation and energy dispersive X-ray spectroscopy (EDS) analysis. As results, these graded microstructure of sintered porous titanium powders reveals apatite-forming ability as osseointegration by calcification in Hanks balanced salt soluion(HBSS) at 37°C.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1265-1269
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of The Desorption-Recombination Temperature On The Microstructure And Magnetic Properties Of HDDR Processed Nd-Fe-B Powders
Wpływ temperatury desorpcji-rekombinacji na mikrostrukturę i właściwości magnetyczne proszków Nd-Fe-B przetwarzanych metodą HDDR
Autorzy:
Lee, J.-G.
Cha, H.-R.
Liu, S.
Yu, J.-H.
Baek, Y.-K.
Kwon, H.-W.
Powiązania:
https://bibliotekanauki.pl/articles/353723.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd-Fe-B
HDDR
permanent magnet
grain boundary
metoda HDDR
magnes trwały
granica ziarna
Opis:
The effect of the desorption-recombination temperature on the microstructure and magnetic properties of hydrogenation-disproportionation-desorption-recombination (HDDR) processed Nd-Fe-B powders was studied. The NdxB6.4Ga0.3Nb20.2Febal (x=12.5-13.5, at.%) casting alloys were pulverized after homogenizing annealing, and then subjected to HDDR treatment. During the HDDR process, desorption-recombination (DR) reaction was induced at two different temperature, 810°C and 820°C. The higher Nd content resulted in enhanced coercivity of the HDDR powder, and which was attributed to the thicker and more uniform Nd-rich phase along grain boundaries. But this uniform Nd-rich phase induced faster grain growth. The remanence of the powder DR-treated at 820°C is higher than that DR-treated at 810°C. In addition, it was also confirmed that higher DR temperature is much more effective to improve squareness.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1499-1501
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Multistep Heat-Treatment Effects on Electrospun Nd-Fe-B-O Nanofibers
Autorzy:
Jeon, E. J.
Eom, N. S. A.
Lee, J.
Lee, B.
Cho, H. M.
On, J. S.
Choa, Y.-H
Kim, B. S.
Powiązania:
https://bibliotekanauki.pl/articles/354311.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd-Fe-B
nanofibers
electrospinning
heat treatment
Opis:
Neodymium-Iron-Boron (Nd-Fe-B) magnets are considered to have the highest energy density, and their applications include electric motors, generators, hard disc drives, and MRI. It is well known that a fiber structure with a high aspect ratio and the large specific surface area has the potential to overcome the limitations, such as inhomogeneous structures and the difficulty in alignment of easy axis, associated with such magnets obtained by conventional methods. I n this work, a suitable heat-treatment procedure based on single-step and multistep treatments to synthesize sound electrospun Nd-Fe-B-O nanofibers of Φ572 nm was investigated. The single-step heat-treated (directly heat-treated at 800°C for 2 h in air) samples disintegrated along with the residual organic compounds, whereas the multistep heat-treated (sequential three-step heat-treated including three steps;: dehydration (250°C for 30 min in an inert atmosphere), debinding (650°C for 30 min in air), and calcination (800°C for 1 h in air)) fibers maintained sound fibrous morphology without any organic impurities. They could maintain such fibrous morphologies during the dehydration and debinding steps because of the relatively low internal pressures of water vapor and polymer, respectively. In addition, the NdFeO3 alloying phase was dominant in the multistep heat-treated fibers due to the removal of barriers to mass transfer in the interparticles.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1433-1437
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Enhanced Microwave Absorption of CNT Composites Mixing with Fe3O4 and Carbonyl Iron
Autorzy:
Park, J. H.
Choi, J.
Lee, K.
Park, J.
Song, J. K.
Jeon, E.
Powiązania:
https://bibliotekanauki.pl/articles/351106.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnetic powders
complex permittivity
complex permeability
composite materials
microwave absorption
Opis:
We fabricated two different kinds of composite materials for absorbing microwave in a frequency range of 2 to 18 GHz using coaxial airline and thru-reflect-line (TRL) method. The composite materials having carbon nanotube (CNT) with carbonyl iron (CI) or iron oxide (Fe3 O4 ) were fabricated by mixing each components. Magnetic properties were measured by SQUID equipment. Complex permittivity and complex permeability were also obtained by measuring S-parameters of the toroidal specimen dispersing CI/CNT and Fe3 O4 /CNT into the 50 weight percent (wt%) epoxy resin. The real permittivity was improved by mixing the CNT however, the real permeability was same as pure magnetic powders. The CI/CNT had a maximum value of real permittivity and real permeability, 11 and 1.4 at 10 GHz, respectively. The CNT composites can be adapted to the radar absorbing materials, band width 8-12 GHz.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1513-1516
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photoluminescence Studies of Aluminum Nitride Nanowires
Autorzy:
Yang, J.
Na, H.
Kim, H.
Kebede, M.
Choi, R.
Jeong, J.
Lee, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505466.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
We report the production of AlN nanowires by the thermal heating method, for exploring their photoluminescence properties. The room-temperature photoluminescence properties were investigated with different annealing environment. While broad emissions with peaks at around 2.45 and 2.95 eV were obtained from both unannealed and annealed samples, the additional 2.1 eV peak was found from the annealed samples. We have suggested the possible emission mechanisms based on the assumption that both 2.45 eV peak and 2.1 eV peak are ascribed to the nitrogen vacancies. Annealing in N_2 environment exhibited lower intensities of 2.45 eV peak and 2.1 eV peak in comparison to those in Ar environment, presumably due to the suppression of nitrogen vacancies.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 125-127
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-50 z 84

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