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    Wyświetlanie 1-55 z 55
    Tytuł:
    Extraction Factor Of Pure Ammonium Paratungstate From Tungsten Scraps
    Współczynnik ekstrakcji czystego parawolframianu amonu z odpadów wolframowych
    Autorzy:
    Pee, J-H.
    Kim, G. H.
    Lee, H. Y.
    Kim, Y. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/356567.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    raw material
    recycling
    ammonium paratungstate
    tungsten scraps
    extraction
    surowce
    recykling
    parawolfrawian amonu
    odpady wolframowe
    ekstrakcja
    Opis:
    Typical oxidation process of tungsten scraps was modified by the rotary kiln with oxygen burner to increase the oxidation rate of tungsten scraps. Also to accelerate the solubility of solid oxidized products, the hydrothermal reflux method was adapted. By heating tungsten scraps in rotary kiln with oxygen burner at around 900° for 2hrs, the scraps was oxidized completely. Then oxidized products (WO3 and CoWO4) was fully dissolved in the solution of NaOH by hydrothermal reflux method at 150° for 2hrs. The dissolution rate of oxidized products was increased with increasing the reaction temperature and concentration of NaOH. And then CaWO4 and H2WO4 could be generated from the aqueous sodium tungstate solution. Ammonium paratungstate (APT) also could be produced from tungstic acid using by aqueous ammonium solution. The morphologies (cubic and plate types) of APT was controlled by the stirring process of purified solution of ammonium paratungstate.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1403-1405
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Extraction Factor Of Tungsten Sources From Tungsten Scraps By Zinc Decomposition Process
    Współczynnik ekstrakcji związków wolframu z odpadów wolframowych w procesie rozkładu cynku
    Autorzy:
    Pee, J-H.
    Kim, G. H.
    Lee, H. Y.
    Kim, Y. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/354774.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    raw material
    recycling
    zinc decomposition process
    tungsten carbide
    tungstic acid
    surowce
    recykling
    proces rozkładu cynku
    węglik wolframu
    kwas wolframowy
    Opis:
    Decomposition promoting factors and extraction process of tungsten carbide and tungstic acid powders in the zinc decomposition process of tungsten scraps which are composed mostly of tungsten carbide and cobalt were evaluated. Zinc volatility was suppressed by the enclosed graphite crucible and zinc volatilization pressure was produced in the reaction graphite crucible inside an electric furnace for ZDP (Zinc Decomposition Process). Decomposition reaction was done for 2hours at 650°, which 100% decomposed the tungsten scraps that were over 30 mm thick. Decomposed scraps were pulverized under 75μm and were composed of tungsten carbide and cobalt identified by the XRD (X-ray Diffraction). To produce the WC(Tungsten Carbide) powder directly from decomposed scraps, pulverized powders were reacted with hydrochloric acid to remove the cobalt binder. Also to produce the tungstic acid, pulverized powders were reacted with aqua regia to remove the cobalt binder and oxidize the tungsten carbide. Tungsten carbide and tungstic acid powders were identified by XRD and chemical composition analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1311-1314
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Spontaneous Formation of Titanium Nitride on the Surface of a Ti Rod Induced by Electro-Discharge-Heat-Treatment in an N2 Atmosphere
    Autorzy:
    Lee, W. H.
    Yoon, Y. H.
    Kim, Y. H.
    Lee, Y. K.
    Kim, J. Y.
    Chang, S. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/352477.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    titanium
    surface modification
    diffusion
    heat treatment
    XPS
    Opis:
    A single pulse of 2.0 to 3.5 kJ of input energy from a 450 mF capacitor was applied to a commercially pure Ti rod in a N2 atmosphere. The surface of the Ti rod transformed from TiO2 into titanium nitride in times as short as 159 msec, providing a bimodal morphology of the cross-section. A much higher value of hardness that was observed at the edge of the cross-section was attributed to nitrogen-induced solid-solution hardening that occurred during the electrical discharge process. The activation energy (Ea) for the diffusion process was estimated to be approximately 86.9 kJ/mol. Results show that the electrical discharge process is a possible potential method for the nitriding of Ti; advantages include a short processing time and control of the nitrided layer without dimensional changes.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1281-1285
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Self-Consolidation and Surface Modification of Mechanical Alloyed Ti-25.0 at.% Al Powder Mixture by Using an Electro-Discharge Technique
    Autorzy:
    Chang, S. Y.
    Jang, H. S.
    Yoon, Y. H.
    Kim, Y. H.
    Kim, J. Y.
    Lee, Y. K.
    Lee, W. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354212.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    sintering
    mechanical alloying
    powder consolidation
    intermetallic compounds
    titanium aluminides
    Opis:
    Electrical discharges using a capacitance of 450 μF at 0.5, 1.0, and 1.5 kJ input energies were applied in a N2 atmosphere to obtain the mechanical alloyed Ti3Al powder without applying any external pressure. A solid bulk of nanostructured Ti3Al was obtained as short as 160 μsec by the Electrical discharge. At the same time, the surface has been modified into the form of Ti and Al nitrides due to the diffusion process of nitrogen to the surface. The input energy was found to be the most important parameter to affect the formation of a solid core and surface chemistry of the compact.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1293-1297
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Self-Consolidation Mechanism of Ti5Si3 Compact Obtained by Electro-Discharge-Sintering Directly from Physically Blended Ti-37.5 At.% Si Powder Mixture
    Autorzy:
    Chang, S. Y.
    Cheon, Y. W.
    Yoon, Y. H.
    Kim, Y. H.
    Kim, J. Y.
    Lee, Y. K.
    Lee, W. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/353022.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    sintering
    mechanical alloying
    powder consolidation
    intermetallic compounds
    titanium silicide
    Opis:
    Characteristics of electro-discharge-sintering of the Ti-37.5at.% Si powder mixture was investigated as a function of the input energy, capacitance, and discharge time without applying any external pressure. A solid bulk of Ti5Si3 was obtained only after in less than 129 μsec by the EDS process. During a discharge, the heat is generated to liquefy and alloy the particles, and which enhances the pinch pressure can condensate them without allowing a formation of pores. Three step processes for the self-consolidation mechanism during EDS are proposed; (a) a physical breakdown of oxide film on elemental as-received powder particles, (b) alloying and densifying the consolidation of powder particles by the pinch pressure, and (c) diffusion of impurities into the consolidated surface.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1299-1302
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Postural and Muscular Responses While Viewing Different Heights of Screen
    Autorzy:
    Lee, T. H.
    Liu, T. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/90519.pdf
    Data publikacji:
    2013
    Wydawca:
    Centralny Instytut Ochrony Pracy
    Tematy:
    visual display terminal
    posture
    viewing angle
    pozycja przy pracy
    kąt widzenia
    ekran
    praca przy komputerze
    Opis:
    This study aimed to examine the effects of visual display terminal (VDT) viewing angle on human postural angle and muscular activity. The participants’ neck, thoracic bending, and trunk inclination angles; and the activity of sternocleidomastoid, trapezius, splenius capitis, and erector spinae at 5 viewing angles (+400, +200, 00, –200, and –400) of a VDT screen were collected for 1 min. This study showed that neck and thoracic bending angles increased with viewing angle, while viewing angle did not significantly affect trunk inclination angle. In addition, the activity of trapezius and erector spinae increased when viewing a higher or lower VDT screen height compared with viewing a horizontal VDT screen height; however, the activity of splenius capitis decreased with viewing angle.
    Źródło:
    International Journal of Occupational Safety and Ergonomics; 2013, 19, 2; 251-258
    1080-3548
    Pojawia się w:
    International Journal of Occupational Safety and Ergonomics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Grip Force and Heart Rate Responses to Manual Carrying Tasks: Effects of Material, Weight, and Base Area of the Container
    Autorzy:
    Lee, T. H.
    Tseng, C. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/91134.pdf
    Data publikacji:
    2014
    Wydawca:
    Centralny Instytut Ochrony Pracy
    Tematy:
    liquid
    solid
    carriage
    manual materials handling
    pracownik fizyczny
    chwyt
    transport ręczny
    Opis:
    This study recruited 16 industrial workers to examine the effects of material, weight, and base area of container on reduction of grip force (ΔGF) and heart rate for a 100-m manual carrying task. This study examined 2 carrying materials (iron and water), 4 carrying weights (4.4, 8.9, 13.3, 17.8 kg), and 2 base areas of container (24 ´ 24 cm, 35 ´ 24 cm). This study showed that carrying water significantly increased ΔGF and heart rate as compared with carrying iron. Also, ΔGF and heart rate significantly increased with carrying weight and base area of container. The effects of base area of container on ΔGF and heart rate were greater in carrying water condition than in carrying iron condition. The maximum dynamic effect of water on ΔGF and heart rate occurred when water occupied ~60%–80% of full volume of the container.
    Źródło:
    International Journal of Occupational Safety and Ergonomics; 2014, 20, 3; 377-383
    1080-3548
    Pojawia się w:
    International Journal of Occupational Safety and Ergonomics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of Porous Silica Fibers by Electrospinning for Sound Absorbing Materials
    Autorzy:
    Cho, Y.-S.
    Lee, H. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/353561.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    electrospinning
    porous silica fiber
    thermal insulator
    sound absorption
    Opis:
    Macroporous silica fibers having spherical cavities were fabricated by electrospinning using the spinning solution prepared from the mixed dispersion of tetraethylorthosilicate (TEOS) and polystyrene nanospheres as precursor and sacrificial templates, respectively, by injection through metallic nozzle. By applying electric field, the electro-spun fibers obtained by evaporation-driven self-assembly were collected on flat substrate or rotating drum, followed by the removal of the templates by calcination. The sound absorption coefficient of the porous fibers was measured by impedance tube, and the measured value was larger than 0.9 at high frequency region of incident waves. The surface of the resulting fibers was modified using fluorine-containing silane coupling agent to produce superhydrophobic fibrous materials to prevent the infiltration of humidity.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1497-1502
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects Of Process Parameters On Cu Powder Synthesis Yield And Particle Size In A Wet-Chemical Process
    Wpływ parametrów procesu na wydajność syntezy proszku Cu i wielkości cząstek w procesie mokrym chemicznym
    Autorzy:
    Shin, Y. M.
    Lee, J. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354168.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    wet-chemical process
    micron-size Cu powder
    Synthesis yield
    particle size
    gibbs free energy difference
    proszek Cu
    proces chemiczny mokry
    wydajność syntezy
    rozmiar cząsteczki
    różnica energii swobodnej Gibbsa
    Opis:
    This study presents a simple wet-chemical process to prepare several micron-size Cu powders. Moreover, changes in powder synthesis yield and particle size are examined with different solvents, synthesis temperatures, and amounts of reducing agent during the synthesis. As a reducing agent and capping agent, L-ascorbic acid and polyvinyl pyrrolidone were used, respectively. The yields in distilled water or an ethylene glycol (EG)/distilled water mixture were higher than that in EG alone, and the yield increased with increasing temperature owing to a lower Δ Gred value. Increasing the L-ascorbic acid concentration also increased the yield. The Cu powder synthesized in 3 h at 90°C in distilled water with 272.8 mM of L-ascorbic acid showed the lowest average particle size of 2.52 μm, indicating mechanisms of short burst nucleation and reduced growth via the increased reduction rate of Cu ions. It is estimated that the nucleation step was nearly completed within 10 min in this system. The Cu powders synthesized in an ethylene glycol/distilled water mixture presented an average particle size of 3.76 μm and the highest yield of 87.9%.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1247-1250
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis of Single Crystalline Titanium Oxide and Sodium Titanate Nanorods via Salt-Assisted Ultrasonic Spray Pyrolysis
    Autorzy:
    Hwangbo, Y.
    Yoo, J.-H.
    Lee, Y.-I.
    Powiązania:
    https://bibliotekanauki.pl/articles/352337.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    TiO2
    nanorods
    salt
    Ultrasonic Spray Pyrolysis
    optical properties
    Opis:
    The simple and continuous synthesis of single crystalline anatase titanium dioxide and sodium titanate nanorods by a saltassisted ultrasonic spray pyrolysis method is demonstrated. This method does not require expensive precursors, long reaction time, and physical templates or surfactant. In addition, its continuous nature makes it a suitable method for the large-scale preparation. Moreover, the effect of a salt concentration in a starting solution on material properties, including morphology and phase of the synthesized products was systematically investigated. The synthesized nanorods had one-dimensionality, a single crystalline and the average diameter of 12.3 nm with dual phases of titanium dioxide and sodium titanate by FE-SEM, XRD, HR-TEM as well as FFT-converted SAED pattern analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1411-1414
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Availability analysis of series redundancy models with imperfect switchover and interrupted repairs
    Analiza gotowości modeli redundancji kaskadowej uwzględniających niedoskonałe przełączanie oraz przerwane naprawy
    Autorzy:
    Shim, J.
    Ryu, H.
    Lee, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/302074.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Polskie Naukowo-Techniczne Towarzystwo Eksploatacyjne PAN
    Tematy:
    gotowość
    redundancja kaskadowa
    niedoskonałe przełączenie
    naprawa przerwana
    ogólny czas naprawy
    availability
    series redundancy
    imperfect switchover
    interrupted repair
    general repair time
    Opis:
    This paper considers N + 1 series redundancy, where N components are active and 1 component is standby in normal state. The active components execute the service, while the standby component is ready to take over the active role if the active components fail. When an active component fails, the standby, if available, automatically takes over system operations. However, the automatic switchover of the standby component to active mode might not be possible due to hardware or software issues. When a component failure or an imperfect switchover occurs, it immediately begins to be repaired. However, the repair process is possible to be interrupted. The most existing literature of redundancy models has focused on Markovian systems with uninterrupted repairs. This paper considers a non-Markovian redundancy model with interrupted repairs, where the repair time, the non-automatic switchover time, and the interrupted time are generally distributed. Using supplementary variable method and integro-differential equations, we obtain the steady-state availability for the redundancy model.
    W niniejszym artykule rozważano przypadek redundancji kaskadowej typu N + 1, w której liczba N elementów pozostaje aktywnych, a jeden komponent jest w trybie gotowości w stanie normalnym. Elementy aktywne wykonują usługę, podczas gdy składowa rezerwowa pozostaje w stanie gotowości do przejęcia roli aktywnej w przypadku, gdyby składniki aktywne uległy uszkodzeniu. Gdy element aktywny przestaje działać, element zastępczy, jeśli jest dostępny, automatycznie przejmuje operacje systemowe. Jednak automatyczne przełączenie komponentu zastępczego na tryb aktywny nie zawsze jest możliwe z powodu problemów ze sprzętem lub oprogramowaniem. Jeśli wystąpi awaria komponentu lub niedoskonałe przełączenie, natychmiast rozpoczyna się naprawa. Proces naprawy może jednak zostać przerwany. Większośćistniejącej literatury na temat modeli nadmiarowości koncentruje się na systemach Markowa, w których nie dochodzi do przerwania naprawy. W niniejszym artykule rozważano niemarkowowski model nadmiarowości uwzględniający możliwość przerwania naprawy, w którym czas naprawy, czas nieautomatycznego przełączenia oraz czas przerwany mają rozkład ogólny. Wykorzystując metodę dodatkowej zmiennej oraz równania całkowo-różniczkowe otrzymano gotowość stacjonarną dla omawianego modelu redundancji.
    Źródło:
    Eksploatacja i Niezawodność; 2017, 19, 4; 640-649
    1507-2711
    Pojawia się w:
    Eksploatacja i Niezawodność
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Development of a high-speed air bearing spindle
    Autorzy:
    Ha, Y.-H.
    Lee, D.-W.
    Hwang, Y.-K.
    Lee, C.-M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1429126.pdf
    Data publikacji:
    2008
    Wydawca:
    Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
    Tematy:
    aerostatic bearing
    metal foam
    porous thrust bearing
    porous radial bearing
    Opis:
    This paper investigates an air spindle with both radial and thrust air bearings of newly developing one-directional porous materials. At present, orifice type and porous type are adopted for thrust air bearings. Orifice type thrust air bearing is fabricated by machining several micro-holes on a bearing pad bearing, permeability significantly affected by particle size and machining conditions is an important factor of performance, but it is hard to c porosities is suggested. It has many micro-porosities through axial direction, so stable and plenty of air can be supplied to the thrust bearing pad. A radial air bearing also can be substituted by a radial direction porous bearing as the same reason. In case of driving parts, built-in motor type is widely applied. But it needs additional cooling parts to drop heat from a motor. So application of an air turbine drive with light-weight shaft is suggested and additionally it will reduce fabricating cost.
    Źródło:
    Journal of Machine Engineering; 2008, 8, 4; 25-31
    1895-7595
    2391-8071
    Pojawia się w:
    Journal of Machine Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structural Properties and Mechanical Behavior of the 2 Step-Reinforced Al-Si/SiCp Metal Matrix Composite by Titanium-Fiber
    Autorzy:
    Oak, J.-J.
    Lee, Y. C.
    Park, Y. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356010.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    metal matrix composite
    sintering
    Ti fiber
    mechanical properties
    diffusion
    Opis:
    In this study, the newly designed Al-9Si/SiC particles (SiCp) + Ti-fiber (2step-reinforced Al-9Si alloy matrix) metal matrix composites (MMCs) were fabricated by hot-pressing sintering at 560°C. 2step-reinforced Al-based MMCs were characterized by thermal shrinkage, phase transition, microstructure and tensile strength. The addition of Ti-fiber reduced thermal shrinkage was caused by temperature difference in sintering process as well as enhanced assistance for tensile strength and plastic deformation at room temperature. Experimental results reveal that the 2step-reinforcment sintering by ceramic and metal has a significant effect to increase interface bonding in boundary of each component material and the improved mechanical properties were due to the influence of interfacial product by diffusion. Tensile strength and elongation at room temperature by 2step-reinforcement were improved in 19.5% and 26.2% more than those of Al-9Si/SiCp, respectively. Especially, it reveals that diffusion direction may be varied by sintering methods at low temperature in this study.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1089-1097
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
    Autorzy:
    Jo, Y. J.
    Yoon, Y. H.
    Kim, Y. H.
    Chang, S. Y.
    Kim, J. Y.
    Lee, Y. K.
    Van Tyne, C. J.
    Lee, W. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356790.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    titanium
    implant
    porous
    sintering
    X-ray photoelectron spectroscopy (XPS)
    Opis:
    A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Morphology Change Of Si Deposit In Molten Salt Electrorefining
    Zmiana morfologii osadu Si podczas elektrorafinacji w stopionych solach
    Autorzy:
    Ryu, H. Y.
    Kwon, S. C.
    Han, M. H.
    An, Y. S.
    Lee, J. S.
    Lee, J. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354346.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    molten salt
    silicon
    morphology
    electrorefining
    current density
    sól stopiona
    krzem
    morfologia
    elektrorafinacja
    gęstość prądu
    Opis:
    The effects of processing parameters on the morphology change in a Si deposit recovered by means of molten salt electrorefining are evaluated using electrochemical techniques such as cyclic voltammetry and chronopotentiometry at 800°C. It was found that concentration of K2SiF6 and current density were important parameters in determining deposit size. Higher concentrations of K2SiF6 were effective in coarsening the silicon deposit and decreasing the cell potential. Silicon nanofiber was recovered at 5 wt% of K2SiF6 whereas dense particles were prepared at 30 and 50 wt% of K2SiF6. The morphology of the Si deposit was determined by the concentration of Si in the electrolyte which is related to the formation of crystal and growth of Si. The formation mechanism of the Si deposit was interpreted by using high resolution TEM as well as electrochemical properties.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1491-1497
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Sire pedigree error estimation and sire verification of the Taiwan dairy cattle population by using SNP markers
    Autorzy:
    Chao, C.H.
    Yeh, Y.H.
    Chen, Y.M.
    Lee, K.H.
    Wang, S.H.
    Lin, T.Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/16539078.pdf
    Data publikacji:
    2022
    Wydawca:
    Polska Akademia Nauk. Czasopisma i Monografie PAN
    Tematy:
    Holstein cattle
    genetic testing
    sire pedigree
    Opis:
    Information regarding the correct pedigree of and relationship between animals is useful for managing dairy breeding, reducing inbreeding, estimating breeding value, and establishing correct breeding programs. Additionally, the successful implementation of progeny testing is crucial for improving the genetics of dairy cattle, which depends on the availability of correct pedigree information. Incorrect pedigree information leads to bias in bull evaluation. In this study, Neogen GeneSeek Genomic Profiler (GGP) 50K SNP chips were used to identify and verify the sire of Taiwanese Holstein dairy cattle and analyze the reasons that lead to incorrect sire records. Samples were collected from 2,059 cows of 36 dairy farms, and the pedigree information was provided by breeders. The results of sire verification can be divided into three categories: submitted unconfirmed sire, submitted confirmed sire, and incorrectly submitted verified sire. Data on the sires of 1,323 (64.25%) and 572 (27.78%) dairy cows were verified and discovered, respectively. Sires of 1,895 (92.03%) dairy cattle were identified, which showed that the paternal pedigree of dairy cattle could be discovered and verified through genetic testing. An error-like analysis revealed that the data of 37 sires were incorrectly recorded because the bull’s NAAB code number was incorrectly entered into the insemination records: for 19 sires, the wrong bull was recorded because the frozen semen of a bull placed in the wrong storage tank was used, 6 had no sire records, and for 12 sires, the NAAB code of the correct bull was recorded but with a wrong stud code, marketing code, or unique number for the stud or breed. To reduce recorded sire error rates by at least 27.78%, automated identification of the mated bull must be adopted to reduce human error and improve dairy breeding management on dairy farms.
    Źródło:
    Polish Journal of Veterinary Sciences; 2022, 25, 1; 61-65
    1505-1773
    Pojawia się w:
    Polish Journal of Veterinary Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of Mo-Si-B Intermetallic Compound Powders Under Different Heat Treatment Conditions
    Autorzy:
    Park, J. H.
    Lee, S.
    Kim, D.
    Kim, Y.
    Yang, S. H.
    Lee, S. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/353369.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Mo-Si-B alloys
    intermetallic compounds
    reitveld refinement
    T2 phase
    A15 phase
    Opis:
    In this research, we investigated the effects of reduction atmospheres on the creation of the Mo-Si-B intermetallic compounds (IMC) during the heat treatments. For outstanding anti-oxidation and elevated mechanical strength at the ultrahigh temperature, we fabricated the uniformly dispersed IMC powders such as Mo5SiB2 (T2) and Mo3Si (A15) phases using the two steps of chemical reactions. Especially, in the second procedure, we studied the influence of the atmospheres (e.g. vacuum, argon, and hydrogen) on the synthesis of IMCs during the reduction. Furthermore, the newly produced IMCs were observed by SEM, XRD, and EDS to identify the phase of the compounds. We also calculated an amount of IMCs in the reduced powders depending on the atmosphere using the Reitveld refinement method. Consequently, it is found that hydrogen atmosphere was suitable for fabrication of IMC without other IMC phases.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1509-1512
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A study on the development of a new grinding processes for high-lead ball screw nuts
    Autorzy:
    Choi, Ch.
    Ha, Y.
    Kim, H.
    Lee, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/99599.pdf
    Data publikacji:
    2010
    Wydawca:
    Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
    Tematy:
    high-lead ball screw nuts
    new grinding process
    surface roughness
    Opis:
    This paper proposes a method that machines the race of high-lead ball screw nuts, which is difficult to machine using the existing geometrical machining method, without any interferences and changes in its load rating in order to perform the high-speed in ball screws. This study calculates the inclination angle of the axis of the grinding stone for avoiding the contact of the axis to the inner diamete of the nut and determines the shape of the grinding stone through changing the inclination angle and dressing curvature determined in a dressing device Then, the grinding condition will be determined by measuring the shape meter of the screw race for solving the problem. Also, the surface roughness of the grinded surface was measured using a surface roughness tester, and check with applying a grinding process of product not being high-lead ball screw.
    Źródło:
    Journal of Machine Engineering; 2010, 10, 1; 50-57
    1895-7595
    2391-8071
    Pojawia się w:
    Journal of Machine Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Positron Annilation Lifetime and Glass Transition Temperatures in $CO_2$ Sorption Polystyrene
    Autorzy:
    Jean, Y.
    Chen, H.
    Lee, L.
    Yang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1812530.pdf
    Data publikacji:
    2008-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.70.Bj
    78.66.Qn
    71.60.+z
    Opis:
    Positron annihilation lifetime spectroscopy was used to measure the free-volume size and distributions as a function of temperature in polystyrene with and without 400 psi $CO_2$ sorption. The transition temperatures in the polystyrene with $CO_2$ sorption obtained from ortho-positronium lifetimes were found to depend on the thermal cycles and a meta-stable state showing a negative thermal expansion coefficient was observed between 53°C and 82°C during the first heating up experiment. The observed $T_g$ in polystyrene with, and without $CO_2$ sorption after annealing from ortho-positronium lifetimes were found to be 86°C and 91°C, which are 5°C higher, and 10°C lower than from the differential scanning calorimetry data, respectively. The observed free-volume variations are discussed in terms of hole expansion, creation, free-volume relaxation, plasticization, and hole filling in amorphous polymers.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 5; 1385-1395
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Non-parametric machine learning methods for evaluating the effects of traffic accident duration on freeways
    Autorzy:
    Lee, Y.
    Wei, C.-H.
    Chao, K.-C.
    Powiązania:
    https://bibliotekanauki.pl/articles/223569.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    accident on freeway
    accident duration
    effect evaluating
    correlation
    artificial neural networks
    k-nearest neighbour method
    wypadek na autostradzie
    czas trwania wypadku
    ocena skutków
    korelacja
    sztuczne sieci neuronowe
    metoda najbliższego sąsiada
    Opis:
    Traffic accidents usually cause congestion and increase travel-times. The cost of extra travel time and fuel consumption due to congestion is huge. Traffic operators and drivers expect an accurately forecasted accident duration to reduce uncertainty and to enable the implementation of appropriate strategies. This study demonstrates two non-parametric machine learning methods, namely the k-nearest neighbour method and artificial neural network method, to construct accident duration prediction models. The factors influencing the occurrence of accidents are numerous and complex. To capture this phenomenon and improve the performance of accident duration prediction, the models incorporated various data including accident characteristics, traffic data, illumination, weather conditions, and road geometry characteristics. All raw data are collected from two public agencies and were integrated and cross-checked. Before model development, a correlation analysis was performed to reduce the scale of interrelated features or variables. Based on the performance comparison results, an artificial neural network model can provide good and reasonable prediction for accident duration with mean absolute percentage error values less than 30%, which are better than the prediction results of a k-nearest neighbour model. Based on comparison results for circumstances, the Model which incorporated significant variables and employed the ANN method can provide a more accurate prediction of accident duration when the circumstances involved the day time or drunk driving than those that involved night time and did not involve drunk driving. Empirical evaluation results reveal that significant variables possess a major influence on accident duration prediction.
    Źródło:
    Archives of Transport; 2017, 43, 3; 91-104
    0866-9546
    2300-8830
    Pojawia się w:
    Archives of Transport
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Compositional Dependence of Hardness of Ge-Sb-Se Glass for Molded Lens Applications
    Zależność stężeniowa twardości szkła Ge-Sb-Se do zastosowań na formowane soczewki
    Autorzy:
    Park, J. K.
    Lee, J. H.
    Shin, S. Y.
    Yi, J. H.
    Lee, W. H.
    Park, B. J.
    Choi, J. H.
    Kim, N. Y.
    Choi, Y. G.
    Powiązania:
    https://bibliotekanauki.pl/articles/352228.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    chalcogenide glasses
    Ge-Sb-Se glass
    infrared lens
    molded lens
    infrared camera
    szkło
    Ge-Sb-Se
    soczewki formowane
    twardość szkła
    kamera termowizyjna
    Opis:
    Chalcogenide glass in the ternary Ge-Sb-Se system is inherently moldable, thus being considered as a strong candidate material for use in infrared-transmitting lens applications from the viewpoint of thermal and mechanical stability. In an effort to experimentally determine compositional region suitable for the molded lens applications, we evaluate its compositional dependence of hardness. Among the constituent atoms, Ge content turns out to exert a most conspicuous correlation with hardness. This phenomenological behavior is then explained in connection with the structural evolution that Ge brings about.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1205-1208
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization Of The Graded Microstructure In Powder Sintered Porous Titanium
    Charakterystyka gradientowej mikrostruktury porowatego tytanu spiekanego z proszku
    Autorzy:
    Oak, J.-J.
    Bang, J. I.
    Bae, K.-C.
    Kim, Y. H.
    Lee, Y. C.
    Chun, H. H.
    Park, Y. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356239.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    titanium
    powder metallurgy
    porous structure
    sintering
    biomaterial
    tytan
    metalurgia proszków
    struktura porowata
    spiekanie
    biomateriał
    Opis:
    The proposed sintering process produce porosity and functional graded microstructure in the sinterd titanium powders. Titanium powders with different micro sizes were sintered at the proposed temperature region at 1200 and 1300°C for 2h. The apatite-forming on the graded microstructure is observed by immersion test in Hanks balanced salt soluion at 37°C. Sintering condition of titanium powders is estimated by thermogravitmetry-differential thermal analysis (TG-DTA). The synthersied surface structures and apatite-forming ability were characterized by a field emission scanning electron microscopy (FE-SEM) observation and energy dispersive X-ray spectroscopy (EDS) analysis. As results, these graded microstructure of sintered porous titanium powders reveals apatite-forming ability as osseointegration by calcification in Hanks balanced salt soluion(HBSS) at 37°C.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1265-1269
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Finite element analysis of three-point bending of a T-beam structural biaxial highly oriented polymer material
    Analiza metodą elementów skończonych zginania trójpunktowego belki teowej wykonanej z wysoko zorientowanego dwuosiowo materiału polimerowego
    Autorzy:
    Wei, C.-L.
    Chang, Y.
    Lee, Y.-C.
    Lee, R.
    Luo, T.-W.
    Chen, J.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/946988.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
    Tematy:
    solid phase processing
    highly oriented polymer (HOP)
    orthotropic materials
    T-beam
    three-point bending
    finite element
    proces w fazie stałej
    wysoko zorientowany polimer
    materiały ortotropowe
    belka teowa
    zginanie trójpunktowe
    elementy skończone
    Opis:
    Polymers with biaxial aligned molecular chains are also orthotropic materials, which are characterized by high tensile strength and low shear strength in the length direction. When orthotropic materials are used as structural shapes with poor shear strength, they are likely to undergo premature failure under shear stress. Therefore, in three-point bending, the cross-section of the entire profile not only bears tensile stress and compressive stress in the length direction, but also simultaneously exhibits shear stress. This study analyzes the distribution of tensile stress, compressive stress and shear stress in the length direction of highly oriented polymers (HOP) by finite element analysis to find the most suitable length-to-height ratio for these materials when used as structural shapes. The finite element analysis software, Abaqus, is utilized to simulate HOP T-beam to analyze the load stress of a T-beam. With a fixed cross–section area, as the length of the material changes, its shear strength also changes. Accordingly, the order of occurrence of tensile failure and shear failure can be investigated. The simulation reveals that when the length-to-height ratio is between 4 : 1 and 20 : 1, a zone of stress in which tensile failure and shear failure occur can be found. This result can be exploited in the design and development of structural beam.
    Polimery o dwuosiowo zorientowanych łańcuchach makrocząsteczek są materiałami ortotropowymi, wykazującymi dużą wytrzymałość na rozciąganie oraz niewielką wytrzymałość na ścinanie w kierunku długości. Elementy konstrukcyjne wytworzone z materiału ortotropowego o małej wytrzymałości na ścinanie są podatne na przedwczesne uszkodzenie pod wpływem naprężeń ścinających. Przy zginaniu trójpunktowym w przekroju ich profilu występują zarówno naprężenia rozciągające i ściskające w kierunku podłużnym, jak i naprężenia ścinające. Metodą elementów skończonych analizowano rozkład naprężeń rozciągających, ściskających i ścinających w kierunku podłużnym wysoko zorientowanych polimerów (HOP) w celu określenia optymalnego stosunku długości do wysokości w kształtach konstrukcyjnych. Do symulacji naprężeń obciążeniowych w zginaniu trójpunktowym belki teowej wykorzystano program komputerowy Abaqus. Stwierdzono, że przy stałej powierzchni przekroju poprzecznego belki jej wytrzymałość na ścinanie zmienia się wraz ze zmianą długości. Badano również kolejność występowania uszkodzeń pod wpływem działania sił rozciągających i ścinających. Symulacja wykazała, że przy stosunku długości do wysokości w zakresie od 4 : 1 do 20 : 1 występuje strefa naprężeń, w której mogą się pojawiać uszkodzenia w wyniku rozciągania lub ścinania. Uzyskane wyniki można wykorzystać w projektowaniu i optymalizacji belek konstrukcyjnych.
    Źródło:
    Polimery; 2018, 63, 3; 219-223
    0032-2725
    Pojawia się w:
    Polimery
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Properties of Copper Doped Neodymium Nickelate Oxide as Cathode Material for Solid Oxide Fuel Cells
    Autorzy:
    Lee, K. J.
    Choe, Y-J.
    Hwang, H-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/351292.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    solid oxide fuel cells
    copper
    electrical conductivity
    excess oxygen
    Opis:
    Mixed ionic and electronic conducting K2NiF4-type oxide, Nd2Ni1-xCuxO4+δ (x=0~1) powders were synthesized by solid state reaction technique and solid oxide fuel cells consisting of a Nd2Ni1-xCuxO4+δ cathode, a Ni-YSZ anode and ScSZ as an electrolyte were fabricated. The effect of copper substitution for nickel on the electrical and electrochemical properties was examined. Small amount of copper doping (x=0.2) resulted in the increased electrical conductivity and decreased polarization resistance. It appears that this phenomenon was associated with the high mean valence of nickel and copper and the resulting excess oxygen (δ). It was found that power densities of the cell with the Nd2Ni1-xCuxO4+δ (x=0.1 and 0.2) cathode were higher than that of the cell with theNd2NiO4+δ cathode.
    Źródło:
    Archives of Metallurgy and Materials; 2016, 61, 2A; 625-628
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Recommended Integrated Mechanism to Enhance OSH Management of Blue-Collar Foreign Workers in Taiwan
    Autorzy:
    Liao, H. C.
    Cheng, S. F.
    Wang, Y.
    Lee, L. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/90376.pdf
    Data publikacji:
    2014
    Wydawca:
    Centralny Instytut Ochrony Pracy
    Tematy:
    occupational safety and health
    Labor Safety and Health Act
    OSH training program
    manpower agency
    blue-collar foreign worker
    bezpieczeństwo i higiena pracy
    zdrowie
    szkolenie BHP
    Opis:
    This study examines the roles and functions of businesses, labor-exporting countries’ representative offices in Taiwan, religious organizations, and manpower agencies in promoting occupational safety and health (OSH). It also offers advice to Taiwanese authorities on making policies and improvements regarding the oversight mechanism mandated by the Labor Safety and Health Act, giving them an idea of what to focus on when enforcing control over blue-collar foreign workers’ OSH conditions. This study also proposes that Taiwanese authorities may serve not only as an overseer/inspector of those hiring blue-collar foreign workers in Taiwan, but also expand their role to lay down policies regarding a variety of OSH teaching materials in the blue-collar foreign workers’ native languages (spoken or written), the qualifications of translators in blue-collar foreign workers’ OSH training programs, and regulations concerning the longer hours such training programs take.
    Źródło:
    International Journal of Occupational Safety and Ergonomics; 2014, 20, 4; 537-549
    1080-3548
    Pojawia się w:
    International Journal of Occupational Safety and Ergonomics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of Heat-Treatment On Microstructure And Magnetic Properties Of Nanocrystallized Mn-Zn Ferrite Powders
    Wpływ obróbki cieplnej na mikrostrukturę i właściwości magnetyczne nanokrystalicznych proszków ferrytu Mn-Zn
    Autorzy:
    Lee, W. H.
    Hong, C. S.
    Chang, S. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/351552.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    high energy ball milling
    nanosized particles
    crystallite size
    magnetic properties
    frezowanie kulowe
    nanocząstki
    wielkości krystalitów
    właściwości magnetyczne
    Opis:
    The initial ferrite powders were subjected to high energy ball milling at 300rpm for 3h, and subsequently heat-treated at 573-1273K for 1h. Based on the observation of microstructure and measurement of magnetic properties, the heat-treatment effect was investigated. The size of initial powders was approximately 70μm. After milling, the powders with approximately 230nm in size were obtained, which were composed of the nano-sized particles of approximately 15nm in size. The milled powders became larger to approximately 550nm after heat-treatment at 973K. In addition, the size of particles increased to approximately 120nm with increasing temperature up to 973K. The coercivity of initial powders was almost unchanged after milling, whereas the saturation magnetization increased. As the heat-treatment temperature increased, the saturation magnetization gradually increased and the maximum coercivity was obtained at 773K.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1347-1350
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Cr Poisoning On Nd2Ni0.95Cu0.05O4+δ Cathode for Solid Oxide Fuel Cells
    Autorzy:
    Choe, Y-J.
    Lee, K. J.
    Hwang, H-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/354728.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    chromium poisoning
    Ruddlesden-Popper
    layered perovskite
    solid oxide fuel cells
    Nd2NiO4
    Opis:
    In this study, Nd2Ni1-xCuxO4+δ (x=0, 0.05, 0.1, and 0.2) layered perovskite powders were synthesized by the glycine nitrate process (GNP) and the chromium poisoning effect on the electrochemical performance of the Nd2Ni0.95Cu0.05O4+δ and La0.6Sr0.4Co0.2Fe0.88O3-δ cathodes were investigated. In the case of the LSCF cathode, the strontium chromite phase formed after the exposure of the gaseous chromium species, while there was no additional phase in the Nd2Ni0.95Cu0.05O4+δ cathode. The area specific resistance (ASR) of the Nd2Ni0.95Cu0.05O4+δ cathode did not change significantly after the exposure of the gaseous chromium species at 800°C
    Źródło:
    Archives of Metallurgy and Materials; 2016, 61, 2A; 629-634
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    High-temperature Oxidation Behavior and Kinetics of Forged 12Cr-MoVW Steel
    Autorzy:
    Kim, Y. H.
    Oak, J.-J.
    Bae, K.-C.
    Lee, W-J.
    Park, Y. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/351450.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    ferritic/martensitic stainless steels
    forging
    oxidation kinetics
    oxide layer
    Opis:
    The oxidation kinetics of forged 12Cr-MoVW steel was investigated in an air (N2+O2) atmosphere at 873-1073 K (Δ50 K) using thermogravimetric analysis. The oxidized samples were characterized using X-ray diffraction, and the surface and cross-sectional morphologies were examined using scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy. The forged 12Cr-MoVW steel samples exhibited parabolic behavior and a low oxidation rate compared with their as-cast counterparts. A protective oxide layer was uniformly formed at relatively low temperature (≤973 K) for the forged samples, which thus exhibited better oxidation resistance than the as-cast ones. These oxides are considered solid-solution compounds such as (Fe, Cr)2O3.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1099-1104
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Self-Consolidation Mechanism Of Porous Ti-6Al-4V Implant Prototypes Produced By Electro-Discharge-Sintering Of Spherical Ti-6Al-4V Powders
    Mechanizm autokonsolidacji prototypów porowatych implantów wytworzonych przez spiekanie sferycznych proszków Ti-6Al-4V
    Autorzy:
    Lee, W. H.
    Jo, Y. J.
    Kim, Y. H.
    Jo, Y. H.
    Seong, J. G.
    Van Tyne, C. J.
    Chang, S. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/356277.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ti-6Al-4V
    implant
    porous
    sintering
    electrodischarge
    porowatość
    spiekanie
    proszki spiekane
    Opis:
    Electro-Discharge-Sintering (EDS) was employed to fabricate Ti-6Al-4V porous implant prototypes from atomized powders (100 – 150 μm), that were subjected to discharges of 0.75 to 2.0 kJ/0.7g-powder from 150, 300, and 450 μF capacitors. Both fully porous and porous-surfaced Ti-6Al-4V compacts with various solid core sizes were self-consolidated in less than 86 – 155 μsec. It is known that EDS can simultaneously produce the pinch pressure to squeeze and deform powder particles and the heat to weld them together. The formation of a solid core in these prototypes depends on the amounts of both the pinch pressure and heat generated during a discharge. The size of the solid core and the thickness of the porous layer can be successfully controlled by manipulating the discharge conditions such as input energy and capacitance.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1185-1189
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects Of Environmental Factors On The Dispersion Behavior Of Iron Oxide In Aqueous Solutions With Poly Acrylic Acid
    Wpływ parametrów charakteryzujących wodne roztwory poli(kwasu akrylowego) na dyspersję tlenku żelaza
    Autorzy:
    Lee, E.-H.
    Kim, K.-M.
    Maeng, W.-Y.
    Hur, D.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354513.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    polyacrylic acid
    dispersion stability
    magnetite
    nanoparticles
    suspension
    poli(kwas akrylowy)
    stabilność dyspersji
    magnetyt
    nanocząstki
    zawiesina
    Opis:
    After preparing aqueous suspensions from magnetite particles with a poly-acrylic acid, we investigated the effects of several experimental parameters. We characterized the stability of the suspensions using visual inspection, sedimentation, adsorption, and thermal stability of the dispersant. The dispersion stability is affected by the solution pH, the concentrations of magnetite particles, the molecular weight, the concentration of the dispersants, and the temperature. The stability of the suspensions increased as the concentration of the dispersant and the temperature increased. In terms of the molecular weights of the dispersant, the suspensions with dispersant of low-molecular weight (1800) were more stable than those of high-molecular weight (250000) at room temperature. However, at high temperature the suspensions with high-molecular weight showed stability. The adsorption efficiency of the dispersant was very low. The dispersant of high-molecular weight showed a higher thermal integrity than that of low-molecular weight. From this work, we obtained the optimum conditions for stable aqueous suspensions of magnetite particles.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1561-1564
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Heat Treatment on the Microstructure and Tensile Deformation Behavior of Oxide Dispersion Strengthened Alloys Manufactured by Complex Milling Process
    Autorzy:
    Kim, Y.-K.
    Kim, J.-H.
    Gwon, J.-H.
    Lee, K.-A.
    Powiązania:
    https://bibliotekanauki.pl/articles/352535.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    ball milling
    oxide dispersion strengthening
    microstructure
    tensile deformation behavior
    Opis:
    This study attempted to manufacture an ODS alloy by combining multiple milling processes in mechanical alloying stage to achieve high strength and fracture elongation. The complex milling process of this study conducted planetary ball milling, cryogenic ball milling and drum ball milling in sequential order, and then the microstructure and tensile deformation behavior were investigated after additional heat treatment. The oxide particles distributed within the microstructure were fine oxide particles of 5~20 nm and coarse oxide particles of 100~200 nm, and the oxide particles were confirmed to be composed of Cr, Ti, Y and O. Results of tensile tests at room temperature measured yield strength, tensile strength and elongation as 1320 MPa, 2245 MPa and 4.2%, respectively, before heat treatment, and 1161 MPa, 2020 MPa and 5.5% after heat treatment. This results indicate that the ODS alloy of this study gained very high strengths compared to other known ODS alloys, allowing greater plastic zones.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1335-1340
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Double Step Sintering Behavior Of 316L Nanoparticle Dispersed Micro-Sphere Powder
    Dwuetapowe spiekanie mikrosferycznych nanocząstek proszku 316L
    Autorzy:
    Jeon, B.
    Sohn, S. H.
    Lee, W.
    Han, C.
    Kim, Y. D.
    Choi, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/355221.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    316L stainless steel
    nanoparticle dispersed micro-sphere
    pulse wire explosion
    sintering
    stal nierdzewna 316L
    spiekanie dwuetapowe
    mikrosferyczne nanocząstki
    Opis:
    316L stainless steel is a well-established engineering material and lots of components are fabricated by either ingot metallurgy or powder metallurgy. From the viewpoints of material properties and process versatility, powder metallurgy has been widely applied in industries. Generally, stainless steel powders are prepared by atomization processes and powder characteristics, compaction ability, and sinterability are quite different according to the powder preparation process. In the present study, a nanoparticle dispersed micro-sphere powder is synthesized by pulse wire explosion of 316L stainless steel wire in order to facilitate compaction ability and sintering ability. Nanoparticles which are deposited on the surface of micro-powder are advantageous for a rigid die compaction while spherical micro-powder is not to be compacted. Additionally, double step sintering behavior is observed for the powder in the dilatometry of cylindrical compact body. Earlier shrinkage peak comes from the sintering of nanoparticle and later one results from the micro-powder sintering. Microstructure as well as phase composition of the sintered body is investigated.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1155-1158
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of The Desorption-Recombination Temperature On The Microstructure And Magnetic Properties Of HDDR Processed Nd-Fe-B Powders
    Wpływ temperatury desorpcji-rekombinacji na mikrostrukturę i właściwości magnetyczne proszków Nd-Fe-B przetwarzanych metodą HDDR
    Autorzy:
    Lee, J.-G.
    Cha, H.-R.
    Liu, S.
    Yu, J.-H.
    Baek, Y.-K.
    Kwon, H.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/353723.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B
    HDDR
    permanent magnet
    grain boundary
    metoda HDDR
    magnes trwały
    granica ziarna
    Opis:
    The effect of the desorption-recombination temperature on the microstructure and magnetic properties of hydrogenation-disproportionation-desorption-recombination (HDDR) processed Nd-Fe-B powders was studied. The NdxB6.4Ga0.3Nb20.2Febal (x=12.5-13.5, at.%) casting alloys were pulverized after homogenizing annealing, and then subjected to HDDR treatment. During the HDDR process, desorption-recombination (DR) reaction was induced at two different temperature, 810°C and 820°C. The higher Nd content resulted in enhanced coercivity of the HDDR powder, and which was attributed to the thicker and more uniform Nd-rich phase along grain boundaries. But this uniform Nd-rich phase induced faster grain growth. The remanence of the powder DR-treated at 820°C is higher than that DR-treated at 810°C. In addition, it was also confirmed that higher DR temperature is much more effective to improve squareness.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1499-1501
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    High Temperature Oxidation Property of SiC Coating Layer Fabricated by Aerosol Deposition Process
    Autorzy:
    Ham, G.-S.
    Kim, S.-H.
    Park, J.-Y.
    Lee, K.-A.
    Powiązania:
    https://bibliotekanauki.pl/articles/352142.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    silicon carbide
    aerosol deposition
    coating
    high temperature oxidation
    Opis:
    This study investigated the high temperature oxidation property of SiC coated layer fabricated by aerosol deposition process. SiC coated layer could be successfully manufactured by using pure SiC powders and aerosol deposition on the Zr based alloy in an optimal process condition. The thickness of manufactured SiC coated layer was measured about 5 μm, and coating layer represented high density structure. SiC coated layer consisted of α-SiC and β-SiC phases, the same as the initial powder. The initial powder was shown to have been crushed to the extent and was deposited in the form of extremely fine particles. To examine the high temperature oxidation properties, oxidized weight gain was obtained for one hour at 1000°C by using TGA. The SiC coated layer showed superior oxidation resistance property than that of Zr alloy (substrate). The high temperature oxidation mechanism of SiC coated layer on Zr alloy was suggested. And then, the application of aerosol deposited SiC coated layer was also discussed.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1347-1351
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Trace Elements (Co, Cr) on the Microstructure and Physical Properties of Al-Si-Cu-Mg-Fe Extruded Alloy
    Autorzy:
    Ahn, S. S.
    Sharief, P.
    Lee, C. H.
    Son, H. T.
    Kim, Y. H.
    Kim, Y. C.
    Hong, S.
    Hong, S. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/352787.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Si alloy
    microstructure
    extrusion
    coefficient of thermal expansion
    trace elements
    Opis:
    Trace elements Co, Cr were added to investigate their influence on the microstructure and physical properties of Al-Si extruded alloy. The Co, Cr elements were randomly distributed in the matrix, forms intermetallic phase and their existence wereconfirmed by XRD, EDS and SEM analysis. With addition of trace elements, the microstructure was modified, Si particle size was reduced and the growth rate of β-(Al5 FeSi) phase limited. Compared to parent alloy, hardness and tensile strength were enhanced while the linear coefficient of thermal expansion (CTE) was significantly reduced by 42.4% and 16.05% with Co and Cr addition respectively. It is considered that the low CTE occurs with addition of Co was due to the formation of intermetallic compound having low coefficient of thermal expansion. The results suggested that Co acts as an effective element in improving the mechanical properties of Al-Si alloy.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 3; 857-862
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Compression Properties of Fe-Cr-B Alloy Manufactured using Laser Metal Deposition
    Autorzy:
    Joo, Y.-A.
    Yoon, T.-S.
    Park, S.-H.
    Lee, K.-A.
    Powiązania:
    https://bibliotekanauki.pl/articles/352075.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Fe-Cr-B composite
    laser Metal Deposition
    bulk type
    microstructure
    compressive properties
    Opis:
    Fe-Cr-B alloy is a material with precipitation of boride inside Fe matrix, and it features outstanding hardness and wear resistance properties. However, Fe-Cr-B alloy is a difficult material to process, making it difficult to use as a bulk type structure material which requires delicate shapes. This study attempted to manufacture Fe-Cr-B alloy using a 3D printing process, laser metal deposition. This study also investigated the microstructure, hardness and compression properties of the manufactured alloy. Phase analysis results is confirmed that α-Fe phase as matrix and (Cr, Fe)2B phase as reinforcement phase. In the case of (Cr, Fe)2B phase, differences were observed according to the sample location. While long, coarse, unidirectional needle-type boride phases (~11 μm thickness) were observed in the center area of the sample, relatively finer boride phases (~6 μm thickness) in random directions were observed in other areas. At room temperature compression test results confirmed that the sample had a compression strength is approximately 2.1 GPa, proving that the sample is a material with extremely high strength. Observation of the compression fracture surface identified intergranular fractures in areas with needle-type boride, and transgranular fractures in areas with random borides. Based on this results, this study also reviewed the deformation behavior of LMD Fe-Cr-B alloy in relation to its microstructures.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1459-1462
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    CO Oxidation Properties Of Selective Dissoluted Metallic Glass Composites
    Utlenianie wybranych rozcieńczonych kompozytów szkieł metalicznych
    Autorzy:
    Kim, S. Y.
    Lee, M. H.
    Kim, T. S.
    Kim, B. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/355092.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    CO oxidation
    metallic glasses
    porous metal
    catalyst materials
    utlenianie
    szkło metaliczne
    metale porowate
    materiał katalityczny
    Opis:
    Porous metallic materials have been widely used in many fields including aerospace, atomic energy, electro chemistry and environmental protection. Their unique structures make them very useful as lightweight structural materials, fluid filters, porous electrodes and catalyst supports. In this study, we fabricated Ni-based porous metallic glasses having uniformly dispersed micro meter pores by the sequential processes of ball-milling and chemical dissolution method. We investigated the application of our porous metal supported for Pt catalyst. The oxidation test was performed in an atmosphere of 1% CO and 3% O2. Microstructure observation was performed by using a scanning electron microscope. Oxidation properties and BET (Brunauer, Emmett, and Teller) were analyzed to understand porous structure developments. The results indicated that CO Oxidation reaction was dependent on the specific surface area.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1227-1229
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
    Autorzy:
    Lee, H.-E.
    Kim, Y. S.
    Park, J. K.
    Oh, S.-T.
    Powiązania:
    https://bibliotekanauki.pl/articles/355552.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    high energy ball milling
    Ni-base ODS superalloy
    particle and crystalline size
    microstructure
    Opis:
    Microstructure evolution of Ni-based oxide dispersion-strengthened alloy powders with milling time is investigated. The elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % were ball-milled by using horizontal rotary ball milling with the change of milling velocity. Microstructure observation revealed that large aggregates were formed in the early stages of ball milling, and further milling to 5 h decreased particle size. The average crystalline size, estimated by the peak broadening of XRD, decreased from 28 nm to 15 nm with increasing milling time from 1 h to 5 h. SEM and EPMA analysis showed that the main elements of Ni and Cr were homogeneously distributed inside the powders after ball milling of 5 h.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1253-1255
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Manufacturing and Macroscopic Properties of Y2O3 Coating Layer on Ceramic (AlN) Substrate Fabricated by Aerosol Deposition
    Autorzy:
    Wi, D.-Y.
    Ham, G.-S.
    Kim, S.-H.
    Lee, K.-A.
    Powiązania:
    https://bibliotekanauki.pl/articles/353052.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    aerosol deposition
    Y2O3 coating layer
    AlN matrix
    nano indentation
    Opis:
    This study attempted to manufacture an Y2O3 ceramic coating layer on a ceramic (AlN) substrate using aerosol deposition (AD) and investigated its macroscopic properties. Pure Y2O3 powder with a polygonal shape and average size of 5.0 μm was used as initial feedstock. Using aerosol deposition with suitable process conditions, an Y2O3 coating layer was successfully fabricated on aluminum nitride (AIN). The thickness of the manufactured coating layer was approximately 10 mm. The coating layer consisted of Y2O3 phase identical to that in the initial powder, and no additional oxides were identified. In regard to the roughness of the Y2O3 coating layer, the average roughness (Ra) measured 1.32 μm, indicating that the surface roughness was relatively even compared to the initial powder size (5 μm). Mechanical properties of the Y2O3 coating layer were measured using nano indentation equipment, and the indentation modulus of the Y2O3 coating layer fabricated by aerosol deposition measured 136.5 GPa. The interface of the coating layer was observed using TEM, and the deposition mechanism of the Y2O3 coating layer manufactured by aerosol deposition was also discussed.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1463-1466
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Heat Treatment on Microstructure and Impact Toughness of Ti-6Al-4V Manufactured by Selective Laser Melting Process
    Autorzy:
    Lee, K.-A.
    Kim, Y.-K.
    Yu, J.-H.
    Park, S.-H.
    Kim, M.-C.
    Powiązania:
    https://bibliotekanauki.pl/articles/354570.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    selective laser melting
    Ti-6Al-4V
    microstructure
    impact toughness
    heat treatment
    Opis:
    This study manufactured Ti-6Al-4V alloy using one of the powder bed fusion 3D-printing processes, selective laser melting, and investigated the effect of heat treatment (650°C/3hrs) on microstructure and impact toughness of the material. Initial microstructural observation identified prior-β grain along the building direction before and after heat treatment. In addition, the material formed a fully martensite structure before heat treatment, and after heat treatment, α and β phase were formed simultaneously. Charpy impact tests were conducted. The average impact energy measured as 6.0 J before heat treatment, and after heat treatment, the average impact energy increased by approximately 20% to 7.3 J. Fracture surface observation after the impact test showed that both alloys had brittle characteristics on macro levels, but showed ductile fracture characteristics and dimples at micro levels.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1341-1346
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
    Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
    Autorzy:
    Son, S. H.
    Park, S. C.
    Kim, J. H.
    Kim, Y. H.
    Lee, M. S.
    Ahn, J.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/352665.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    electrorefining
    tin
    electronic waste
    recycling
    high purity
    elektrorafinacja
    cyna
    odpady elektroniczne
    recykling
    Opis:
    The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Multistep Heat-Treatment Effects on Electrospun Nd-Fe-B-O Nanofibers
    Autorzy:
    Jeon, E. J.
    Eom, N. S. A.
    Lee, J.
    Lee, B.
    Cho, H. M.
    On, J. S.
    Choa, Y.-H
    Kim, B. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/354311.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B
    nanofibers
    electrospinning
    heat treatment
    Opis:
    Neodymium-Iron-Boron (Nd-Fe-B) magnets are considered to have the highest energy density, and their applications include electric motors, generators, hard disc drives, and MRI. It is well known that a fiber structure with a high aspect ratio and the large specific surface area has the potential to overcome the limitations, such as inhomogeneous structures and the difficulty in alignment of easy axis, associated with such magnets obtained by conventional methods. I n this work, a suitable heat-treatment procedure based on single-step and multistep treatments to synthesize sound electrospun Nd-Fe-B-O nanofibers of Φ572 nm was investigated. The single-step heat-treated (directly heat-treated at 800°C for 2 h in air) samples disintegrated along with the residual organic compounds, whereas the multistep heat-treated (sequential three-step heat-treated including three steps;: dehydration (250°C for 30 min in an inert atmosphere), debinding (650°C for 30 min in air), and calcination (800°C for 1 h in air)) fibers maintained sound fibrous morphology without any organic impurities. They could maintain such fibrous morphologies during the dehydration and debinding steps because of the relatively low internal pressures of water vapor and polymer, respectively. In addition, the NdFeO3 alloying phase was dominant in the multistep heat-treated fibers due to the removal of barriers to mass transfer in the interparticles.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1433-1437
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of AZ31/CNT Surface Nano-composite by Double-pass Friction Stir Processing
    Autorzy:
    Kim, J. Y.
    Hwang, J.-W.
    Kim, H. Y.
    Lee, S. M.
    Jung, W.-S.
    Byeon, J.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/355624.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    surface modification
    Double-pass Friction Stir Processing
    AZ31
    composite
    CNT
    Opis:
    Double-pass Friction Stir Processing (FSP) was applied to fabricate an AZ31/CNT nano-composite for surface hardening of lightweight structural components. The effects of double-pass FSP as well as groove depth (i.e., volume fraction of CNT) on the CNT distribution, dynamically recrystallized grain size, and resulting microhardness were studied. Double-pass FSP was performed for the CNT-filled plate-type specimen with different groove depths of 2, 3, and 4 mm. By applying double-pass FSP, the average size of CNT clusters decreased, implying a more homogeneous distribution. Compared with the FSPed specimen without CNT, grain size was refined from 19 μm to 3 μm and microhardness increased from 52 Hv to 83 Hv (i.e., 71% increase).
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1039-1042
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of the Calcination Temperature on the Optical and Mechanical Properties of Y2O3-MgO Nanocomposite
    Autorzy:
    Yong, S.-M.
    Choi, D. H.
    Lee, K.
    Ko, S.-Y.
    Cheong, D.-I.
    Powiązania:
    https://bibliotekanauki.pl/articles/351252.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    infrared transparent ceramics
    Y2O3-MgO nanocomposites
    sol-gel combustion synthesis
    calcination
    spark plasma sintering
    Opis:
    Y2O3-MgO nanocomposites are one of the most promising materials for hypersonic infrared windows and domes due to their excellent optical transmittance and mechanical properties. In this study, influence of the calcination temperature of Y2O3-MgO nanopowders on the microstructure, IR transmittance, and hardness of Y2O3-MgO nanocomposites was investigated. It was found that the calcination temperature is related to the presence of residual intergranular pores and grain size after spark plasma sintering. The nanopowders calcined at 1000°C exhibits the highest infrared transmittance (82.3% at 5.3 μm) and hardness (9.99 GPa). These findings indicated that initial particle size and distribution of the nanopowders are important factors determining the optical and mechanical performances of Y2O3-MgO nanocomposites.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1481-1484
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Oxidation Behavior of Steel with Cr Content and Water Flow Rate
    Autorzy:
    Kim, D.-J.
    Kim, K. M.
    Shin, J. H.
    Cheong, Y. M.
    Lee, E. H.
    Lee, G. G.
    Kim, S. W.
    Kim, H. P.
    Choi, M. J.
    Lim, Y. S.
    Hwang, S. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/351548.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    steel
    flow accelerated corrosion
    Cr content
    flow rate
    surface oxides
    Opis:
    Fast water flow facilitates ferrous ion transport leading to flow accelerated corrosion (FAC) of carbon steel and the possibility of a large accident through a failure of a secondary pipe in a nuclear power plant. Ion transport is directly linked to oxide properties such as the thickness, chemical composition and porosity. This work deals with a precise observation of the cross section of the corroded specimen focusing on an oxide passivity and its thickness using SEM (scanning electron microscope) and TEM (transmission electron microscope) as well as an apparent weight loss and a surface observation for the specimens corroded using a rotating cylindrical electrode autoclave system in pure water of pH 7 at 150°C having dissolved oxygen below 1 ppb within a flow rate range of 0 to 10 m/s. The Cr content in steel was changed from 0.02 to 2.4 wt%. Increasing the Cr content in the alloy, the FAC rate and oxide thickness decreased. The oxide porosity tends to decrease with the Cr content and immersion time owing to the development of Cr containing oxide. The oxidation behavior is not changed with the immersion time.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1383-1387
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of Cladding Hull Wastes from Used Nuclear Fuels
    Charakterystyka odpadów z okładzin reaktora wodnego ciśnieniowego
    Autorzy:
    Kang, K. H.
    Lee, C. H.
    Jeon, M. K.
    Han, S. Y.
    Park, G. I.
    Hwang, S.-M.
    Powiązania:
    https://bibliotekanauki.pl/articles/357036.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    used nuclear fuels
    metal waste
    cladding hulls
    zircaloy
    radioactivity
    reaktor wodny ciśnieniowy
    odpady metalowe
    odpady z okładzin
    radioaktywność
    Opis:
    Used cladding hulls from pressurized water reactor (PWR) are characterized to provide useful information for the treatment and disposal of cladding hull wastes. The radioactivity and the mass of gamma emitting nuclides increases with an increase in the fuel burn-up and their removal ratios are found to be more than 99 wt.% except Co-60 and Cs-137. In the result of measuring the concentrations of U and Pu included in the cladding hull wastes, most of the residues are remained on the surface and the removal ratio of U and Pu are revealed to be over 99.98 wt.% for the fuel burn-up of 35,000 MWd/tU. An electron probe micro-analyzer (EPMA) line scanning shows that radioactive fission products are penetrated into the Zr oxide layer, which is proportional to the fuel burn-up. The oxidative decladding process exhibits more efficient removal ratio of radionuclides.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1199-1203
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    An analysis on the thermal characteristics according to the viscosity of bearing lubricant and the cooling condition for the high speed motor spindle
    Autorzy:
    Choi, D. B.
    Lee, J. J.
    Kim, S. T.
    Kwon, H. D.
    Kim, C. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/1429194.pdf
    Data publikacji:
    2008
    Wydawca:
    Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
    Tematy:
    high speed motor spindle
    thermal displacement cooling condition
    lubricant viscosity
    Opis:
    Thermal displacement of the high speed machine tools has a large influence on machining accuracy. The high speed motor spindle with many heat sources is widely used for the high speed machine tools recently. The important problem in this spindle is to reduce and minimize the thermal effects by motor and bearings. This paper presents the analysis on thermal characteristics for high speed motor spindle system with oil-air lubricated angular contact ceramic ball bearings and built-in motor. An analysis on the thermal characteristics of spindle is performed according to the cooling conditions and the viscosity of bearing lubricants by using finite element method. This results can be applied to the design and manufacturing for the high speed motor spindle.
    Źródło:
    Journal of Machine Engineering; 2008, 8, 4; 88-98
    1895-7595
    2391-8071
    Pojawia się w:
    Journal of Machine Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Warm Tensile Deformation Behavior and Constitutive Equation of Supersaturated Solid-Solutionized Al-9Mg Extruded Alloy
    Autorzy:
    Yang, Seung Y.
    Kim, Bong H.
    Lee, Da B.
    Choi, Kweon H.
    Kim, Nam S.
    Ha, Seong H.
    Yoon, Young O.
    Lim, Hyun K.
    Kim, Shae
    Kim, Young J.
    Powiązania:
    https://bibliotekanauki.pl/articles/2048882.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    aluminum alloy
    Al-9Mg alloy
    tensile test
    constitutive equation
    Opis:
    In this paper, as a purpose to apply the supersaturated solid-solutionized Al-9Mg alloy to the structural sheet parts of automotive, tensile tests were conducted under the various conditions and a constitutive equation was derived from the tensile test results. Al-9Mg alloy was produced using a special Mg master alloy containing Al2Ca during the casting process and extruded into the sheet. In order to study the deformation behavior of Al-9Mg alloy in warm temperature forming environments, tensile tests were conducted under the temperature of 373 K-573 K and the strain rate of 0.001/s~0.1/s. in addition, by using the raw data obtained from tensile tests, a constitutive equation of the Al-9Mg alloy was derived for predicting the optimized condition of the hot stamping process. Al-9Mg alloy showed uncommon deformation behavior at the 373 K and 473 K temperature conditions. The calculated curves from the constitutive equation well-matched with the measured curves from the experiments particularly under the low temperature and high strain rate conditions.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 4; 1013-1018
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Mechanical Properties of Hot-deformed AlMg4 Alloys with the Variations of Mn, Fe, and Si Contents
    Autorzy:
    Lee, Da B.
    Kim, Bong H.
    Choi, Kweon H.
    Yang, Seung Y.
    Kim, Nam S.
    Ha, Seong H.
    Yoon, Young O.
    Lim, Hyun K.
    Kim, Shae
    Hyun, Soong K..
    Powiązania:
    https://bibliotekanauki.pl/articles/351603.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Mg alloy
    intermetallic compounds
    homogenization
    hot-rolling
    microstructure
    Opis:
    This paper aims to investigate the microstructural evolution and mechanical properties of hot-deformed AlMg4 alloys with Mn, Fe, and Si as the main impurities. For this purpose, solidification behavior and microstructural evolution during hot-rolling and heat-treatment processes are investigated by using theoretical calculations and experimental characterization. The crystallization and morphological transformation of intermetallic Al3 Fe, Al6 Mn, and Mg2 Si phases are revealed and discussed in terms of the variation in chemical composition. Following a homogenization heat-treatment, the effect of heat treatment on the intermetallic compounds is also investigated after hot-rolling. It was revealed that the Mg2 Si phase can be broken into small particles and spherodized more easily than the Al3 Fe intermetallic phase during the hot-rolling process. For the Mn containing alloys, both yield and ultimate tensile strength of the hot-rolled alloys increased from 270 to 296 MPa while elongation decreased from 17 to 13%, which can be attributed to Mn-containing intermetallic as well as dispersoid.
    Źródło:
    Archives of Metallurgy and Materials; 2020, 65, 4; 1255-1259
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Carbon Co-Deposition During Gas Reduction of Water-Atomized Fe-Cr-Mo Powder
    Autorzy:
    Ali, B.
    Choi, S. H.
    Seo, S. J.
    Maeng, D. Y.
    Lee, C. G.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/352709.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    water atomization
    Fe-based powder
    oxide reduction
    powder metallurgy
    sinter-hardening alloys
    Opis:
    The water atomization of iron powder with a composition of Fe-3Cr-0.5Mo (wt.%) at 1600°C and 150 bar creates an oxide layer, which in this study was reduced using a mixture of methane (CH4) and argon (Ar) gas. The lowest oxygen content was achieved with a 100 cc/min flow rate of CH4, but this also resulted in a co-deposition of carbon due to the cracking of CH4. This carbon can be used directly to create high-quality, sinter hardenable steel, thereby eliminating the need for an additional mixing step prior to sintering. An exponential relationship was found to exist between the CH4 gas flow rate and carbon content of the powder, meaning that its composition can be easily controlled to suit a variety of different applications.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1119-1124
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Supercontinuum fiber laser source for water quality and heavy metals detection
    Autorzy:
    Teh, P. C.
    Ho, Y. H.
    Ong, C. E.
    Lee, S. C.
    Lo, P. K.
    Lai, K. C.
    Yeap, K. H.
    Loh, S. H.
    Teh, P. S.
    Tey, K. L.
    Powiązania:
    https://bibliotekanauki.pl/articles/174135.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    supercontinuum generation
    master oscillator power amplifier
    nonlinear optics
    transmittance measurement
    heavy metal contaminants
    Opis:
    We report a compact, all fiber, 150 ps fiber master oscillator power amplifier operating at 1064 nm that has the ability of producing a maximum average output power of 2.16 W with peak power as high as 10 kW. The output from the master oscillator power amplifier is spliced with a highly nonlinear photonic crystal fiber, generating a supercontinuum with an average power of 250 mW at repetition rate of 1 MHz and spectrum bandwidth spanning from 600 to 1700 nm. The developed supercontinuum system is used to detect the presence of heavy metal contaminants in water by a simple light transmittance method to ensure that the water is free from heavy metal contaminants and safe for consumption. The supercontinuum laser source was shone onto a water sample with a detector placed at another end in order to measure the transmitted supercontinuum light. By measuring the amount of light attenuated at particular wavelength, the concentration of heavy metal contaminants present in the water sample could be determined.
    Źródło:
    Optica Applicata; 2017, 47, 3; 445-456
    0078-5466
    1899-7015
    Pojawia się w:
    Optica Applicata
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Argon Plasma in a New Process for Improving the Physical and Anti-bacterial Properties of Crosslinked Cotton Cellulose with Dimethyloldihydroxyethyleneurea-Maleic Acid
    Zastosowanie plazmy niskotemperaturowej w środowisku argonu w procesie obróbki tkanin bawełnianych sieciowanych za pomocą kwasu dimetylodihydroxyetylenourylomaleinowego dla polepszenia właściwosci fizycznych oraz antybakteryjnych
    Autorzy:
    Tsou, C H
    Suen, M C
    Tsou, C Y
    Chen, J C
    Yeh, J T
    Lin, S M
    Lai, Y C
    Hwang, J Z
    Huang, S H
    Hung, W S
    Hu, C C
    Lee, K R
    Lai, J Y
    Powiązania:
    https://bibliotekanauki.pl/articles/232331.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
    Tematy:
    cotton
    plasma
    antibacterial
    crosslinking
    crosslink length
    crosslinks number per anhydroglucose
    surface distribution
    odour absorption
    bawełna
    plazma
    właściwości antybakteryjne
    sieciowanie tkanin bawełnianych
    kwas dimetylodihydroxyetylenourylomaleinowy
    odporności na zagniecenia
    pochłanianie zapachów
    żywica termoutwardzalna
    Opis:
    This study reports the findings of an argon (Ar) plasma treatment added to the traditional pad-dry-cure process between dry and cure treatments. This new process is called the "paddry-plasma-cure process". The crosslinking agent was a mixture of dimethyloldihydroxyethyleneurea (DMDHEU) and maleic acid (MA). Results show that Ar plasma treatment can increase the bonded crosslinking agent (i.e., the nitrogen content). The dry crease recovery angle (DCRA), wet crease recovery angle (WCRA), and tensile strength retention (TSR) of the pad-dry-plasma-cure finished fabrics were higher than those of traditional pad-dry-cure finished fabrics at a given nitrogen content. Additionally it was found that the number of crosslinks per anhydroglucose unit (CL/AGU) and the length of crosslinks of pad-dry-plasma-cure-finished fabrics were higher than that of traditional pad-dry-cure finished fabrics at the same resin concentration in the pad bath. DCRA, WCRA and TSR values of pad-dry-plasma-cure-finished fabrics were higher than those of pad-dry-curefinished fabrics at the same CL/AGU value. However, activation energies for the pad-dryplasma-cure process were higher than those for the pad-dry-cure process. The anti-bacterial ability and odour absorption of the pad-dry-plasma-cure and pad-dry-plasma-cure finished fabrics were higher than those for the pad-dry-cure finished fabrics. The surface distribution of crosslinking agents for the pad-dry-plasma-cure process was higher than that of the pad-dry-cure process. Thus the pad-dry-plasma-cure process is excellent for improving the physical properties, bacterial inhibition, and odour absorption of finished cotton fabrics and for decreasing their formaldehyde release.
    Artykułu odnosi się do problematyki możliwości i celowości wprowadzenia modyfikacji plazmowej w warunkach niskociśnieniowych i w środowisku argonu do konwencjonalnego procesu wykończenia przeciw mnącego z zastosowaniem reaktywnych żywic termoutwardzalnych. Badano kąt odprężenia na sucho i na mokro, i stwierdzono polepszenie właściwości odporności na zagniecenia w wyniku dodatkowego zastosowania plazmy. Badano również właściwości antybakteryjne i pochłanianie zapachów, które okazały się korzystniejsze dla dodatkowej obróbki plazmowej. W wyniku zmodyfikowanej obróbki uzyskano mniejsze wydzielanie formaldehydu z gotowej tkaniny.
    Źródło:
    Fibres & Textiles in Eastern Europe; 2015, 1 (109); 49-56
    1230-3666
    2300-7354
    Pojawia się w:
    Fibres & Textiles in Eastern Europe
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication and Characterization of GaN/Polymer Composite p-n Junction with PEDOT Nanoparticle Interface Layer
    Autorzy:
    Kim, M.
    Jin, S.
    Choi, H.
    Kim, G.
    Yim, K.
    Kim, S.
    Nam, G.
    Yoon, H.
    Kim, Y.
    Lee, D.
    Kim, Jin
    Kim, Jong
    Leem, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1505152.pdf
    Data publikacji:
    2011-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    73.61.Ey
    81.15.Gh
    Opis:
    A heavily Si-doped GaN/polymer hybrid structure with p-type poly(3,4-ethylene-dioxythiophene):beta-1,3-glucan (PEDOT nanoparticle) interface layer has been fabricated. The Si-doped GaN thin film with carrier concentration of 1 × $10^{19} cm^{-3}$ was grown by metal-organic chemical vapor deposition. The PEDOT nanoparticle with various sizes ranging from 60 to 120 nm was synthesized via a miniemulsion polymerization process. The electrical conductivity of the PEDOT nanoparticle is less than 1.2 S/cm. The current-voltage (I-V) characteristic of the hybrid structure shows diode-like behavior. The I-V characteristic was examined in the framework of the thermionic emission model. The ideality factor of the structure without PEDOT nanoparticle interface layer is 12.9. However, the ideality factor of the hybrid structure with PEDOT nanoparticle interface layer is obtained as 1.9. The value of ideality factor is dramatically decreased by inserting the PEDOT nanoparticle interface layer.
    Źródło:
    Acta Physica Polonica A; 2011, 119, 6; 875-879
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of a Spherical Titanium Powder by Combined Combustion Synthesis and DC Plasma Treatment
    Autorzy:
    Choi, S. H.
    Ali, B.
    Hyun, S. K.
    Sim, J. J.
    Choi, W. J.
    Joo, W.
    Lim, J. H.
    Lee, Y. J.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/356067.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    combustion synthesis
    DC plasma treatment
    titanium powder
    3D printing process
    combustion parameters
    Opis:
    Combustion synthesis is capable of producing many types of refractory and ceramic materials, as well as metals, with a relatively lower cost and shorter time frame than other solid state synthetic techniques. TiO2 with Mg as reductant were dry mixed and hand compacted into a 60 mm diameter mold and then combusted under an Ar atmosphere. Depending on the reaction parameters (Mg concentration 2 ≤ α ≤ 4), the thermocouples registered temperatures between 1160°C and 1710°C . 3 mol of Mg gave the optimum results with combustion temperature (Tc) and combustion velocity (Uc) values of 1372°C and 0.26 cm/s respectively. Furthermore, this ratio also had the lowest oxygen concentration in this study (0.8 wt%). After combustion, DC plasma treatment was carried out to spheroidize the Ti powder for use in 3D printing. The characterization of the final product was performed using X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, and N/O analysis.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1057-1062
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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