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Wyświetlanie 1-15 z 104
Tytuł:
Effect of Acid Dissolution Conditions on Recovery of Valuable Metals from Used Plasma Display Panel Scrap
Autorzy:
Kim, C.- M.
Dharmaiah, P.
Kim, H.-S.
Koo, J.-M.
Yoon, J.-S.
Hong, S.-H.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/355713.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high energy ball milling
waste plasma display panels
dissolution
recovery
Opis:
The objective of this particular study was to recover valuable metals from waste plasma display panels using high energy ball milling with subsequent acid dissolution. Dissolution of milled (PDP) powder was studied in HCl, HNO3, and H2SO4 acidic solutions. The effects of dissolution acid, temperature, time, and PDP scrap powder to acid ratio on the leaching process were investigated and the most favorable conditions were found: (1) valuable metals (In, Ag, Mg) were recovered from PDP powder in a mixture of concentrated hydrochloric acid (HCl:H2O = 50:50); (2) the optimal dissolution temperature and time for the valuable metals were found to be 60°C and 30 min, respectively; (3) the ideal PDP scrap powder to acid solution ratio was found to be 1:10. The proposed method was applied to the recovery of magnesium, silver, and indium with satisfactory results.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1173-1177
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxidation Behavior of Steel with Cr Content and Water Flow Rate
Autorzy:
Kim, D.-J.
Kim, K. M.
Shin, J. H.
Cheong, Y. M.
Lee, E. H.
Lee, G. G.
Kim, S. W.
Kim, H. P.
Choi, M. J.
Lim, Y. S.
Hwang, S. S.
Powiązania:
https://bibliotekanauki.pl/articles/351548.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
steel
flow accelerated corrosion
Cr content
flow rate
surface oxides
Opis:
Fast water flow facilitates ferrous ion transport leading to flow accelerated corrosion (FAC) of carbon steel and the possibility of a large accident through a failure of a secondary pipe in a nuclear power plant. Ion transport is directly linked to oxide properties such as the thickness, chemical composition and porosity. This work deals with a precise observation of the cross section of the corroded specimen focusing on an oxide passivity and its thickness using SEM (scanning electron microscope) and TEM (transmission electron microscope) as well as an apparent weight loss and a surface observation for the specimens corroded using a rotating cylindrical electrode autoclave system in pure water of pH 7 at 150°C having dissolved oxygen below 1 ppb within a flow rate range of 0 to 10 m/s. The Cr content in steel was changed from 0.02 to 2.4 wt%. Increasing the Cr content in the alloy, the FAC rate and oxide thickness decreased. The oxide porosity tends to decrease with the Cr content and immersion time owing to the development of Cr containing oxide. The oxidation behavior is not changed with the immersion time.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1383-1387
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Multistep Heat-Treatment Effects on Electrospun Nd-Fe-B-O Nanofibers
Autorzy:
Jeon, E. J.
Eom, N. S. A.
Lee, J.
Lee, B.
Cho, H. M.
On, J. S.
Choa, Y.-H
Kim, B. S.
Powiązania:
https://bibliotekanauki.pl/articles/354311.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd-Fe-B
nanofibers
electrospinning
heat treatment
Opis:
Neodymium-Iron-Boron (Nd-Fe-B) magnets are considered to have the highest energy density, and their applications include electric motors, generators, hard disc drives, and MRI. It is well known that a fiber structure with a high aspect ratio and the large specific surface area has the potential to overcome the limitations, such as inhomogeneous structures and the difficulty in alignment of easy axis, associated with such magnets obtained by conventional methods. I n this work, a suitable heat-treatment procedure based on single-step and multistep treatments to synthesize sound electrospun Nd-Fe-B-O nanofibers of Φ572 nm was investigated. The single-step heat-treated (directly heat-treated at 800°C for 2 h in air) samples disintegrated along with the residual organic compounds, whereas the multistep heat-treated (sequential three-step heat-treated including three steps;: dehydration (250°C for 30 min in an inert atmosphere), debinding (650°C for 30 min in air), and calcination (800°C for 1 h in air)) fibers maintained sound fibrous morphology without any organic impurities. They could maintain such fibrous morphologies during the dehydration and debinding steps because of the relatively low internal pressures of water vapor and polymer, respectively. In addition, the NdFeO3 alloying phase was dominant in the multistep heat-treated fibers due to the removal of barriers to mass transfer in the interparticles.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1433-1437
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrical Conductivity and Morphology Study of Polyaniline Powder Synthesised with Various Doping Ions
Autorzy:
Golba, S.
Popczyk, M.
Miga, S.
Jurek-Suliga, J.
Zubko, M.
Powiązania:
https://bibliotekanauki.pl/articles/351230.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
polyaniline
conductive polymers
conductivity
morphology
Opis:
Powdered polyaniline (PANI) was synthesised chemically with different doping anions namely hydrochloric acid, sulphuric acid and para-toluenesulfonic acid (pTSA). Two-step synthetic procedure was utilised at low temperature. The highest reaction efficiency was found for chlorine-doped PANI. Structural characterization with FTIR revealed the vibration bands characteristicto formation of the emeraldine salt. The surface morphology of doped PANIs was studied by SEM images which showed near globular shape and porous structures with different size of the aggregated particles. They were smaller for Cl-- or pTS--doped PANI while for SO4 2- the size was markedly larger. The XRD patterns revealed that there are ordered regions especially for pTS- doped PANI, while the highest conductivity value was recorded for Cl- doped one followed by organic pTS- doped and SO4 2- doped one.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 1023-1028
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of High-Strength Gray Cast Iron Using Permanent Magnet Scrap
Autorzy:
Park, S.-Y.
Kim, J. H.
Seo, S. J.
On, J. S.
Lim, K. M.
Powiązania:
https://bibliotekanauki.pl/articles/352204.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gray cast iron
rare earth element
Nd-Fe-B magnet scrap
graphite formation
microstructure
Opis:
In this study, we have developed the manufacturing technology for high strength gray cast irons by using the spent permanent magnet scraps. The cast specimen inoculated by using a spent magnet scraps showed the excellent tensile strength up to 306MPa. This tensile strength value is 50MPa higher than that of the specimen cast without inoculation, and is similar to that of the specimen inoculated by using the expensive misch-metal. These superior mechanical properties are attributed to complex sulfides created during solidification that promote the formation and growth of Type-A graphite. It is therefore concluded that spent magnets scrap can provide an efficient and cost-effective inoculation agent for the fabrication of high-performance gray cast iron.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1113-1117
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Physical Simulation of Individual Heat-Affected Zones in S960MC Steel
Autorzy:
Mičian, M.
Winczek, J.
Harmaniak, R.
Koňár, R.
Gucwa, M.
Moravec, J.
Powiązania:
https://bibliotekanauki.pl/articles/2049636.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
mechanical properties of heat affected zone
steel S960MC
physical simulation
Gleeble 3500
Opis:
This research is focused on the analysis of heat-affected sub-zones in 2 mm thick steel S960MC samples, with the aim of observing and evaluating the mechanical properties after exposure to temperatures corresponding to individual heat-affected sub-zones. Test samples were prepared using a Gleeble 3500 thermo-mechanical simulator. The samples were heated in the range from 550°C to 1350°C and were subsequently quickly cooled. The specimens, together with the base material, were then subjected to tensile testing, impact testing, and micro-hardness measurements in the sample cross-section, as well as evaluation of their microstructure. Fracture surfaces are investigated in samples after impact testing. The heat-affected sub-zones studied indicate high sensitivity to the thermal input of welding. There is a significant decrease in tensile strength and yield strength at temperatures around 550°C.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 1; 81-89
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of Grain Boundary Morphologies on Stress Corrosion Cracking of Alloy 600
Autorzy:
Kim, H. P.
Choi, M. J.
Kim, S. W.
Kim, D. J.
Lim, Y. S.
Hwang, S. S.
Powiązania:
https://bibliotekanauki.pl/articles/352569.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
alloy 600
NaOH
stress corrosion cracking
grain boundary morphologies
Opis:
Effects of grain boundary morphologies on stress corrosion cracking (SCC) of Alloy 600 have been studied in 40% NaOH at 315°C using C-ring specimens. The configuration of the grain boundary and the intergranular carbide density were controlled by heat treatment. SCC tests were performed at +150 mV above the corrosion potential. The specimen with a serrated grain boundary showed higher SCC resistance than that with a straight grain boundary. This appears to be caused by the fact that the specimen with the serrated grain boundary has longer SCC path. SCC resistance also increased with intergranular carbide density probably due to enhanced relaxation of stress at intergranular carbide.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1415-1419
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Impact of Composition and the Densification Level of Furan Molding Compounds on the Strength of Large-Size Casting Molds
Autorzy:
Petrus, Ł.
Bulanowski, A.
Kołakowski, J.
Urbanowicz, M.
Sobieraj, J.
Jelonek, M.
Brzeżański, M.
Zych, J. S.
Janerka, K.
Powiązania:
https://bibliotekanauki.pl/articles/356951.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
molding sand
adhesive
densification
properties molding sand
Opis:
The paper presents the test results of molding compounds, sand casting molds and their analysis. The subject of testing was compound containing furan resins prepared according to the following recipe: matrix – regenerate 90% + fresh sand – 10%, furanresin – 1.10% by weight, hardener – 0.40% by weight. The impact of adhesive type and its quantity (Quan = 0.90, 1.1 and 1.5%) on the strength indexes of molding compound subject to densification was analyzed. The publication presents the test results: tensile strength Rm, compressive strength Rc and flexural strength Rg, as well as compound permeability as function of its density. The analysis also covers the impact of density level on mold strength and the distribution of density level along the mold height. Based on the test results, it was found that the best method to obtain high strength molds made from compounds with chemical adhesives was to densify it by vibrating the system: match plate – molding flask – compound filling the mold. The effectiveness of this densification method depends on the amplitude and frequency of vibrations.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 4; 1431-1436
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Additives on the Densification Processes and Properties of Silica-Based CMCs
Autorzy:
Ko, S.-Y.
Yong, S.-M.
Lee, S. J.
Cheong, D.-I.
Baek, S.
Powiązania:
https://bibliotekanauki.pl/articles/355134.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ceramic matrix composite
CMC
silica
densification
mechanical properties
Opis:
The effect of additives on the densification behavior and mechanical properties of pure and additive (Zr, B and Mg)-added silica ceramics were investigated for their application to the matrix phase of a silica fiber reinforced silica (SiO2 /SiO2f ) composite. The additives affected the rate of densification and crystallization (or transformation) of the amorphous silica. Among the compositions, pure silica ceramics sintered at 900°C for 1h showed the maximum flexural strength. Based on the results, SiO2 /SiO2f was fabricated by a repeated vacuum-assisted infiltration method followed by the heat treatment at 900°C for 1h. The relative density of the composite was 78.2% with a flexural strength of 22.4 MPa. Fractography revealed that the composite was damaged by strong bonding at the fiber/matrix interface and the fracture of fiber.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1485-1488
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of AZ31/CNT Surface Nano-composite by Double-pass Friction Stir Processing
Autorzy:
Kim, J. Y.
Hwang, J.-W.
Kim, H. Y.
Lee, S. M.
Jung, W.-S.
Byeon, J.-W.
Powiązania:
https://bibliotekanauki.pl/articles/355624.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
surface modification
Double-pass Friction Stir Processing
AZ31
composite
CNT
Opis:
Double-pass Friction Stir Processing (FSP) was applied to fabricate an AZ31/CNT nano-composite for surface hardening of lightweight structural components. The effects of double-pass FSP as well as groove depth (i.e., volume fraction of CNT) on the CNT distribution, dynamically recrystallized grain size, and resulting microhardness were studied. Double-pass FSP was performed for the CNT-filled plate-type specimen with different groove depths of 2, 3, and 4 mm. By applying double-pass FSP, the average size of CNT clusters decreased, implying a more homogeneous distribution. Compared with the FSPed specimen without CNT, grain size was refined from 19 μm to 3 μm and microhardness increased from 52 Hv to 83 Hv (i.e., 71% increase).
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1039-1042
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermal Diffusion of 57Co into Rh Foil for Preparing Mössbauer Source
Autorzy:
Uhm, Y. R.
Kim, J. J.
Choi, S. M.
Son, K. J.
Powiązania:
https://bibliotekanauki.pl/articles/352775.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mössbauer source
diffusion
electroplating
57Co/Rh
Opis:
To establish the coating conditions for 57 Co, non-radioactive Co ions are dissolved in an acid solution and electroplated on to a rhodium plate. The thermal diffusion of electroplated Co into a rhodium matrix was studied to apply a 57 Co Mössbauer source. The procedure to form a Co deposited onto Rh foil was established using two different electroplating baths: the acid-based buffer (pH 3) containing boric acid, sodium chloride, and saccharin, and the alkaline-based buffer (pH 10) containing hydrazine hydrate and ammonium citrate. The influence of different annealing conditions was investigated. From the results, the best diffusion degree of electrodeposited Co onto the rhodium matrix was obtained in an annealing process performed at 1100°C for 3 h in vacuum over 10-5 hPa.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1249-1252
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development of Hydrophobic Surgical Forceps using Powder Injection Molding and Surface Treatment
Autorzy:
Park, D. Y.
Park, B. R.
Gal, C. W.
Lin, D.
Han, J. S.
Jeong, M.-S.
Bollina, R.
Hwang, W.
Park, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/352093.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powder injection molding
hydrophobic
debinding
sintering
surface treatment
Opis:
Hydrophobic surgical forceps of end-effectors for laparoscopic operations or minimally invasive surgery were developed through powder injection molding (PIM) and surface treatment. Processing conditions for mixing, debinding, and sintering were investigated to produce defect-free components. An optimum solid loading was determined by torque rheometry experiments. The optimized processing conditions for debinding and sintering were designed through the measurement of weight loss and shrinkage behavior by thermogravimetric analysis and dilatometry experiments. After producing the surgical forceps based on the optimized processing conditions via PIM, surface treatment was carried out to generate the hydrophobic structure on the surface.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 473-480
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of the Thermal and Magnetic Properties of Amorphous Fe61Co10Zr2.5Hf2.5Me2W2B20 (Where Me = Mo, Nb, Ni Or Y) Ribbons
Autorzy:
Gruszka, K.
Nabiałek, M.
Szota, M.
Bloch, K.
Gondro, J.
Pietrusiewicz, P.
Sandu, A. V.
Mustafa Al Bakri, A. M.
Walters, K.
Walters, S.
Garus, S.
Dośpiał, M.
Mizera, J.
Powiązania:
https://bibliotekanauki.pl/articles/355886.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
thermal stability
magnetic properties
Opis:
The paper presents the results of structural and magnetic properties and thermal stability for a group of functional materials based on Fe61Co10Zr2.5Hf2.5Me2W2B20 (where Me = Mo, Nb, Ni or Y). Samples were obtained in the form of ribbons using melt-spinning method. The X-ray diffraction patterns of investigated samples confirmed their amorphous structure. Based on the analysis of DSC curves characteristic temperatures: glass forming temperature (Tg), crystallization temperature (Tx) and temperature range of the supercooled liquid ΔTx were determined. Small addition of transition metals elements has strong influence on magnetic and thermal parameters of studied materials. The comprehensive studies revealed that in terms of magnetic properties the Ni-addition resulted in highest reduction in coercivity and anisotropy field.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 641-644
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Shot Peening With Glass Microspheres on the Fatigue Behavior of a Low Carbon Steel
Autorzy:
de Lacerda, J. C.
Pereira, I. R.
Costa, J. M. G.
Pinto, J. S.
Souza, H. F. M.
Fonseca, M. A.
Powiązania:
https://bibliotekanauki.pl/articles/352156.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
fatigue
shot peening
Wöhler curve
low carbon steel
glass microspheres
Opis:
The present work has the objective of studying the effect of shot peening with glass microspheres on SAE 1020 steel in its resistance to fatigue. Fatigue tests were carried out by rotary bending with load control and loading on balance in specimens with and without shot peening. A rotation speed of approximately 750 rpm (12.5 Hz) was employed in the fatigue tests. Vickers microhardness tests were performed in order to verify the surface hardening produced by shot peening with glass microspheres. Analysis of the steel surface and fatigue fractures was performed using scanning electron microscopy (SEM). Fatigue tests were performed in order to obtain S-N curves (Wöhler curves). It was observed that shot peening with glass microspheres improved the fatigue strength of the steel at high cycle.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1513-1518
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Milling Time Parameter on the Microstructure and the Thermoelectric Properties of n-Type Bi2Te2.7Se0.3 Alloys
Autorzy:
Sharief, P.
Madavali, B.
Koo, J. M.
Kim, H. J.
Hong, S.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/354418.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
milling time
microstructure
thermoelectric properties
ZT
Opis:
Nanostructured thermoelectric materials receiving great attention for its high thermoelectric performance. In this research, nanostructured n-type Bi2 Te2.7 Se0.3 alloys have prepared using high energy ball milling and followed by spark plasma sintering. Also, we have varied ball milling time to investigate milling time parameter on the thermoelectric properties of n-type Bi2 Te2.7 Se0.3 powder. The powders were discrete at 10 min milling and later particles tend to agglomerate at higher milling time due to cold welding. The bulk fracture surface display multi-scale grains where small grains intersperse in between large grains. The maximum Seebeck coefficient value was obtained at 20-min milling time due to their lower carrier density. The κ values were decreased with increasing milling time due to the decreasing trend observed in their κL values. The highest ZT of 0.7 at 350 K was observed for 30-min milling time which was ascribed to its lower thermal conductivity. The Vickers hardness values also greatly improved due to their fine microstructure.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 585-590
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 104

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