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Wyszukujesz frazę "scanning electron microscopy," wg kryterium: Temat


Tytuł:
Investigation and vizualization of the cells grown on ceramic coating by electron microscopy techniques
Autorzy:
Karbowniczek, J.
Gruszczyński, A.
Kruk, A
Czyrska-Filemonowicz, A.
Powiązania:
https://bibliotekanauki.pl/articles/285222.pdf
Data publikacji:
2017
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
biocompatibility
biomaterials
scanning electron microscopy
Źródło:
Engineering of Biomaterials; 2017, 20, no. 143 spec. iss.; 37
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Use of scanning electron microscopy for the study of Hoplopleura (Phthiraptera, Anoplura) lice taxonomy
Autorzy:
Kozina, P.
Izdebska, J.N.
Mierzynski, L.
Powiązania:
https://bibliotekanauki.pl/articles/5924.pdf
Data publikacji:
2016
Wydawca:
Polskie Towarzystwo Parazytologiczne
Tematy:
scanning electron microscopy
Hoplopleura
Phthiraptera
Anoplura
taxonomy
Źródło:
Annals of Parasitology; 2016, 62, Suppl.
0043-5163
Pojawia się w:
Annals of Parasitology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Prospective observational study of adenoidal biofilms in a paediatric population and its clinical implications
Autorzy:
Subtil, Joao
Bajanca-Lavado, Maria Paula
Rodrigues, Joao
Duarte, Aida
Reis, Lucia
Nogueira, Isabel
Jordao, Luisa
Powiązania:
https://bibliotekanauki.pl/articles/1397787.pdf
Data publikacji:
2019
Wydawca:
Index Copernicus International
Tematy:
Adenoids
biofilms
scanning electron microscopy
Haemophilus
child.
Opis:
INTRODUCTION: Adenoids are nasopharyngeal lymphoid tissue with a relevant role in host defence against infection of upper respiratory tract. Nevertheless, adenoids are also a reservoir of microorganisms that can cause infections of upper respiratory tract and otitis particularly in children. OBJECTIVE: Evaluate and compare the association between biofilm assembly on adenoids and the incidence of recurrent infections in a paediatric population submitted to adenoidectomy by either infectious or non-infectious indication. METHODS: Scanning electron microscopy was used to assess biofilms on adenoid surface; biofilm assembly in vitro was monitored by crystal violet assay; antibiotic susceptibility was assessed following EUCAST guidelines; Hinfluenzae capsular typing was performed by PCR. RESULTS: Biofilms were present in 27.4% of adenoid samples and no statistical difference was found between infectious and non-infectious groups. In vitro, the most clinically relevant bacteria, H.influenzae, S.aureus, S.pyogenes, S.pneumoniae and M.catarrhalis, were mostly moderate biofilm assemblers (71.7%). 55.3% of these bacteria were intermediate/resistant to at least one of the tested antibiotics. No association was found between the ability to assemble biofilms in vitro and the presence of biofilms on adenoids nor antibiotic resistance. All H.influenzae were characterized as non-typeable. CONCLUSION: The presence of biofilms on adenoid surface was independent from clinical sample background. Bacterial ability to assemble biofilms in vitro cannot be used to predict biofilm assembly in vivo. The lack of correlation between biofilm formation and infectious respiratory diseases found contributes to question the relevance of biofilms on the pathogenesis of infectious diseases.
Źródło:
Polish Journal of Otolaryngology; 2019, 73, 1; 22-28
0030-6657
2300-8423
Pojawia się w:
Polish Journal of Otolaryngology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Deformation Mechanisms and Fracture of Ni-Based Metallic Glasses
Autorzy:
Lesz, S.
Griner, S.
Nowosielski, R.
Powiązania:
https://bibliotekanauki.pl/articles/353790.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metals
transmission electron microscopy
scanning electron microscopy
fracture
shear bands
Opis:
The cracking of materials and fracture surface is of great practical and academic importance. Over the last few years the development of the fractography of crystalline alloys resulted in a useful tool for the prediction or failure analysis. Many attempts have been made to observe cracks using optical microscopy, X-ray topography and transmission electron microscopy (TEM). Of these techniques, the resolution of optical microscopy and X-ray topography is too poor. By contrast, the resolution of TEM is high enough for detailed information to be obtained. However, in order to apply TEM observations, a thin foil specimen must be prepared, and it is usually extremely difficult to prepare such a specimen from a pre-selected region containing a crack. In the present work, deformation mechanisms fracture surfaces of Ni-based metallic glass samples have been studied by specially designed experiments. In order to study the deformation mechanisms and fracture the Ni-based metallic glasses have been investigated in the tensile test. The structure and fracture surfaces after the decohesion process in tensile tests were observed using transmission electron microscope (TEM) and scanning electron microscope (SEM), respectively. The studies of structure were performed on thin foils. Moreover the investigated tape was subjected to a banding test. Then, the tape was straightened and the thin foil from the area of maximum strain was prepared. This thin foil sample was deformed before the TEM investigation to obtain local tears.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 791-796
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Diversity of labellar micromorphological structures in selected species of Malaxidinae [Orchidales]
Autorzy:
Kowalkowska, A
Margonska, H.B.
Powiązania:
https://bibliotekanauki.pl/articles/58622.pdf
Data publikacji:
2009
Wydawca:
Polskie Towarzystwo Botaniczne
Tematy:
light microscopy
scanning electron microscopy
Orchidaceae
micromorphology
Malaxidinae
pollination
Opis:
There are no papers examining the labellar micromorphology in Malaxidinae in detail. The aim of this paper is to present the results of labellar micromorphology of our studies on Malaxidinae. The micromorphology of nine species was examined and described (calli, nectaries, OP structures, concavities). These species are divided into six groups of which the lip morphology probably represents different forms of attracting and rewarding pollinators. Group one consists of Disticholiparis gregaria and Platystyliparis aurita with characteristic globular nectary and pad-like callus. The second group with Liparis nervosa has two conelike convexities. The third one is represented by Liparis sutupensis with spread lip, the basal callus, and the epichile often eroding with age. The fourth group (Stichorkis cespitosum) has a massive hypochil with basal callus and delicate epichil. The fifth group (Microstylis ophioglossoides, Dienia ophrydis) is characterized by a lip with developed lateral lobes, three deep concavities in the middle part, an erect callus, and many raphide cells.Crepidium cf. rheedii and Crepidium dryadum from the sixth group have a three-lobed lip with entire or toothed mid-lobe, basal callus, cavity surrounded by a rim and OP structures with raphide cells. We also emphasized the different way and place of nectar secretion in the subtribe and gave some suggestions about pollination strategies.
Źródło:
Acta Societatis Botanicorum Poloniae; 2009, 78, 2; 141-150
0001-6977
2083-9480
Pojawia się w:
Acta Societatis Botanicorum Poloniae
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Scanning electron microscopic picture of the concentration and distribution of protein structures in the seed endosperm of low and high protein varietes of rye (Secale cereale L.)
Badania porównawcze ilości i rozmieszczenia białek w komórkach endospermy ziarniaków nisko- i wysokobiałkowych odmian żyta
Autorzy:
Kubiczek, R.
Luczak, W.
Molski, B.
Moczydłowski, J.
Powiązania:
https://bibliotekanauki.pl/articles/1399430.pdf
Data publikacji:
1989
Wydawca:
Instytut Rozrodu Zwierząt i Badań Żywności Polskiej Akademii Nauk w Olsztynie
Tematy:
rye
scanning electron microscopy
endosperm structures
protein structure
Opis:
Comparative studies of subaleurone and inner endosperm cells of dry mature caryopses from 8 low-protein and 7 high-protein varieties of rye, grown in similar conditions of isolated collection, were performed by means of scanning electron microscopy technique. Low protein varieties contained starch granules differentiated in the diameter embedded in the less dense protein matrix of the wide subaluerone region. High protein varieties, besides the larger aleurone cells had in some examples wider subaluerone layer with the dense protein matrix, which was very regular and less packed with starch granules. The inner endosperm cells of high-protein caryopses contained much more dense protein matrix all around the starch granules in contrast to low-protein caryopses, which were tightly packed with starch and had only a thin layer of protein matrix around them. Comparative pronase treatment of low- and high-protein rye caryopses confirmed the above observations. No granular protein bodies in any cells, besides the aleurone ones, could be observed.
Przeprowadzono badania porównawcze ilości i rozmieszczenia składników białkowych komórek warstw podaleuronowych i głębszych warstw endospermy w suchych, dojrzałych ziarniakach 8 niskobiałkowych i 7 wysokobiałkowych odmian żyta (tab.), wyhodowanych w 1974/75 r. w Skierniewicach i 1976/77 r. w Powsinie w identycznych warunkach izolowanej kolekcji zachowawczej z wykorzystaniem skaningowego mikroskopu elektronowego (SEM). W odmianach niskobiałkowych ziarna skrobiowe o zróżnicowanej średnicy były zatopione w grubej warstwie matrycy białkowej w komórkach cienkiej warstwy podaleuronowej (fot. 1, 2, 3). W odmianach wysokobiałkowych, oprócz zdarzających się w wypadku niektórych odmian większych komórek warstwy aleuronowej, warstwa podaleuronowa była lepiej wykształcona z dużą ilością matrycy białkowej i regularnymi i mniej upakowanymi w niej ziarnami skrobi (fot. 4, 5). Również w głębszych warstwach endospermy komórki ziarniaków odmian wysokobiałkowych zawierały więcej matrycy białkowej otaczającej ziarna skrobi w przeciwieństwie do niskobiałkowych, których komórki wypełnione są szczelnie ziarnami skrobi i zawierają niewielkie ilości białek pomiędzy nimi oraz białko cytoplazmatyczne pod ścianami komórek. Porównawcze trawienie pronazą skrawków ziarniaków odmian nisko- i wysokobiałkowych (fot.8) potwierdziło powyższe twierdzenia. Nie zauważono w komórkach innych niż aleuronowe granularnych ciał białkowych w żadnej z badanych odmian żyta.
Źródło:
Acta Alimentaria Polonica; 1989, 15(39), 2; 185-195
0137-1495
Pojawia się w:
Acta Alimentaria Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mössbauer study of the El Hammami olivine-bronzite meteorite
Autorzy:
Zarek, W.
Popiel, E.
Tuszyński, M.
Teper, E.
Powiązania:
https://bibliotekanauki.pl/articles/147220.pdf
Data publikacji:
2004
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
meteorite
XRD
scanning electron microscopy
Mössbauer spectroscopy
kamacite
Opis:
The phase composition of the El Hammami meteorite was investigated by X-ray, magnetostatic, Mössbauer effect and environmental scanning electron microscopy methods. Performed investigations indicated that this meteorite consists of aluminosilicates, olivine (Mg,Fe)2SiO4, pyroxene (Ca,Mg,Fe)SiO3, kamacite (bcc Fe-Ni alloy) and troilite (FeS). Some inclusions of Ti and Cr were observed by scanning electron microscopy. The concentration of Ni in kamacite was determined by comparison of the Mössabauer spectra of Fe-Ni phase in the meteorite with those for synthetic bcc Fe-Ni alloys (5, 10, 25% Ni).
Źródło:
Nukleonika; 2004, 49,suppl.3; 59-62
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of the Quenching Rate on the Structure and Magnetic Properties of the Fe-Based Amorphous Alloy
Autorzy:
Nabiałek, M.
Powiązania:
https://bibliotekanauki.pl/articles/350944.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
transmissions electron microscopy
scanning electron microscopy
amorphous matrials
free volumes
quasidislocation
Opis:
This paper presents the results of investigations into the structure, microstructure and magnetic properties of Fe61Co10Y8W1B20 amorphous alloy. The alloy samples were in two physical forms: (1) plates of approximate thickness 0.5 mm (so-called bulk amorphous alloys) and (2) a ribbon of approximate thickness 35 μm (so-called classic amorphous alloy). The investigations comprised: X-ray diffractometry, Mössbauer spectrometry, transmission electron microscopy, and selected magnetic measurements; all of the investigations were carried out on samples in the as-quenched state. Analysis of the obtained SEM and TEM images, X-ray diffraction patterns, Mössbauer spectrometry results and measurements of the magnetisation in a high magnetic field facilitated collectively the detailed description of the structure of the investigated alloy, which was found to depend on the quenching speed.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 439-444
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Milling Time on Amorphization of Mg-Zn-Ca Powders Synthesized by Mechanical Alloying Technique
Autorzy:
Lesz, S.
Kremzer, M.
Gołombek, K.
Nowosielski, R.
Powiązania:
https://bibliotekanauki.pl/articles/354717.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mg-based powders
transmission electron microscopy
scanning electron microscopy
mechanical alloying
Opis:
Mg60 Zn35 Ca5 amorphous powder alloys were synthesized by mechanical alloying (MA) technique. The results of the influence of high-energy ball-milling time on amorphization of the Mg60 Zn35 Ca5 elemental blend (intended for biomedical application) were presented in the study. The amorphization process was investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM). Initial elemental powders were mechanically alloyed in a Spex 8000 high-energy ball mill at different milling times (from 3 to 24 h). Observation of the powder morphology after various stages of milling leads to the conclusion that with the increase of the milling time the size of the powder particles as well as the degree of aggregation change. The partially amorphous powders were obtained in the Mg60 Zn35 Ca5 alloy after milling for 13-18h. The results indicate that this technique is a powerful process for preparing Mg60 Zn35 Ca5 alloys with amorphous and nanocrystalline structure.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 845-851
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microscopic analysis of the nanostructures impact on endothelial cells
Autorzy:
Kołodziejczyk, Agnieszka Maria
Kucińska, Magdalena
Jakubowska, Aleksandra
Siatkowska, Małgorzata
Sokołowska, Paulina
Kotarba, Sylwia
Makowski, Krzysztof
Komorowski, Piotr
Walkowiak, Bogdan
Powiązania:
https://bibliotekanauki.pl/articles/1844983.pdf
Data publikacji:
2020
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
nanostructures
atomic force microscopy
transmission electron microscopy
scanning electron microscopy
cell morphology
Opis:
Nowadays nanostructures are more and more often designed as carriers for drug delivery, especially to improve the drug pharmacokinetics and pharmaco-dynamics. Numerous kinds of nanostructures are considered a good prospect for medical applications thanks to their small size, acceptable biocompatibility and toxicity. Due to the fact that nanotechnology is a new field of science, every nano-scale product must be thoroughly examined regarding its toxicity to the human body. This study provides new insights into effects of exposing endothelial cells to the selected nanostructures. Dendrimers of the fourth generation (PAMAMs), multi-walled carbon nanotubes (MWCNTs) and silver nanoparticles (SNPs) were used to evaluate nanostructures influence on endothelial cells in vitro. The nanostructures were evaluated via transmission electron microscopy and dynamic light scattering technique. The cells previously exposed to the nanostructures were observed and analyzed via the atomic force microscopy and scanning electron microscopy to obtain a quantitative evaluation of the cells morphology. The presence of multi-walled carbon nanotubes and silver nanoparticles on the cells surface was confirmed by the scanning electron microscopy. Our results confirm that the surface association and/or uptake of nanostructures by the cells resulting from physicochemical and biological processes, affect the cells morphology. Morphological changes can be induced by the membrane proteins interaction with nanomaterials, which trigger a sequence of intracel-lular biological processes.
Źródło:
Engineering of Biomaterials; 2020, 23, 154; 2-8
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microscopic analysis of the nanostructures impact on endothelial cells
Autorzy:
Kołodziejczyk, Agnieszka Maria
Kucińska, Magdalena
Jakubowska, Aleksandra
Siatkowska, Małgorzata
Sokołowska, Paulina
Kotarba, Sylwia
Makowski, Krzysztof
Komorowski, Piotr
Walkowiak, Bogdan
Powiązania:
https://bibliotekanauki.pl/articles/970974.pdf
Data publikacji:
2020
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
nanostructures
atomic force microscopy
transmission electron microscopy
scanning electron microscopy
cell morphology
Opis:
Nowadays nanostructures are more and more often designed as carriers for drug delivery, especially to improve the drug pharmacokinetics and pharmaco-dynamics. Numerous kinds of nanostructures are considered a good prospect for medical applications thanks to their small size, acceptable biocompatibility and toxicity. Due to the fact that nanotechnology is a new field of science, every nano-scale product must be thoroughly examined regarding its toxicity to the human body. This study provides new insights into effects of exposing endothelial cells to the selected nanostructures. Dendrimers of the fourth generation (PAMAMs), multi-walled carbon nanotubes (MWCNTs) and silver nanoparticles (SNPs) were used to evaluate nanostructures influence on endothelial cells in vitro. The nanostructures were evaluated via transmission electron microscopy and dynamic light scattering technique. The cells previously exposed to the nanostructures were observed and analyzed via the atomic force microscopy and scanning electron microscopy to obtain a quantitative evaluation of the cells morphology. The presence of multi-walled carbon nanotubes and silver nanoparticles on the cells surface was confirmed by the scanning electron microscopy. Our results confirm that the surface association and/or uptake of nanostructures by the cells resulting from physicochemical and biological processes, affect the cells morphology. Morphological changes can be induced by the membrane proteins interaction with nanomaterials, which trigger a sequence of intracel-lular biological processes.
Źródło:
Engineering of Biomaterials; 2020, 23, 154; 2-8
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electron microscope study of NaCl- and Pb[CH3COO]2-treated kaolinite
Autorzy:
Kharitonova, G.V.
Manucharov, A.S.
Chernomorchenko, N.I.
Pavluykov, I.A.
Powiązania:
https://bibliotekanauki.pl/articles/24784.pdf
Data publikacji:
2006
Wydawca:
Polska Akademia Nauk. Instytut Agrofizyki PAN
Tematy:
soil treatment
scanning electron microscopy
kaolinite
lead
clay mineral
Źródło:
International Agrophysics; 2006, 20, 3
0236-8722
Pojawia się w:
International Agrophysics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphological Evaluation of Variously Intercalated Pre-baked Clay
Autorzy:
Ullah, H.
Imtiaz, A.
Powiązania:
https://bibliotekanauki.pl/articles/778613.pdf
Data publikacji:
2014
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
clay
alkali metal intercalation
inorganic modifier
scanning electron microscopy
Opis:
The use of porous materials is enjoying tremendous popularity and attention of the advance scientific communities due to their excellent adsorptive and catalytic activities. Clays are one of the most important candidates in the porous community which shows the above mentioned activities after modifing with a different intercalating agent. The paper is focused on the infiuence of some inorganic intercalating agents (NaOH) on the morphology of the variously intercalated clay samples. The alkali metal was used as the inorganic intercalating agent. The effect of intercalation temperature, intercalation agent concentration and intercalation time on the pre-baked clay morphology were also part of the study. Scanning electron microscopy (SEM) study was performed to evaluate the morphological changes of the resultant intercalates. Different morphological properties were improved significantly in the case of the inorganically modified clay samples. Thus, such intercalations are suggested to be effective if the clays under study are to be used for different industrial process at elevated conditions.
Źródło:
Polish Journal of Chemical Technology; 2014, 16, 2; 5-11
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Aging and Degradation of Human Fingernail Plates Upon Cosmetic Agents
Autorzy:
Kulesza, S.
Bramowicz, M.
Gwoździk, M.
Wilczyński, S.
Goździejewska, A. M.
Powiązania:
https://bibliotekanauki.pl/articles/354662.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Atomic Force Microscopy
Scanning Electron Microscopy
fractal characterization
nanoscale property mapping
Opis:
The knowledge whether and how chemical species react with tissues is important because of protection against harmful factors, diagnose of dermatological diseases, validation of dermatological procedures as well as effectiveness of topical therapies. In presented work the effects of chemical agents on plates of human fingernails were studied using Atomic Force Microscopy and Scanning Electron Microscopy. Apart from that, mapping of the elastic properties of the nails was also carried out. To obtain reliable measures of spatial evolution of the surface variations, recorded images were analyzed in terms of scaling invariance brought by fractal geometry, instead of common though not unique statistical measures.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 1; 181-184
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical properties of Ni-Fe-Cu-P-B alloy produced by two component melt spinning (TCMS)
Autorzy:
Wojciechowska, M.
Ziewiec, K.
Kąc, S.
Prusik, K.
Powiązania:
https://bibliotekanauki.pl/articles/351728.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metallic glasses
scanning electron microscopy (SEM)
nanoindentation
transmission electron microscopy TEM
mechanical properties
Opis:
The aim of this work was to investigate the microstructure and mechanical properties of the two-component melt-spun (TCMS) alloy produced from Ni40Fe40B20 and Ni70Cu10P20 melts. The Ni40Fe40B20, Ni70Cu10P20, Ni55 Fe20 Cu5 P10 B10 alloys were arc-melted. Then the alloys were melt-spun in the two different ways i.e.: by casting from a single-chamber crucible and from the two-chamber crucible. All of the above mentioned alloys were processed in the first way and the Ni40Fe40B20 and Ni70Cu10P20 were simultaneously cast on the copper roller from the two-chamber crucible. The microstructure of the alloy was studied using transmission electron microscopy (TEM), scanning electron microscopy (SEM) with energy dispersive spectrometry (EDS) and light microscopy. The mechanical properties were investigated using tensile testing and nanoindentation. The two-component melt-spun (TCMS) amorphous Ni55 Fe20 Cu5 P10 B10 alloy present hardness, tensile strength and Young modulus on the significantly higher level than for a single phase amorphous Ni55 Fe20 Cu5 P10 B10 alloy and slightly below the corresponding values for the Ni40Fe40B20.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 137-140
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Complexing Agent on the Structural, Optical and Electrical Properties of Polycrystalline Indium Sulfide Thin Films Deposited by Chemical Bath Deposition
Autorzy:
Göde, F.
Kariper, İ.
Güneri, E.
Ünlü, S.
Powiązania:
https://bibliotekanauki.pl/articles/1031534.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
scanning electron microscopy
thin film
optical constant
growth from solutions
Opis:
Indium sulfide (β-In₂S₃) thin films are synthesized by chemical bath deposition method using three different complexing agent volumes, triethanolamine (TEA) (0.30, 0.45, and 0.60 ml). The effect of complexing agent on the structural, morphological, optical and electrical properties of chemically deposited indium sulfide (β-In₂S₃) thin films have been investigated in this work. The characterization of the present films is carried out using X-ray diffraction, scanning electron microscopy, UV-vis spectroscopy and electrical measurements. The structure of the films is polycrystalline with a cubic phase of β-In₂S₃. Firstly, the band gap of the film decreases from 3.74 eV to 3.15 eV by adding 0.30 ml TEA. Then, it increases to 3.79 eV with increasing TEA. Nevertheless, previously, the refractive index of the films increases from 2.13 to 2.67 for the 0.30 mL TEA and then it decreases to the value of 2.11 with increasing TEA. Extinction coefficient, real and dielectric constant of the films are calculated using the absorption and transmittance spectra. Firstly, the electrical resistivity of the films decreases from 3.46×10⁸ Ω cm to 1.33×10⁷ Ω cm by adding 0.30 ml TEA. Then, it increases to the value of 2.16×10⁹ Ω cm with increasing TEA. Eventually, the more conductive film with worm-like morphology detected from the scanning electron microscopy is synthesized using 0.30 ml TEA. These results show that complexing agent has an important effect on the structural, morphological, optical and electrical properties of the deposited films.
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 527-530
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of the Powder Consolidation Method Type on the Microstructure and Selected Properties of Al2O3-Cu-Ni Composite
Autorzy:
Zygmuntowicz, J.
Wachowski, M.
Piotrkiewicz, P.
Kaszuwara, W.
Powiązania:
https://bibliotekanauki.pl/articles/351724.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
composites
Pulse Plasma Sintering
Uniaxial Powder Pressing
Scanning Electron Microscopy
Opis:
The present research is focused on the characterization of the composites from Al2O3-Cu-Ni system. Two methods of ceramic-metal composite forming were applied: uniaxial powder pressing and Pulse Plasma Sintering (PPS). To obtain the samples the powder mixtures containing 85 vol.% of Al2O3 and 15 vol.% of metal powders were used. Influence of the sintering process on microstructure and mechanical properties of the two series of the composites was analyzed in detail. The selected physical properties of samples were characterized by Archimedes immersion method. Vickers hardness and the fracture toughness of the composites was determined as well. The microstructure of the composites was characterized by XRD, SEM, EDX. Fractography investigation was carried out as well. Independently on composite production method Al2O3, Cu, Ni, and CuNi phases were revealed. Fractography investigation results revealed different character of fracture in dependence of fabrication method. Pulse Plasma Sintered samples were characterized by higher crack resistance and higher Vickers hardness in comparison to the specimens manufactured by uniaxial pressing.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 967-974
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Papposphaera heldalii sp. nov. (Haptophyta, Papposphaeraceae) from Svalbard
Autorzy:
Thomsen, Helge Abildhauge
Egge, Jorun Karin
Powiązania:
https://bibliotekanauki.pl/articles/763513.pdf
Data publikacji:
2016
Wydawca:
Uniwersytet Jagielloński. Wydawnictwo Uniwersytetu Jagiellońskiego
Tematy:
Papposphaera, P. heldalii sp. nov., Papposphaeraceae, Svalbard, scanning electron microscopy
Opis:
In an attempt to establish a taxonomy for the polar contingent of lightly calcified coccolithophores, we are currently dealing with species of Papposphaera. Here we describe a new species, Papposphaera heldalii sp. nov., based on material from Svalbard. The species is unique in terms of calyx design, which is an elegant modification of the standard P. sagittifera theme, and also in terms of the absence of central area calcification in body coccoliths. The species thus occupies a further step in a sequence of five Arctic forms ranging from P. sagittifera via P. sarion, P. arctica and P. iugifera to P. heldalii showing a gradual reduction of central area calcification in body coccoliths. P. heldalii is unique also in the sense that the species has not been found during any of the major Arctic TEM nanoplankton surveys conducted during the last decades.
Źródło:
Acta Protozoologica; 2016, 55, 1
1689-0027
Pojawia się w:
Acta Protozoologica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sedimentological analysis of sandy - gravel accumulations, Serra da Estrela plateaux (Portugal)
Autorzy:
Vieira, G.T.
Mycielska-Dowgiałło, E.
Woronko, B.
Powiązania:
https://bibliotekanauki.pl/articles/295228.pdf
Data publikacji:
2003
Wydawca:
Stowarzyszenie Geomorfologów Polskich
Tematy:
wind erosion
water erosion
scanning electron microscopy
Central Cordillera
Portugal
Opis:
Sandy-gravel accumulations are frequent features on the plateaux of the Serra da Estrela II and other granitic mountains in Portugal. Their genesis has been attributed to both eolian and water processes and a detailed sedimentological study is needed to better understand the mechanisms involved. The present paper provides results obtained from the heavy mineral analysis and optical and scanning electron microscope study of samples from two sandy-gravel accumulations from the Serra da Estrela. The results indicate that the finer fractions of the original sediment have been illuviated. A well-sorted surface layer and poorly sorted subsurface of the accumulation have resulted from this process. A very short duration of eolian processes is evident from the analysis. Although wind seems to have been the responsible for the morphology of the accumulation, its action was not enough to produce significant abrasion in the surface of quartz grains.
Źródło:
Landform Analysis; 2003, 4; 99-107
1429-799X
Pojawia się w:
Landform Analysis
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nanopores with controlled profiles in track - etched membranes
Autorzy:
Sartowska, B. A.
Powiązania:
https://bibliotekanauki.pl/articles/146896.pdf
Data publikacji:
2012
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
nanopore
scanning electron microscopy (SEM)
surfactant
track-etched membranes (TMs)
Opis:
Track-etched membranes are porous systems consisting of a polymer foil with thin channels-pores - from surface to surface. The increasing interest in this kind of material is connected with the development of nanoporous materials with unique properties such as diode-like effects in membranes with highly asymmetrical nanopores. The materials can be used for molecular sensors and atom beam optics, development of nanocapillary bodies for modelling the transport of molecules and ions in constrained volumes. Control over pore geometry opens the way to a number of new applications of track-etch membranes (TMs). The nanopores were obtained by the ion-track etching method using surfactant-doped alkaline solutions. Control over the pore profile and dimensions was achieved by varying the alkali concentration in the etchant and the etching time. The pore geometry was characterized in detail using field-emission scanning electron microscopy (SEM). SEM images of the surfaces and cleavages of TMs with different pore morphology are shown.
Źródło:
Nukleonika; 2012, 57, 4; 575-579
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of computer image analysis and scanning electron microscopy in environmental engineering and waste management
Autorzy:
Szponder, D. K.
Trybalski, K.
Powiązania:
https://bibliotekanauki.pl/articles/115780.pdf
Data publikacji:
2011
Wydawca:
Fundacja na Rzecz Młodych Naukowców
Tematy:
scanning electron microscopy
computer image analysis
solid waste
environmental engineering
Opis:
Creation and refinement of modern research methods in the last century had a signifi cant impact on the dynamic development of various fields of science. Special attention deserves computer image analysis and scanning electron microscopy. These methods can be used in virtually any field of science dealing with solids. Modern methods have many applications in environmental engineering. Studies, using the above advanced testing methods are also widely used in waste management. The article presents progressive research methodology of using image analysis and scanning electron microscopy in environmental engineering and waste management. It especially presents the application of these methods to determine physical, chemical and mineralogical properties of solid waste.
Źródło:
Challenges of Modern Technology; 2011, 2, 2; 56-62
2082-2863
2353-4419
Pojawia się w:
Challenges of Modern Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Quartz grain features in modern glacial and proglacial environments: A microscopicstudy from the Russell Glacier, southwest Greenland
Autorzy:
Kalińska-Nartiša, Edyta
Lamsters, Kristaps
Karušs, Jānis
Krievāns, Māris
Rečs, Agnis
Meija, Raimonds
Powiązania:
https://bibliotekanauki.pl/articles/2042159.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Arctic
Greenland
modern glacial environment
Quartz grains
Scanning electron microscopy
Źródło:
Polish Polar Research; 2017, 38, 3; 265-289
0138-0338
2081-8262
Pojawia się w:
Polish Polar Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Biological and mechanical research of titanium implants covered with bactericidal coating
Autorzy:
Malisz, Klaudia
Świeczko-Żurek, Beata
Powiązania:
https://bibliotekanauki.pl/articles/2172010.pdf
Data publikacji:
2022
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
nanometals
scanning electron microscopy
wettability
nanoindentation
antibacterial properties
mechanical properties
Opis:
Materials used in bone implants should not only be non- -toxic to the surrounding tissues, but also should promote osseointegration and minimize the risk of infection. Infections are a serious problem contributing to implantation failure. They are associated with pain, immobilization, and the necessity of reoperation. In extreme cases, they can lead to significant inflammatory changes in the bones, which, in turn, can lead to amputation and even death. After implantation, the surrounding tissues are damaged. In addition, implants are susceptible to bacterial colonization due to the lack of microcirculation. Therefore, scientists are working on antibacterial coatings to prevent the adhesion of bacteria before tissue regeneration. The paper concerns the biological and mechanical properties of titanium implants with an antibacterial coating. The Ti13Zr13Nb alloy samples were coated with hydroxyapatite (HAp) coatings using the electrophoretic deposition technique (EPD). Subsequently, the surface of the samples was modified with silver, copper, and nickel nanoparticles by the immersion method. Different titanium sample types (i.e. HAp-only and nanometals-enriched coatings) were placed in a bacterial solution for a period of one month. Each sample was examined using scanning electron microscopy (SEM), nanoindentation, nanoscratch, and contact angle tests. The significant amount of dead biofilm on the surface proves the effectiveness of antibacterial activity. The wettability assessment showed that the samples were hydrophilic. The conducted tests of mechanical properties indicate the heterogeneity of the coatings.
Źródło:
Engineering of Biomaterials; 2022, 25, 165; 17--22
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Health risk assessment in the vicinity of a copper smelter: particulate matter collected on a spider web
Autorzy:
Trzyna, Agnieszka
Rybak, Justyna
Bartz, Wojciech
Górka, Maciej
Powiązania:
https://bibliotekanauki.pl/articles/2202388.pdf
Data publikacji:
2022
Wydawca:
Polskie Towarzystwo Mineralogiczne
Tematy:
air pollution
spider web
PM
Scanning Electron Microscopy
health hazard
Opis:
We used spider webs as a particulate matter (PM) sampler to assess the possible health risk to the inhabitants of Legnica city (Poland). We aimed to find out if it is a useful material and could provide reliable information. We selected two spider families (Agelenidae and Linyphiidae) whose webs structure enhances the PM accumulation. The collected particles were analysed using a Scanning Electron Microscope equipped with Energy Dispersive X-Ray (SEM-EDX) and Inductively Coupled Plasma Mass Spectrometry (ICP-MS) which provided morphological and chemical information and allowed to indicate possible sources of pollution. The results showed that PM10, the fraction of particles smaller than 10 µm, was dominated by the particles of natural origin, while fine fractions were composed of diverse anthropogenic particles, whose origin can be connected with the activity of the copper smelter and in smaller quantity with the road traffic. The carcinogenic and non-carcinogenic health risk was assessed for these pathways: inhalation, ingestion, and dermal, for children and adults. The non-carcinogenic risk was very high (Hazard Index: HI > 1) both for children (Cu, Ni, Pb, Cd) and adults (Cu, As, Pb, Cd). Moreover, high carcinogenic risk (>10-4) was found in most of the sampling points. The study shows that spider webs are useful in biomonitoring of PM and can also be used for health risk assessment. In the studied region, it was found that the possible negative impact of air pollution on human health exists.
Źródło:
Mineralogia; 2022, 53, 1; 36--50
1899-8291
1899-8526
Pojawia się w:
Mineralogia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of Microwave Sintered Aluminium Composite Reinforced with Hydroxyapatite Extracted from Rihu Fish Scales
Autorzy:
Venkatesh, V.S.S.
Prasad, Kalapala
Deoghare, Ashish B.
Powiązania:
https://bibliotekanauki.pl/articles/27765073.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czasopisma i Monografie PAN
Tematy:
hydroxyapatite
aluminium matrix
microwave sintering
mechanical properties
Scanning Electron Microscopy
Opis:
In this study, Hydroxyapatite (HAp) is extracted from the Rihu fish scales which are generally dumped as garbage. The aluminium composite was fabricated through the powder metallurgy technique by reinforcing HAp (0, 5, 10 and 15 wt%) as a reinforcement. The fabricated samples were sintered through microwave sintering at 530℃ for 15 min under an argon gas environment. The fabricated composites were subjected to X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and Energy Dispersive Spectroscopy (EDS) analysis to confirm the constituting elements and to describe the reinforcement dispersion in the matrix. Uniform reinforcement dispersion was observed for the composite reinforces with 5% HAp, 10% HAp particles. The mechanical characterization results reveal that the Al-10% HAp composite exhibits a microhardness value of 123 ± 3 Hv and maximum ultimate tensile strength of 263 ± 10 MPa and 299 ± 9 MPa compression strength was obtained due to the presence of a strong bond among the aluminium and HAp particles.
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 2; 617--624
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A comparison of various imaging modes in scanning electron microscopy during evaluation of selected Si/refractory sessile drop couples after wettability tests at ultra-high temperature
Autorzy:
Polkowska, A.
Warmuzek, M.
Kalarus, J.
Polkowski, W.
Sobczak, N.
Powiązania:
https://bibliotekanauki.pl/articles/391383.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
Tematy:
scanning electron microscopy
sessile drop method
silicon
refractories
in-lens detectors
Opis:
In this work, FEI SciosTM field emission gun scanning electron microscope (FEG SEM) equipped with a unique combination of analytical and imaging detectors was utilized to examine structure and chemistry of selected Si/ refractory couples. The couples were obtained in wettability tests performed by the sessile drop method coupled with contact heating of a refractory substrate (h-BN, SiC) at ultra-high temperature (up to 1750°C). The SEM observations were carried out on top-views of the couples, in order to evaluate surface and interfacial phenomena in Si/h-BN and Si/SiC systems. A full range of available detectors (e.g. classical Everhart-Thornley detector (ETD) or advanced in-lens detectors) working under various operation modes (secondary electrons (SE), backscattered electrons (BSE), a mixed mode), were used upon analyses in order to reveal specific features of obtained structures.
Źródło:
Prace Instytutu Odlewnictwa; 2017, 57, 4; 337-344
1899-2439
Pojawia się w:
Prace Instytutu Odlewnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of Nonmetallic Inclusions in Aluminum–Silicon Alloys
Autorzy:
Galek, Tomasz
Łączek, Andrzej
Łysiak, Karol
Powiązania:
https://bibliotekanauki.pl/articles/176066.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum–silicon alloy
nonmetallic inclusions
scanning electron microscopy
X-ray tomography
Opis:
In this article, a study of nonmetallic inclusions introduced during the casting process of the aluminum–silicon alloy is presented. The samples were investigated using a scanning electron microscope to find the chemical composition and X-ray tomography to check the volumetric content of the non-metallic inclusions. The samples were made from AlSi7Mg alloy, used for car wheels, with 7% weight content of Si, 89% of Al, and 0.3% of Mg. The main goal of our investigations was to find out the chemical composition of the impurities and to identify the stage of the casting process at which the impurities are introduced.
Źródło:
Advances in Manufacturing Science and Technology; 2020, 44, 1; 28-31
0137-4478
Pojawia się w:
Advances in Manufacturing Science and Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pathogenicity of Phoma complanata (Tode) Desm. towards angelica (Archangelica officinalis Hoffm.)
Patogeniczność Phoma complanata (Tode) Desm. dla arcydzięgla litwora (Archangelica officinalis Hoffm.)
Autorzy:
Machowicz-Stefaniak, Z.
Zalewska, E.D.
Zimowska, B.
Król, E.D.
Powiązania:
https://bibliotekanauki.pl/articles/11542857.pdf
Data publikacji:
2014
Wydawca:
Uniwersytet Przyrodniczy w Lublinie. Wydawnictwo Uniwersytetu Przyrodniczego w Lublinie
Tematy:
pathogenicity
Phoma complanata
fungi
angelica
Archangelica officinalis
inoculation
scanning electron microscopy
Opis:
The plants of angelica Archangelica officinalis may be colonized by various species of fungi including Phoma species. The paper concerns the fungus Phoma complanata, isolated from above-ground and underground parts of angelica in 2009–2011. Pathogenicity tests according to Koch’s postulates were carried out on angelica plants using various methods of inoculation. Observations of the infection process were made using the scanning electron microscope (SEM). Three our own isoletes and reference isolate of P. complanata were used in the study. P. complanata was found to be a facultative pathogen of angelica, which enters to the plant through stomata and wounds without creating appressoria in the top part of the germination hyphae.
Arcydzięgiel litwor (Archangelica officinalis Hoffm.) może być zasiedlany przez różne gatunki grzybów, w tym również przez grzyby Phoma sensu lato. Przeprowadzone badania dotyczą gatunku Phoma complanata wyizolowanego z nadziemnych i podziemnych części arcydzięgla w latach 2009–2011. Testy patogeniczności przeprowadzono zgodnie z postulatami Kocha, z uwzględnieniem różnych metod inokulacji. Potwierdziły one patogeniczny charakter polskich izolatów P. complanata oraz izolatu referencyjnego dla wybranych organów arcydzięgla. Obserwacje przebiegu procesu infekcji wykonano przy użyciu skaningowego mikroskopu elektronowego (SEM). Na podstawie przeprowadzonych badań P. complanata uznano za fakultatywny patogen arcydzięgla. Grzyb wnika do tkanek przez aparaty szparkowe bez tworzenia na końcu strzępki kiełkowej struktury adhezyjnej w postaci appresorium.
Źródło:
Acta Scientiarum Polonorum. Hortorum Cultus; 2014, 13, 6; 45-58
1644-0692
Pojawia się w:
Acta Scientiarum Polonorum. Hortorum Cultus
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fractography analysis of AW-7020 alloy joints welded by FSW
Autorzy:
Dudzik, K.
Charchalis, A.
Powiązania:
https://bibliotekanauki.pl/articles/244221.pdf
Data publikacji:
2014
Wydawca:
Instytut Techniczny Wojsk Lotniczych
Tematy:
friction stir welding (FSW)
aluminum alloys
welding
fractography
scanning electron microscopy
Opis:
Technology development of Friction Stir Welding (FSW) method for joining AW-7020 aluminum alloy elements was described. Two kinds of tools were used during research: with a regular pin and with a „TRI-FLUTE” pin. Tools were with different dimensions and the following parameters changed mandrel’s rotary speed Vn [rev/min], welding speed Vz [mm/min], angle of tool deflection αz [o]. The thickness of the joining sheets was g = 12 mm. The sheets were one side milled to a thickness of 10 mm in the contact portion. Samples were tested by Charpy impact strength according to PN-EN ISO 148-1:2010. After these tests, the samples were analysed by means of fractographic examination. The tests were made with using a scanning electron microscope (SEM) Philips XL-30. The analysis has shown that there is the influence of the joining parameters and chosen tools for the possibility of occurrence welding defects in joints. Welding defects detected in the structure of joints after impact studies were: incomplete fusion, separations dissection, and cracks. During the development of friction stir welding technology, the best results, in terms of structure homogeneity and the absence of welding defects, were achieved for the tool with TRI-FLUTE pin and joining parameters: Vn = 450 rev/min, Vz = 180 mm/min, αz = 88.5 °.
Źródło:
Journal of KONES; 2014, 21, 1; 67-74
1231-4005
2354-0133
Pojawia się w:
Journal of KONES
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Studies of unicellular microorganisms Saccharomyces cerevisiae by means of positron annihilation lifetime spectroscopy
Autorzy:
Kubicz, E.
Jasińska, B.
Zgardzińska, B.
Bednarski, T.
Białas, P.
Czerwiński, E.
Gajos, A.
Gorgol, M.
Kamińska, D.
Kapłon, Ł.
Kochanowski, A.
Korcyl, G.
Kowalski, P.
Kozik, T.
Krzemień, W.
Niedźwiecki, S.
Pałka, M.
Raczyński, L.
Rajfur, Z.
Rudy, Z.
Rundel, O.
Sharma, N. G.
Silarski, M.
Słomski, A.
Strzelecki, A.
Wieczorek, A.
Wiślicki, W.
Zieliński, M.
Moskal, P.
Powiązania:
https://bibliotekanauki.pl/articles/147902.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
environmental scanning electron microscopy (ESEM)
free volume
inverted microscopy
positron annihilation
positronium
yeasts
Opis:
Results of positron annihilation lifetime spectroscopy (PALS) and microscopic studies on simple microorganisms, brewing yeasts, are presented. Lifetime of ortho-positronium (o-Ps) were found to change from 2.4 to 2.9 ns (longer-lived component) for lyophilized and aqueous yeasts, respectively. Also hygroscopicity of yeasts in time was examined, allowing to check how water – the main component of the cell – affects PALS parameters, thus lifetime of o-Ps were found to change from 1.2 to 1.4 ns (shorter-lived component) for the dried yeasts. The time sufficient to hydrate the cells was found below 10 hours. In the presence of liquid water, an indication of reorganization of yeast in the molecular scale was observed. Microscopic images of the lyophilized, dried, and wet yeasts with best possible resolution were obtained using inverted microscopy (IM) and environmental scanning electron microscopy (ESEM) methods. As a result, visible changes to the surface of the cell me mbrane were observed in ESEM images.
Źródło:
Nukleonika; 2015, 60, No. 4, part 1; 749-753
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Porosity assessment of suspension and saturated composite castings with the use of microscopic examinations
Autorzy:
Staude, Marek
Powiązania:
https://bibliotekanauki.pl/articles/2033595.pdf
Data publikacji:
2021
Wydawca:
Akademia Morska w Szczecinie. Wydawnictwo AMSz
Tematy:
composites
castings
defects
porosity
suspension composite
saturated composite
light microscopy
scanning electron microscopy
Opis:
Good quality in composite castings can be confirmed primarily by their user. The producer is obliged to create a good product that meets the user’s needs that should undergo quality control. Omission of technological procedures and improper quality control may result in various defects like porosity. This paper presents the characteristics of the casting defect, namely porosity, with a particular focus on porosity in suspension and saturated metal composites. This defect is different, specific to composite castings, making its identification very difficult. The aim of the study is to detect and describe porosity in composites with the use of microscopic and submicroscopic examinations. The assessment of the porosity of the microstructure of composite castings allowed for the formulation of the following conclusions: in addition to the porosity that occurs in castings of classic materials (cast steel, cast iron, and non-ferrous metal alloys), metal composites also distinguish between primary and secondary agglomerates, leaving the reinforcement space not filled, occluded bubbles, and separated gas bubbles.
Źródło:
Zeszyty Naukowe Akademii Morskiej w Szczecinie; 2021, 67 (139); 53--57
1733-8670
2392-0378
Pojawia się w:
Zeszyty Naukowe Akademii Morskiej w Szczecinie
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Scanning electron microscopy (SEM) in the analysis of the structure of polymeric nanofiltration membranes
Skaningowa mikroskopia elektronowa (SEM) w analizie struktury polimerowych membran nanofiltracyjnych
Autorzy:
Kowalik-Klimczak, A.
Bednarska, A.
Grądkowski, M.
Powiązania:
https://bibliotekanauki.pl/articles/258006.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Technologii Eksploatacji - Państwowy Instytut Badawczy
Tematy:
scanning electron microscopy
nanofiltration
polymeric membranes
skaningowa mikroskopia elektronowa
nanofiltracja
membrana polimerowa
Opis:
The authors examined the possible use of a scanning electron microscope (SEM) for polymeric nanofiltration membranes testing. The analysis of results allowed us to conclude that SEM technique is useful for the determination of the construction of “skin” and the support layer of nanofiltration polymeric membranes and that Energy-dispersive X-ray spectroscopy (EDS, EDX) provides “average” data from both layers.
W pracy zweryfikowano możliwość zastosowania skaningowego mikroskopu elektronowego do badania polimerowych membran nanofiltracyjnych. Analiza uzyskanych wyników pozwoliła na stwierdzenie, że SEM może być pomocna w określaniu budowy warstw naskórkowej i wzmacniającej polimerowych membran nanofiltracyjnych, a technika EDX dostarcza „uśrednionych” danych obejmujących obie warstwy.
Źródło:
Problemy Eksploatacji; 2016, 1; 119-128
1232-9312
Pojawia się w:
Problemy Eksploatacji
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cooling Characteristic and Microstructure of Ni-Si-B-Ag Alloy
Autorzy:
Wojciechowska, M.
Ziewiec, K.
Mucha, D.
Powiązania:
https://bibliotekanauki.pl/articles/356071.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous/crystalline composite
scanning electron microscopy
X-ray diffraction
thermography
melt spinning
Opis:
The aim of this work was to investigate the possibility of obtaining an amorphous/crystalline composite starting from Ni-SiB-based powder grade 1559-40 and silver powder. The alloy was produced using arc melting of 95% wt. Ni-Si-B-based powder (1559-40) and 5% wt. Ag powder. Ingot was re-melted on a copper plate and observed while cooling using a mid-wave infra-red camera. The alloy was then melt-spun in a helium atmosphere. The microstructure of the ingot as well as the melt-spun ribbon was studied using light microscopy and scanning electron microscopy with energy dispersive spectrometry. Phase identification was performed by means of X-ray diffraction. The observations confirmed an amorphous/crystalline microstructure of the ribbon where the predominant constituent of the microstructure was an amorphous phase enriched with Ni, Si, and B, while the minor constituent was an Ag-rich crystalline phase distributed in a film along the melt-spinning direction.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1357-1360
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Intermittent Microwave-Vacuum Drying Effects on Pears
Autorzy:
Taskin, Onur
Polat, Ahmet
Izli, Nazmi
Asik, Baris B.
Powiązania:
https://bibliotekanauki.pl/articles/1369555.pdf
Data publikacji:
2019
Wydawca:
Instytut Rozrodu Zwierząt i Badań Żywności Polskiej Akademii Nauk w Olsztynie
Tematy:
microwave-vacuum drying
mineral content
protein
rehydration ratio
color
scanning electron microscopy
Opis:
In the present study, the effects of intermittent microwave-vacuum drying on the “Deveci” pear in terms of the drying kinetics, mineral content, protein content, rehydration ratio, color, energy, specific energy and microstructure were investigated. According to the drying treatments, increased microwave power (100 and 200 W) and vacuum (200 and 400 mmHg) applications provided higher drying rates and protein content. Dried pear samples had a higher mineral content than fresh samples because of the increasing dry matter content. At the higher vacuum level experiments, the energy consumption reduced and the rehydration ratio increased. Moreover, the higher microwave power caused a decrease of the L* (lightness) value. However, a regular pore size and pore distribution in all drying experiments were observed in the microstructures of microwave-vacuum-dried samples.
Źródło:
Polish Journal of Food and Nutrition Sciences; 2019, 69, 1; 101-108
1230-0322
2083-6007
Pojawia się w:
Polish Journal of Food and Nutrition Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface analysis and chemical composition of dust from dry dedusting system of moulding sand with bentonite using scanning electron microscopy (SEM)
Analiza morfologii powierzchni i składu chemicznego pyłów z suchego odpylania mas formierskich z bentonitem z wykorzystaniem skaningowej mikroskopii elektronowej (SEM)
Autorzy:
Bobrowski, A.
Żymankowska-Kumon, S.
Powiązania:
https://bibliotekanauki.pl/articles/391488.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
Tematy:
bentonit
pył
odpylanie
skaningowa mikroskopia elektronowa
bentonite
dust
dedusting
scanning electron microscopy
Opis:
The article presents the results of surface morphology of dust from dry dedusting of moulding sand with bentonite and mixtures of bentonite with lustrous carbon carrier using scanning electron microscopy. The study identifies the approximate chemical composition of the dust, and compares it with the composition of starting mixtures. The mixtures of bentonite with lustrous carbon carrier from different manufacturers differ in chemical composition. The process of de- dusting should be carried out using properly selected operating parameters of the dedusting equipment. If the process of dedusting is carried out incorrectly, it can lead to the loss of valuable components.
W artykule przedstawiono wyniki badań morfologii powierzchni pyłów z suchego odpylania mas formierskich z bentonitem oraz mieszanek bentonitu z nośnikiem węgla błyszczącego z wykorzystaniem mikroskopii skaningowej. Badania pozwoliły wskazać przybliżony skład chemiczny pyłu i porównać go ze składem mieszanek wyjściowych. Mieszanki bentonitu z nośnikiem węgla błyszczącego oferowane przez ich producentów różnią się pod względem składu chemicznego. Proces odpylania mas formierskich z bentonitem powinien przebiegać przy odpowiednio dobranych parametry pracy urządzeń odpylających. Niewłaściwie prowadzony proces odpylania może doprowadzić do utraty cennych składników.
Źródło:
Prace Instytutu Odlewnictwa; 2017, 57, 3; 181-185
1899-2439
Pojawia się w:
Prace Instytutu Odlewnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of hydrothermal treatment on the starch of corn grain
Wpływ obróbki hydrotermicznej na skrobię wybranych zbóż
Autorzy:
Fornal, J.
Powiązania:
https://bibliotekanauki.pl/articles/1396398.pdf
Data publikacji:
1985
Wydawca:
Instytut Rozrodu Zwierząt i Badań Żywności Polskiej Akademii Nauk w Olsztynie
Tematy:
corn
hydrothermal processes
starch
intra-grain cavities
dextrins
amylopectin
scanning electron microscopy
Opis:
The results if the conducted analysis of microstructure of corn grain using a scanning electron microscope were presented, with special consideration of changes in the morphological structure of starch granules during the manufacture of corn flakes. Attempts were also undertaken to compare the microscopic image of dextrins and amylopectins of raw materiał and product. Significant changes in the microstructure of corn grit, appearing together with the prolonged time of heat and water treatment, were demonstrated. It was stated that the presence of inra-grain cavities was not an artefact and their diameter was dependent on the time of heat and water action during the process of grit cooking. When analysing the microscopic images of dextrins and amylopectin of grit and of flakes it was noticed that differences in their structure were caused by the effect of high temperatures on starch.
Proces produkcji płatków z grysu kukurydzanego opiera się na działaniu ciepła i wody oraz sił mechanicznych, co prowadzi do nadania produktowi odpowiedniej tekstury, cech smakowo-zapachowych oraz wartości odżywczej. W niniejszej pracy, za pomocą skaningowego mikroskopu elektronowego, zbadano wpływ procesu technologicznego na mikrostrukturę grysu kukurydzanego ze szczególnym uwzględnieniem głównego jego składnika - skrobi. Na uzyskanych elektronomogramach potwierdzono występowanie w skrobi kukurydzy „zagłębień wewnątrzziarnowych", których obecność była dotąd dyskusyjna (rys. 3), a ponadto ustalono, że ich średnica zmienia się wraz z czasem parowania (rys. 4, 5, 6). Stwierdzono, że przyrost średnicy zagłębień wewnątrzziarnowych jest funkcją czasu działania ciepła i wody i ma charakter prostoliniowy. Płatkowanie grysu i opiekanie płatków powoduje dalsze zmiany strukturalne, przejawiające się zanikiem struktury komórkowej, całkowitą żelatynizacją skrobi i powstaniem licznych pęcherzyków powietrznych otoczonych cienkimi ścianami (rys. 7). Powyższe obserwacje potwierdzone zostały wynikami analizy mikroskopowej skrobi wyosobnionej z grysu o różnym stopniu uparowania (rys. 8-11). Analiza uzyskanych nomogramów dekstryn grysu i płatków oraz amylopektyny wytrąconej z wyosobnionych skrobi tych samych prób wykazała istotny wpływ obróbki hydrotermicznej na ich obrazy mikroskopowe (rys. 12-16). Dekstryny, występujące w surowcu w postaci drobin o średnicy 0,2-0,7 μm pod wpływem procesu technologicznego przekształciły się w produkcie gotowym w konglomerat kulistych struktur o znacznie większych rozmiarach i uporządkowanej, sieciowo-gąbczastej strukturze wewnętrznej. Amylopektyna mająca w skrobi surowca charakter otoczek ziarn skrobiowych, ze skrobi wyosobnionej z produktu wytrącała się jako nieuporządkowana masa. Na podstawie uzyskanych wyników uznano, że przyczyn zmian obrazu mikroskopowego analizowanych preparatów można dopatrywać się w naruszeniu naturalnego układu sił wewnątrzcząsteczkowych ziarna skrobi kukurydzy w procesie obróbki hydrotermicznej.
Źródło:
Acta Alimentaria Polonica; 1985, 11, 1; 141-151
0137-1495
Pojawia się w:
Acta Alimentaria Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of enzymatic effects on pit membranes using light and scanning electron microscopy
Autorzy:
Durmaz, S.
Yildiz, U.C.
Ozturk, M.
Serdar, B.
Powiązania:
https://bibliotekanauki.pl/articles/52338.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Technologii Drewna
Tematy:
investigation
enzymatic effect
pit membrane
light electron microscopy
scanning electron microscopy
spruce wood
permeability
enzymatic treatment
Źródło:
Drewno. Prace Naukowe. Doniesienia. Komunikaty; 2016, 59, 198
1644-3985
Pojawia się w:
Drewno. Prace Naukowe. Doniesienia. Komunikaty
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Skaningowa mikroskopia elektronowa
Autorzy:
Faryna, M.
Powiązania:
https://bibliotekanauki.pl/articles/274331.pdf
Data publikacji:
2014
Wydawca:
Roble
Tematy:
skaningowa mikroskopia elektronowa
Pracownia Skaningowej Mikroskopii Elektronowej
Instytut Metalurgii i Inżynierii Materiałowej PAN
scanning electron microscopy
Laboratory of Scanning Electron Microscopy
Institute of Metallurgy and Materials Science PAS
Źródło:
LAB Laboratoria, Aparatura, Badania; 2014, 19, 1; 11-14
1427-5619
Pojawia się w:
LAB Laboratoria, Aparatura, Badania
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructural Analysis of Concrete Using Cow Bone Ash for Alkali-Silica Reaction (ASR) Suppression
Autorzy:
Adanikin, Ariyo
Falade, Funsho
Olutaiwo, Adewale
Powiązania:
https://bibliotekanauki.pl/articles/106963.pdf
Data publikacji:
2020
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
petrographic analysis
Scanning Electron Microscopy
Cow Bone Ash
Alkali-Silica Reaction
concrete pavement
Opis:
Concrete pavements are prone to microstructural changes and deterioration when exposed to Alkali-Silica Reaction (ASR). ASR results in strength reduction, cracking, spalling and other defects in the concrete if left unchecked. Supplementary Cementitious Materials (SCMs) such as Cow Bone Ash (CBA) however can be used to improve concrete performance, hence its use in this study. Concrete samples were prepared at replacement levels of 0%, 5%, 10%, 15%, 20% and 30% of cement with Cow Bone Ash. The concrete samples were then subjected to petrographic and Scanning Electron Microscopy (SEM) analysis. Petrographic examination shows that the minimal and least amount of ASR gels and micro cracking were observed at 15% CBA replacement of cement in the concrete samples. Scanning Electron Microscopy (SEM) analysis shows that changes in the elemental composition of the concrete samples is related to the effect of CBA which enhances adhesion in the concrete. SEM analysis show that, in general, the change in microstructure in the concrete was mainly due to the change in the arrangement of the C-H-S compounds. The microstructure analysis indicates that CBA in concrete influences the densification of the concrete at the transition zone, resulting in a much lower porosity. This results in the concrete having a tightly bound layer that repels ingress of water and thereby inhibiting cracks and gel formation as water is a contributing factor to the ASR in concrete.
Źródło:
Journal of Casting & Materials Engineering; 2020, 4, 2; 34-40
2543-9901
Pojawia się w:
Journal of Casting & Materials Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nectary structure and nectar secretion of Echium russicum J.F.Gmel. flowers
Budowa nektarnikow i sekrecja nektaru w kwiatach Echium russicum J.F.Gmel.
Autorzy:
Chwil, M
Weryszko-Chmielewska, E
Powiązania:
https://bibliotekanauki.pl/articles/27065.pdf
Data publikacji:
2007
Wydawca:
Polskie Towarzystwo Botaniczne
Tematy:
epidermis
nectar secretion
botany
scanning electron microscopy
flower
nectary structure
Boraginaceae
Echium russicum
Opis:
In this study, the micromorphology of nectaries in Echium russicum J. F. Gmel. flowers was determined by using scanning electron microscopy (SEM) and their anatomy by using light microscopy (LM). The rate of nectar production of flowers and sugar concentration in nectar were investigated. The nectary gland is located below the ovary of the pistil. It is composed of 4 parts corresponding to the parts of the ovary. The widest regions of the nectar-producing tissue are situated by the furrows separating the adjacent parts of the ovary. Nectar is secreted through anomocytic stomata, located only in the lower part of the nectary. The stomata were distributed evenly or they formed clusters of 2-3. The average number of stomata on the surface of the whole nectary was 184. At the nectar secretion stage, open and closed, as well as not fully mature stomata were observed. The orientation of most of the stomata was parallel to the nectary base. The cuticle surface of the cells of the upper and lateral part of the nectary was smooth, whereas in the region producing stomata it showed various folds facilitating the retention of nectar. The flowers produced nectar throughout the flowering period. The weight of nectar secreted throughout the lifetime of ten flowers was, on the average, 20 mg, with the concentration of sugars of 58% and their weight reaching 17 mg.
W przeprowadzonych badaniach określono mikromorfologię nektarników w kwiatach Echium russicum J. F. Gmel. przy użyciu skaningowego mikroskopu elektronowego (SEM) oraz anatomię przy zastosowaniu mikroskopu świetlnego (LM). Zbadano obfitość nektarowania kwiatów i koncentrację cukrów w nektarze. Gruczoł nektamikowy położony jest poniżej zalążni słupka. Składa się z 4 części odpowiadających członom zalążni. Najszersze strefy tkanki nektaronośnej znajdują się przy bruzdach, oddzielających sąsiednie części zalążni. Wydzielanie nektaru odbywało się przez anomocytyczne aparaty szparkowe, położone tylko w dolnej części nektarnika. Szparki były rozmieszczone równomiernie lub tworzyły skupienia po 2-3. Średnia liczba aparatów szparkowych na powierzchni całego nektarnika wynosiła 184. W fazie sekrecji nektaru obserwowano zarówno otwarte, jak i zamknięte oraz nie w pełni dojrzałe aparaty szparkowe. Orientacja większości aparatów szparkowych była równoległa do podstawy nektamika. Powierzchnia kutykuli komórek górnej i bocznej części nektarnika była gładka, natomiast w strefie wytwarzającej szparki wykazywała różne pofałdowania, ułatwiające zatrzymywanie nektaru. Kwiaty nektarowały przez całą długość kwitnienia. Masa nektaru wydzielana przez całe życie dziesięciu kwiatów wynosiła średnio 29 mg, o koncentracji cukrów 58% i masie cukrów osiągającej 17 mg.
Źródło:
Acta Agrobotanica; 2007, 60, 1
0065-0951
2300-357X
Pojawia się w:
Acta Agrobotanica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analiza SEM czarnego tonera na wydrukach. Część I
SEM analysis of black toners on printouts. Part I
Autorzy:
Łasińska, Anna
Powiązania:
https://bibliotekanauki.pl/articles/501609.pdf
Data publikacji:
2019-11-29
Wydawca:
Agencja Bezpieczeństwa Wewnętrznego
Tematy:
toner
Canon
Dell
Epson
Ricoh
skaningowa mikroskopia elektronowa
SEM
toners
scanning electron microscopy
Opis:
W publikacji przedstawiono wyniki analizy struktury powierzchni czarnych tonerów na wydrukach, dokonanej za pomocą skaningowego mikroskopu elektronowego. Przeprowadzono testy tonerów z kilku wydruków pochodzących z 18-laserowych urządzeń drukujących czterech firm: Canon, Dell, Epson i Ricoh. Wdrożenie skaningowej mikroskopii elektronowej do kryminalistycznych badań dokumentów stworzyło nowe możliwości identyfikacji laserowych urządzeń drukujących. Uzyskane obrazy mikroskopowe pozwoliły na przyporządkowanie charakterystycznych cech tonerów do poszczególnych grup urządzeń.
black toners commercialized in Poland. A total of eighteen printouts of Canon, Dell, Epson and Ricoh manufacturer was analyzed. The analysis showed that the implementation of a much more sensitive method, such as the scanning electron microscopy (SEM) provided new opportunities for the identification of laser printing. The microscopic images obtained allowed us to allocate the characteristic features of toners to specific groups of devices.
Źródło:
Przegląd Bezpieczeństwa Wewnętrznego; 2019, 11, 21; 211-246
2080-1335
2720-0841
Pojawia się w:
Przegląd Bezpieczeństwa Wewnętrznego
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
SEM analysis of black toners on printouts. Part I
Analiza SEM czarnego tonera na wydrukach. Część I
Autorzy:
Łasińska, Anna
Powiązania:
https://bibliotekanauki.pl/articles/501627.pdf
Data publikacji:
2019-11-29
Wydawca:
Agencja Bezpieczeństwa Wewnętrznego
Tematy:
toners
Canon
Dell
Epson
Ricoh
scanning electron microscopy
SEM
toner
skaningowa mikroskopia elektronowa
Opis:
This paper describes the use of scanning electron microscopy in the analysis of original black toners commercialized in Poland. A total of eighteen printouts of Canon, Dell, Epson and Ricoh manufacturer was analyzed. The analysis showed that the implementation of a much more sensitive method, such as the scanning electron microscopy (SEM) provided new opportunities for the identification of laser printing. The microscopic images obtained allowed us to allocate the characteristic features of toners to specific groups of devices.
W publikacji przedstawiono wyniki analizy struktury powierzchni czarnych tonerów na wydrukach, dokonanej za pomocą skaningowego mikroskopu elektronowego. Przeprowadzono testy tonerów z kilku wydruków pochodzących z 18-laserowych urządzeń drukujących czterech firm: Canon, Dell, Epson i Ricoh. Wdrożenie skaningowej mikroskopii elektronowej do kryminalistycznych badań dokumentów stworzyło nowe możliwości identyfikacji laserowych urządzeń drukujących. Uzyskane obrazy mikroskopowe pozwoliły na przyporządkowanie charakterystycznych cech tonerów do poszczególnych grup urządzeń.
Źródło:
Przegląd Bezpieczeństwa Wewnętrznego; 2019, 11, 21; 363-392
2080-1335
2720-0841
Pojawia się w:
Przegląd Bezpieczeństwa Wewnętrznego
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pollen morphology of Pinus uliginosa Neum. and Pinus uncinata Ramond ex DC in an experimental culture
Autorzy:
Klimko, M.
Bykowska, J.
Powiązania:
https://bibliotekanauki.pl/articles/790611.pdf
Data publikacji:
2015
Wydawca:
Uniwersytet Przyrodniczy w Poznaniu
Tematy:
pollen morphology
pollen grain
Pinus uliginosa
Pinus uncinata
experimental culture
scanning electron microscopy
Opis:
Pollen grains of Pinus uliginosa and P. uncinata were examined by light and scanning electron microscopy. The pollen grains were bisaccate and monosulcate. The corpus-saccus attachment was distinct. The pollen corpus exine sculpture was verrucate-rugulate and deeply sculptured. The surface of the tectum was with or without small grana and it was perforate. The saccus sexine ornamentation was reticulate and irregularly perforate. The tectum surface characters in the proximal and distal view of the corpus and saccus were less variable and they did not provide good criteria to identify the species under study. Among the P. uncinata from the Forest Arboretum there were differences observed in the size, shape and height of elevation and sculpture on the corpus between pollen grains of the same specimen. This study of the pollen grain morphology of the corpus and saccus provided some important new data.
Źródło:
Steciana; 2015, 19, 3
1689-653X
Pojawia się w:
Steciana
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Materiały dla jednowarstwowych ogniw paliwowych
Materials for single layer fuel cells
Autorzy:
Winiarz, P.
Powiązania:
https://bibliotekanauki.pl/articles/134696.pdf
Data publikacji:
2016
Wydawca:
ADVSEO
Tematy:
fuel cell
composite material
proton conductor
lanthanum niobate
scanning electron microscopy
x-ray diffraction
Opis:
A composite material, which may be further applied as a single layer fuel cell, was synthesized using solid state synthesis method. Composite consisted of two components. The first was a nanoceramic proton conductor – calcium doped lanthanum niobate. The second one was a nanoceramic semiconductor oxide composed of lithium, nickel and zinc oxides respectively. Structural and electrical investigations were performed on the received material. Scanning electron microscope images showed that the microstructure on the surface of this material is homogeneous. Energy dispersive X-Ray diffraction confirms that the components of the investigated composite are mixed together in a volume of material allowing to current flow through the percolation threshold. Open circuit voltage was changing during measurement from 0.8V to 0.6V. Moreover, the material did not change its structural properties during the current flow, hence it could be a good candidate to the production of single layer fuel cells.
Źródło:
Technical Issues; 2016, 4; 104-109
2392-3954
Pojawia się w:
Technical Issues
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Monotonic behaviour of typical Al-Cu-Mg alloy pre-strained at elevated temperature
Autorzy:
Tomczyk, A.
Seweryn, A.
Doroszko, M.
Powiązania:
https://bibliotekanauki.pl/articles/281485.pdf
Data publikacji:
2018
Wydawca:
Polskie Towarzystwo Mechaniki Teoretycznej i Stosowanej
Tematy:
creep and tensile tests
metals and alloys
scanning electron microscopy
numerical calculations
mechanical properties
Opis:
This paper presents results of monotonic tensile and creep tests conducted on typical Al-Cu-Mg alloy (commercial 2024) specimens. Tensile tests carried out at room (20°C) and elevated (100°C, 200°C, 300°C) temperatures made it possible to determine strength properties of the material (Young’s modulus, yield stress, ultimate tensile strength). Creep tests were performed at elevated temperature (100°C, 200°C and 300°C) with a constant force. In order to obtain material creep characteristics, creep-rupture tests were carried out. Then creep tests were conducted with two different strain values: one corresponding to the beginning of the secondary creep and the other corresponding to a certain value of the tertiary creep. After preliminary creep deformation at two various strain levels, specimens were cooled at ambient temperature and then subjected to monotonic tensile tests. The characteristics of the material were obtained for pre-strained specimens at different temperatures. Specimens fracture surfaces obtained as a result of tensile (at elevated and room temperature), creep and combined tests were analyzed.
Źródło:
Journal of Theoretical and Applied Mechanics; 2018, 56, 4; 1055-1068
1429-2955
Pojawia się w:
Journal of Theoretical and Applied Mechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Transition in SrZnO Laser Pulse Deposited Alloy
Autorzy:
Albrithen, H. A.
Elnaggar, M.
Ozga, K.
Szota, M.
Alahmed, Z. A.
Alanazi, A. Q.
Alshahrani, H.
Alfaifi, E.
Djouadi, M. A.
Labis, J. P.
Powiązania:
https://bibliotekanauki.pl/articles/355190.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
oxide materials
solid state alloys
structural phase transition
X-ray diffraction
scanning electron microscopy
Opis:
We have discovered a structural transition for the SrZnO alloy films from a wurtzite to a rock-salt structure, leading to a reduction in the (112̲0)/(0001) surface energy ratio. The films were grown by pulsed laser deposition using different SrO ratios, x. We have revealed that growth at a higher temperature, 750°C, resulted in a sharp 0002 peak at a low SrO content (5%), whereas growth at a higher SrO content (10%) resulted in a non-crystalline film with minute crystallites with a (112̲0) orientation. Generally the crystallinity decreased as the SrO content increased. No results obtained for the crystalline films showed any orientation of significant peaks besides the peak attributed to the (0001) plane, suggesting epitaxial growth. Optical measurements showed difference in transmission widows of alloys with different SrO percentage, and this was correlated to SrO influence on growth mode as indicated by scanning electron imaging. The studied SrZnO films, with SrO/(SrO + ZnO) ≤ 0.25, were grown by pulsed laser deposition using different SrO ratios, x. The effects of temperature and oxygen pressure during growth on the films’ structural properties were investigated. XRD results indicate that the film crystallinity was improved as the temperature and O2 pressure increased up to 650°C and 0.5 Torr, respectively.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 211-216
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The impact of calcination on changes in the physical and mechanical properties of the diatomites of the Leszczawka Member (the Outer Carpathians, Poland)
Autorzy:
Figarska-Warchoł, Beata
Rembiś, Marek
Stańczak, Grażyna
Powiązania:
https://bibliotekanauki.pl/articles/955169.pdf
Data publikacji:
2019
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
silica
thermal modification
scanning electron microscopy
Vickers microindentation hardness
porosity
apparent density
water absorption
Opis:
The work concerned the effects of the thermal treatment of diatomites from the Jawornik deposit (an example of the diatomites of the Leszczawka Member of the Polish Outer Carpathians). Five distinct lithological varieties were subjected to calcination at 600°C in ambient air. The thermal impact induced the following changes to the rocks. Their overall rock porosity increased, most distinctly in the initially softer varieties, and the internal pores of the siliceous frustules themselves usually became larger due to the initial melting of the silica phases. Most of the diatoms, quartz and feldspars cracked as a result of their brittle fracturing under compressive strain resulting from substantial and differing size changes of growing grains. Clay minerals were thermally transferred, changing their volume. The organic matter dispersed throughout the diatomites was partly oxidized and removed. At the same time, the structure of the rocks was strengthened, as confirmed by an increase in their microhardness. The microhardness of soft and porous diatomite varieties increased considerably on heating, but that of the hard and compact variety changed to a smaller degree. The increase is directly related to the content of the clay minerals. The impact of other mineral components was not detected. The calcination of lithologically diversified diatomites provided the mineral with raw material with deicing and antisliding properties. The technology of its production has been determined by the authors and submitted as a patent.
Źródło:
Geology, Geophysics and Environment; 2019, 45, 4; 269-282
2299-8004
2353-0790
Pojawia się w:
Geology, Geophysics and Environment
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Scanning optical and electron microscopes with computer image acquisition
Autorzy:
Konstankiewicz, K.
Pukos, A.
Powiązania:
https://bibliotekanauki.pl/articles/25623.pdf
Data publikacji:
1995
Wydawca:
Polska Akademia Nauk. Instytut Agrofizyki PAN
Tematy:
electron microscope
scanning optical microscope
microscopic method
tandem scanning reflected light microscope
computer image analysis
scanning electron microscopy
biological material
rotary microtome
confocal microscopy
Źródło:
International Agrophysics; 1995, 09, 4
0236-8722
Pojawia się w:
International Agrophysics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cast iron component failure: A metallurgical investigation
Autorzy:
Sudhakar, K. V.
Powiązania:
https://bibliotekanauki.pl/articles/382757.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cast iron
hardness test
optical microscopy
scanning electron microscopy
fractography
żeliwo
testy twardości
mikroskopia optyczna
mikroskop skaningowy
Opis:
A fractured nutcracker was examined for determining the root cause/s for premature fracture/failure. This is one of the common tools used typically for cracking hard nuts. In this study, metallurgical failure analysis techniques namely, visual inspection, optical microscopy, SEM, and hardness tests were used in investigating the broken product. From the metallurgical analysis, it was determined that the combined effect of low carbon equivalent and presence of inclusions contributed to the sudden fracture of the nut cracking tool.
Źródło:
Archives of Foundry Engineering; 2012, 12, 2s; 67-70
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
In situ-formed bacterial exopolysaccharide (EPS) as a potential carrier for anchorage-dependent cell cultures
Autorzy:
Komorowski, Piotr
Kołodziejczyk, Agnieszka
Makowski, Krzysztof
Kotarba, Sylwia
Walkowiak, Bogdan
Powiązania:
https://bibliotekanauki.pl/articles/1844871.pdf
Data publikacji:
2021
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
bacterial exopolysaccharides
dextran- -based “microcarriers”
scanning electron microscopy
atomic force microscopy
roughness parameters
three-dimensional cell culture
Opis:
The study involved the use of a bacterial strain isolated from environmental samples which produce the biopolymer in the form of pellets in the submerged culture. This material (bacterial exopolysaccharide) is produced by bacteria of the Komogateibacter xylinus which are prevalent in the environment. The aim of this study was to characterize bacterial exopolysaccharides and commercial dextran-based “microcarriers” in terms of their roughness and cell culture effects, including the morphology and viability of the human hybridoma vascular endothelial cell line EA.hy926. The pellets were characterized using scanning electron microscopy (SEM) and atomic for¬ce microscopy (AFM). The resulting structures were used for cell culture of adherent cells (anchorage¬-dependent cells). At the same time, the cultures with commercial, dextran-based “microcarriers” were carried out for comparative purposes. After com¬pletion of the cell culture (24 hours of culture), the cellulose and commercial “carriers” were analyzed using SEM and AFM. Finally, the obtained cell dens¬ities (fluorescence labelling) and their morphological characteristics (SEM) were compared. The obtained results strongly support the applicability of bacterial exopolysaccharide (EPS) in tissue engineering to build innovative 3D scaffolds for cell culture, the more so that it is technologically possible to produce EPS as spatially complex structure
Źródło:
Engineering of Biomaterials; 2021, 24, 159; 18-23
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Using scanning electron microscopy to study slug morphology
Autorzy:
Kaluski, T.
Gawlak, M.
Cieluch, P.
Kozlowski, J.
Powiązania:
https://bibliotekanauki.pl/articles/84768.pdf
Data publikacji:
2012
Wydawca:
Uniwersytet Mikołaja Kopernika. Wydział Biologii i Ochrony Środowiska. Stowarzyszenie Malakologów Polskich
Tematy:
scanning electron microscopy
slug
Arion lusitanicus
Arion rufus
pest
cultivated plant
animal population
animal morphology
Źródło:
Folia Malacologica; 2012, 20, 1
1506-7629
Pojawia się w:
Folia Malacologica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Diatomaceous rocks of the Jawornik deposit (the Polish Outer Carpathians): petrophysical and petrographical evaluation
Autorzy:
Figarska-Warchoł, B.
Stańczak, G.
Rembiś, M.
Toboła, T.
Powiązania:
https://bibliotekanauki.pl/articles/184292.pdf
Data publikacji:
2015
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
critical raw materials
diatomite
silica
scanning electron microscopy (SEM)
chemical analysis
porosity
Vickers microindentation hardness
Opis:
Diatomites belonging to a list of raw materials used in the EU criticality assessment are essential to many industrial applications due to a unique combination of their physical properties, i.e. porous and permeable structure, high specific surface area and adsorption capacity, low density and thermal conductivity, and chemical inertness. The present study was undertaken to analyse the relationships between the pore network characteristics, petrophysical parameters, and mineralogical variability of the Lower Miocene diatomites from the Jawornik deposit (Skole Unit, the Polish Outer Carpathians, SE Poland). Five varieties of the diatomites, distinguished on the basis of the macroscopic features, i.e., colour and fracturing effects, have been investigated by SEM, chemical and XRD analysis, mercury intrusion porosimetry, helium pycnometry, and the Vickers hardness tests. Significantly differing are two varieties. The light-coloured, massive and block-forming diatomites (variety BL) consist mainly of poorly cemented siliceous skeletal remains of diatoms, and represent the rocks with high total porosity (38–43%), low bulk density (1.28–1.38 g/cm3) and low microhardness (10.7 HV0.3). The dark-gray silicified diatomites with a platy or prismatic splitting (variety PD) reveal obscured microfossils of diatoms and are the most compact and hard rocks (80.8 HV0.3), with poor total porosity (17–24%) and higher bulk density (1.70–1.78 g/cm3). The spatial distribution of the field identifiable rock varieties allows selective exploitation of the diatomites with the predictable petrophysical characteristics that define their future use.
Źródło:
Geology, Geophysics and Environment; 2015, 41, 4; 311-331
2299-8004
2353-0790
Pojawia się w:
Geology, Geophysics and Environment
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of selected diffractive and microscopic methods to evaluate the physical state of drug and morphology of microspheres obtained by spray drying of furosemide with Eudragit L30 D-55.
Autorzy:
Ostróżka-Cieślik, Aneta
Sarecka-Hujar, Beata
Krzykawski, Tomasz
Karcz, Jagna
Banyś, Anna
Jankowski, Andrzej
Powiązania:
https://bibliotekanauki.pl/articles/895685.pdf
Data publikacji:
2018-06-30
Wydawca:
Polskie Towarzystwo Farmaceutyczne
Tematy:
X-ray diffraction
scanning electron microscopy
Microsphere
furosemide
laser diffraction
Eudragit L30 D-55
Opis:
In pharmaceutical technology, the analysis of physicochemical properties of raw materials, intermediates and products is part of quality control testing at each stage of designing formulations and in the routine evaluation of the final product. The aim of the study was to analyse the physical state of drug and the morphology of microspheres obtained by spray drying, where furosemide was incorporated in the polymeric matrix of Eudragit L30 D-55. The following optimal parameters of the spray drying process were established: aspirator capacity of 80%, T.in: 140 ° C, pump capacity: 10%. The laser diffraction method was used to analyse the size distribution of microspheres in the following furosemide-Eudragit L30 D-55 systems: 1:1, 1:3, 1:5. X-ray powder diffraction was applied to compare the degrees of crystallinity of the final product and the starting material. Furosemide has crystal structure both before and after spray drying, it occurs in the polymorphic forms (form I crystals). No reflection from the crystalline phase has been found on the diffraction pattern of Eudragit. This is an amorphous substance.
Źródło:
Acta Poloniae Pharmaceutica - Drug Research; 2018, 75, 3
0001-6837
2353-5288
Pojawia się w:
Acta Poloniae Pharmaceutica - Drug Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of structural relaxations within the amorphous structure on the magnetic properties of amorphous tapes from FeCoB family
Autorzy:
Szota, M.
Powiązania:
https://bibliotekanauki.pl/articles/354999.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous materials
free volumes
quasidislocation dipoles
scanning electron microscopy
approach to ferromagnetic saturation
magnetic moments
Opis:
The paper presents the research results for the Fe78Co2Si9B11 amorphous alloy, and after the process of annealing resulting only in the relaxation of the material. The structure relaxations occurring in the volume of test samples lead to the changes in their magnetic and mechanic properties. Therefore the studies on the effect of the structure defects on the properties of these type of materials are important. Understanding the processes occurring during the magnetizing of amorphous alloys can be helpful in the design of modern functional materials for special purposes. The main purpose of this elaboration was to determine the effect of the amorphous structure defects in the state after solidification and after heat treatment on the changes in the magnetizing process and in such parameters as the saturation magnetization and the coercivity field.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 217-222
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of some compounds on development of Sphaerotheca pannosa var. rosae
Autorzy:
Wojdyla, A T
Powiązania:
https://bibliotekanauki.pl/articles/66257.pdf
Data publikacji:
2000
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
plant disease
Sphaerotheca pannosa var.rosae
control
biopreparation
rose
development
scanning electron microscopy
oil
compound
Opis:
Influence of triforine (standard), garlic juice, Antifung 20 SL (20% vermicompost), Atpolan 80 EC (76% mineral oil), Biosept (grapefruit juice) and Atonik AL on development of Sphaerotheca pannosa var. rosae was evaluated. Garlic juice, Atpolan 80 EC and Biosept applied as rose spray gave similar effect in the control S. pannosa var. rosae as triforine. Observations under scanning electron microscop indicated that 24 hrs after rose spraying all tested compounds cause almost complete collapse of conidia and hyphe.
W przeprowadzonych badaniach polowych oraz w uprawie róż pod osłonami oceniano aktywność biologiczną biopreparatów (Antifung 20 SL), Biosept, sok z czosnku, oleju (Atpolan 80 EC) i stymulatora wzrostu roślin (Atonik AL) do zwalczania S. pannosa var. rosae. Krzewy róż opryskiwano co 7 lub 14 dni. W drugiej części badań przy użyciu mikroskopu skaningowego oceniano wpływ badanych związków na grzyba. W tym celu krzewy róż uprawiane pod osłonami opryskano jeden raz, a po 24 godzinach pobrano liście do obserwacji. Badane preparaty wykazywały wysoką skuteczność w zwalczaniu S. pannosa var. rosae. Niektóre z nich dorównywały (sok z czosnku) bądź nieznacznie ustępowały (Antifung 20 SL, Atpolan 80 EC, Biosept) skutecznością fungicydowi standardowemu Saprol 190 EC. Zdecydowanie niższą skuteczność wykazywał Atonik AL. Z kolei wzrost stężenia preparatów Biosept oraz soku z czosnku wiązał się ze wzrostem ich skuteczności. Natomiast Antifung 20 SL stosowany co 14 dni wykazywał niższą skuteczność aniżeli przy aplikowaniu co 7 dni. Już po 24 godzinach od wykonania opryskiwania w obserwacji przeprowadzonej przy użyciu mikroskopu skaningowego stwierdzono, że badane związki powodowały prawie całkowite spłaszczenie i deformację grzybni, trzonków oraz zarodników konidialnych. Jednak w przypadku preparatu Atonik AL tylko fragmenty grzybni były całkowicie zniszczone. Z kolei po zastosowaniu oleju Atpolan 80 EC stwierdzono rozpad fragmentów grzyba, a następnie ich łączenie się w płatowate, strzępiaste - dosyć duże struktury.
Źródło:
Journal of Plant Protection Research; 2000, 40, 2
1427-4345
Pojawia się w:
Journal of Plant Protection Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Scanning electron microscope at low voltage operation – a unique characterization tool for graphene layers
Skaningowy mikroskop elektronowy pracujący w zakresie niskich wartości napięcia przyspieszającego jako unikatowe narzędzie do charakteryzacji warstw grafenu
Autorzy:
Jóźwik, I.
Powiązania:
https://bibliotekanauki.pl/articles/192086.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Technologii Materiałów Elektronicznych
Tematy:
graphene
graphene characterization
low-kV scanning electron microscopy
grafen
charakteryzacja grafenu
niskoenergetyczna skaningowa mikroskopia elektronowa
Opis:
Graphene grown on Cu foils by chemical vapor deposition (CVD) technique has been investigated using commercially available scanning electron microscope at low voltage operation. The optimized conditions of SEM imaging carried out in a double-channel mode (registering secondary electrons type 1 (SE1) and backscattered electrons (BSE) images in a single scan) allowed for the visualization of typical features of graphene on Cu, such as folds, cracks and add-layers. The mechanism of thickness contrast observed in the BSE images was described in terms of low loss-BSE detection. Antioxidant qualities of graphene sheets on metallic substrate were confirmed by the ability of observation of the channeling contrast in Cu substrates at primary electrons energy of 0.5 keV.
Próbki grafenu otrzymywanego metodą chemicznego osadzania z fazy gazowej na podłożach Cu poddano badaniom przy użyciu komercyjnego skaningowego mikroskopu elektronowego (SEM) pracującego w zakresie niskich wartości napięcia przyspieszającego. Optymalizacja warunków obrazowania SEM prowadzona w trybie dwukanałowym (rejestracja obrazów SE1 i BSE podczas tego samego skanu) pozwoliła na wizualizację typowych cech grafenu na Cu takich jak fałdy, pęknięcia i dodatkowe warstwy. Mechanizm kontrastu związanego ze zmianami liczby warstw grafenu obserwowanego w obrazach BSE został przedstawiony w oparciu o detekcję elektronów BSE o niskich stratach energii. Przeciwutleniające właściwości grafenu na metalicznych podłożach zostały potwierdzone poprzez możliwość obserwacji kontrastu kanałowania elektronów w podłożach Cu przy energii elektronów pierwotnych rzędu 0,5 keV.
Źródło:
Materiały Elektroniczne; 2016, T. 44, nr 2, 2; 11-16
0209-0058
Pojawia się w:
Materiały Elektroniczne
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of different grain size of expanded perlite aggregate and content of silica aerogel on the characteristics of lightweight cementitious composite
Autorzy:
Vashchuk, Andrii
Ślosarczyk, Agnieszka
Powiązania:
https://bibliotekanauki.pl/articles/24085741.pdf
Data publikacji:
2023
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
lightweight composite
expanded perlite aggregate
silica aerogel
mechanical characteristic
thermal conductivity coefficient
scanning electron microscopy
Opis:
In this research, an attempt was made to investigate effects of expanded perlite aggregate grain size on consistency, density, compressive strength, thermal conductivity and microstructure of 15 different composite mixes with silica aerogel. As for the samples preparation, expanded perlite aggregate of 5 different groups based on grain size, were used for sample preparation, then partially replaced by volume for 20% and 40% of hydrophobic silica aerogel particles. The results showed, that density of the samples varied between 0.35 g/cm3 and 1.5 g/cm3, flexural strength varied between 3.4 MPa and 7.4 MPa, compressive strength was in the range between 12.3 MPa and 55 MPa, thermal conductivity coefficient was in the range between 0.130 W/mK and 0.190 W/mK. Scanning electron microscopy showed that expanded perlite aggregates and silica aerogel particles are capable of being mixed and formed homogenous mixture. Nevertheless, microscope images indicated weaker adhesion of silica aerogel particles at interfacial zone as compared with expanded perlite aggregate particles. Results revealed, that both of the factors: grain size of expanded perlite aggregate particles silica aerogel content influenced the density, compressive strength and thermal conductivity. The study also indicated feasibility of expanded perlite aggregate and silica aerogel for achieving homogeneous mixture of the lightweight cementitious composites. Study demonstrated that using different size fractions of expanded perlite aggregate affects differently physical, mechanical and thermal characteristics of the lightweight cementitious composite with silica aerogel.
Źródło:
Physicochemical Problems of Mineral Processing; 2023, 59, 4; art. no. 174338
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Early stage development of IS-group isolates of Heterobasidion annosum on Abies alba roots - scanning electron microscopical studies
Autorzy:
Werner, A
Lakomy, P.
Idzikowska, K.
Zadworny, M.
Powiązania:
https://bibliotekanauki.pl/articles/41782.pdf
Data publikacji:
2006
Wydawca:
Polska Akademia Nauk. Instytut Dendrologii PAN
Tematy:
Abies alba
root
Heterobasidion annosum
isolate
early stage
scanning electron microscopy
adhesion
hypha behaviour
root surface
Opis:
The growth of hyphae and prepenetration phenomena on Abies alba roots after inoculation with the P-, S- and F-group isolates of Heterobasidion annosum were observed using scanning electron microscope. Elongated hyphae emanating from the inocula grew indiscriminately across and along root tips and entered the cortical cells randomly, while in subapical root areas they quite often grew along grooves at points of cell junctions. The ridges, folds and depressions seen on the root surface obviously directed the hyphal growth and their further entrance into roots through natural crevices or cracks. Although hyphae of all the isolates could penetrate the roots directly through small openings, the hyphae of the F isolate penetrated preferably more eroded and older parts of roots. A peculiar habit of the direct penetration, characterized by formation a structure resembling infection peg, was observed only after inoculation with the P and S isolates. It is suggested that specifically frequent penetration the roots in eroded areas by the hyphae of the F isolate may be one of the factors connecting with its lower pathogenic capabilities.
Źródło:
Dendrobiology; 2006, 55; 57-63
1641-1307
Pojawia się w:
Dendrobiology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Mechanical Characteristics of the Ternary SnZnAl Lead-Free Alloy
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Sobczak, N.
Powiązania:
https://bibliotekanauki.pl/articles/380398.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead free alloy
microstructure
mechanical properties
scanning electron microscopy
stop bezołowiowy
mikrostruktura
właściwości mechaniczne
mikroskop skaningowy
Opis:
The paper describes the studies of ternary SnZn9Al1.5 lead-free alloy from the viewpoint of its mechanical behavior as well as microstructure examined by the light and scanning electron microscopy. The authors focused their attention specifically on the fatigue parameters determined by the original modified low-cycle fatigue method (MLCF), which in a quick and economically justified way allows determination of a number of mechanical parameters based on the measurement data coming from one test sample only. The effect of the addition of 1.5% Al to the binary eutectic SnZn9 alloy on its microstructure and the obtained level of mechanical parameters was analyzed. The phases and intermetallic compounds occurring in the alloy were identified based on the chemical analysis carried out in micro-areas by the SEM/EDS technique. It was shown that the addition of 1.5% Al to the binary eutectic SnZn9 alloy resulted in a more favorable microstructure and consequently had a positive effect on the mechanical parameters of the alloy. Based on the conducted research, it was recommended to use a combinatorial method based on the phase quanta theory to quickly evaluate the microstructure and the original MLCF method to determine a number of mechanical parameters.
Źródło:
Archives of Foundry Engineering; 2018, 18, 3; 31-36
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Właściwości mechaniczne i morfologia folii piezoelektrycznych na bazie kompozytów z polipropylenu
Autorzy:
Chylińska, M.
Kaczmarek, H.
Królikowski, B.
Klimiec, E.
Powiązania:
https://bibliotekanauki.pl/articles/277989.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Inżynierii Materiałów Polimerowych i Barwników
Tematy:
materiały piezoelektryczne
polipropylen
właściwości mechaniczne
skaningowa mikroskopia elektronowa
piezoelectric materials
polypropylene
mechanical properties
scanning electron microscopy
Źródło:
Przetwórstwo Tworzyw; 2017, T. 23, Nr 1 (175), 1 (175); 6
1429-0472
Pojawia się w:
Przetwórstwo Tworzyw
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study by scanning electron microscopy of the morphogenesis of filiform and fungiform papillae in the rabbit, Oryctolagus cuniculus f. domestica
Badanie przy pomocy mikroskopu elektronowego skaningowego morfogenezy brodawek nitkowatych i grzybowatych u królika, Oryctolagus cuniculus f. domestica
Autorzy:
Kulawik, M.
Godynicki, S.
Powiązania:
https://bibliotekanauki.pl/articles/44839.pdf
Data publikacji:
2013
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
domestic rabbit
rabbit
Oryctolagus cuniculus f.domestica
scanning electron microscopy
morphogenesis
filiform papilla
fungiform papilla
papilla
Opis:
Rudiments of fungiform papillae were observed at day 18 of prenatal development. They were arranged only on the dorsal surface of the apex of the tongue and its margins. The fungiform papillae looked like a hemispherical, dome-shaped eminences. From day 22 of prenatal development, scanning electron microscope showed also that rudiments of fungiform papillae appeared on the body of the tongue at the front of forming torus linguae, and on its both sides. No rudiments of filiform papillae were observed at day 22 of prenatal development. However, after removal the epithelium, the connective tissue cores of rudiments of fungiform and filiform papillae were visible. Scanning electron microscopy showed on the surface of the tongue numerous filiform papillae at day 26 of prenatal development. They were arranged on the entire dorsal surface of the apex and body of the tongue, and on its margins. During morphogenesis two types of filiform papillae were noticed. One type of filiform papillae was similar to separated cones, another had 3–4 processes more. The similar changes was with the shape of connective tissue core. The fungiform papillae were located among filiform papillae. Scanning electron microscope showed three types connective tissue cores of developing fungiform papillae. One type was mace-shaped, another one was bowl-shaped and yet barred-shaped. At day 30 of postnatal development on the surface of the connective tissue cores of fungiform papillae, from its top towards its base there were parallel and longitudinal folds.
Zawiązki brodawek grzybowatych obserwowano w 18 dniu rozwoju prenatalnego. Były one rozmieszczone na powierzchni grzbietowej wierzchołka języka i na jego brzegach. Brodawki grzybowate wyglądały jak półkoliste, kopulaste wyniosłości. Od 22 dnia rozwoju prenatalnego, mikroskop elektronowy skaningowy wykazał, że zawiązki brodawek grzybowatych pojawiły się także na trzonie języka przed formującym się wałem języka i po jego bokach. Żadnych zawiązków brodawek nitkowatych nie obserwowano w 22 dniu rozwoju prenatalnego. Jednak po usunięciu nabłonka, zręby łącznotkankowe zawiązków brodawek grzybowatych i nitkowatych były widoczne. Mikroskop elektronowy skaningowy wykazał na powierzchni języka liczne brodawki nitkowate dopiero w 26 dniu rozwoju prenatalnego. Były one rozmieszczone na całej powierzchni grzbietowej wierzchołka i trzonu języka i na jego brzegach. Podczas morfogenezy zanotowano dwa typy brodawek nitkowatych. Jeden typ brodawek nitkowatych był podobny do pojedynczych stożków a drugi miał dodatkowe 3-4 wyrostki. Podobne zmiany dotyczyły kształtu zrębu łącznotkan- kowego. Brodawki grzybowate zlokalizowane były pośród brodawek nitkowatych. Mikroskop elektronowy skaningowy wykazał trzy typy zrębów łącznotkankowych brodawek grzybowatych. Jeden typ był kształtu buławkowatego, drugi miseczkowa- tego a kolejny beczułkowatego. W 30 dniu rozwoju postnatalnego, na powierzchni zrębów łącznotkankowych brodawek grzybowatych, od ich wierzchołka w kierunku podstawy przebiegały podłużne i równoległe fałdy.
Źródło:
Acta Scientiarum Polonorum. Zootechnica; 2013, 12, 4
1644-0714
Pojawia się w:
Acta Scientiarum Polonorum. Zootechnica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface analysis of long-term hemodialysis catheters made of carbothane (poly(carbonate)urethane) before and after implantation in the patients’ bodies
Autorzy:
Nycz, M.
Paradowska, E.
Arkusz, K.
Kudliński, B.
Krasicka-Cydzik, E.
Powiązania:
https://bibliotekanauki.pl/articles/306579.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
chropowatość powierzchni
mikroskopia sił atomowych
mikroskopia skaningowa
surface roughness
atomic force microscopy
scanning electron microscopy
Catheter-tissue contact
film
Opis:
The vascular cannulation is associated with a number of complications. The aim of this work was to study the composition and distribution of the film covering the surfaces of Mahurkar Maxid and Palindrome catheters, which were removed from the body of long-term hemodialysis patients. Moreover, the roughness and contact angle of the catheters were evaluated. Methods: Two brand new (as a reference) and thirty used catheters were the subject of the study. Their implantation period lasted from 4 months to a year and the reason for removal was the production of another vascular access or obstruction. Surfaces were analyzed by scanning electron microscope, atomic force microscope and goniometer. Results: The inner surfaces of the used catheters were covered with a film of various complexity which includes a plurality of protein, blood cell counts and the crystals. The closer to the distal part the film becomes more complex and multi-layered. Even the surfaces of brand new catheter were not completely smooth. The only significant difference between analyzed models was the presence of thrombus in the distal part of Mahurkar Maxid catheters, not in the Palindrome. Conclusions: The distal part of the catheters is the place most exposed to obstruction and infection, which may be due to not reaching the anticoagulant agent into this part. Not only the occurrence of side holes affects the formation of thrombus, but also their quantity, geometry and distribution which effect on fluid mechanics. The surface of the catheters needs to improvement to minimize the occurrence of defects and cracks.
Źródło:
Acta of Bioengineering and Biomechanics; 2018, 20, 2; 47-53
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of the electrolytically polished skeletal dentures surfaces using various nano- and microscopic technologies
Autorzy:
Dąbrowa, Tomasz
Majstrzyk, Wojciech
Tamulewicz, Magdalena
Piasecki, Tomasz
Kunicki, Piotr
Więckiewicz, Włodzimierz
Gotszalk, Teodor
Powiązania:
https://bibliotekanauki.pl/articles/306706.pdf
Data publikacji:
2019
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
chropowatość powierzchni
skaningowa mikroskopia elektronowa
proteza ruchoma
mikroskopia skaningowa
surface roughness
scanning electron microscopy
removable partial denture
scanning probe microscopy
optical profilometry
Opis:
The surface roughness of the dental restorations is significant to the denture plaque adhesion. Methods: In this work, we present the complex analysis of the electropolished CoCrW alloy remanium® star (Dentaurum, Germany) samples with laserengraved fiducial marks performed using complementary set of micro- and nanoscopic techniques: optical profilometry (OP), atomic force microscopy (AFM), scanning electron microscopy (SEM) and focused ion beam (FIB) milling. Results: Both mean and RMS roughness of the samples were reduced by electopolishing process, however, the results obtained using OP and AFM exhibited some discrepancies. This was caused by the relatively high local protruding defects developed on the processed surface. The cross-sections of the protrusions were made to analyze the cause of their formation as the EDS elemental content maps revealed that their composition was uniform. We also analyzed the local roughness in the smaller areas free from the defects. Conclusions: In that case, both OP and AFM techniques delivered the same results. Analysis of results showed that various methods used for the surface roughness evaluation have to be used simultaneously to obtain complete and true analysis of the technological CoCrW samples.
Źródło:
Acta of Bioengineering and Biomechanics; 2019, 21, 4; 123-129
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ocena wpływu zewnętrznych pól magnetycznych i elektromagnetycznych na działanie skaningowego mikroskopu elektronowego
Estimation of external magnetic and electromagnetic fields influence on Scanning Electron Microscope operation
Autorzy:
Płuska, M.
Oskwarek, Ł.
Powiązania:
https://bibliotekanauki.pl/articles/151432.pdf
Data publikacji:
2007
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
mikroskopia elektronowa
skaningowy mikroskop elektronowy
zakłócenia elektromagnetyczne
indukcja magnetyczna
scanning electron microscopy (SEM)
electromagnetic distortions
magnetic induction
Opis:
Tematyka artykułu odnosi się do aktualnych zagadnień z zakresu skanin-gowej mikroskopii elektronowej. Odkształcenia obrazu struktury badanego obiektu spowodowane wpływem zewnętrznych pól magnetycznych lub elektromagnetycznych są jednym z najczęstszej spotykanych niepożądanych efektów w mikroskopii. Prowadzone w tym zakresie analizy i badania mają na celu przede wszystkim uzyskanie oceny ilościowej dotyczącej indukcji pola magnetycznego przenikającego przez komorę mikroskopu oraz jej wpływu na wartość odchylenia wiązki padającej na obiekt badany (np. element półprzewodnikowy).
In the paper some tasks deal with Scanning Electron Microscope (SEM) are presented. Image deformation caused by electromagnetic interference (EMI) is one of the most frequent undesirable effects in practical scanning electron microscopy. They usually appear as a constant or periodic deformation of vertical edges of an observed specimen. Available, but still very expensive methods for decreasing their influence are shielding and electromagnetic field compensation. The other approach is digital image processing for its correction. However, elimination of the distortions (with hardware or software methods) would be more effective when their influence on microscope system are known or predictable. The main goal of current investigations is work out a method for quantitative measurement of magnetic field in the microscope chamber and estimation of its influence on electon beam deflaction. The results obtained by the use of scanning electron microscope were verified by comparing its with the ones obtained using alternative magnetic field meter.
Źródło:
Pomiary Automatyka Kontrola; 2007, R. 53, nr 9, 9; 61-64
0032-4140
Pojawia się w:
Pomiary Automatyka Kontrola
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analiza SEM czarnego tonera na wydrukach. Część II
SEM analysis of black toner on printouts. Part II
Autorzy:
Łasińska, Anna
Powiązania:
https://bibliotekanauki.pl/articles/1052550.pdf
Data publikacji:
2021-04-29
Wydawca:
Agencja Bezpieczeństwa Wewnętrznego
Tematy:
toner
brother
konica minolta
skaningowa mikroskopia elektronowa
mikroanaliza rentgenowska
sem/edx
scanning electron microscopy
x-ray
microanalysis
Opis:
Eksperci w zakresie badań dokumentów są często proszeni o określenie, czy wydruk pochodzi z określonej drukarki laserowej. Drukarkę rzadko można zidentyfikować, chyba że na wydruku są widoczne jej unikalne wady lub nieprawidłowości. W artykule przedstawiono możliwości identyfikacji i weryfikacji tonerów na wydrukach uzyskanych z różnych drukarek laserowych przy użyciu skaningowej mikroskopii elektronowej. W sumie 21 wydruków uzyskano z 21 różnych modeli maszyn drukujących Brother i Konica Minolta. Szesnaście wydruków uzyskano z drukarek, w których były oryginalne kasety z tonerem, a pięć z drukarek z zamiennikami. Ustalono jasne kryteria oceny indywidualnej. Na podstawie zdjęć SEM oraz tych kryteriów ujawniono szczegóły topografii struktury tonera. Na podstawie przeprowadzonych badań określono różnice lub podobieństwa tonerów na badanych wydrukach.
Document examiners are frequently asked to determine whether or not a printout originated from a particular laser printer. The printer can rarely be identified unless some unique defects or irregularities of the printing are present on the printout. This article presents an overview of a systematic approach to characterizing and discriminating the toner of different laser printers using scanning electron microscopy. A total of twenty-one collected printouts were printed on twenty-one different Brother and Konica Minolta printing machine models. Sixteen printouts were obtained using printers with original toner cartridges while five printouts were obtained using printers with compatible cartridges. Clear criteria were established for individual assessment. Based on the SEM images and established criteria the details of topography of the toner structure were revealed. Due to this tudy, the differences or similarities of toners on tested printouts were determined. The SEM technique can be successfully, simply, and rapidly applied to the analysis of toners on paper documents.
Źródło:
Przegląd Bezpieczeństwa Wewnętrznego; 2021, 13, 24; 221-249
2080-1335
2720-0841
Pojawia się w:
Przegląd Bezpieczeństwa Wewnętrznego
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Tribological tests of the nanomaterials used to reconstruct molars and premolars with the application of the direct method
Badania tribologiczne nanomateriałów do odbudowy zębów trzonowych i przedtrzonowych metodą bezpośrednią
Autorzy:
Ryniewicz, W.
Herman, M.
Ryniewicz, A. M.
Bojko, Ł.
Pałka, P.
Ryniewicz, A.
Madej, T.
Powiązania:
https://bibliotekanauki.pl/articles/190528.pdf
Data publikacji:
2017
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
stomatognathic system
composite
friction
wear
SEM (scanning electron microscopy)
nanostructure
układ stomatognatyczny
kompozyt
tarcie
zużycie
SEM
nanostruktura
Opis:
Physiological abrasion of teeth is a process of gradual loss of the hard tissue of opposite teeth resulting from age-related natural dental wear. In abrasion, the cusps and their slopes in the jaw and the mandible become flattened due to the mechanical load applied. The aim of this paper is to carry out a tribological and microstructural evaluation of modern composite materials used to reconstruct the teeth in the lateral part of the dental arch. Five light-cured composite materials were selected for tests. The tests involved the coefficient of friction and resistance to wear in a sliding contact in the presence of artificial saliva and the microstructure of the external surface of samples before the wear process and in the wear-related damaged area. The test method applied, which combines a biomechanical analysis of resistance to wear and the analysis of the microstructure before the wear process and in the wear-related damaged area, makes it possible to evaluate the tribological properties of composite materials used to reconstruct teeth in the lateral part of the dental arch.
Fizjologiczne starcie zębów jest to proces stopniowej utraty twardych tkanek zębów przeciwstawnych w wyniku naturalnego zużycia postępującego z wiekiem. Starcie to polega na jednoczesnym spłaszczaniu guzków i ich stoków w zębach szczęki i żuchwy w warunkach obciążeń biomechanicznych. Celem pracy jest ocena tribologiczna i mikrostrukturalna nowoczesnych materiałów kompozytowych stosowanych do odbudowy ubytków w bocznym odcinku łuku zębowego. Do badań wybrano 5 materiałów kompozytowych utwardzanych światłem. Przeprowadzono badania współczynnika tarcia i odporności na zużycie w kontakcie ślizgowym, w obecności sztucznej śliny oraz badania mikrostrukturalne warstwy wierzchniej próbek przed procesem zużycia oraz w strefie skazy zużyciowej. Zastosowana metoda badań łącząca biomechaniczną analizę odporności na zużycie z analizą mikrostruktury przed procesem zużycia oraz w skazie zużyciowej pozwala na ocenę właściwości tribologicznych materiałów kompozytowych do odbudowy zębów w bocznym odcinku łuku.
Źródło:
Tribologia; 2017, 273, 3; 155-164
0208-7774
Pojawia się w:
Tribologia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Flowering pattern, the structure of nectary surface and nectar secretion in two varieties of Ocimum basilicum L.
Autorzy:
Chwil, M
Powiązania:
https://bibliotekanauki.pl/articles/27488.pdf
Data publikacji:
2007
Wydawca:
Polskie Towarzystwo Botaniczne
Tematy:
pollen grain
nectar secretion
stoma
nectary
Lamiaceae
Ocimum basilicum
scanning electron microscopy
flowering pattern
flower
flowering
cuticle
Opis:
The studies conducted in the years 2003-2004 covered two varieties of Ocimum basilicum L.: var. purpurascens Benth. and var. lactucaefolium I. The flower lifetime, daily flowering pattern, morphology of pollen grains and the abundance of nectar secretion of flowers were compared. The surface of the nectaries of O. basilicum var. lactucaefolium was observed using scanning electron microscopy (SEM). The automorphic nectaries of basil formed the following parts: a flat part from the side of the upper lip and a convex part with three protrusions on the opposite side. On the top of two outer protrusions, stomatal areas were located, responsible for nectar secretion. The stomata occurred at the level of other epidermal cells. On the average, nectar contained 42% of sugars. The sugar yield of flowers of var. lactucaefolium was 36% higher than this feature in var. purpurascens. In terms of their size, the pollen grains were rated as medium-sized. Their viability ranged 88-96%. The shape of the pollen grains was described as oblate and suboblate.
Źródło:
Acta Agrobotanica; 2007, 60, 1
0065-0951
2300-357X
Pojawia się w:
Acta Agrobotanica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Scanning electron microscopy investigation of bacterial colonization of marine beach sand grains
Badania skaningowe bakterii kolonizujących ziarna piasku plaży morskiej
Autorzy:
Mudryk, Z.J.
Podgorska, B.
Powiązania:
https://bibliotekanauki.pl/articles/85221.pdf
Data publikacji:
2006
Wydawca:
Akademia Pomorska w Słupsku
Tematy:
scanning electron microscopy
bacterial colonization
sea beach
marine beach zob.sea beach
sand grain
bacteria
sand
beach
Opis:
Scanning electron microscopy was employed for the investigation of bacteria living on sand grains in a sandy marine beach in the Gulf of Gdansk (southern Baltic Sea). Bacteria colonize the sand grains; individual topography and shape of the grains were decisive for the colonization. Grains of diverse topography characterised by a great irregularity of shape were preferred, and protected surface sites were favoured. Many of the attached bacteria were found to produce polymer secretions; entire colonies attached by means of polymer nets were observed. A significant morphological diversity of bacteria in the vertical profile of the beach was determined. Bacteria inhabiting the sand grains showed the ability to reproduces.
W pracy przedstawiono wyniki badań dotyczących bakterii kolonizujących ziarna piasku plaży morskiej zlokalizowanej w rejonie Sopotu. Próby piasku pobierano z morza z odległości około 1,5 m od linii brzegowej (st. 1), z linii brzegowej (st. 2), środkowej części plaży (st. 3) oraz wydmy (st. 4). Przy użyciu mikroskopu skaningowego badano rozmieszczenie bakterii na ziarnach piasku, mechanizm ich adsorpcji do powierzchni ziaren piasku, zróżnicowanie morfologiczne i wymiary oraz ich zdolność do rozmnażania. Badania te wykazały, że bakterie maja zdolność do selektywnego kolonizowania ziaren piasku preferując głównie osłonięte i nieregularne powierzchnie (szpary, szczeliny, wklęśnięcia, fałdy, rysy). Wiele komórek bakterii kolonizujących ziarna piasku tworzyło charakterystyczne struktury włókniste, za pomocą których organizmy te trwale wiązały się z podłożem. Wykazano istotne zróżnicowanie morfologiczne bakterii na poszczególnych stanowiskach badawczych. Wiele bakterii zaabsorbowanych do ziaren piasku charakteryzowało się zdolnością do rozmnażania.
Źródło:
Baltic Coastal Zone. Journal of Ecology and Protection of the Coastline; 2006, 10
1643-0115
Pojawia się w:
Baltic Coastal Zone. Journal of Ecology and Protection of the Coastline
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Seed bio-priming with phosphate-solubilizing bacteria strains to improve rice (Oryza sativa L. var. FARO 44) growth under ferruginous ultisol conditions
Autorzy:
Musa, Saheed I.
Ikhajiagbe, Beckley
Powiązania:
https://bibliotekanauki.pl/articles/16688832.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czasopisma i Monografie PAN
Tematy:
bio-priming
ferruginous soil
phosphate-solubilizing bacteria
plant-growth-promoting capabilities
sustainable agriculture
rice
scanning electron microscopy
Opis:
This study investigated the possibility of using phosphate-solubilizing bacteria (PSB) with plant-growth-promoting (PGP) capabilities to improve the growth properties of rice plants under ferruginous ultisol (FU) conditions through bio-priming. The following PSB with PGP properties were used in this study: Bacillus cereus strain GGBSU 1, Proteus mirabilis strain TL14-1, and Klebsiella variicola strain AUH-KAM-9, which were previously isolated and characterized based on 16S rRNA gene sequencing. Biosafety analysis of the PSB isolates was conducted using blood agar. The rice seeds were then bio primed with the PSB for 3, 12, and 24 h and then sown in a composite FU soil sample. Differences in germinat ion bioassay were investigated 15 weeks after bio-priming using scanning electron microscopy (SEM), morphology, physiology, and biomass parameters. The composite FU soil used in this study had high pH, low bioavailable phosphorus, low water-holding capacity, and high iron levels, which resulted in low growth properties of rice seeds without bio-priming in the FU soil. Germination parameters were improved in seeds bio primed with the PSB, especially after 12 h of priming, compared with seeds without priming. SEM showed higher bacterial colonization in bio primed seeds. Bio-priming of rice seeds with the studied PSB under FU soil conditions significantly improved seed microbiome, rhizocolonization, and soil nutrient properties, thereby enhancing the growth properties of rice. This indicated the ability of PSB to solubilize and mineralize soil phosphate and improve phosphorus availability and soil properties for optimum plant usage in phosphate-stressed and iron toxic soils.
Źródło:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology; 2023, 104, 1; 33-51
0860-7796
Pojawia się w:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Metallographic analysis of selected cobalt-based alloys with carbon additive
Autorzy:
Woźna, A.
Powiązania:
https://bibliotekanauki.pl/articles/98793.pdf
Data publikacji:
2011
Wydawca:
Politechnika Śląska. Katedra Biomechatroniki
Tematy:
cobalt alloy
biomaterial
metallographic analysis
light microscopy
scanning electron microscopy
stop kobaltu
biomateriał
analiza metalograficzna
mikroskopia świetlna
skaningowa mikroskopia elektronowa
Opis:
In this paper an analysis of the microstructure of cobalt-based alloys used for implants with different chemical composition was held. Metallographic analysis was conducted using the methods of light microscopy and scanning electron microscopy. Characterization and description of the phases occurring in the investigated alloys was carried out using X-ray microanalysis, X-ray diffraction analysis and hardness measurements. The aim of this study was to determine the nature of the structure, chemical composition and its selected properties that affect their use application.
Źródło:
Aktualne Problemy Biomechaniki; 2011, 5; 177-184
1898-763X
Pojawia się w:
Aktualne Problemy Biomechaniki
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystallization of FeSiB Amorphous Ribbons Induced by Laser Interference Irradiation
Autorzy:
Kusinski, J.
Czyż, O.
Radziszewska, A.
Morgiel, J.
Ostrowski, R.
Strzelec, M.
Czyż, K.
Rycyk, A.
Powiązania:
https://bibliotekanauki.pl/articles/379811.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
laser interference heating
FeSiB alloy
amorphous alloy
scanning electron microscopy
transmission electron microscopy
stop FeSiB
stop amorficzny
skaningowa mikroskopia elektronowa
transmisyjna mikroskopia elektronowa
Opis:
Detailed studies on the effects of pulsed laser interference heating on surface characteristics and subsurface microstructure of amorphous Fe80Si11B9 alloy are reported. Laser interference heating, with relatively low pulsed laser energy (90 and 120 mJ), but with a variable number (from 50-500) of consecutive laser pulses permitted to get energy accumulation in heated areas. Such treatment allowed to form two- Dimensional micro-islands of laser-affected material periodically distributed in amorphous matrix. The crystallization process of amorphous FeSiB ribbons was studied by means of scanning and transmission electron microscopy. Detailed microstructural examination showed that the use of laser beam, resulted in development of nanostructure in the heated areas of the amorphous ribbon. The generation of nanocrystalline seed islands created by pulsed laser interference was observed. This key result may evidently give new knowledge concerning the differences in microstructure formed during the conventional and lased induced crystallization the amorphous alloys. Further experiments are needed to clarify the effect of pulsed laser interference crystallization on magnetic properties of these alloys.
Źródło:
Archives of Foundry Engineering; 2018, 18, 2; 27-30
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The structure of secretory tissue of the stigma and septal nectaries as well as nectar secretion of flowers of Hosta fortunei Baker L. H. Bailey (Funkiaceae)
Autorzy:
Chwil, M.
Powiązania:
https://bibliotekanauki.pl/articles/26646.pdf
Data publikacji:
2009
Wydawca:
Polskie Towarzystwo Botaniczne
Tematy:
tissue structure
secretory tissue
stigma
septal nectary
nectary
nectar secretion
flower
Hosta fortunei
Funkiaceae
flowering
scanning electron microscopy
Opis:
A study of Hosta fortunei Baker L. H. Bailey (Funkiaceae) flowers was conducted in the years 2007 – 2008. The flower life span and flowering duration as well as the nectar production rate were determined. The structure of the tissues of the stigma and nectary was investigated using stereoscopic, light and scanning electron microscopy (SEM). The plants flowered over a period of five weeks. Flowers of H. fortunei lived two days, on the average. Developed a pistil with an elongated ovary terminating in a discal stigma. On the surface of the stigma, unicellular glandular trichomes grew densely, composed of a stalk with a length of 113 – 213 μm and a head which was characterised by a large diameter range of 54 – 96 μm. The cuticle on the apical surface of a part of the trichomes was smooth, whereas it was striated on the stalk. Their protoplast was characterised by dense cytoplasm and weak vacuolisation. In the head of the trichomes fatty substances were accumulated. Septal nectaries occurred in the ovary of the superior pistil. Nectar was exuded onto the surface through three openings, situated in the upper part of the ovary of the pistil. At these places, epidermal cells formed a smooth or slightly wrinkled cuticle. The outer walls of the cells of the epidermis covering the duct accumulating nectar were thick. The glandular tissue of the nectary was made up of 2 layers of different-shaped, thin-walled cells and a deeply stained protoplast. They contained dense cytoplasm and a large, frequently lobate nucleus. At the final stage of secretion, fine vacuoles were observed in the cytoplasm of the glandular cells. Nectar secretion was abundant. In its initial stage, secretion droplets, increasing during the activity of the glandular tissue, were observed on the epidermis surface around the nectar openings. The weight of nectar from 10 flowers was 92.41 mg. The sugar concentration in the nectar was within a range of 23% – 30%, with an average value of 26%. Sugar yield was 23.83 mg/from 10 flowers.
W latach 2007 – 2008 przeprowadzono badania kwiatów Hosta fortunei Baker L. H. Bailey (Funkiaceae). Określono długość życia kwiatu i kwitnienia roślin oraz obfitość nektarowania. Strukturę tkanek znamienia i nektarnika badano przy użyciu mikroskopii stereoskopowej, świetlnej i skaningowej elektronowej (SEM). Rośliny kwitły przez okres pięciu tygodni. Kwiaty H. fortunei żyły średnio dwa dni. Wykształcały słupek z wydłużoną zalążnią i długą szyjką zakończoną tarczowatym znamieniem. Na powierzchni znamienia wyrastały gęsto jednokomórkowe włoski gruczołowe, zbudowane z trzonka o długości 113 – 213 μm i główki, która charakteryzowała się dużą rozpiętością średnicy (54 – 96 μm). Kutykula na powierzchni szczytowej części włosków była gładka, natomiast na trzonku prążkowana. Ich protoplast charakteryzował się gęstą cytoplazmą i słabą wakuolizacją. W główce włosków gromadziły się substancje tłuszczowe. W zalążni górnego słupka występowały nektarniki przegrodowe. Nektar wypływał na powierzchnię przez trzy ujścia, usytuowane w górnej części zalążni słupka. Komórki epidermy tworzyły w tych miejscach gładką lub lekko zmarszczoną kutykulę. Zewnętrzne ściany komórek skórki okrywającej kanał gromadzący nektar były zgrubiałe. Tkankę gruczołową nektarnika tworzyły 2 warstwy komórek o zróżnicowanym kształcie, cienkich ścianach i intensywnie barwiącym się protoplaście. Zawierały gęstą cytoplazmę i duże, często płatowate jądro. W końcowej fazie sekrecji w cytoplazmie komórek gruczołowych obserwowano drobne wakuole. Sekrecja nektaru była obfita. W jej pierwszej fazie obserwowano na powierzchni epidermy wokół ujść nektaru krople wydzieliny, powiększające się podczas aktywności tkanki gruczołowej. Masa nektaru z 10 kwiatów wynosiła 92,41 mg. Koncentracja cukrów w nektarze wahała się w przedziale 23% – 30% ze średnią wartością 26%. Wydajność cukrowa wynosiła 23,83 mg/z 10 kwiatów.
Źródło:
Acta Agrobotanica; 2009, 62, 1
0065-0951
2300-357X
Pojawia się w:
Acta Agrobotanica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Poisson’s ratio of anisotropic biological media
Wspolczynnik Poissona anizotropowych materialow biologicznych
Autorzy:
Gladyszewska, B.
Powiązania:
https://bibliotekanauki.pl/articles/792311.pdf
Data publikacji:
2012
Wydawca:
Komisja Motoryzacji i Energetyki Rolnictwa
Tematy:
Poisson's ratio
tomato skin
mechanical property
honeycomb cell
structure
cell structure
mechanical parameter
scanning electron microscopy
uniaxial test
Źródło:
Teka Komisji Motoryzacji i Energetyki Rolnictwa; 2012, 12, 2
1641-7739
Pojawia się w:
Teka Komisji Motoryzacji i Energetyki Rolnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Płyty azbestowo-cementowe - badania mikrostrukturalne włókien azbestu
Asbestos-cement panels - microstructural investigations of asbestos fibres
Autorzy:
Iwaszko, J.
Powiązania:
https://bibliotekanauki.pl/articles/103504.pdf
Data publikacji:
2016
Wydawca:
Uniwersytet Humanistyczno-Przyrodniczy im. Jana Długosza w Częstochowie. Wydawnictwo Uczelniane
Tematy:
płyta azbestowo-cementowa
azbest
analiza mikrostrukturalna
skaningowa mikroskopia elektronowa
asbestos cement panels
asbestos
microstructural analysis
scanning electron microscopy
Opis:
W pracy podjęto się analizy materiałoznawczej włókien azbestu występujących w płytach azbestowo-cementowych. Do zobrazowania mikrostruktury włókien wykorzystano mikroskopię optyczną i skaningową mikroskopię elektronową. W oparciu o badania mikrostrukturalne dokonano oceny zagrożeń dla życia i zdrowia człowieka, wynikających z eksploatacji eternitu. Badaniom mikrostrukturalnym poddano ponadto płyty azbestowo-cementowe po obróbce termicznej. Badania te miały na celu zobrazowanie ewentualnych zmian w strukturze płyty oraz występujących w nich włókien azbestu, jakie mogą wystąpić w wyniku oddziaływania wysokiej temperatury, w tym także otwartego ognia np. w trakcie pożaru. Naświetlono ponadto aktualną sytuację w zakresie eliminowania zagrożeń, wynikających z użytkowania wyrobów zawierających azbest i przedstawiono metody utylizacji tego typu wyrobów.
In this study, the material science analysis of asbestos fibres present in asbestos-cement panels was undertaken. To illustrate the microstructure of asbestos fibres, both optical and scanning electron microscopy was used. Based on the microstructural analysis, the risk to human life and health resulting from the use of eternit was assessed. In addition, structural investigations were carried out for asbestos-cement panels, subjected to thermal treatment. These investigations were aimed at illustrating the possible changes in panel microstructure and the asbestos fibres present within, which can come about as the result of the effect of a high temperature, including from a naked flame, e.g. during a fire. In addition, the current situation in the removal of risk resulting from the use of products containing asbestos fibres was made clear and methods of recycling such products were presented.
Źródło:
Prace Naukowe Akademii im. Jana Długosza w Częstochowie. Technika, Informatyka, Inżynieria Bezpieczeństwa; 2016, T. 4; 215-224
2300-5343
Pojawia się w:
Prace Naukowe Akademii im. Jana Długosza w Częstochowie. Technika, Informatyka, Inżynieria Bezpieczeństwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of WO3 on the morphology and photodegradation of dimethyl phthalate of TiO2 nanotube array photoelectrode
Autorzy:
Xin, Y.
Wang, G.
Liu, Y.
Zang, Z.
Gao, M.
Powiązania:
https://bibliotekanauki.pl/articles/206886.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
degradation
esters
morphology
scanning electron microscopy
tungsten
water treatment
degradacja
estry
morfologia
skaningowa mikroskopia elektronowa
wolfram
oczyszczalnia ścieków
Opis:
WO3 modified TiO2 nanotube array (WO3/TNAs) photoelectrodes were fabricated via electrochemical deposition on TNAs/Ti photoelectrodes. The morphology and structure of WO3/TNAs photoelectrodes were investigated by scanning electron microscopy (SEM) and X-ray diffractometer (XRD). The effects of deposition potential, deposition duration, NaWO4 concentration, and calcination temperature on the morphology and the photocatalytic activity were investigated. The results showed that suitable amounts of WO3 promoted the photocatalytic activity of TNAs photoelectrodes for the degradation of dimethyl phthalate (DMP). The optimal conditions for the fabrication of WO3/TNAs photoelectrodes were as follows: deposition voltage 3.0 V, 10 min deposition duration, 0.01 mol/dm3 Na2WO4 concentration, 1.5 cm electrode gap, and 550 °C annealing temperature. The degradation rate of DMP reached 77% after 60 min of illumination by WO3/TNAs photoelectrode. Additionally, WO3/TNA photoelectrodes possessed superb stability for maintaining a high DMP degradation efficiency at more than 75% after 10 times of successive use with 60 min irradiation for each cycle. The enhancement of photocatalytic performance by the efficient combination of WO3 with TNAs would provide a theoretical basis for the practical application of WO3/TNA photoelectrodes in water treatment.
Źródło:
Environment Protection Engineering; 2018, 44, 3; 129-139
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wpływ procesu redukcji na właściwości strukturalne i mechaniczne szkieł tlenkowych z grupy (Pb,Bi)-(Si,Ge)-O
Influence of reduction process on the structural and mechanical properties of (Pb,Bi)-(Si,Ge)-O oxide glasses
Autorzy:
Bochentyn, B.
Powiązania:
https://bibliotekanauki.pl/articles/134776.pdf
Data publikacji:
2015
Wydawca:
ADVSEO
Tematy:
szkła tlenkowe
skaningowa mikroskopia elektronowa
analiza rentgenowska
oxide glass
reduction
Scanning Electron Microscopy
Energy Dispersive X-Ray Analysis
Opis:
The effect of the reduction process in H2 at 380 °C on the microstructure and elemental composition of a glass Bi0.4Pb0.2Si0.4Ox has been investigated. It has been shown that after reduction a clearly separated top layer with a thickness of approx. 50 µm was formed on the surface of the sample. This layer is depleted of oxygen and has higher electrical conductivity than the interior of the glass. It has also been found that some granules of metallic bismuth with a diameter of tens to hundreds of nanometers were formed on the surface of the glass. Furthermore, depletion of lead was observed in these samples in relation to the initial stoichiometry of the glass prior to trial reduction.
Źródło:
Technical Issues; 2015, 2; 3-8
2392-3954
Pojawia się w:
Technical Issues
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Impact of Dry Cleaning on the Electromagnetic Shield Characteristics of Interlining Fabric
Wpływ suchego prania na efekt ekranowania fal elektromagnetycznych tkanin podszewkowych
Autorzy:
Šaravanja, B
Malarić, K
Pušić, T.
Ujević, D
Powiązania:
https://bibliotekanauki.pl/articles/232321.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
interlining fabric
dry cleaning
electromagnetic shield
scanning electron microscopy
tkaniny podszewkowe
suche pranie
pochłanianie fal elektromagnetycznych
skaningowa mikroskopia elektronowa
Opis:
The research deals with the protective properties of sewn interlining fabric (IF) intended for pockets of jackets, trousers and other garments in order to protect the user from the harmful effects of microwave radiation from mobile devices. The IF was produced from polyamide filaments coated with copper. Measurements of the electromagnetic shielding effectiveness of the face and reverse side of the IF were made at frequencies of 0.9, 1.8, 2.1 and 2.4 GHz, which were repeated after the dry cleaning process and also following ironing in 10 cycles. Surface modification of the IF tested was examined by scanning electron microscopy - SEM. The results showed a complete loss of material protective properties after ten dry-cleaning and ironing cycles. Damage to the surface copper layer that allowed the passage of electromagnetic micro waves in the fabric cycles was also confirmed by SEM micrographs.
Badania dotyczą właściwości wszywanych tkanin podszewkowych przewidzianych dla kieszeni spodni, marynarek i innych ubiorów zabezpieczających użytkownika przed szkodliwym działaniem promieniowania mikrofalowego telefonów komórkowych. Tkaniny podszewkowe wyprodukowano z włókien poliamidowych pokrytych miedzią. Zbadano pochłanianie fal elektromagnetycznych przez przygotowane próbki, przy czym różnicowano obydwie strony w stosunku do źródła promieniowania. Przy badaniach stosowano częstotliwości 0.9, 1.8, 2.1 i 2.4 GHz. Badania prowadzono przed i po 10 suchych praniach połączonych z prasowaniem. Wyniki badań wskazują na całkowitą utratę właściwości ekranujących przez materiał po 10 suchych praniach z prasowaniem. Badania tłumienia potwierdzono mikrofotografiami SEM.
Źródło:
Fibres & Textiles in Eastern Europe; 2015, 1 (109); 104-108
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Obrazowanie wybranych własności utworów solnych za pomocą różnych metod badawczych
Defining selected salt rocks properties using various research methods
Autorzy:
Cebulski, D.
Urbaniec, A.
Kasprzyk, K.
Powiązania:
https://bibliotekanauki.pl/articles/1835436.pdf
Data publikacji:
2017
Wydawca:
Instytut Nafty i Gazu - Państwowy Instytut Badawczy
Tematy:
sól kamienna
halit
komputerowa tomografia rentgenowska
skaningowy mikroskop elektronowy
salt rocks
halite
X-ray computer tomography
scanning electron microscopy
Opis:
Artykuł przedstawia wyniki przeprowadzonych analiz materiału rdzeniowego z wybranych utworów solnych, reprezentujących cechsztyńską i mioceńską formację solonośną. W celu określenia charakterystycznych parametrów i własności badanych skał solnych wykorzystano następujące metody: rentgenowską tomografię komputerową (CT), analizę w skaningowym mikroskopie elektronowym (SEM), analityczne oznaczenia składu chemicznego, fluorescencję rentgenowską (XRF) oraz dyfrakcję rentgenowską (XRD). Zastosowane metody badawcze pozwoliły określić zróżnicowanie najbardziej charakterystycznych cech analizowanych utworów.
The article presents the results of well core analysis from salt rocks, representing the Zechstein and the Miocene salt formations. The following methods were applied in order to determine the characteristic parameters and properties of the analyzed salt rock: X-ray computer tomography (CT), scanning electron microscopy (SEM), methods of the chemistry identification, X-ray fluorescence (XRF) and X-ray diffraction (XRD). The applied research methods helped to identify the diversity of the most characteristic features of the tested rocks.
Źródło:
Nafta-Gaz; 2017, 73, 4; 227-235
0867-8871
Pojawia się w:
Nafta-Gaz
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ilościowa i jakościowa analiza mieszanin pirotechnicznych – SEM/EDS
Quantitatvie and qualitative analysis of pirotechnical mixtures – SEM/EDS
Autorzy:
Łasińska, Anna
Barszcz, Krystyna
Powiązania:
https://bibliotekanauki.pl/articles/501617.pdf
Data publikacji:
2014
Wydawca:
Agencja Bezpieczeństwa Wewnętrznego
Tematy:
Mieszaniny pirotechniczne
skaningowa mikroskopia elektronowa
SEM
mikroanaliza rentgenowska
EDS
Pyrotechnic mixtures
scanning electron microscopy
energy-dispersive spectrometry
SEM/EDS
Opis:
Rozwój techniki pozwala na tworzenie nowszych i doskonalszych sposobów identyfikacji śladów przestępstw. Przez samą naturę różnych przestępstw objętych dochodzeniem kryminalistycznym mikroskop elektronowy SEM/EDS musi zapewnić najwyższą wszechstronność i wydajność. Metoda ta pozwala jednocześnie na obserwację badanego obiektu przy dużych powiększeniach oraz oznaczenie jego składu pierwiastkowego. W publikacji zaprezentowano analizę powierzchni ziaren mieszanin pirotechnicznych za pomocą skaningowego mikroskopu elektronowego SEM. Na podstawie map rozkładu stężenia pierwiastków w wybranych obszarach skanowania podjęto próbę identyfikacji konkretnych związków chemicznych, które były użyte do sporządzenia mieszanin pirotechnicznych. Było to możliwe dzięki określeniu pewnych cech wspólnych widocznych na mapach, takich jak rozkład i intensywność zabarwienia. Metoda ta w pewnych przypadkach nie zawsze jednak dawała jednoznaczne wyniki. Wyraźne zróżnicowanie ilościowego udziału danego pierwiastka w mieszaninie w istotny sposób wpływało na wynik analizy EDS.
The development of technology allows to create newer and better ways to identify traces of crime. Due to the nature of the various crimes under forensic investigation, the electron microscope SEM / EDS must provide the very highest flexibility and performance. Our method allows the observation of the object at high magnifications while simultaneously indicating its elemental composition. We describe the use of the SEM scanning electron microscope to analyze the morphological surface of grains of pyrotechnic mixtures. Based on mapping the distribution of the concentration of elements in selected areas the scan attempts to identify specific chemical compounds used in the preparation of pyrotechnic mixtures. This was made possible by defining certain common features shown on the maps, such as the distribution and intensity of color. In certain situations, however, our method did not always produce unequivocal results. Significant differences in the proportion of a given element in the mixture significantly affected the outcome of the analysis using EDS.
Źródło:
Przegląd Bezpieczeństwa Wewnętrznego; 2014, 6, 11; 177-205
2080-1335
2720-0841
Pojawia się w:
Przegląd Bezpieczeństwa Wewnętrznego
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of the Chemical Unhairing Process on Pulled Wool Characteristics
Autorzy:
Abdellaoui, Olfa
Harizi, Taoufik
Msahli, Slah
Powiązania:
https://bibliotekanauki.pl/articles/2171990.pdf
Data publikacji:
2022
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
ATR-FTIR
red face Barbary sheep
sheep breed
chemical unhairing process
pulled wool
SEM
scanning electron microscopy
X-ray
Opis:
Textile research is being driven to find sustainable materials as an alternative to raw fibers. In fact, reusing fibrous waste, as a byproduct, is one of the most important environmental challenges that confront the world. This research focused on studying pulled wool fibers as a natural fiber to reduce environmental loading. There are large amounts of residual pulled wool fibers that can be recycled and valorised. Therefore, raw and pulled wool fibers were characterized and compared. Scanning Electron Micrographs (SEM) results show that on the pulled wool fiber, the surface became rougher and the scales appear affected and less dense. Based on the X-ray diffraction (XRD) results, the crystallinity of the pulled fiber decreased lightly. Attenuated Total Reflectance-Fourier Transform Infra Red (ATR-FTIR) spectroscopy analyzes presented some changes in chemical composition. A High-Performance Liquid Chromatography (HPLC) test showed an increase in the amount of cystic acids. The pulled wool fiber indicates that it might have damaged some crosslinks of macromolecular chains in the fiber. Thus, physical, chemical and mechanical properties are affected during the chemical unhairing process. This research purpose was to increase the potential for better value of pulled wool as it presents the natural fiber most used in several applications.
Źródło:
Fibres & Textiles in Eastern Europe; 2022, 3 (151); 70--78
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Engine-generated solid particles - a case study
Autorzy:
Szramowiat, K.
Woodburn, J.
Pacura, W.
Berent, K.
Bielaczyc, P.
Gołaś, J.
Powiązania:
https://bibliotekanauki.pl/articles/134094.pdf
Data publikacji:
2018
Wydawca:
Polskie Towarzystwo Naukowe Silników Spalinowych
Tematy:
engine emissions
particulate matter
nanoparticles
scanning electron microscopy
SEM
morphology
emisja spalin
cząstki stałe
nanocząstki
elektronowy mikroskop skaningowy
morfologia
Opis:
Current ecological trends and resulting legislation like European emissions standards Euro 6d or Best Available Techniques are setting new challenges in the field of environmental protection. Since the problem of emissions of particulate matter from diesel engines was solved by the application of diesel particulate filters (DPFs or FAPs) and due to the global dominance of gasoline fuelled passenger cars, particular concern has been focused on improvement of emissions performance of gasoline vehicles, including hybrids, as well as heavy-duty and non-road vehicles. This paper presents the results of preliminary studies on the chemical and physical properties of gasoline engine-generated particles, including nanoparticles. SEM images were presented which allowed identification of the character of particulate matter and estimates of the dimensions of particles. Moreover, the particles were found to be composed of different elements, including Cu, Si, Na, Ca, Zn and P, pointing to the origination of these particles from the pistons and lubricant additives.
Źródło:
Combustion Engines; 2018, 57, 3; 33-39
2300-9896
2658-1442
Pojawia się w:
Combustion Engines
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Atomic force microscopy investigation of electron beam (EB) irradiated composites based on biodegradable polymers and coconut fiber*
Autorzy:
Kodama, Y.
Oishi, A.
Nagasawa, N.
Nakayama, K.
Tamada, M.
Machado, L. D. B.
Powiązania:
https://bibliotekanauki.pl/articles/147470.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
atomic force microscopy (AFM)
coconut fiber
electron beam (EB) radiation
force modulation microscopy (FMM)
poly(ε-caprolactone) (PCL)
poly(L-lactic acid) (PLLA)
scanning electron microscopy (SEM)
Opis:
In this study, the addition of natural fibers to biodegradable PCL, PLLA blend and the effect of ionizing radiation on the surface of composites were investigated by force modulation microscopy (FMM), atomic force microscopy (AFM) and scanning electron microscopy (SEM). Hot pressed sheets were prepared using pellets of twin extruded PCL:PLLA 20:80 (w:w) blend containing 5% or 10% weight concentration of coconut fiber. In this study coconut fibers non treated chemically and acetylated ones were used. Irradiation was performed using an electron beam (EB) accelerator and an absorbed dose of 100 kGy. FMM images acquisition was obtained using a silicon cantilever, intermittent contact mode (tapping mode). Also, AFM images were obtained using tapping mode but J scanner. By FMM, it was possible to observe regions with different elasticity indicating fiber presence under the surface of the composite. Furthermore, it appears that the spherical structures size decreased on composites. This probably was induced by ionizing radiation.
Źródło:
Nukleonika; 2013, 58, 4; 459-468
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Composition of seed soluble carbohydrates and ultrastructural diversity of testa in lupins from the Mediterranean Region
Autorzy:
Piotrowicz-Cieslak, A I
Powiązania:
https://bibliotekanauki.pl/articles/56576.pdf
Data publikacji:
2005
Wydawca:
Polskie Towarzystwo Botaniczne
Tematy:
Mediterranean Region
gas chromatography
Fabaceae
Lupinus
scanning electron microscopy
seed coat
lupin
cyclitol
carbohydrate
galactosyl cyclitol
raffinose family oligosaccharide
seed
Opis:
This article present a comparison of soluble sugar levels in seeds of Lupinus atlanticus, Lupinus cosentinii, Lupinus palaestinus and Lupinus pilosus, Lupinus hispanicus subsp. hispanicus and Lupinus luteus of Juno variety. Considering that sugars are accumulated in embryos, only the embryonic tissues were used for biochemical analyses. Additionally, the share of testa and embryo in seed tissues was evaluated. The seed-coat thickness was measured using scanning electron microscopy. The seed coat had the largest share in seeds of Lupinus pilosus and Lupinus palaestinus, and the least share in seeds of Lupinus hispanicus subsp. hispanicus and Lupinus luteus of Juno variety. In the seed of Lupinus pilosus the thickness of the seed coat was 1100 µm, while in Lupinus luteus it was 300 µm. The analysed Lupinus seeds accumulated from 73 mg/g d.m. (dry matter of seed embryo) to 155 mg of soluble sugars/g d.m. The highest quantity of oligosaccharides of the raffinose series was found in seeds of Lupinus luteus, while the lowest amount in seed of Lupinus palaestinus. Galactosyl cyclitols appeared in largest amount in seeds of Lupinus palaestinus and Lupinus pilosus, appropriately 41.93 and 33.75 mg/g dm. The lowest amount of galactosyl cyclitols appeared in Lupinus atlanticus, Lupinus cosentinii and Lupinus hispanicus.
Źródło:
Acta Societatis Botanicorum Poloniae; 2005, 74, 4
0001-6977
2083-9480
Pojawia się w:
Acta Societatis Botanicorum Poloniae
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Rumex thyrsiflorus Fingerh. – sex ratios among seedlings and explants cultured in vitro
Autorzy:
Dziedzic, K.
Cygan, M.
Mizia, P.
Kwolek, D.
Slesak, H.
Powiązania:
https://bibliotekanauki.pl/articles/81088.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
conference
Rumex thyrsiflorus
Rumex acetosa
sex ratio
sex chromosome
seedling
explant
in vitro culture
chromosome
scanning electron microscopy
DNA marker
Źródło:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology; 2015, 96, 1
0860-7796
Pojawia się w:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation, characterization and optimization of cross-linked fructosyltransferase aggregates for the production of prebiotic fructooligosaccharides
Autorzy:
Ademakinwa, A.N.
Ayinla, Z.A.
Omitogun, O.G.
Agboola, F.K.
Powiązania:
https://bibliotekanauki.pl/articles/81247.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
fructosyltransferase
Aureobasidium pullulans
fructooligosaccharide
prebiotic
statistical optimization
scanning electron microscopy
X-ray spectroscopy
Fourier transform infrared spectroscopy
biotransformation
chemometric analysis
Źródło:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology; 2018, 99, 4
0860-7796
Pojawia się w:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Two-body wear simulation influence on some direct and indirect dental resin biocomposites : A qualitative analysis
Autorzy:
Caracostea, A.
Morar, N.
Florea, A.
Soanca, A.
Badea, M. E.
Powiązania:
https://bibliotekanauki.pl/articles/307539.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
mikroskop elektronowy skaningowy
skaningowy mikroskop elektronowy
mikroskop optyczny
system CAD
biokompozyt
scanning electron microscopy
optical microscopy
two-body wear
CAD system
advanced biocomposites
Opis:
Purpose: The aim of this study was to qualitatively assess the outcomes of two in vitro aging methods, thermal-cycling and twobody wear simulation accomplished with a dual-axis chewing device, on the surface characteristics of eight direct and indirect dental resin biocomposites. Methods: Eighty mesial-occlusal-distal dental cavities were restored with four direct nanohybrid composite materials and with four nano- and micro-hybrid lab-fabricated resin composite inlays. After the restored teeth were subjected to thermal-cycling and wear simulation based on mechanical loading, the surface texture features of the restorations were separately analysed for each of the methods, on epoxy resin models using a digital camera, computer-aided-design system, optical stereo-microscopy and scanning electron microscopy. Results: All the dental restorative resin based composites used in this investigation displayed different cyclic wear patterns after undergoing mechanical loading. After thermal-cycling, the group of resin composite inlays showed a better adaptation, a smoother and more polished occlusal surface compared with direct restorative materials. Only two of direct nanohybrid resin composites performed better after two aging methods. One nanohybrid and the other two microhybrid resin inlays did not perform as expected when they were subjected to simulated wear compared to the rest of test materials. Conclusions: The use of the two-body wear simulation method revealed important information about the behavior of the dental resin-based composites when multiple oral factors are involved in a lab-simulated condition. Furthermore, the macro- and micro-morphological analysis showed different abrasion patterns among the materials being tested according to the filler percentage and distribution of the particles within the resin matrix.
Źródło:
Acta of Bioengineering and Biomechanics; 2016, 18, 3; 61-72
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oznaczanie grzybów pleśniowych na powierzchni materiału i ocena oddziaływania grzybów na materiał budowlany
Marking of moulds on material surface and impact assessment of fungals on building material
Autorzy:
Horbik, Daria
Powiązania:
https://bibliotekanauki.pl/articles/161083.pdf
Data publikacji:
2019
Wydawca:
Polski Związek Inżynierów i Techników Budownictwa
Tematy:
grzyb pleśniowy
materiał budowlany
oddziaływanie
metody oznaczania
mikroskop skaningowy
badanie
mould
construction material
influence
determination methods
scanning electron microscopy
research
Opis:
W pierwszej części artykułu przedstawiono występowanie, budowę i wpływ grzybów na człowieka. W drugiej części przedstawiono metody oznaczania grzybów pleśniowych na powierzchni materiału, a w szczególności na elewacjach budynków mieszkalnych (oznaczanie zawartości ergosterolu, obrazy mikroskopowe SEM, natężenie emitowanej przez grzyby bioluminescencji, bezwzorcową mikroanalizę EDS).
In the first part of the paper occurrence, structure and effect of fungi on human are presented. In the second part of the paper methods of marking moulds on the surface of material and in particular on the elevation of residential buildings are presented (ergosterol contents, microscope images SEM, intensity of the bioluminescence emitted by moulds, EDS microanalysis).
Źródło:
Przegląd Budowlany; 2019, 90, 6; 20-25
0033-2038
Pojawia się w:
Przegląd Budowlany
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The influence condition of electro-spark alloying by Al and sequent laser treatment on surface layer of steel GradeB A284
Autorzy:
Smolina, I.
Franchik, N.
Lobachova, G.
Powiązania:
https://bibliotekanauki.pl/articles/115562.pdf
Data publikacji:
2011
Wydawca:
Fundacja na Rzecz Młodych Naukowców
Tematy:
electro-spark alloying (ESA)
laser treatment (LT)
steel GradeB A284
surface layer
hardened surface
microhardness
scanning electron microscopy (SEM)
Opis:
In the present paper structure and properties of alloying by aluminum surface layer of steel GradeB A284, which were obtain by electro-spark alloying (ESA) and sequent laser treatment (LT) are described. The properties of coatings were investigated by SEM and X-ray diff raction, microstructure and microhardness analysis. It has been shown that next laser treatment can increase the depth of hardened layer doped with 50 to 80…100 μm, but in comparison with ESA, reduces the value of microhardness from 10 to 5 GPa.
Źródło:
Challenges of Modern Technology; 2011, 2, 3; 25-28
2082-2863
2353-4419
Pojawia się w:
Challenges of Modern Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Metody mikroskopowe w ocenie procesów wykończania wyrobów włókienniczych
Evaluation of finishing processes for textile products using the microscopic methods
Autorzy:
Machnowski, Waldemar
Wrzosek, Henryk
Powiązania:
https://bibliotekanauki.pl/articles/1818683.pdf
Data publikacji:
2020
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Skórzanego
Tematy:
mikroskopia optyczna
SEM
skaningowa mikroskopia elektronowa
bawełna
jakość tekstyliów
procesy wykończenia tekstyliów
optical microscopy
scanning electron microscopy
cotton
textiles quality
textile finishing processes
Opis:
Badanie wyrobów włókienniczych odgrywa istotną rolę w systemie zapewnienia jakości tekstyliów, a także w pracach nad rozwojem nowych technologii i produktów włókienniczych. Istnieje wiele metod oceny struktury i właściwości włókien i wyrobów włókienniczych. Bardzo ważne miejsce wśród tych metod zajmują techniki mikroskopowe, w szczególności mikroskopia optyczna i skaningowa mikroskopia elektronowa (SEM). W artykule podano krótki przegląd możliwych zastosowań metod mikroskopowych do analizy efektów niektórych operacji wytwarzania tekstyliów. Wykorzystanie mikroskopu optycznego umożliwiło identyfikację przyczyn powodujących nierównomierność barwy wyrobów bawełnianych. Z przeglądu literatury oraz doświadczeń własnych autorów wynika, że metody mikroskopowe stanowią cenne narzędzie w badaniu włókien i wyrobów włókienniczych.
Fabric testing plays an important role in the quality assurance system and in the development of new textile technologies and products. There are many test methods used to evaluate the structure and properties of fibers and textile materials. Among these methods, microscopic techniques – especially optical microscopy and scanning electron microscopy (SEM) – are one of the most important methods. This paper provides a brief overview of the possible uses the microscopic methods for determining the results of some textile manufacturing processes. A review of the literature and the authors experiences in this field indicate that microscopic methods are a valuable tool for the testing and assessing the performance of fibers and textile products.
Źródło:
Technologia i Jakość Wyrobów; 2020, 65; 4--20
2299-7989
Pojawia się w:
Technologia i Jakość Wyrobów
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The origin and chronology of medieval silver coins based on the analysis of chemical composition
Autorzy:
Pańczyk, E.
Sartowska, B.
Waliś, L.
Dudek, J.
Weker, W.
Widawski, M.
Powiązania:
https://bibliotekanauki.pl/articles/147506.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
elemental composition
medieval Central Europe coins
scanning electron microscopy (SEM)
laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)
numismatists
Opis:
Medieval Central Europe coins – the Saxon coins, also called as the Otto and Adelheid denarii, as well as the Polish ones, the Władysław Herman and Bolesław Śmiały coins – were examined to determine their provenance and dating. Their attribution and chronology often constitute a serious problem for historians and numismatists. For hundreds of years, coins were in uncontrolled conditions and in variable environment. Destructed and inhomogeneous surface were the effect of corrosion processes. Electron microscopy with energy dispersive X-ray analysis (scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDS)), X-ray fluorescence (XRF) analysis (energy dispersive X-ray fluorescence (EDXRF) and total reflection X-ray fluorescence (TXRF)), and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) were applied. The results of these investigations are significant for our knowledge of the history of Central European coinage, especially of Polish coinage.
Źródło:
Nukleonika; 2015, 60, No. 3, part 2; 657-663
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Identification of the cause of the stem neck fracture in the hip joint endoprosthesis
Autorzy:
Ryniewicz, A. M.
Bojko, Ł.
Ryniewicz, A.
Pałka, P.
Ryniewicz, W.
Powiązania:
https://bibliotekanauki.pl/articles/265412.pdf
Data publikacji:
2018
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
proteza plastyczna
złamanie zmęczeniowe
metoda elementów skończonych
skaningowa mikroskopia elektronowa
prosthetic arthroplasty
stem construction
fatigue fracture
FEM
SEM (scanning electron microscopy)
Opis:
Endoprosthesis stem fractures are among the rarest complications that occur after hip joint arthroplasty. The aim of this paper is to evaluate the causes of the fractures of the Aura II stem neck, which is an element of an endoprosthesis implanted in a patient. In order to achieve it, a radiogram was evaluated, the FEM analysis was carried out for the hip joint replaced using the Aura II prosthesis and scanning tests as well as a chemical analysis were performed for the focus of fatigue. The tests performed indicate that the most probable causes leading to the fatigue fracture of the Aura II stem under examination were material defects in the process of casting and forging (forging the material with delamination and the presence of brittle oxides and carbides) that resulted in a significant reduction of strength and resistance to corrosion. In the light of an unprecedented stem neck fracture, this information should be an indication for non-destructive tests of ready-made stems aiming to discover the material and technological defects that may arise in the process of casting and drop forging.
Źródło:
International Journal of Applied Mechanics and Engineering; 2018, 23, 1; 223-234
1734-4492
2353-9003
Pojawia się w:
International Journal of Applied Mechanics and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterisation of Mg-Zn-Ca-Y powders manufactured by mechanical milling
Autorzy:
Lesz, S.
Tański, T.
Hrapkowicz, B.
Karolus, M.
Popis, J.
Wiechniak, K.
Powiązania:
https://bibliotekanauki.pl/articles/1818808.pdf
Data publikacji:
2020
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
Mg-based alloys
scanning electron microscopy
X-ray diffraction analysis
mechanical alloying
stopy magnezu
skaningowa mikroskopia elektronowa
rentgenowska analiza dyfrakcyjna
mechaniczna synteza
Opis:
Purpose: This paper explains mechanical synthesis which uses powders or material chunks in order to obtain phases and alloys. It is based on an example of magnesium powders with various additives, such as zinc, calcium and yttrium. Design/methodology/approach: The following experimental techniques were used: X-ray diffraction (XRD) method, scanning electron microscopy (SEM), determining particle size distributions with laser measuring, Vickers microhardness. Findings: The particle-size of a powder and microhardness value depend on the milling time. Research limitations/implications: Magnesium gained its largest application area by creating alloys in combination with other elements. Magnesium alloys used in various industry contain various elements e.g. rare-earth elements (REE). Magnesium alloys are generally made by casting processes. Consequently, the search for new methods of obtaining materials such as mechanical alloying (MA) offers new opportunities. The MA allows for the production of materials with completely new physico-chemical properties. Originality/value: Thanks to powder engineering it is possible to manufacture materials with specific chemical composition. These materials are characterized by very high purity, specified porosity, fine-grain structure, complicated designs. These are impossible to obtain with traditional methods. Moreover it is possible to refine the process even further minimalizing the need for finishing or machining, making the material losses very small or negligible. Furthermore material manufactured in such a way can be thermally or chemically processed without any problems.
Źródło:
Journal of Achievements in Materials and Manufacturing Engineering; 2020, 103, 2; 49--59
1734-8412
Pojawia się w:
Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Understanding technical cleanliness: importance, assessment, maintenance
Autorzy:
Faber, Joanna
Brodzik, Krzysztof
Nycz, Marta
Powiązania:
https://bibliotekanauki.pl/articles/2097549.pdf
Data publikacji:
2021
Wydawca:
Polskie Towarzystwo Naukowe Silników Spalinowych
Tematy:
technical cleanliness
component cleanliness code
contaminations
particles
optical microscopy
SEM
scanning electron microscopy
czystość techniczna
kod czystości komponentu
zanieczyszczenia
cząstki
mikroskopia optyczna
skaningowa mikroskopia elektronowa
Opis:
Development of the automotive industry, including so-called dowsizing and rightsizing, entails the need to ensure, and hence to verify, the stringent cleanliness levels of an increasing number of car components. The assurance of proper cleanliness level requires knowledge of the entire production process and precise information on the contaminants that will allow to identify their sources. Obtaining reliable cleanliness information requires establishing of many different factors, i. a. selection of proper contamination extraction and collection technique, proper parameters of extraction, validation of extraction procedure, methods of particles analysis. Analytical techniques which are implemented include gravimetric, optical microscopy and advanced techniques like scanning electron microscopy. This work present’s actual state of knowledge regarding technical cleanliness analysis of components. Important aspects of QA&QC in technical cleanliness assessment are also discussed.
Źródło:
Combustion Engines; 2021, 60, 3; 41--50
2300-9896
2658-1442
Pojawia się w:
Combustion Engines
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
X-ray techniques in the investigation of a Gothic sculpture : the risen Christ
Autorzy:
Mikołajska, A.
Walczak, M.
Kaszowska, Z.
Urbańczyk-Zawadzka, M.
Powiązania:
https://bibliotekanauki.pl/articles/146866.pdf
Data publikacji:
2012
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
cultural heritage
X-ray image
X-ray dual source computed tomography (DSCT)
scanning electron microscopy energy dispersed X-ray spectroscopy (SEM-EDX)
Opis:
For over a century, X-ray radiation has played an important role in the area of the conservation and restoration of cultural heritage objects. X-ray techniques are amongst the most fundamental and helpful methods used in the investigation of art works. This paper reviews the application of traditional radiography, X-ray dual source computed tomography (DSCT) and scanning electron microscopy combined with energy dispersed X-ray spectroscopy (SEM-EDX) to the investigation of a wooden, Gothic sculpture, The risen Christ. Thanks to the properties of X-ray radiation (different absorption by various materials) first two methods allow the assessment of the preservation state and the observation of the internal structure of an object in 3-D. While SEM-EDX analysis permits the elemental analysis of the polychrome layers. As a result 2-D and 3-D images, permitting the full volume inspection of an object, were taken in a totally non-destructive way. The morphological and physical information about the inner structure of the investigated wooden sculpture was obtained, revealing changes related to previous restorations, as well as ageing effects. Employing the SEM-EDX, painting materials (pigments and filers), were identified. Gained data is essential for restorers to understand the whole structure of the studied object and to decide which further investigation and restoration steps have to be undertaken.
Źródło:
Nukleonika; 2012, 57, 4; 627-631
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Precursory siphuncular membranes in the body chamber of Phyllopachyceras and comparisons with other ammonoids
Autorzy:
Tanabe, K
Kulicki, C.
Landman, N.H.
Powiązania:
https://bibliotekanauki.pl/articles/22378.pdf
Data publikacji:
2005
Wydawca:
Polska Akademia Nauk. Instytut Paleobiologii PAN
Tematy:
Ammonoidea
Late Cretaceous
organic membrane
scanning electron microscopy
morphogenesis
Hokkaido
body chamber
Japan
chamber formation
Phyllopachyceras ezoense
septal epithelium
paleontology
Phyllopachyceras
ammonoid
Opis:
Organic membranes preserved in the rear part of the body chamber of the Late Cretaceous phylloceratid ammonite Phyllopachyceras ezoense were examined with scanning electron microscopy (SEM) on the basis of well−preserved specimens from Hokkaido, Japan. SEM observations revealed that the membranes are continuous with the siphuncular tube wall in the phragmocone and consist of two layers, both of which are made of a dark, primarily conchiolin material; namely, a thinner inner homogeneous layer and a thicker outer layer with gently inclined pillar−like units. Hence, they are interpreted as the precursory siphuncular membranes. The precursory siphuncular membranes are not associated with any other organic components such as the siphuncular sheets reported in some Paleozoic and Mesozoic ammonoids. Unlike the tube−like condition in the phragmocone, the precursory siphuncular membranes in the body chamber of the specimens examined do not form a tube shape; on the ventral side the membranes are truncated and directly contact the outer shell wall. These observations suggest that the inner and outer layers of the precursory siphuncular membranes in the body chamber were respectively formed by the siphuncular epithelium from the inner side and by the invaginated septal epithelium from the outer side. It is also postulated that at the initial stage of septal formation, the rear part of the body moved slowly forward, developing a circumsiphonal invagination of the septal epithelium. Because similar conchiolin membranes are occasionally preserved in the body chambers of other phylloceratids, the above morphogenetic process applies to all members of the Phylloceratina. The tube−shaped structure in the rear part of the body chamber of desmoceratid Damesites consists only of nacreous layer. We interpret it as a pathologically overgrown prochoanitic septal neck.
Źródło:
Acta Palaeontologica Polonica; 2005, 50, 1
0567-7920
Pojawia się w:
Acta Palaeontologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Environmentally hazard and toxic exoskeletons of marine crustaceans wastes in synthesizing N-deacetylated chitin
Zastosowanie niebezpiecznych i toksycznych dla środowiska egzoszkieletów skorupiaków morskich w syntezie N-deacetylowanej chityny
Autorzy:
El-Mekawy, Rasha E.
Powiązania:
https://bibliotekanauki.pl/articles/2202580.pdf
Data publikacji:
2022
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
chitosan
shrimp shells
scanning electron microscopy
thermal gravimetric analysis
X-ray
diffraction
chitozan
skorupki krewetek
skaningowa mikroskopia elektronowa
analiza termograwimetryczna
dyfrakcja rentgenowska
Opis:
High molecular weight chitosan was synthesized from shrimp shells. Chemical structure of chitosan was confirmed using FT-IR, XRD, TGA, and SEM analyses. Physicochemical properties of chitosan such as molecular weight (800 000 g/mol), deacetylation degree (80%), ash content (1%) indicating effectiveness of demineralization step in removing minerals, water binding capacity (4220%), and fat binding capacity (537%), were determined. FT-IR spectra exhibited characteristic joint band at 3365 cm-1 due to –OH and –NH2 regarding to the conversion of chitin acetyl group to NH2 of chitosan.
Z muszli krewetek zsyntetyzowano chitozan o wysokiej masie cząsteczkowej. Strukturę chemiczną chitozanu potwierdzono metodami FT-IR, XRD, TGA i SEM. Określono właściwości fizykochemiczne chitozanu takie jak masa cząsteczkowa (800 000 g/mol), stopień deacetylacji (80%), wskazu jącą na skuteczność procesu demineralizacji zawartość popiołów (1%), zdolność wiązania wody (4220%) i zdolność wiązania tłuszczu (537%). Widma FT-IR wykazały charakterystyczne pasmo przy liczbie falowej 3365 cm-1, pochodzące od grup –OH i–NH2, wynikające z przekształcenia grupy acetylowej chityny w NH2 chitozanu.
Źródło:
Polimery; 2022, 67, 10; 503--508
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphological and anatomical structure of generative organs of Salsola kali ssp. ruthenica [Iljin] Soo at the SEM level
Autorzy:
Idzikowska, K
Powiązania:
https://bibliotekanauki.pl/articles/58452.pdf
Data publikacji:
2005
Wydawca:
Polskie Towarzystwo Botaniczne
Tematy:
flower
pistil
structure
scanning electron microscopy
generative organ
morphology
flower part
fruit
seed
stamen
anatomy
semi-section
light microscopy
Salsola kali ssp.ruthenica
sepal
Chenopodiaceae
embryo
Opis:
The morphology and anatomy of generative organs of Salsola kali ssp. ruthenica was examined in detail using the light (LM) and scanning electron microscopy (SEM). The whole flowers, fruits and their parts (pistil, stamens, sepals, embryo, seed) were observed in different developmental stages. In the first stage (June), flower buds were closed. In the second stage (August), flowers were ready for pollination/fertilization. In the third stage (September), fruits were mature. Additionally, the anatomical and morphological structure of sepals was observed by means of LM and SEM. Thanks to the transverse and longitudinal semi-sections through sepals, the first phase of wing formation was recorded by SEM. The appearance of stomata in the epidermal cells of sepals above the forming wings was very interesting, too. The stomata were observed also in mature fruits.
Źródło:
Acta Societatis Botanicorum Poloniae; 2005, 74, 2
0001-6977
2083-9480
Pojawia się w:
Acta Societatis Botanicorum Poloniae
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-healing cement materials – microscopic techniques
Samoleczące tworzywa cementowe – techniki mikroskopowe
Autorzy:
Dudek, Marta
Powiązania:
https://bibliotekanauki.pl/articles/390873.pdf
Data publikacji:
2020
Wydawca:
Politechnika Lubelska. Wydawnictwo Politechniki Lubelskiej
Tematy:
optical microscopy
scanning electron microscopy
tensile stage
self-healing cementitious materials
micro-mechanical properties
mikroskop optyczny
elektronowy mikroskop skaningowy
stolik naprężeniowy
samoleczące tworzywa cementowe
właściwości mikromechaniczne
Opis:
The article presents a general classification of intelligent materials with self-healing (self-repairing) properties, focusing on self-healing cementitious materials. The purpose of the paper is to describe the prospects of two of the most popular micro-observation techniques, i.e. with the use of an optical and scanning electron microscope. In addition, it describes the advantages of using a tensile stage mounted in the microscope chamber for testing self-healing materials. The advantages and disadvantages of these devices have been characterized, and the results of preliminary research have been provided. The tests include the optical microscopy and scanning electron microscopy observations of the microstructure of cracks before and after the process of healing. They were carried out using ZEISS Discovery V20 optical microscope and ZEISS EVO-MA 10 scanning electron microscope on mortar samples modified with macro capsules filled with polymer. In addition to observations, chemical analysis was performed with the use of an EDS detector. The microscopic observations and chemical analyses provide the basis for assessing the effectiveness of the self-healing process, showing that the crack has been healed. Moreover, the preliminary results of the tests of micro-mechanical properties, carried out with the use of a tensile stage, have been described. The problems of using this research technique are also listed. This study shows the usefulness of this kind of tests for microcapsules for self-healing materials.
Artykuł przedstawia ogólną klasyfikację materiałów inteligentnych o właściwościach samoleczących (samonaprawiających), ze szczególnym uwzględnieniem samoleczących tworzyw cementowych. Celem niniejszej publikacji jest przedstawienie dwóch najpopularniejszych technik mikroobserwacji, tj. mikroskopii optycznej i skaningowej. Ponadto opisano, jakie możliwości w badaniach samoleczących materiałów daje stolik naprężeniowy, zamontowany w komorze mikroskopu. Scharakteryzowano zalety i wady tych urządzeń oraz przedstawiono wyniki wstępnych badań. Badania obejmują obserwacje mikrostruktury pęknięć przed i po procesie gojenia, zarówno w mikroskopie optycznym jak i skaningowym. Przeprowadzono je przy użyciu mikroskopu optycznego ZEISS Discovery V20 i skaningowego mikroskopu elektronowego ZEISS EVO-MA 10, na próbkach zaprawy modyfikowanej makrokapsułkami wypełnionymi polimerem. Oprócz obserwacji wykonano analizę chemiczną z wykorzystaniem detektora EDS. Obserwacje mikroskopowe i analiza chemiczna dają podstawę do oceny skuteczności procesu samoleczenia, wykazując, że pęknięcie zostało zagojone. Opisano również wstępne wyniki badań właściwości mikromechanicznych, przeprowadzonych z wykorzystaniem stolika naprężeniowego. Wymieniono także trudności związane z wykorzystaniem tej techniki badawczej. Artykuł przedstawia przydatność tego rodzaju testów dla mikrokapsułek używanych do modyfikacji materiałów samoleczących.
Źródło:
Budownictwo i Architektura; 2020, 19, 2; 33-40
1899-0665
Pojawia się w:
Budownictwo i Architektura
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Charakterystyka fotoutwardzalnych żywic akrylowych do zastosowań w przemyśle drzewnym
Characteristics of photocurable acrylic resins for use in wood industry
Autorzy:
Jurczyk-Kowalska, Magdalena
Płocińska, Magdalena
Choińska, Emilia
Zagórski, Andrzej
Powiązania:
https://bibliotekanauki.pl/articles/947137.pdf
Data publikacji:
2019
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
polimery akrylowe
właściwości termiczne
skaningowa mikroskopia elektronowa SEM
lepkość
utwardzanie promieniowaniem UV
acrylic polymers
thermal properties
scanning electron microscopy SEM
viscosity
UV-curing
Opis:
Fotoutwardzalne polimery na bazie żywic akrylowych stanowią szeroką grupę materiałów o złożonej budowie chemicznej. Z zastosowaniem spektroskopii w podczerwieni (IR) scharakteryzowano żywice pochodzące od trzech czołowych producentów materiałów polimerowych stosowanych w przemyśle drzewnym: AkzoNobel, Klumpp oraz Kneho-Lacke. W otrzymanych widmach stwierdzono obecność pasm charakterystycznych zarówno dla struktury akrylanów, jak i epoksydów. Analiza mikrostruktury pozwoliła na stwierdzenie obecności w strukturze badanych żywic znacznej ilości napełniaczy. Wykazano, że żywica firmy AkzoNobel, charakteryzująca się najmniejszą lepkością, stabilnością termiczną oraz najsłabszymi właściwościami adhezyjnymi i twardością, zawiera najwięcej cząstek napełniaczy. Natomiast żywica firmy Klumpp wykazywała najmniejszą podatność na zmienne warunki sieciowania, co przejawiało się jej najlepszymi właściwościami adhezyjnymi. Stwierdzono też, że na właściwości termiczne i mechaniczne żywic w większym stopniu wpływa budowa chemiczna niż ilość zastosowanych napełniaczy.
The UV light cured polymeric materials, based on acrylic monomers, constitute a wide group of products with a complex chemical structure. The resins obtained from three leading manufacturers of polymeric materials used in wood industry: AkzoNobel, Klumpp and Kneho-Lacke were investigated. The chemical structure of the resins was characterized by infrared spectroscopy (IR). The obtained spectra revealed the presence of absorption bands which are characteristic for the structure of acrylates as well as epoxides. The analysis of microstructure indicated the presence of significant amounts of fillers in the structure of tested resins. Our study showed that the AkzoNobel resin, characterized by the lowest viscosity, thermal stability, adhesion properties and hardness, contained the most amount of filler particles. The Klumpp resin was least susceptible to changes in the crosslinking conditions and showed the best adhesive properties. It was found, that the chemical structure influences the thermal and mechanical properties of the resins to a larger extent than the filler content.
Źródło:
Polimery; 2019, 64, 5; 340-347
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and characterization of composite materials based on porous ceramic preform infiltrated by elastomer
Autorzy:
Chabera, P.
Boczkowska, A.
Witek, A.
Oziębło, A.
Powiązania:
https://bibliotekanauki.pl/articles/202111.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ceramic matrix composites
ceramic
mechanical properties
damage mechanics
scanning electron microscopy
kompozyty z matrycą ceramiczną
ceramika
właściwości mechaniczne
mechanika szkód
skaningowa mikroskopia elektronowa
Opis:
The paper presents the experimental results of fabrication and characterization of ceramic- elastomer composites. They were obtained using pressure infiltration of porous ceramics by elastomer As a result the composites in which two phases are interpenetrating three-dimensionally and topologically throughout the microstructure were obtained. In order to enhance mechanical properties of preforms a high isostatic pressure method was utilized. The obtained ceramic preforms with porosity gradient within the range of 20-40% as well as composites were characterized by X-ray tomography. The effect of volume fraction of pores on residual porosity of composites was examined. These results are in accordance with SEM images which show the microstructure of composites without any delaminations and voids. Such composites exhibit a high initial strength with the ability to sustain large deformations due to combining the ceramic stiffness and rubbery elasticity of elastomer. Static compression tests for the obtained composites were carried out and the energy dissipated during compression was calculated as the area under the stress-strain curve. The dynamic behavior of the composite was investigated using the split Hopkinson pressure bar technique. It was found that ceramic-elastomer composites effectively dissipate the energy. Moreover, a ballistic test was carried out using armor piercing bullets.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2015, 63, 1; 193-199
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł

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