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Wyświetlanie 1-25 z 68
Tytuł:
Effect of Annealing, Stoichiometry, and Surface on Magnetism of (Pr,Dy)FeCoB Microparticles Ensemble
Autorzy:
Kablov, E. N.
Ospennikova, O. G.
Kunitsyna, E. I.
Piskorskii, V. P.
Korolev, D. V.
Morgunov, R. B.
Powiązania:
https://bibliotekanauki.pl/articles/356579.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
rare earth metals
magnets
magnetisation
Mössbauer spectroscopy
X-ray spectroscopy
Opis:
Magnetic properties of powder (Pr,Dy)FeCoB ferrimagnetic alloys and effects of annealing, surface states were analyzed. X-ray photoelectron spectroscopy and Mössbauer spectra of powders indicate the effect of surface states on phase composition and magnetic properties of the studied powder, if particles average size is smaller than 10 μm. Effect of stoichiometry on magnetic anisotropy was found. Thermal stability of anisotropy field was proved by replacement of Fe atoms with Co atoms.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 3; 1923-1930
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Advanced microstructure diagnostics and interface analysis of modern materials by high-resolution analytical transmission electron microscopy
Autorzy:
Neumann, W.
Kirmse, H.
Hausler, I.
Mogilatenko, A.
Zheng, C.
Hetaba, W.
Powiązania:
https://bibliotekanauki.pl/articles/199872.pdf
Data publikacji:
2010
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electron microscopy
energy dispersive X-ray spectroscopy
electron energy loss spectroscopy
electron holography
Opis:
Transmission electron microscopy (TEM) is a powerful diagnostic tool for the determination of structure/property relationships of materials. A comprehensive analysis of materials requires a combined use of a variety of complementary electron microscopical techniques of imaging, diffraction and spectroscopy at an atomic level of magnitude. The possibilities and limitations of quantitative TEM analysis will be demonstrated for interface studies of the following materials and materials systems: Nickel-based superalloy CMSX-10, (Zn,Cd)O/ZnO/Al2O3, (Al,Ga)N/AlN/Al2O3, GaN/LiAlO2 and FeCo-based nanocrystalline alloys.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2010, 58, 2; 237-253
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of Investment Casting Technology from Bronze Age. Casting Workshop in Grzybiany (Southwest Poland)
Autorzy:
Garbacz-Klempka, A.
Suchy, J. S.
Kwak, Z.
Tokarski, T.
Klempka, R.
Stolarczyk, T.
Powiązania:
https://bibliotekanauki.pl/articles/352158.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
archeometallurgy
copper alloys
investment casting technology
lost wax casting
x-ray spectroscopy
Opis:
Investment casting technology that utilizes lost-wax casting is one of the most-important achievements of ancient society. In Lower Silesia, Poland (Grzybiany, Legnica county), a 7-6 BC casting workshop was discovered with numerous artifacts, confirming the existence of the manufacturing process of metal ornaments using ceramic molds. The paper presents the research of molds and casts from the Bronze and Early Iron Ages. Microscopic analyses of the casting molds were performed, along with radiographic and chemical composition tests of the artifacts (the latter employing the use of the X-ray fluorescence spectroscopy method). The clustering method was used for alloy classification. The microstructure was analyzed by means of Scanning Electron Microscopy with Energy Dispersive Spectroscopy. Conclusions from the research were utilized in further experiments.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 615-624
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Towards a viable method of reusing silicon carbide. Physicochemical analyses in the studies on the industrial application of the material
Autorzy:
Niemczyk-Wojdyla, Anna
Fornalczyk, Agnieszka
Willner, Joanna
Zawisz, Rafał
Powiązania:
https://bibliotekanauki.pl/articles/2032847.pdf
Data publikacji:
2021
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
silicon carbide
X-ray spectroscopy
Acheson process
węglik krzemu
spektroskopia rentgenowska
proces Achesona
Opis:
The paper presents an investigation on the feasibility of recovery of the highly valuable silicon carbide (SiC) from the slurry waste generated from silicon wafer production in the photovoltaic and semiconductor industry. Compared to the other techniques of recycling, a facile and low-cost method of waste treatment via heat drying followed by low-energy mixing in a shaker mixer was proposed. As the result of the treatment, the slurry waste was converted into a powdered form with dominant content of SiC. Separated SiC material was characterized by scanning electron microscopy, energy-dispersive X-ray spectroscopy, X-ray powder diffraction, and sieve analysis. In addition, analyses of the bulk density, moisture content and melting test were carried out. As was confirmed by the physicochemical analyses, the dominant sieve fraction was in the range of 0.1-0.06 mm, the purity level was a minimum 99% mass of SiC, the moisture content - 0.3%, the bulk density - 1.3 g/cm3. The physicochemical characteristics of the material were crucial for understanding the material performance, assessment of the material quality and determining the perspective directions of the industrial application. The studies revealed that the material exhibited a high application potential as abrasive, especially in abrasive grinding and waterjet cutting.
Źródło:
Environment Protection Engineering; 2021, 47, 4; 43-52
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Carbon nanotubes functionalized by salts containing stereogenic heteroatoms as electrodes in their battery cells
Autorzy:
Zdanowska, S.
Pyzalska, M.
Drabowicz, J.
Kulawik, D.
Pavlyuk, V.
Girek, T.
Ciesielski, W.
Powiązania:
https://bibliotekanauki.pl/articles/779468.pdf
Data publikacji:
2016
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
multi-walled carbon nanotubes (MWCNT)
battery
bromination
charge transfer
X-ray spectroscopy
electronic structure
Opis:
This paper concentrates on electrochemical properties of groups of multi-walled carbon nanotubes (MWCNT) functionalized with substituents containing a stereogenic heteroatom bonded covalently to the surface of the carbon nanotube. This system was tested in Swagelok-type cells. The cells comprised a system (functionalized CNT with salts containing S and P atoms) with a working electrode, microfiber separators soaked with electrolyte solution, and a lithium foil counter/reference (commercial LiCoO2 ) electrode. The electrolyte solution was 1 M LiPF6  in propylene carbonate. Using standard techniques (cyclic voltammetry/chronopotentiometry), galvanostatic cycling was performed on the cells at room temperature with a CH Instruments Model 600E potentiostat/galvanostat electrochemical measurements. Methods of functionalization CNT were compared in terms of the electrochemical properties of the studied systems. In all systems, the process of charge/discharge was observed.
Źródło:
Polish Journal of Chemical Technology; 2016, 18, 4; 22-26
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
TiO2 thin films grown on SiO2–Si(111) by the reactive evaporation method
Autorzy:
Grodzicki, M
Wasielewski, R
Mazur, P
Zuber, S
Ciszewski, A
Powiązania:
https://bibliotekanauki.pl/articles/173459.pdf
Data publikacji:
2013
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
titanium oxide
wettability
X-ray photoelectron spectroscopy
UV radiation
Opis:
TiO2 thin films were grown on silicon substrates using an electron-beam evaporator. Grainy TiO was used as the evaporation material. Temperature substrate during TiO2 growth was relatively low (about 150 °C), what is important for many optoelectronic devices and multilayers mirrors. High vacuum condition allows to maintain clean surfaces substrates before and during oxide growth. The morphology of titanium oxide thin films was ex situ investigated using atomic force microscopy operating in contact mode, X-ray photoelectron spectroscopy, X-ray powder diffractometry, and by means of a contact angle analyzer. The influence of annealing treatment and exposure to UV–VIS radiation on the morphology has been also discussed.
Źródło:
Optica Applicata; 2013, 43, 1; 99-107
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of adsorption of heavy metals from water solutions by wood of selected domestic species using X-Ray Fluorescence (XRF)
Autorzy:
Balicka, Adrianna
Szadkowski, Jan
Powiązania:
https://bibliotekanauki.pl/articles/2200144.pdf
Data publikacji:
2020
Wydawca:
Szkoła Główna Gospodarstwa Wiejskiego w Warszawie. Wydawnictwo Szkoły Głównej Gospodarstwa Wiejskiego w Warszawie
Tematy:
X-Ray Fluorescence Spectroscopy
wood shaving
adsorption
heavy metals
Opis:
Analysis of adsorption of heavy metals from water solutions by wood of selected domestic species using X-Ray Fluorescence (XRF).The aim of this study was to analyze the absorption of three specific heavy metals from model water solution by wood species from domestic Polish forests. This paper focuses on XRF method to determine metal content in samples. European aspen (Populus tremula L.) and Black locust (Robinia pseudoacacia L.) have been chosen. Firstly, shavings were prepared and soaked with standard solutions of lead (II) nitrate, cadmium nitrate and mercury (II) chloride for 7 days. Then, the material was dried and reduced to ashes using muffle furnace. Finally, content of absorbed metal was marked (XRF) and analyzed with a view to initial contents of metal ions in standard solutions. It was established, that the higher the concentration of mercury in standard solution is, the higher impulse counts is obtained for European aspen. This reversal of the dependence is noticeable for second analyzed species.
Badanie adsorpcji metali ciężkich z modelowych roztworów wodnych przez drewno wybranych gatunków krajowych za pomocą Spektrometrii Fluorescencji Rentgenowskiej (XRF). Celem wykonanych badań było sprawdzenie poziomu adsorpcji wytypowanych metali ciężkich tj. ołowiu, kadmu oraz rtęci, przez dwa gatunki rodzime topolę (Populus tremula L.) oraz robinię akacjową (Robinia pseudoacacia L.). W fazie przygotowawczej materiał został znacznie rozdrobniony i rozdzielony na kilka frakcji. Działanie to miało na celu zwiększenie powierzchni adsorpcji badanego drewna. Azotan kadmu (II), azotan ołowiu oraz chlorek rtęci (II) zostały rozpuszczone w destylowanej wodzie w takich proporcjach, aby stworzyć po cztery roztwory – każdy o innym stężeniu. Wybrana frakcja wiórów została poddana obróbce termicznej w wodzie destylowanej w celu usunięcia zawartego powietrza. Następnie frakcję podzielono na próbki 1 gramowe. Drewno nasiąkało w modelowych roztworach przez ok. 168 godzin. Finalnie zostało ono odsączone, wysuszone i spopielone w piecu muflowym. Tak przygotowane próbki zostały poddane badaniu z wykorzystaniem spektrometrii fluorescencji rentgenowskiej (XRF). Urządzenie analizowało zawartość metali w pyle za pomocą dwóch różnych programów i trzech czasów naświetlania. Otrzymane wartości analizowano pod kątem ilościowym a nie jakościowym.
Źródło:
Annals of Warsaw University of Life Sciences - SGGW. Forestry and Wood Technology; 2020, 111; 73--82
1898-5912
Pojawia się w:
Annals of Warsaw University of Life Sciences - SGGW. Forestry and Wood Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
X-ray techniques in the investigation of a Gothic sculpture : the risen Christ
Autorzy:
Mikołajska, A.
Walczak, M.
Kaszowska, Z.
Urbańczyk-Zawadzka, M.
Powiązania:
https://bibliotekanauki.pl/articles/146866.pdf
Data publikacji:
2012
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
cultural heritage
X-ray image
X-ray dual source computed tomography (DSCT)
scanning electron microscopy energy dispersed X-ray spectroscopy (SEM-EDX)
Opis:
For over a century, X-ray radiation has played an important role in the area of the conservation and restoration of cultural heritage objects. X-ray techniques are amongst the most fundamental and helpful methods used in the investigation of art works. This paper reviews the application of traditional radiography, X-ray dual source computed tomography (DSCT) and scanning electron microscopy combined with energy dispersed X-ray spectroscopy (SEM-EDX) to the investigation of a wooden, Gothic sculpture, The risen Christ. Thanks to the properties of X-ray radiation (different absorption by various materials) first two methods allow the assessment of the preservation state and the observation of the internal structure of an object in 3-D. While SEM-EDX analysis permits the elemental analysis of the polychrome layers. As a result 2-D and 3-D images, permitting the full volume inspection of an object, were taken in a totally non-destructive way. The morphological and physical information about the inner structure of the investigated wooden sculpture was obtained, revealing changes related to previous restorations, as well as ageing effects. Employing the SEM-EDX, painting materials (pigments and filers), were identified. Gained data is essential for restorers to understand the whole structure of the studied object and to decide which further investigation and restoration steps have to be undertaken.
Źródło:
Nukleonika; 2012, 57, 4; 627-631
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Corrosion Properties of Ca65-xMg17.5Zn17.5+x (x = 0, 2.5, 5) Alloys
Autorzy:
Babilas, R.
Wojciechowski, P.
Bajorek, A.
Sakiewicz, P.
Cesarz-Andraczke, K.
Powiązania:
https://bibliotekanauki.pl/articles/352466.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ca-based alloys
corrosion
hydrogen evolution
X-ray photoelectron spectroscopy
Opis:
The aim of the paper is to study the effect of zinc addition on the corrosion behavior of Ca65-xMg17.5Zn17.5+x(x = 0, 2.5, 5 at.%) alloys in simulated physiological fluids at 37°C. The electrochemical measurements allowed to determine a corrosion potential, which showed a positive shift from –1.60 V for Ca65Mg17.5Zn17.5 alloy to –1.58 V for Ca60Mg17.5Zn22.5 alloy, adequately. The more significant decrease of hydrogen evolution was noticed for Ca60Mg17.5Zn22.5 alloy (22.4 ml/cm2) than for Ca62.5Mg17.5Zn20 and Ca65Mg17.5Zn17.5 samples (29.9 ml/cm2 and 46.4 ml/cm2), consequently. The corrosion products after immersion tests in Ringer’s solution during 1 h were identified by X-ray diffraction and X-ray photoelectron spectroscopy as calcium, magnesium oxides, carbonates, hydroxides and calcium hydrate.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 1033-1040
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Species formed on iron surface during removal of copper ions from aqueous solutions
Autorzy:
Suponik, T.
Winiarski, A.
Szade, J.
Powiązania:
https://bibliotekanauki.pl/articles/110906.pdf
Data publikacji:
2015
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
water
zero-valent iron
copper
X-ray photoelectron spectroscopy
diffraction
Opis:
The subject of the research covered in this paper is the removal of copper (Cu2+) cations from water at low pH (initial values of pH 3 and 6) by means of zero-valent iron. The chemical states and atomic concentrations of solids formed on the surface of zero-valent iron, and the type of deposited polycrystalline substances have been analyzed with the use of XPS and XRD. The type of process causing the copper removal from water at low pH, corresponding to the effect of acid mine drainage, has been identified by analyzing the changes of physicochemical parameters and specified chemicals content in water. Cu2+ was removed from water for the initial pH of 6 was much more effective than at lower pH. The formation of CuxFe3-xO4 , where x≤1, and to a lesser degree Cu2O, Cu0 and/or CuO and/or Cu2S, were the basic processes of the removal of copper at almost neutral pH of water (pH about 6), while the formation of copper in metallic form and Cu2O, as well as probably CuO, were the basic processes for lower pH (pH about 3). The adsorption of Cu2+ on the surface of shell covering square-shaped cold-rolled steel sheet cell was an additional process causing the removal of copper from water at almost neutral pH.
Źródło:
Physicochemical Problems of Mineral Processing; 2015, 51, 2; 731-743
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of X-ray photoelectron spectroscopy (XPS) and a functional near infrared spectroscopy (fNIRS) in medicine
Autorzy:
Szklarczyk, Marek
Powiązania:
https://bibliotekanauki.pl/articles/1891232.pdf
Data publikacji:
2021-12-02
Wydawca:
Gdański Uniwersytet Medyczny
Tematy:
X-ray photoelectron spectroscopy
XPS
functional near infrared spectroscopy
fNIRS
brain activity
Opis:
The development of modern clinical medicine and the truthful medical diagnosis require hard physicochemical data. Furthermore, the social demands for more accurate and collected data, which refer to human health in real conditions and in real time, force the quest for techniques which would be possible to be applied in a broadly understood clinical field. In this article two techniques are described. A high vacuum technique which is an X-ray photoelectron spectroscopy (XPS), and a functional near infrared spectroscopy (fNIRS), which might be applied in vivo condition. For the both techniques, the results pointing their applicability in the clinical and modern biochemical research are described.
Źródło:
European Journal of Translational and Clinical Medicine; 2021, 4, 2; 86-93
2657-3148
2657-3156
Pojawia się w:
European Journal of Translational and Clinical Medicine
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Poznawanie własności materii w skali atomowej za pomocą absorpcji promieniowania synchrotronowego
Autorzy:
Drzewiecka, A.
Wolska, A.
Klepka, M. T.
Ławniczak-Jabłońska, K.
Powiązania:
https://bibliotekanauki.pl/articles/274182.pdf
Data publikacji:
2012
Wydawca:
Roble
Tematy:
promieniowanie synchrotronowe
rentgenowska spektroskopia absorpcyjna
synchrotron radiation
X-ray absorption spectroscopy
Źródło:
LAB Laboratoria, Aparatura, Badania; 2012, 17, 6; 16-21
1427-5619
Pojawia się w:
LAB Laboratoria, Aparatura, Badania
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation, characterization and optimization of cross-linked fructosyltransferase aggregates for the production of prebiotic fructooligosaccharides
Autorzy:
Ademakinwa, A.N.
Ayinla, Z.A.
Omitogun, O.G.
Agboola, F.K.
Powiązania:
https://bibliotekanauki.pl/articles/81247.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
fructosyltransferase
Aureobasidium pullulans
fructooligosaccharide
prebiotic
statistical optimization
scanning electron microscopy
X-ray spectroscopy
Fourier transform infrared spectroscopy
biotransformation
chemometric analysis
Źródło:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology; 2018, 99, 4
0860-7796
Pojawia się w:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The archaeometric, formal and stylistic analysis of a black-glazed fish-plate from the National Museum in Poznań
Autorzy:
Głuszek, Inga
Krueger, Michał
Powiązania:
https://bibliotekanauki.pl/articles/958155.pdf
Data publikacji:
2019
Wydawca:
Uniwersytet Rzeszowski. Instytut Archeologii Uniwersytetu Rzeszowskiego. Muzeum Okręgowe w Rzeszowie
Tematy:
black-glaze pottery
X-ray fluorescence spectroscopy
provenience
multivariate analyses
museum collections
Opis:
This paper presents the results of the XRF, formal and stylistic analyses of a black-glaze fish-plate from the National Museum in Poznań. A non-invasive portable X-ray fluorescence spectrometer (pXRF) has been used to determine the chemical composition of the plate. Analysis of the shape and decoration provided data on the chronology, typology and provenance of the vessel. The obtained results were used to determine the possible region of the fish-plate’s production. The form of the fish-plate represents features characteristic for the early stage of Italian black-glaze production, which is combination of Athenian traditions with new solutions in terms of proportion and shape. The analysis of X-ray fluorescence spectrometry data and comparative studies with already known results of the Italian black glaze pottery chemical analyses allowed the fish-plate to be identified as an example of the Campania A group from ancient Naples workshops, dated to the second half of the 4th century BC.
Źródło:
Analecta Archaeologica Ressoviensia; 2019, 14; 81-90
2084-4409
Pojawia się w:
Analecta Archaeologica Ressoviensia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of a Castings Quality and Metalworking Technology. Treasure of the Bronze Age Axes
Autorzy:
Garbacz-Klempka, A.
Kaczmarek, Ł.
Kwak, Z.
Kozana, J.
Piękoś, M.
Perek-Nowak, M.
Długosz, P.
Powiązania:
https://bibliotekanauki.pl/articles/382751.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
non-destructive testing
archeometallurgy
tin bronze
X-ray spectroscopy
castings defects
badania nieniszczące
archeometalurgia
brąz
spektroskopia rentgenowska
wady odlewów
Opis:
Cast axes are one of the most numerous categories of bronze products from earlier phases of the Bronze Age found in Poland. They had multiple applications since they were not only used objects such as tools or weapons but also played the prestigious and cult roles. Investigations of the selected axes from the bronze products treasure of the Bronze Age, found in the territory of Poland, are presented in the hereby paper. The holder of these findings is the State Archaeological Museum in Warsaw. Metallurgical investigations of axes with bushing were performed in respect of the casting technology and quality of obtained castings. Macroscopic observations allowed to document the remains of the gating system and to assess the range and kind of casting defects. Light microscopy revealed the microstructure character of these relicts. The chemical composition was determined by means of the X-ray fluorescence method with energy dispersion (ED-XRF) and by the scanning electron microscopy with X-ray energy dispersion analysis in micro-areas (SEM-EDS). The shape and dimensions of cores, reproducing inner parts of axes were identified on the basis of the X-ray tomography images. Studies reconstructed production technology of the mould with gating system, determined chemical composition of the applied alloys and casting structures as well as revealed the casting defects being the result of construction and usage of moulds and cores.
Źródło:
Archives of Foundry Engineering; 2018, 18, 3; 179-285
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Determination of elements by atomic absorption spectrometry and energy dispersive X-ray spectroscopy in humic acids and soil samples
Oznaczanie pierwiastków za pomocą atomowej spektrometrii absorpcyjnej i spektrometrii rentgenowskiej energii rozproszonej w próbkach kwasów huminowych oraz gleby
Autorzy:
Konečná, M.
Pospíšilová, L.
Škarpa, P.
Powiązania:
https://bibliotekanauki.pl/articles/125973.pdf
Data publikacji:
2011
Wydawca:
Towarzystwo Chemii i Inżynierii Ekologicznej
Tematy:
humic acids
labile forms
atomic absorption spectrometry
energy dispersive X-ray spectroscopy
kwasy huminowe
formy labilne
spektrometria absorpcji atomowej
spektroskopia z dyspersją energii promieniowania X
Opis:
Determination of various elements in humic acids and soil samples is important with regard to their biological availability. This work was focused on the identification of trace elements presented in soil samples and humic acids preparates. The object of our study was the samples of grassland soil classified according to FAO as Eutric Cambisol (locality Vatín, Czech-Moravian Upland). Labile and total several element contents in the studied samples were determined. The labile forms were measured in the 0.01 M CaCl2 extract by using high resolution continuum source atomic absorption spectrometer. Total element contents were determined after extraction in aqua regia. Basic soil properties were measured by commonly used methods - soil reaction and conductivity by potentiometric method, texture by pipette method, CEC according to Kappen method and Cox by titrimetric oxidation. Soil humic acids (HA) were isolated according to standard IHSS method. Elemental composition of HA was determined by CHSN/O analyzer. Energy dispersive X-ray spectroscopy allowed us to detect elements in situ in HA molecule and following elements were found: Fe, Cu, Zn, Ti, Ca, K, S, P, Si and Br. The presence of mentioned elements in humic acids preparates was compared with the determined amounts of labile forms and total contents in the soil samples.
Źródło:
Proceedings of ECOpole; 2011, 5, 2; 377-381
1898-617X
2084-4557
Pojawia się w:
Proceedings of ECOpole
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Charakterystyka właściwości adsorpcyjnych i energetycznych utlenionego i zredukowanego grafenu
The characteristic of the adsorption and energetic properties of the oxidised and reduced graphene
Autorzy:
Grajek, H.
Farczak, Ł.
Wawer, T.
Jabłoński, P.
Purchała, M.
Powiązania:
https://bibliotekanauki.pl/articles/1366455.pdf
Data publikacji:
2015
Wydawca:
Centralny Ośrodek Badawczo-Rozwojowy Aparatury Badawczej i Dydaktycznej, COBRABiD
Tematy:
grafen
odwrócona chromatografia gazowa
rentgenowska spektrometria fotoelektronów
graphene
inverse gas chromatography
X-ray photoelectron spectroscopy
Opis:
Scharakteryzowano oddziaływania wybranych atomów i cząsteczek z powierzchniami próbek utlenionego i zredukowanego grafenu. Ponadto analizowano właściwości adsorpcyjne i akceptorowo-donorowe grafenu. Do charakterystyki oddziaływań zastosowano równania funkcji potencjalnych Lennarda-Jonesa (12-6) i (10-4) oraz funkcję potencjalną Steele (10-4-3). Na podstawie danych niskotemperaturowej (77 K) adsorpcji N2 wyznaczono metodą porównawczą as parametry struktury porowatej badanego grafenu. Jako adsorpcyjne układy odniesienia zastosowano dane adsorpcji N2 na sadzach grafityzowanych Carbopack F i Cabot BP280. Charakterystyka energetycznych właściwości powierzchniowych badanego grafenu obejmowała chromatograficzne wyznaczenie wartości składowej specyficznej swobodnej energii powierzchniowej oraz właściwości akceptorowo-donorowych. Grafen utleniony charakteryzował się właściwościami elektrono-akceptorowymi, natomiast zredukowany elektrono-donorowymi.
The interaction of the selected atoms and molecules with the surfaces of oxidised and reduced graphene samples have been characterised. Moreover, the adsorption and acceptor-donor properties have been analysed. The equations of the Lennard-Jones (12-6) and (10-4) and the Steele (10-4-3) potential functions have been employed for the characterisation of the interactions. The parameters of the pore structure have been determined by means of the as comparative method on the basis of the N2 low-temperature adsorption data at 77 K. The N2 adsorption data on the Carbopack F and Cabot BP280 graphitised carbon blacks have been used as the reference adsorption data. The characteristics of the surface energetic properties of the tested graphene have encompassed the determination of the specific component of the surface energy and the acceptor-donor properties. The oxidised graphene has been characterised by the electron-acceptor properties, whereas the reduced graphene by the electron-donor properties.
Źródło:
Aparatura Badawcza i Dydaktyczna; 2015, 20, 3; 214-223
2392-1765
Pojawia się w:
Aparatura Badawcza i Dydaktyczna
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wpływ czynników chemicznych na strukturę i budowę włosów ludzkich
The influence of chemical factors on the structure of human hair
Autorzy:
Dobosz, Magda
Kalska-Szostko, Beata
Powiązania:
https://bibliotekanauki.pl/articles/171505.pdf
Data publikacji:
2020
Wydawca:
Polskie Towarzystwo Chemiczne
Tematy:
badanie włosów
chemia kryminalistyczna
skaningowa mikroskopia elektronowa
spektroskopia rentgenowska z dyspersją energii
energy dispersive X-ray spectroscopy
hair tests
forensic chemistry
scanning electron microscopy
Opis:
The main purpose of the presented study was to investigate the influence of chemical factors on the morphology of human hair. Few factors that may occurduring criminal offenses were selected for testing, including aqueous solutions of hydrochloric acid (HCl), sodium hydroxide (NaOH), lead(II) nitrate (Pb(NO3)2), cadmium(II) nitrate (Cd(NO3)2), sodium chloride (NaCl), ethanol (C2H5OH), water (H2O). The description of the effects of chosen chemical compounds on hair was made mainly on the basis of Scanning Electron Microscopy (SEM). In addition, the elemental composition of the hair as an effect of interaction with solution was examined and analyzed using an EDX (Energy - Dispersive X-ray) spectrometry. Performed tests show the degree of human hair degradation and contamination depending on the examined factor and time.
Źródło:
Wiadomości Chemiczne; 2020, 74, 7-8; 453-476
0043-5104
2300-0295
Pojawia się w:
Wiadomości Chemiczne
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Działanie czynników mechanicznych oraz termicznych na morfologię włosów ludzkich i zwierzęcych
Effect of mechanical and thermal factors on the structure of human and animal hair
Autorzy:
Dobosz, Magda
Kalska-Szostko, Beata
Powiązania:
https://bibliotekanauki.pl/articles/1410887.pdf
Data publikacji:
2021
Wydawca:
Polskie Towarzystwo Chemiczne
Tematy:
badanie włosów
chemia kryminalistyczna
skaningowa mikroskopia elektronowa
spektroskopia rentgenowska z dyspersją energii
energy dispersive X-ray spectroscopy
hair tests
forensic chemistry
scanning electron microscopy
Opis:
The main purpose of the presented study was to investigate and compare the influence of mechanical and thermal factors on the morphology of human and animal hair. Several factors that may occur during criminal offenses were selected for testing including cutting by a scalpel or scissors, damaging by a hammer; and high, or low-temperature thermal treatment (heating for 1h, or 24 hours at elevated temperatures 100°C, 200°C, and 300°C, as well as freezing for 24 hours at -20°C, or for 10 minutes in liquid nitrogen (-197°C)). The impact of selected mechanical and temperature factors on human and animal hair was made mainly on the basis of Scanning Electron Microscopy (SEM). Moreover, the elemental composition of the hair was investigated and analyzed using an EDX (Energy - Dispersive X-ray) spectrometry. Performed tests show the degree of human hair degradation depending on the examined factor and time.
Źródło:
Wiadomości Chemiczne; 2021, 75, 5-6; 823-844
0043-5104
2300-0295
Pojawia się w:
Wiadomości Chemiczne
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Archaeometallurgical Investigations of the Early Iron Age Casting Workshop at Kamieniec. A Preliminary Study
Autorzy:
Garbacz-Klempka, A.
Kowalski, Ł.
Kozana, J.
Gackowski, J.
Perek-Nowak, M.
Szczepańska, G.
Piękoś, M.
Powiązania:
https://bibliotekanauki.pl/articles/383062.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
non-destructive testing
investment casting
X-ray fluorescence spectroscopy
archaeometallurgy
Lusatian culture
badania nieniszczące
odlewnictwo
promieniowanie rentgenowskie
kultura łużycka
Opis:
(Chełmno land, Poland) as it is reflected through casting workshop recovered during recent excavations. Among ready products, the ones giving evidence of local metallurgy (e.g. casting moulds and main runners) were also identified. With the shrinkage cavities and dendritic microstructures revealed, the artifacts prove the implementing a casting method by the Lusatian culture metalworkers. The elemental composition indicates application of two main types of bronzes: Cu-Sn and Cu-Pb. Aside these main alloying additions, some natural impurities such as silver, arsenic, antimony and nickel were found which may be attributed to the origin of the ore and casting technology. The collection from Kamieniec was described in terms of its structure and composition. The investigations were made by means of the energy dispersive X-ray fluorescence spectroscopy (ED-XRF), scanning electron microscopy (SEM) coupled with an energy dispersive X-ray analysis system (EDS) and optical microscopy (OM). In order to fingerprint either local or non-local profile of the alloys, the ED-XRF data-set was statistically evaluated using a factor analysis (FA).
Źródło:
Archives of Foundry Engineering; 2016, 16, 3; 29-34
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of the decay of some effects of modification of polylactide surface layers
Analiza zaniku wybranych efektów modyfikowania warstwy wierzchniej polilaktydu
Autorzy:
Stepczyńska, M.
Powiązania:
https://bibliotekanauki.pl/articles/947480.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
polylactide
surface layer modification
corona discharge
X-ray photoelectron spectroscopy (XPS)
polilaktyd
modyfikacja warstwy wierzchniej
wyładowania koronowe
spektroskopia fotoelektronowa (XPS)
Opis:
The results of an investigation into the effects of modifying a surface layer (SL) of polylactide (PLA) as a function of time are presented. The PLA modification was performed by the method of corona discharges (CD) in the air using unit energy values (Eu) equal to 3.5 and 10 kJ/m2. The extent of oxidation and contact angle of the SL were determined by the methods of X-ray photoelectron spectroscopy (XPS) and goniometry, respectively. The measurements were carried out immediately after the modification process, as well as 1, 2, and 3 months later.
Analizowano zanik wczasie zmian wywołanych modyfikowaniem za pomocą wyładowań koronowych (CD) warstwy wierzchniej (SL) polilaktydu (PLA). Modyfikowanie prowadzono w atmosferze powietrza, z zastosowaniem jednostkowej energii (Eu) modyfikowania o wartości 3,5 i 10 kJ/m2. Stopień utlenienia oraz wartość kąta zwilżania SL badano metodą spektroskopii fotoelektronowej (XPS) oraz goniometrii, bezpośrednio po procesie modyfikowania oraz po upływie 1, 2 i 3 miesięcy.
Źródło:
Polimery; 2015, 60, 7-8; 462-467
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A multi-analytical approach for the analysis of cation distribution in a aluminoceladonite structure
Autorzy:
Kądziołka-Gaweł, Mariola
Dulski, Mateusz
Czaja, Maria
Krzykawski, Tomasz
Szubka, Magdalena
Powiązania:
https://bibliotekanauki.pl/articles/2172615.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminoceladonite
ions position characterization isomorphic substitutions
Fe bearing phyllosilicates
X-ray photoelectron spectroscopy
Mössbauer spectroscopy
Raman spectroscopy
glinokrzemiany
krzemiany warstwowe
rentgenowska spektrometria fotoelektronów
XPS
spektroskopia mössabuerowska
spektroskopia Ramana
Opis:
In this paper cation arrangement in two samples of aluminoceladonite, emerald green and dark-green were studied by Mössbauer, Raman and X-ray photoelectron spectroscopies. The X-ray photoelectron spectroscopy (XPS) spectra obtained in the region of the Si2p, Al2p, Fe2p, K2p, and O1s core levels provided information, for the first time highlighting a route to identify the position of Si, Al, K, and Fe cations in a structure of layered silicates. The XPS analysis showed the presence of Al in tetrahedral and octahedral coordination while the K2p line indicated the possibility of K+ substitution by other cations in interlayer sites. Mössbauer spectroscopy provided information about crystal chemistry with respect to the local electronic and geometric environment around the Fe atom and to distortions of the polyhedra. It turned out that iron was located mostly in the cis-octahedra position wherein about 75% of iron appeared in the form of Fe3+. The most preferred cation combinations around Fe corresponded to 3Fe3+ ions and MgFe2+Fe3+/2MgFe3+. Raman spectroscopy illustrated aluminium substitution in silicon and iron positions wherein the concentration of the aluminium determined the degree of structural distortion within the layered system. These isomorphic substitutions implied a typical band arrangement in the hydroxyl region, which has not been observed in celadonites so far.
Źródło:
Acta Geologica Polonica; 2022, 72, 3; 353--368
0001-5709
Pojawia się w:
Acta Geologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analiza składu chemicznego i fazowego cienkich warstw metalicznych
Autorzy:
Lukaszkowicz, K.
Staszuk, M.
Nuckowski, P.
Powiązania:
https://bibliotekanauki.pl/articles/274354.pdf
Data publikacji:
2017
Wydawca:
Roble
Tematy:
dyfraktometria rentgenowska
XPS
spektroskopia fotoelektronów w zakresie promieniowania X
GDS/GDOES
emisyjna spektroskopia optyczna z wyładowaniem jarzeniowym
cienkie warstwy metaliczne
X-ray diffractometry
x-ray photoelectron spectroscopy
glow discharge optical emission spectrometry
metallic thin layers
Źródło:
LAB Laboratoria, Aparatura, Badania; 2017, 22, 5; 24-29
1427-5619
Pojawia się w:
LAB Laboratoria, Aparatura, Badania
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wideband spectral emission measurements from laser-produced plasma EUV/SXR source based on a double gas puff target
Autorzy:
Arikkatt, Antony Jose
Wachulak, Przemysław
Fiedorowicz, Henryk
Bartnik, Andrzej
Czwartos, Joanna
Powiązania:
https://bibliotekanauki.pl/articles/1849155.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Plasma Spectroscopy
X-ray coherence tomography
soft X-ray
Opis:
We present spectral emission characteristics from laser-plasma EUV/SXR sources produced by irradiation of < 1 J energy laser pulse on eleven different double stream gas puff targets, with most intense electronic transitions identified in the spectral range from 1 nm to 70 nm wavelength which corresponds to photon energy from 18 eV to 1240 eV. The spectra were obtained using grazing incidence and transmission spectrographs from laser-produced plasma emission, formed by the interaction of a laser beam with a double stream gas puff target. Laser pulses with a duration of 4 ns and energy of 650 mJ were used for the experiment. We present the results obtained from three different spectrometers in the wavelength ranges of SXR (1-5.5 nm), SXR/EUV (4-15.5 nm), and EUV (10-70 nm). In this paper, detailed information about the source, gas targets under investigation, the experimental setup, spectral measurements and the results are presented and discussed. Such data may be useful for the identification of adequate spectral emissions from gasses in the EUV and SXR wavelength ranges dedicated to various experiments (i.e. broadband emission for the X-ray coherence tomography XCT) or may be used for verification of magnetohydrodynamic plasma codes.
Źródło:
Metrology and Measurement Systems; 2020, 27, 4; 701-719
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
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