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Tytuł:
Vickers Hardness and Positron Annihilation Study of Eurofer97 and ODS Eurofer
Autorzy:
Bartošová, I.
Čížek, J.
Lukáč, F.
Slugeň, V.
Powiązania:
https://bibliotekanauki.pl/articles/1196045.pdf
Data publikacji:
2014-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
28.52.Fa
Opis:
This paper describes investigations of Eurofer97 and oxide dispersion strengthened version of this steel, in as received state and after annealing. Vickers hardness test was performed on the as received specimens and after annealing at various temperatures to obtain information about development of the strength of studied materials. After identifying the temperature region where significant changes of the strength take place we applied positron annihilation spectroscopy to probe the microstructural changes in ferritic/martensitic steels. An observation of phase transformation was observed in both steels at various temperatures indicating different behaviour of the base material and its strengthened version. All applied methods proved the importance of strengthening by oxides to improve properties of steels.
Źródło:
Acta Physica Polonica A; 2014, 125, 3; 702-705
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Performance of a High-Resolution Digital Positron-Lifetime Spectrometer
Autorzy:
Bečvář, F.
Čížek, J.
Procházka, I.
Powiązania:
https://bibliotekanauki.pl/articles/1812465.pdf
Data publikacji:
2008-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
Opis:
This work describes a digital positron-lifetime spectrometer based on two ultrafast digitizers. Performance of the digital spectrometer in conditions of a routine measurement is compared with an analogue setup connected to the same detectors. It was found that engagement of the digital setup leads to an improvement of timing resolution (FWHM for $\text{}^{22}Na$) from 169 ps for the traditional analogue setup to 146 ps for the digital setup. The coincidence count rate for 1.2 MBq $\text{}^{22}Na$ source is 75-80 coinc./s for both configurations. These results clearly demonstrate the advantages of the digital timing over the traditional analogue setup.
Źródło:
Acta Physica Polonica A; 2008, 113, 5; 1279-1284
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Use of Energy Summing for Selection of Coincidence Events in Positron-Lifetime Spectroscopy
Autorzy:
Bec̆vár̆, F.
C̆iz̆ek, J.
Procházka, I.
Powiązania:
https://bibliotekanauki.pl/articles/2007883.pdf
Data publikacji:
1999-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
Opis:
A BaF$\text{}_{2}$ positron-lifetime spectrometer equipped with a coincidence system that represents a compromise between the traditional fast-fast and fast-slow arrangements is described. The main difference of the present configuration from both the fast-slow and fast-fast ones consists in use of a sum of the energy signals from the start and stop detectors to select the coincidence events. Quality of the spectrometer response function (≈ 150 ps FWHM for $\text{}^{22}$Na) is very close to that observed for our fast-slow configuration with the equivalent detectors but throughput of the present apparatus is increased almost by a factor of two. Moreover, the electronic scheme becomes less complicated, which has also a positive impact on its cost.
Źródło:
Acta Physica Polonica A; 1999, 95, 4; 448-454
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Defects in Ultra-Fine Grained Mg and Mg-Based Alloys Prepared by High Pressure Torsion Studied by Positron Annihilation
Autorzy:
Čížek, J.
Procházka, I.
Smola, B.
Stulíková, I.
Kužel, R.
Matěj, Z.
Cherkaska, V.
Islamgaliev, R.
Kulyasova, O.
Powiązania:
https://bibliotekanauki.pl/articles/2043304.pdf
Data publikacji:
2005-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
61.72.-y
Opis:
Despite the favourable strength and thermal stability, a disadvantage of the Mg-based alloys consists in a low ductility. Recently it has been demonstrated that ultra fine grained metals with grain size around 100 nm can be produced by high pressure torsion. A number of ultra fine grained metals exhibit favourable mechanical properties consisting in a combination of a very high strength and a significant ductility. For this reason, it is highly interesting to examine microstructure and physical properties of ultra fine grained Mg-based light alloys. Following this purpose, microstructure investigations and defect studies of ultra fine grained pure Mg and ultra fine grained Mg-10%Gd alloy prepared by high pressure torsion were performed in the present work using positron annihilation spectroscopy combined with X-ray diffraction, TEM observations, and microhardness measurements. Positrons are trapped at dislocations in Mg and Mg-10%Gd alloy deformed by high pressure torsion. A number of dislocations increases with the radial distance r from the centre to the margin of the sample. No microvoids (small vacancy clusters) were detected. Mg-10%Gd alloy deformed by high pressure torsion exhibits a homogeneous ultra fine grained structure with a grain size around 100 nm and high dislocations density. On the other hand, pure Mg deformed by high pressure torsion exhibits a binomial type of structure which consists of "deformed regions" with ultra fine grained structure and a high dislocation density and dislocation-free "recovered regions" with large grains. It indicates a dynamic recovery of microstructure during high pressure torsion processing.
Źródło:
Acta Physica Polonica A; 2005, 107, 5; 738-744
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hydrogen Interaction with Vacancies in Electron Irradiated Niobium
Autorzy:
Čižek, J.
Procházka, I.
Brauer, G.
Anwand, W.
Gemma, R.
Nikitin, E.
Kirchheim, R.
Pundt, A.
Powiązania:
https://bibliotekanauki.pl/articles/1812478.pdf
Data publikacji:
2008-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
61.72.-y
Opis:
Defect studies of Nb irradiated with 10 MeV electrons were performed in the present work by means of positron annihilation spectroscopy. The lattice defects were characterized by positron lifetime spectroscopy. Moreover, defect depth profiles were studied by slow positron implantation spectroscopy. The experimental investigations were accompanied by first principles theoretical calculations of positron parameters. It was found that irradiation-induced vacancies in Nb specimens are surrounded by H, which causes a shortening of the lifetime of trapped positrons. The influence of a Pd and Cr over-layer on the H concentration in the Nb specimens was examined.
Źródło:
Acta Physica Polonica A; 2008, 113, 5; 1293-1299
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Ceramic Nanoparticles on Thermal Stability of Ultra Fine Grained Copper
Autorzy:
Čížek, J.
Procházka, I.
Cieslar, M.
Islamgaliev, R.
Kulyasova, O.
Powiązania:
https://bibliotekanauki.pl/articles/1812477.pdf
Data publikacji:
2008-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
Opis:
A detailed study of the bulk ultra fine grained pure copper and copper with $Al_2O_3$ particles was carried out in the present work. The specimens were prepared by the high-pressure torsion and their microstructure was investigated by positron lifetime spectroscopy combined with transmission electron microscopy and microhardness tests. Defects in the as-deformed materials were characterized and the thermal stability of the ultra fine grained microstructure was subsequently examined in annealing experiments. An addition of $Al_2O_3$ nanoparticles was found to improve significantly the thermal stability of the ultra fine grained structure, the optimum content of $Al_2O_3$ being ≈0.5 wt.%.
Źródło:
Acta Physica Polonica A; 2008, 113, 5; 1285-1292
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron Lifetime Spectroscopy of Nanocrystalline Copper
Autorzy:
C̆ížek, J.
Procházka, I.
Vostrý, P.
Chmelík, F.
Islamgaliev, R. K.
Powiązania:
https://bibliotekanauki.pl/articles/2007957.pdf
Data publikacji:
1999-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
Opis:
Positron lifetime spectroscopy was applied to investigate the thermal stability of nanocrystalline copper prepared by severe plastic torsion deformation. Positrons annihilating in as prepared specimens exhibited free positron component τ$\text{}_{1}$ and two defect components τ$\text{}_{2}$=164 ps and τ$\text{}_{3}$=255 ps. Evolution of the lifetimes and relative intensities of all the three components with increasing annealing temperature during step-by-step isochronal annealing up to 630°C was studied. Behaviour of positrons in nanocrystalline copper could not be interpreted in the frame of conventional 3-state trapping model due to highly inhomogeneous defect distribution. Therefore a modified trapping model was developed and applied to explain the experimental results.
Źródło:
Acta Physica Polonica A; 1999, 95, 4; 487-495
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positronium Formation in Nanostructured Metals
Autorzy:
Čížek, J.
Melikhova, O.
Hruška, P.
Vlček, M.
Anwand, W.
Liedke, M.
Novotný, M.
Bulíř, J.
Powiązania:
https://bibliotekanauki.pl/articles/1033937.pdf
Data publikacji:
2017-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
41.75.Fr
36.10.Dr
Opis:
Positronium formation in Au films was studied using a magnetically guided continuous slow positron beam with variable energy. Black Au film with porous morphology was compared with conventional smooth Au film. In the smooth Au film positronium is formed on the film surface only. The black Au film exhibits porous sub-surface region containing micro-cavities interconnected with surface. Positronium is formed on inner surfaces of micro-cavities in the sub-surface region and travels through interconnected cavities towards the surface. 3-γ annihilation of ortho-positronium leaves a clear signature in two-dimensional coincidence Doppler broadening spectra. Measures of 3-γ annihilation contribution calculated from single γ-ray and coincidence Doppler broadening spectra were calculated and compared.
Źródło:
Acta Physica Polonica A; 2017, 132, 5; 1579-1584
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ultra Fine-Grained Metals Prepared by Severe Plastic Deformation: A Positron Annihilation Study
Autorzy:
Čížek, J.
Procházka, I.
Kužel, R.
Matĕj, Z.
Cherkaska, V.
Cieslar, M.
Smola, B.
Stulíková, I.
Brauer, G.
Anwand, W.
Islamgaliev, R. K.
Kulyasova, O.
Powiązania:
https://bibliotekanauki.pl/articles/2043303.pdf
Data publikacji:
2005-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
Opis:
Recent investigations of ultra fine-grained metals (Cu, Fe, Ni) performed within a Prague-Rossendorf-Ufa collaboration will be reviewed. The specimens were prepared by severe plastic deformation: the high-pressure torsion and equal channel angular pressing. Positron annihilation spectroscopy was used as the main method including (i) the conventional lifetime and the Doppler broadening measurements with $\text{}^{22}$Na and (ii) the slow-positron implantation spectroscopy with the Doppler broadening measurement. Other methods were also involved: transmission electron microscopy, X-ray diffraction, and microhardness. First, the mean grain size was determined and defects were identified in the as-deformed materials. Defects concentration and spatial distribution were studied in detail. Dislocations situated in distorted regions along grain boundaries, and a few-vacancy clusters distributed homogeneously inside dislocations-free grains, were observed in the ultra fine-grained Cu, Fe, and Ni. Subsequently, the thermal evolution of the ultra fine-grained structures during isochronal annealing was studied.
Źródło:
Acta Physica Polonica A; 2005, 107, 5; 745-752
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Resonance contributions to low-energy electron collisions with molecular hydrogen
Autorzy:
Horácek, J.
Cížek, M.
Houfek, K.
Kolorenc, P.
Pichl, L.
Powiązania:
https://bibliotekanauki.pl/articles/148461.pdf
Data publikacji:
2003
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
electron scattering
molecules
attachment
vibrational excitation
Opis:
Calculations of electron dissociative attachment and vibrational excitation of molecular hydrogen by low-energy electrons based on an improved nonlocal resonance model are reported. The role of the rotational excitation of the target molecules is discussed.
Źródło:
Nukleonika; 2003, 48, 2; 109-112
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of Defects in Titanium Created by Hydrogen Charging
Autorzy:
Hruška, P.
Čížek, J.
Knapp, J.
Melikhova, O.
Havela, L.
Mašková, S.
Lukáč, F.
Powiązania:
https://bibliotekanauki.pl/articles/1033958.pdf
Data publikacji:
2017-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
61.72.-y
Opis:
Hydrogen interaction with vacancies in α-Ti was investigated employing positron lifetime spectroscopy combined with ab initio theoretical modeling of vacancy-hydrogen complexes. Ab initio modeling revealed that multiple hydrogen atoms up to 7 can be trapped at vacancies in the α-Ti lattice. Trapped H atoms are located close to the nearest neighbor tetrahedral sites around the centre of vacancy. Lifetimes of positrons trapped at vacancies associated with various numbers of hydrogen atoms were calculated. Positron lifetime measurement of H-loaded α-Ti samples revealed that phase transition into the hydride phase introduced dislocations. Vacancies were created by H loading as well and agglomerated into small vacancy clusters.
Źródło:
Acta Physica Polonica A; 2017, 132, 5; 1606-1610
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Precipitation Effects in Mg-Zn Alloys Studied by Positron Annihilation and Hardness Testing
Autorzy:
Hruška, P.
Čížek, J.
Vlček, M.
Melikhova, O.
Procházka, I.
Powiązania:
https://bibliotekanauki.pl/articles/1196079.pdf
Data publikacji:
2014-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
61.72.J-
Opis:
In the present work positron annihilation spectroscopy combined with Vickers hardness testing were employed in order to investigate precipitation effects in Mg-Zn alloys. It was found that incoherent precipitates of a metastable Zn-rich phase formed in the samples isochronally annealed above 200C cause hardening of the alloy.
Źródło:
Acta Physica Polonica A; 2014, 125, 3; 718-721
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Defects Studies of ZnO Single Crystals Prepared by Various Techniques
Autorzy:
Lukáč, F.
Čížek, J.
Procházka, I.
Melikhova, O.
Anwand, W.
Brauer, G.
Powiązania:
https://bibliotekanauki.pl/articles/1196118.pdf
Data publikacji:
2014-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
61.72.J-
Opis:
The aim of the present work was a comparison of defects in ZnO crystals grown by various techniques available nowadays, namely hydrothermal growth, pressurized melt, Bridgman method growth and vapor phase growth. Positron annihilation spectroscopy was employed as a principal tool for characterization of defects in ZnO crystals grown by above mentioned various techniques. ZnO crystals can be divided into two groups: (i) hydrothermal grown crystals, which exhibit positron lifetime of 179-182 ps and (ii) ZnO crystals grown by the other techniques (pressurized melt, Bridgman method, vapor phase growth) which are characterized by the lower lifetimes falling in the range of 160-173 ps. Comparison of experimental data with ab initio theoretical calculations revealed that HT grown ZnO crystals contains Zn vacancies associated with hydrogen atom in a bond-centered site. On the other hand, ZnO crystals prepared by other techniques contain most probably stacking faults created by stresses induced by temperature gradients in the melt.
Źródło:
Acta Physica Polonica A; 2014, 125, 3; 748-751
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hydrogen-Induced Defects in Palladium
Autorzy:
Melikhova, O.
Čížek, J.
Procházka, I.
Powiązania:
https://bibliotekanauki.pl/articles/1338026.pdf
Data publikacji:
2014-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
61.72.-y
Opis:
In the present work positron annihilation spectroscopy was employed for investigation of hydrogen-induced defects in Pd. Well annealed Pd samples were electrochemically charged with hydrogen and development of defects with increasing hydrogen concentration $x_{H}$ was investigated. At low concentrations (α-phase, $x_{H}$ < 0.017 H/Pd) hydrogen loading introduced vacancies, since absorbed hydrogen segregating at vacancies lowers remarkably the vacancy formation energy. When hydrogen concentration exceeds 0.017 H/Pd, particles of palladium hydride (PdH) are formed. Stress induced by growing PdH particles leads to plastic deformation which generates dislocations and vacancies in the sample.
Źródło:
Acta Physica Polonica A; 2014, 125, 3; 752-755
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Simulation of Positron Annihilation Response to Mechanical Deformation of Nanostructured AgCo
Autorzy:
Melikhova, O.
Kuriplach, J.
Čížek, J.
Procházka, I.
Hou, M.
Pisov, S.
Zhurkin, E.
Powiązania:
https://bibliotekanauki.pl/articles/1812541.pdf
Data publikacji:
2008-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
71.15.Pd
61.46.Hk
Opis:
Nanostructured materials attract nowadays a broad attention due to their specific properties. Defects play an essential role in material properties so their characterisation is very important. The evolution of the various open volume defects in AgCo nanowire modelled samples obtained using molecular dynamics was studied. Isothermal and isoenergetic deformation mechanisms are considered. General analyses of open volume defects concerning their size and their chemical environment were performed. Positron lifetimes, binding energies, and high momentum parts of the momentum distribution of annihilationγ-quanta were calculated for selected defects.
Źródło:
Acta Physica Polonica A; 2008, 113, 5; 1455-1464
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 23

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