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Wyświetlanie 1-15 z 27
Tytuł:
Positron Lifetime Spectroscopy of Nanocrystalline Copper
Autorzy:
C̆ížek, J.
Procházka, I.
Vostrý, P.
Chmelík, F.
Islamgaliev, R. K.
Powiązania:
https://bibliotekanauki.pl/articles/2007957.pdf
Data publikacji:
1999-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
Opis:
Positron lifetime spectroscopy was applied to investigate the thermal stability of nanocrystalline copper prepared by severe plastic torsion deformation. Positrons annihilating in as prepared specimens exhibited free positron component τ$\text{}_{1}$ and two defect components τ$\text{}_{2}$=164 ps and τ$\text{}_{3}$=255 ps. Evolution of the lifetimes and relative intensities of all the three components with increasing annealing temperature during step-by-step isochronal annealing up to 630°C was studied. Behaviour of positrons in nanocrystalline copper could not be interpreted in the frame of conventional 3-state trapping model due to highly inhomogeneous defect distribution. Therefore a modified trapping model was developed and applied to explain the experimental results.
Źródło:
Acta Physica Polonica A; 1999, 95, 4; 487-495
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Use of Energy Summing for Selection of Coincidence Events in Positron-Lifetime Spectroscopy
Autorzy:
Bec̆vár̆, F.
C̆iz̆ek, J.
Procházka, I.
Powiązania:
https://bibliotekanauki.pl/articles/2007883.pdf
Data publikacji:
1999-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
Opis:
A BaF$\text{}_{2}$ positron-lifetime spectrometer equipped with a coincidence system that represents a compromise between the traditional fast-fast and fast-slow arrangements is described. The main difference of the present configuration from both the fast-slow and fast-fast ones consists in use of a sum of the energy signals from the start and stop detectors to select the coincidence events. Quality of the spectrometer response function (≈ 150 ps FWHM for $\text{}^{22}$Na) is very close to that observed for our fast-slow configuration with the equivalent detectors but throughput of the present apparatus is increased almost by a factor of two. Moreover, the electronic scheme becomes less complicated, which has also a positive impact on its cost.
Źródło:
Acta Physica Polonica A; 1999, 95, 4; 448-454
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Concentration of Defects at Grain Boundaries in Sintered Alumina Determined by Positron Annihilation Lifetime Spectroscopy
Autorzy:
Kansy, J.
Si Ahmed, A.
Liebault, J.
Moya, G.
Powiązania:
https://bibliotekanauki.pl/articles/2028969.pdf
Data publikacji:
2001-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
77.84.Bw
61.72.Mm
Opis:
Sintered alumina samples of grain diameters spanning from 1.2 to 4.5μm have been investigated by positron annihilation lifetime spectroscopy. One series of samples was produced from material containing about 150 ppm impurities (mainly SiO$\text{}_{2}$). The second one was made from material having about 2700 ppm of various elements (SiO$\text{}_{2}$, MgO, CaO). Two models of positron trapping at grain boundaries are compared: The first one relates to the diffusion-limited regime; and the other one - to the transition-limited regime of trapping. As a result the relative change of surface concentration of defects at grain boundaries is determined. Additionally, the positron diffusion constant in bulk alumina at room temperature, D$\text{}_{+}$=0.36±10 cm$\text{}^{2}$/s, is estimated.
Źródło:
Acta Physica Polonica A; 2001, 100, 5; 737-742
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Relaxation of Free Volume in Polycarbonate and Polystyrene Studied by Positron Annihilation Lifetime Spectroscopy
Autorzy:
Cangialosi, D.
Wübbenhorst, M.
Schut, H.
Picken, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/2042204.pdf
Data publikacji:
2005-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
82.35.Lr
64.70.Kb
Opis:
We present the time evolution of polycarbonate and polystyrene free volume probed by positron annihilation lifetime spectroscopy, which occurs after thermal rejuvenation above the glass transition temperature (T$\text{}_{g}$) and after plastic deformation via cold rolling. The ortho-positronium (τ$\text{}_{o-Ps}$) lifetime and its intensity (I$\text{}_{o-Ps}$) are used to characterise, respectively, size and concentration of the free volume holes. Our results suggest that the effect of plastic deformation on the polymer microstructure is far different from that of a thermally rejuvenated sample contrarily to common beliefs. In particular, plastic deformation results in an increase inτ$\text{}_{o-Ps}$ and a decrease in I$\text{}_{o-Ps}$, whereas rejuvenation above T$\text{}_{g}$ results in an increase in I$\text{}_{o-Ps}$ whileτ$\text{}_{o-Ps}$ remains unchanged. In addition, physical aging below T$\text{}_{g}$ after plastic deformation manifests as a reduction of τ$\text{}_{o-Ps}$, whereas a decrease in I$\text{}_{o-Ps}$ is observed after thermal rejuvenation. These results corroborate the idea of an amorphous-amorphous transition induced by plastic deformation.
Źródło:
Acta Physica Polonica A; 2005, 107, 4; 690-696
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hydrolytic Degradation of Poly(L-Lactide-co-Glycolide) Studied by Positron Annihilation Lifetime Spectroscopy and Other Techniques
Autorzy:
Pamuła, E.
Dryzek, E.
Dobrzyński, P.
Powiązania:
https://bibliotekanauki.pl/articles/2047148.pdf
Data publikacji:
2006-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
82.35.-x
82.35.Lr
78.70.Bj
61.18.Fs
82.56.Ub
83.85.Jn
68.37.Ps
Opis:
Changes of the poly(L-lactide-co-glycolide) structure as a function of degradation time in phosphate-buffered saline for 7 weeks were investigated by gel permeation chromatography, differential scanning calorimetry, nuclear magnetic resonance ($\text{}^{1}$H NMR), and positron annihilation lifetime spectroscopy. Surface properties as wettability by sessile drop and topography by atomic force microscopy were also characterized. Chain-scission of polyester bonds in hydrolysis reaction causes a quite uniform decrease in molecular weight, and finally results in an increase in semicrystallinity. Molecular composition of the copolymer and water contact angle do not change considerably during degradation time. Atomic force microscopy studies suggest that the copolymer degrades by "in bulk" mechanism. The average size of the molecular-level free volume holes declines considerably after one week of degradation and remains constant till the sixth week of degradation. The free volume fraction decreases as a function of degradation time.
Źródło:
Acta Physica Polonica A; 2006, 110, 5; 631-640
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron Annihilation Lifetime Spectroscopy and Dielectric Measurements of Natural Kaolinite and Kaolinite Intercalated by Potassium Acetate
Autorzy:
Leluk, K.
Orzechowski, K.
Jerie, K.
Baranowski, A.
Słonka, T.
Głowiński, J.
Powiązania:
https://bibliotekanauki.pl/articles/2047141.pdf
Data publikacji:
2006-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
91.60.-x
77.22.-d
78.70.Bj
Opis:
Intercalation of clay minerals consists in inserting of guest molecules into interlayer area. It results in expanding the interlayer distance and changes of physical and chemical properties of the material. Dielectric spectroscopy, positron annihilation lifetime experiments, X-ray, and thermoanalysis were jointly applied to investigate the structural changes accompanying intercalation.
Źródło:
Acta Physica Polonica A; 2006, 110, 5; 621-629
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Free-Volume Studies in Polycaprolactone/Poly(propylene oxide) Urethane/Urea Membranes by Positron Lifetime Spectroscopy
Autorzy:
Ferreira Marques, M.
Gordo, P.
de Lima, A.
Queiroz, D.
Norberta de Pinho, M.
Major, P.
Kajcsos, Zs.
Powiązania:
https://bibliotekanauki.pl/articles/1812490.pdf
Data publikacji:
2008-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.41.+e
78.70.Bj
82.30.Gg
Opis:
Positron annihilation lifetime spectroscopy was used to study the free volume parameters in polypropylene oxide-based tri-isocyanate terminated prepolymer/polycaprolactone diol bi-soft urethane/urea membranes (PU/PCL) with PCL content from 5 up to 25 wt%. Positron annihilation lifetime spectroscopy measurements carried out in the temperature range 298-324 K mirrored the phase separation of the various soft and hard segments present in the membranes. The size and amount of free volume holes determined by positron annihilation lifetime spectroscopy appear to be correlated with the $CO_2$ gas permeability through the membranes.
Źródło:
Acta Physica Polonica A; 2008, 113, 5; 1359-1364
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron annihilation lifetime spectroscopy study of thermal processing and rehydration of dry leek (Allium porrum L.)
Autorzy:
Zaleski, R.
Wawryszczuk, J.
Sobczak, K.
Powiązania:
https://bibliotekanauki.pl/articles/146309.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
positron annihilation
lifetime spectroscopy
food processing
rehydration
leek (Allium porrum L.)
Opis:
New application of positron annihilation lifetime spectroscopy (PALS) to development of food processing techniques is tested. Dehydrated leeks were an object of the study. Three experiments were performed consisting of evacuating air and volatile compounds from the sample, applying thermal treatment and rehydrating the sample. Distinct changes in positron lifetime spectra allowed the monitoring of alterations in the sample structure. The most likely origin of the particular components present in the spectra was able to be proposed from these data. Changes of the components were ascribed to the various processes occurring in the samples.
Źródło:
Nukleonika; 2010, 55, 1; 73-78
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Gas filling of SBA - 15 silica micropores probed by positron annihilation lifetime spectroscopy (PALS)
Autorzy:
Gorgol, M.
Zaleski, R.
Kierys, A.
Powiązania:
https://bibliotekanauki.pl/articles/147961.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
SBA-15 porous silica
positron annihilation
Opis:
Positron annihilation lifetime measurements were conducted in situ while two gasses (nitrogen and oxygen, respectively) were introduced into the SBA-15 porous silica sample. Slow changes in lifetime spectra were observed during a long lasting gas interaction with the sample. Introduced gases slowly filled the free volumes, starting from the smallest ones, especially small micropores. In the presence of a gas, the rate of change of ortho-positronium (o-Ps) and unbound positron intensity was larger than the rate of change of lifetime. This suggests the existence of an additional process, which reduces the number of ortho-positronium atoms due to the interaction with the gas. Moreover, the process of filling pores with gas was slower than the process of emptying them while the gas was pumped out.
Źródło:
Nukleonika; 2013, 58, 1; 229-233
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of neoplastic therapy on the investigated blood using positron annihilation lifetime spectroscopy
Autorzy:
Pietrzak, R.
Borbulak, S.
Szatanik, R.
Powiązania:
https://bibliotekanauki.pl/articles/147997.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
blood
positron annihilation
Opis:
The influence of neoplastic radiotherapy and chemotherapy was investigated using annihilation lifetime spectroscopy in blood types 0 Rh+ -AB Rh+. Changes in the parameters of the longest lived component of the spectrum were analyzed depending on the time between the moment of taking the blood sample from a patient and that of taking measurements, and also the time passing from the cessation of radio- and chemotherapy.
Źródło:
Nukleonika; 2013, 58, 1; 199-202
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ortho-positronium migration in mesopores of MCM-41, MSF and SBA-3
Autorzy:
Zaleski, R.
Błażewicz, A.
Kierys, A.
Powiązania:
https://bibliotekanauki.pl/articles/147955.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
nitrogen adsorption/desorption
porous materials
positron annihilation lifetime spectroscopy (PALS)
positronium migration
Opis:
Three materials: MCM-41, MSF and SBA-3 with a very similar pore diameter but different lengths of cylindrical pores were investigated using the nitrogen sorption method and positron annihilation lifetime spectroscopy. The size of primary pores and interparticle spaces obtained by both methods is similar. However, volume ratios between the discussed kinds of pores found by the above-mentioned methods differ significantly. Such discrepancy is the result of both ortho-positronium migration and the inaccessibility of the pores for nitrogen. Comparing the results of nitrogen sorption and positron annihilation lifetime spectroscopy allows us to estimate that connectivity between the primary pores and the interparticle spaces is the highest in MCM-41 and lowest in SBA-3.
Źródło:
Nukleonika; 2013, 58, 1; 235-240
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
PALS investigation of resorcinol under high pressure
Autorzy:
Tydda, M.
Jasińska, B.
Pieniążek, A.
Powiązania:
https://bibliotekanauki.pl/articles/147999.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
free volume
ortho-positronium (o-Ps)
pressure
positron annihilation lifetime spectroscopy (PALS)
Opis:
Two kinds of measurements were conducted with resorcinol at high pressure : the first one with the use of a mechanical press and the second one with the use of a gaseous compressor. In the second case, due to some gas penetrating the material structure, the lifetime spectra obtained were difficult to analyze. The free volumes in resorcinol were influenced both by high pressure and the gas coming into the crystallographic structure.
Źródło:
Nukleonika; 2013, 58, 1; 195-198
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photoluminescence and positron annihilation lifetime studies on pellets of ZnO nanocrystals
Autorzy:
Karbowski, A.
Fedus, K.
Patyk, J.
Bujak, Ł.
Służewski, K.
Karwasz, G.
Powiązania:
https://bibliotekanauki.pl/articles/148001.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
photoluminescence (PL)
positron annihilation lifetime spectroscopy (PALS)
X-ray diffraction (XRD)
ZnO nanocrystals
Opis:
We explore the interrelationships between the X-ray diffraction patterns, the photoluminescence spectra and the positron lifetimes obtained from circular pellets composed of commercial ZnO nanoparticles. The experimental results are studied as a function of thermal treatment at different temperatures. X-ray diffractograms reveal the temperature- independent wurtzite phase structure of nanocrystals and show huge enlargement of ZnO grains after annealing at temperatures higher than 700 centigrade. Photoluminescence measurements exhibit two emission bands : a near band edge emission in UV (small tilde 378 nm) and a defect-related broad visible peak with a maximum in the green region ( small tilde 502 nm). The significant enhancement of the green emission at the expense of UV luminescence is observed after sample sintering at 800 and 1000 centigrade. The positron annihilation lifetime spectroscopy (PALS) is applied in order to study the thermally induced evolution of defects. The lifetime components show a step-like dependence on the thermal treatment, but do not follow exactly the variation in crystallographic phases and only vaguely follow differences in photoluminescence. The positron data indicate therefore some additional structural and/or defect changes. The possible origin of green luminescence from ZnO pellets is discussed.
Źródło:
Nukleonika; 2013, 58, 1; 189-194
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Porosity structure in photon active glasses
Autorzy:
Jasińska, B.
Śniegocka, M.
Reisfeld, R.
Zigansky, E.
Powiązania:
https://bibliotekanauki.pl/articles/147953.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
glass
ortho-positronium (o-Ps)
porosity
positron annihilation lifetime spectroscopy (PALS)
sol-gel technique
Opis:
Two kinds of photon active glasses were investigated using positron annihilation lifetime spectroscopy (PALS). Both kinds of glasses were prepared using a sol-gel technique, doped by complex of ruthenium tris bipyridyl chloride. Glasses differed from the initial matrix: the first one was prepared using silicon oxide while the second one - zircon oxide. The ortho-positronium (o-Ps) lifetime and intensities were determined from lifetime spectra. Different porosity structure concluded from PALS measurements was found in both cases. In the silica based glasses small free volumes (angstrom size) and pores (from 1 to 10 nm) existed in the material. On the contrary, in zirconia based glasses small intermolecular voids were produced in the structure only, independently of the way of material preparation.
Źródło:
Nukleonika; 2013, 58, 1; 241-244
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Positron Annihilation Lifetime Spectroscopy Study of the Formation of Mesoporous Materials from the Zeolite Precursor
Autorzy:
Bosnar, S.
Bosnar, D.
Gržeta, B.
Powiązania:
https://bibliotekanauki.pl/articles/1196124.pdf
Data publikacji:
2014-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
81.05.Rm
61.43.Gt
Opis:
In this work, positron annihilation lifetime spectroscopy was used for the structural characterisation of porous materials prepared from amorphous zeolite precursors acting as the starting materials and hexadecyltrimethylammonium bromide acting as a mesoporous template. The best fits of the obtained lifetime spectra provide a four-component exponential decomposition. The lifetime values of the long-lived components point to the presence of mesoporous voids. Infrared and X-ray analyses show that the obtained materials consist partly of a crystalline zeolite structure.
Źródło:
Acta Physica Polonica A; 2014, 125, 3; 775-777
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 27

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