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Tytuł:
Effect of Surfactant Types on the Size of Tin Oxide Nanoparticles
Autorzy:
Boran, F.
Çetinkaya, S.
Şahin, M.
Powiązania:
https://bibliotekanauki.pl/articles/1031632.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
nanoparticle
tin oxide
surfactant
Opis:
In this study, tin oxide (SnO₂) nanoparticles were synthesized by hydrothermal method in the presence of hydrazine and ammonia by adding surfactant for 12 h in a Teflon autoclave at 100°C reaction temperature. Tin(II) chloride hydrate as an inorganic precursor, hexadecyl trimethyl ammonium bromide (CTAB), and tetrapropyl ammonium bromide (TPAB) as cationic, and sodium dodecyl sulfonate (SDS) as anionic surfactants were used. The results showed that the size and shape of nanoparticles depended on the surfactant types. The nanoparticles sizes between 17.5 and 19.7 nm were obtained by changing types of surfactants. Synthesized tin oxide nanoparticles were characterized by field emission scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and the Fourier transform infrared spectroscopy.
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 546-548
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Parameter Characterization in Processing of Silver - Aluminum Based Electrical Contact Materials
Autorzy:
Praveen Kumar, S.
Parameshwaran, R.
Ananthi, A.
Jenil Jaba Sam, J.
Powiązania:
https://bibliotekanauki.pl/articles/352711.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrical contactor
silver
aluminum
tin oxide
conduction
Opis:
An electrical contractor is one which plays significant role in day todays life in industries as well as in home appliances. In current scenario the materials for conducting purpose has an overwhelming research capability. Now a day the silver based electrical contact composite material have provided the potential applications in aerospace and automobile industries. Among silver based contact material the silver cadmium oxide and silver tin oxide plays a vital role in fabrication of electrical contactors. In this research an attempt has been made to study the influence of adding Aluminum with silver based electrical contact composite materials by two different processing routes namely stir-casting and powder metallurgy. Silver and aluminum matrix plays a virtual role in composite world owing to their highest conductivity. Optimum parameters were identified for attaining the maximum properties such as conductivity, hardness, density, and porosity of composition. By this better conducting property and mechanical property of the electrical contact can be improved by this system. Thus a screening test has be conducted with addition of Al with silver tin oxide compositions hence this paper aims to process the aluminum – silver based electrical contact materials by stir casting processing and powder metallurgy route and compare the results obtained.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 3; 1895-1901
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of a Novel Silver-Based Electrical Contact Composites and Assessment of Its Mechanical and Electrical Properties
Autorzy:
Kumar, Praveen S.
Senthil, S. M.
Parameshwaran, Rathinasamy
Rathanasamy, Rajasekar
Powiązania:
https://bibliotekanauki.pl/articles/2049131.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silver tin oxide
electrical contact
composites
tungsten oxide
conductivity
Opis:
The electrical contactors play a crucial role in closing the circuit in many power distribution components like overhead lines, underground cables, circuit breakers, transformers, and control systems. The failure in these components mainly occurs due to the break-down of contactors due to the continuous opening and closing action of contacts. Silver (Ag)-based oxide contact materials are widely used in practice, among which silver tin oxide (AgSnO2) is most common. An attempt is made in increasing the performance of AgSnO2, by adding Tungsten Oxide (WO3) in various weight proportions, thus finding the optimal proportion of AgSnO2WO3 to have increased mechanical and electrical performances. All the composite samples are fabricated in-house using powder metallurgy process. The assessment of physical and electrical properties namely, density, hardness, porosity, and electrical conductivity, showed that 90%Ag-8.5%SnO2-1.5%WO3 composite yielded superior results. With help of morphological tests, wear characteristics are also investigated, which showed that 90%Ag-8.5%SnO2-1.5%WO2 composite has a wear coefficient of 0.000227 and a coefficient of friction of 0.174 at an optimized load of 10 N and sliding velocity of 0.5 mm/s.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 4; 1087-1094
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods
Autorzy:
Matysiak, W.
Tański, T.
Smok, W.
Polishchuk, O.
Powiązania:
https://bibliotekanauki.pl/articles/351688.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
thin films
nanofibers
tin oxide
electrospinning
optical properties
Opis:
The aim of this work was to produce a thin SnO2 film by a technique combining the sol-gel method and electrospinning from a solution based on polyvinylpyrrolidone and a tin chloride pentahydrate as a precursor. The spinning solution was subjected to an electrospinning process, and then the obtained nanofiber mats were calcined for 10 h at 500°C. Then, the scanning electron microscopy morphology analysis and chemical composition analysis by X-ray microanalysis of the manufactured thin film was performed. It was shown that an amorphous-crystalline layer formed by the SnO2 nanofiber network was obtained. Based on the UV-Vis spectrum, the width of the energy gap of the obtained layer was determined.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 761-765
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrical Characteristics of Tin Oxide Films Grown by Thermal Atomic Layer Deposition
Autorzy:
Yoon, Seong Yu
Choi, Byung Joon
Powiązania:
https://bibliotekanauki.pl/articles/352926.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
atomic layer deposition
tin oxide
electrical property
oxygen adsorption
Opis:
Tin dioxide (SnO2 ) is an n-type semiconductor and has useful characteristics of high transmittance, excellent electrical properties, and chemical stability. Accordingly, it is widely used in a variety of fields, such as a gas sensor, photocatalyst, optoelectronics, and solar cell. In this study, SnO2 films are deposited by thermal atomic layer deposition (ALD) at 180°C using Tetrakis(dimethylamino)tin and water. A couple of 5.9, 7.4 and 10.1nm-thick SnO2 films are grown on SiO2 /Si substrate and then each film is annealed at 400°C in oxygen atmosphere. Current transport of SnO2 films are analyzed by measuring current – voltage characteristics from room temperature to 150°C. It is concluded that electrical property of SnO2 film is concurrently affected by its semiconducting nature and oxidative adsorption on the surface.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 3; 1041-1044
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evaluation of electrical resistivity, residual stress and surface roughness of sputtering indium tin oxide films with different thicknesses
Autorzy:
Tien, Chuen-Lin
Lin, Tsai-Wei
Su, Shu-Hui
Powiązania:
https://bibliotekanauki.pl/articles/2033888.pdf
Data publikacji:
2021
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
indium tin oxide
magnetron sputtering
residual stress
surface roughness
Opis:
This paper investigates the influence of film thickness on the electrical and mechanical properties of transparent indium tin oxide (ITO) thin films. Two groups of ITO thin films deposited on unheated substrates were prepared by the radio-frequency magnetron sputtering technique. The biaxial residual stress and surface roughness for two groups of ITO thin films were measured by a Twyman–Green interferometer and a Linnik microscopic interferometer, respectively. The electrical resistivity of the ITO films was measured by a four-point probe apparatus, the thickness was determined mechanically with a profilometer. The measurement results show that the average resistivity of ITO thin films decreases with increasing the deposited thickness. The compressive residual stress in the ITO thin films decreases with increasing the deposited thickness. We also find that an anisotropic stress in the two groups of ITO films is more compressive in a certain direction. The RMS surface roughness in the two groups of ITO films is less than 1 nm.
Źródło:
Optica Applicata; 2021, 51, 4; 499-512
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fluorine-Doped SnO2 Thin Films in Solar Cell Applications. Morphological, Optical and Electrical Properties
Autorzy:
Lisnic, Petru
Hrostea, Laura
Leontie, Liviu
Girtan, Mihaela
Powiązania:
https://bibliotekanauki.pl/articles/27313873.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czasopisma i Monografie PAN
Tematy:
fluorine tin oxide
FTO
thin films
spray pyrolysis
solar cells
Opis:
This study examines the optimal parameters for obtaining fluorine-doped SnO2 (FTO) films with promising potential for photovoltaic applications. Due to its properties, tin oxide is used in a wide range of technologies, among which the manufacture of solar cells is one of the most important. Being doped with fluorine, tin dioxide becomes a good transparent and conductive electrode, suitable for solar cell applications. The chemical stability and low cost of the doped SnO2 makes it an advantageous alternative to tin-doped indium oxide (ITO). Among the most important characteristics of FTO thin films are high photoconductivity under sunlight irradiation and strong UV absorption. The SnO2 compound, doped with fluorine, exhibits a considerable chemical and physical stability, good electrical conductivity and high transmission (over 85%) in the visible range. The spray pyrolysis technique is the most preferable and efficient deposition method of fluorine-doped SnO2 thin films. This work aims to identify the optimal parameters for the spray pyrolysis of SnO2:F films and to analyze the morphology, transparency and strength of as obtained films in relation to the doping amount in the precursor solution, spraying distance and film thickness.
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 2; 483--490
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Joining Of Green Body And Dense Substrate For Indium Tin Oxide Under Uniaxial Pressure In An Open Condition
Łączenie zielonej masy i gęstego podłoża z tlenku cyny indu w warunkach jednoosiowego ściskania w stanie otwartym
Autorzy:
Moon, G.-S.
Chung, T.-J.
Yang, S. H.
Hong, G.-S.
Oh, K.-S.
Powiązania:
https://bibliotekanauki.pl/articles/355654.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
transparent conducting oxide
indium tin oxide
green body
joining
tlenek indu
zielona masa
łączenie
Opis:
The green body and dense substrate of indium tin oxide was joined by uniaxially pressing at 0.3 MPa at 1300°C to test the restoring of the eroded part of transparent conducting oxide target. The green body was sintered to 98% of theoretical density under the suppression of shrinkage along the boundary below 5%. The boundary between two parts was free of pore but could be recognized from the difference in grain sizes. The joined part had the virtually same density with the substrate, but the grain size was less than one fifth compared with that of substrate.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1209-1212
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Temperature Effect on the Growth Rate and Physical Characteristics of SnO2 Thin Films Grown by Atomic Layer Deposition
Autorzy:
Kim, D.
Kim, D. H.
Riu, D.-H.
Choi, B. J.
Powiązania:
https://bibliotekanauki.pl/articles/353808.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
atomic layer deposition
tin oxide
growth rate
film density
optical band gap
Opis:
Among the various thin film coating techniques, atomic layer deposition (ALD) has features of good controllability of the thickness, excellent step-coverage in 3-dimensional object even in the sub-nm thickness range at the relatively low deposition temperature. In this study, SnO2 thin films were grown by ALD in the variation of substrate temperatures from 150 to 250°C. Even such a low temperature may influence on the growth kinetics of the ALD reaction and thus the physical characteristics of thin films, such as crystallinity, film density and optical band gap, etc. We observed the decrease of the growth rate with increasing substrate temperature, at the same time, the density of the film was decreased with increasing temperature. Steric hindrance effect of the precursor molecule was attributed to the inverse relationship of the growth temperature and growth rate as well as the film density. Optical indirect band gap energy (~3.6 eV) of the ALD-grown amorphous SnO2 films grown at 150°C was similar with that of the literature value, while slightly lower band gap energy (~3.4 eV) was acquired at the films grown at higher temperature.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1061-1064
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sieciowanie kauczuku chloroprenowego tlenkiem cyny
Tin oxide cross-linking of chloroprene rubber
Autorzy:
Smejda-Krzewicka, A.
Rzymski, W. M.
Kowalski, D.
Powiązania:
https://bibliotekanauki.pl/articles/947344.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
kauczuk chloroprenowy
sieciowanie
tlenek cyny
palność
chloroprene rubber
cross-linking
tin oxide
flammability
Opis:
Przedstawiono nową metodę sieciowania kauczuku chloroprenowego (CR) za pomocą tlenku cyny (SnO). Najlepsze właściwości mechaniczne wykazały wulkanizaty usieciowane tlenkiem cyny w ilości 1—2 cz. mas./100 cz. mas. CR (phr), tj. zdecydowanie mniejszej niż ilości ZnO i MgO użyte do standardowego sieciowania CR. Stwierdzono, że wytrzymałość na rozciąganie wulkanizatu CR usieciowanego tlenkiem cyny jest większa niż wulkanizatu CR usieciowanego standardowo. Oznaczone wartości objętościowego pęcznienia równowagowego i stałych elastyczności świadczą o obecności większej liczby wiązań intermolekularnych. Wykazano, że wprowadzenie do mieszanki kauczukowej krzemionki lub sadzy zwiększyło wytrzymałość na rozciąganie wulkanizatu usieciowanego za pomocą 1 phr SnO, natomiast dodanie kaolinu — nieznacznie pogorszyło właściwości mechaniczne wulkanizatów, jednak wyraźnie zmniejszyło ich palność, o czym świadczy większa wartość wskaźnika tlenowego (OI).
A new method of cross-linking chloroprene rubber (CR) with tin oxide (SnO) is presented. From the viewpoint of the mechanical properties, the optimal SnO contentis between 1 and 2 phr of CR (Table 1, Fig. 1), i.e. definitely less than the amount of ZnO and MgO typically used in CR cross-linking. CR vulcanizate cured with tin oxide demonstrates significantly higher tensile strength than CR cross-linked using a conventional mixture of ZnO and MgO. The determined values of equilibrium volume swelling and Mooney-Rivlin elasticity constants indicate a greater number of intermolecular cross-links. It was found that the incorporation of silica or carbon black into CR leads to an increase in the tensile strength of the vulcanizate crosslinked with 1 phr SnO (Table 2). Although the addition of kaolin to CR cured with SnO results in a slight decrease in the mechanical properties of vulcanizates, it causes a marked reduction of their flammability, as indicated by increase in the oxygen index value (Fig. 2).
Źródło:
Polimery; 2015, 60, 3; 186-191
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of morphology and optical properties of SnO₂ nanowires prepared by electrospinning
Autorzy:
Tański, Tomasz
Smok, Weronika
Matysiak, Wiktor
Powiązania:
https://bibliotekanauki.pl/articles/2090673.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nanowires
nanofibers
electrospinning
tin oxide
optical properties
nanodruty
nanowłókna
elektroprzędzenie
tlenek cyny
właściwości optyczne
Opis:
The growing interest in one-dimensional tin oxide-based nanomaterials boosts research on both high-quality nanomaterials as well as production methods. This is due to the fact that they present unique electrical and optical properties that enable their application in various (opto)electronic devices. Thus, the aim of the paper was to produce ceramic SnO₂ nanowires using electrospinning with the calcination method, and to investigate the influence of the calcination temperature on the morphology, structure and optical properties of the obtained material. A scanning electron microscope (SEM) and Fourier-transform infrared spectroscopy (FTIR) were used to examine the morphology and chemical structure of obtained nanomaterials. The optical properties of manufactured one-dimensional nanostructures were investigated using UV-Vis spectroscopy. Moreover, based on the UV-Vis spectra, the energy band gap of the prepared nanowires was determined. The analysis of the morphology of the obtained nanowires showed that both the concentration of the precursor in the spinning solution and the calcination temperature have a significant impact on the diameter of the nanowires and, consequently, on their optical properties.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2021, 69, 5; e137507, 1--8
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Optoelectronic properties of Fluoride tin oxides/porous silicon/p-Silicon heterojunction
Autorzy:
Hadi, H. A.
Powiązania:
https://bibliotekanauki.pl/articles/411926.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
porous silicon
electrochemical etching
spray pyrolysis
fluoride-doped tin oxide film
nanostructures
SEM
AFM
photodetector
Opis:
In this paper, formation of a nanostructure semi transparence fluoride tin oxides (FTO) by spray pyrolysis technique on porous silicon PS layer. Porous silicon PS layer was prepared by anodization of p-type silicon wafers to fabricate of the UV- Visible Fluoride-doped tin oxide /Porous silicon /p-Si heterojunction photodetector. Optical properties of FTO thin films were measured. The optical band gap of 3.77 eV for SnO2 : F for film was deduced. From (I-V) and (C-V) measurements, the barrier ØB height for FTO/PS diode was of 0.77, and the built in voltage Vbi, which was of 0.95 V. External quantum efficiency was 55 % at 500 nm which corresponding to peak responsivity of 1.15 A/W at 1 V bias. The PS band gap in the vicinity of PS/c-Si heterojunction was 1.38 eV.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 17, 2; 142-152
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preliminary studies on hydrometallurgical tin recovery from waste of tin stripping of copper wires
Wstępne badania hydrometalurgicznego odzysku cyny z odpadów procesu odcynowania drutów miedzianych
Autorzy:
Rudnik, E.
Wincek, D.
Powiązania:
https://bibliotekanauki.pl/articles/263862.pdf
Data publikacji:
2017
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
electrolysis
leaching
tin
tin(IV) oxide
waste
elektroliza
ługowanie
cyna
cyna(IV)
odpady
Opis:
This paper presents the results of tin leaching and electrowinning from SnO2 waste originating from the industrial process of tin stripping of copper wires. The sludge was leached by acids (sulfuric, hydrochloric, tartaric, oxalic) and sodium hydroxide at various temperatures (40–80°C). The highest efficiency of tin leaching (12–18%) was obtained in an oxalic solution, while the lowest effectiveness (0.2–0.5%) was found for sulfuric acid. Tin leaching was accompanied by a transfer of copper residues to the solution. The electrowinning stage was realized under potentiostatic and galvanostatic conditions using oxalate solutions. Cyclic voltammetry was applied to select the potentials for the selective deposition of metals.
W artykule przedstawiono wyniki uzyskane w trakcie ługowania i elektrolitycznego odzysku cyny z odpadów SnO2 pochodzących z przemysłowego procesu usuwania cyny z drutów miedzianych. Szlam ługowano w roztworach kwasów (siarkowego, solnego, winowego, szczawiowego) i wodorotlenku sodu, w różnych temperaturach (40–80°C). Najwyższą skuteczność ługowania cyny (12–18%) otrzymano w roztworze szczawianowym, podczas gdy najniższą wydajność (0,2–0,5%) stwierdzono w przypadku kwasu siarkowego. Ługowaniu cyny towarzyszyło przejście pozostałości miedzi do roztworu. Elektrolityczny odzysk metali został zrealizowany w warunkach potencjostatycznych i galwanostatycznych z zastosowaniem roztworu szczawianowego. Warunki potencjałowe selektywnego osadzania metali wytypowano, opierając się na badaniach metodą woltamperometrii cyklicznej.
Źródło:
Metallurgy and Foundry Engineering; 2017, 43, 1; 7-20
1230-2325
2300-8377
Pojawia się w:
Metallurgy and Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Review on metallic oxide nanoparticles and their application in optoelectronic devices
Autorzy:
Sosna-Głębska, Aleksandra
Szczecińska, Natalia
Znajdek, Katarzyna
Sibiński, Maciej
Powiązania:
https://bibliotekanauki.pl/articles/105973.pdf
Data publikacji:
2019
Wydawca:
Centrum Badań i Innowacji Pro-Akademia
Tematy:
metallic oxide
nanoparticles
ZnO
TiO2
Indium-Tin Oxide
ITO
solar cell
tlenek metalu
nanocząstki
tlenek cynku
dwutlenek tytanu
tlenek indowo-cynowy
ogniwo słoneczne
Opis:
Among the large family of metallic oxides, there is a considerable group possessing excellent semiconducting properties. What follows, they are promising materials for applications in the field of optoelectronics and photonics. Thanks to the development of nanotechnology in the last few decades, it is now possible to manufacture a great variety of different nanostructures. By controlling their size, shape, composition and crystallinity, one can influence such properties as band gap, absorption properties, surface to volume ratio, conductivity, and, as a consequence, tune the material for the chosen application. The following article reviews the research conducted in the field of application of the metallic oxide nanoparticles, especially ZnO, TiO2 and ITO (Indium-Tin Oxide), in such branches of optoelectronics as solid-state lightning, photodetectors, solar-cells and transparent conducting layers.
Źródło:
Acta Innovations; 2019, 30; 5-15
2300-5599
Pojawia się w:
Acta Innovations
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The effect of fluorine and tungsten co-doping on optical, electrical and structural properties of tin (IV) oxide thin films prepared by sol–gel spin coating method
Autorzy:
Keskenler, E F
Turgut, G
Aydin, S.
Dogan, S
Duzgun, B
Powiązania:
https://bibliotekanauki.pl/articles/175016.pdf
Data publikacji:
2013
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
tin (IV) oxide (SnO2)
fluorine (F) and tungsten (W) co-doping
sol-gel
Opis:
Fluorine and tungsten co-doped tin (IV) oxide (WFTO) thin films have been prepared first time by a sol–gel spin coating method. The effect of F and W co-dopant ratio on optical, electrical and structural properties of SnO2 was investigated. It was found that the optical properties of the films were obviously affected by the co-dopant ratio. When the F:W co-dopant ratio increases from 0.25:0.25 to 0.75:0.50, the transmittance in the short wavelengths slightly increases and transmittance edge shifts towards shorter wavelength. With an increase in the co-dopant ratio, the reduction and red shifts in the optical transmittance edge are very obvious at all wavelengths. Transmittance values at 550 nm for the films have varied between 79.64% and 50.20%. The indirect and direct band gap values for WFTO-1, WFTO-2, WFTO-3 and WFTO-4 samples were calculated to be 3.73, 3.79, 3.48, 3.40 eV and 4.03, 4.04, 3.98, 3.97 eV, respectively. The crystal structure of the films has been investigated by X-ray diffraction patterns. It has been observed that WFTO-1 and WFTO-2 samples have (111) preferential orientation corresponding to SnO2 cubic phase. This orientation almost disappears and changes to tetragonal phase (110) orientation for WFTO-3 and WFTO-4. To the best of our knowledge, this is the first cubic structure observation for SnO2 grown by the sol–gel technique. The electrical properties were also changed with co-doping ratio. The best optical, electrical and structural properties were obtained for mole ratio 0.75:0.50 (F:W).
Źródło:
Optica Applicata; 2013, 43, 4; 663-677
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 17

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