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Tytuł:
A method of magnetic field measurement in a scanning electron microscope using a microcantilever magnetometer
Autorzy:
Orłowska, Karolina
Mognaschi, Maria E.
Kwoka, Krzysztof
Piasecki, Tomasz
Kunicki, Piotr
Sierakowski, Andrzej
Majstrzyk, Wojciech
Podgórni, Arkadiusz
Pruchnik, Bartosz
di Barba, Paolo
Gotszalk, Teodor
Powiązania:
https://bibliotekanauki.pl/articles/220725.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
scanning electron microscope
magnetometry
microcantilever
Opis:
Scanning electron microscopy (SEM) is a perfect technique for micro-/nano-object imaging [1] and movement measurement [2, 3] both in high and environmental vacuum conditions and at various temperatures ranging from elevated to low temperatures. In our view, the magnetic field expanding from the pole-piece makes it possible to characterize the behaviour of electromagnetic micro- and nano-electromechanical systems (MEMS/NEMS) in which the deflection of the movable part is controlled by the electromagnetic force. What must be determined, however, is the magnetic field expanding from the e-beam column, which is a function of many factors, like working distance (WD), magnification and position of the device in relation to the e-beam column. There are only a few experimental methods for determination of the magnetic field in a scanning electron microscope. In this paper we present a method of the magnetic field determination under the scanning electron column by application of a silicon cantilever magnetometer. The micro-cantilever magnetometer is a silicon micro-fabricated MEMS electromagnetic device integrating a current loop of lithographically defined dimensions. Its stiffness can be calibrated with a precision of 5% by the method described by Majstrzyk et al. [4]. The deflection of the magnetometer cantilever is measured with a scanning electron microscope and thus, through knowing the bias current, it is possible to determine the magnetic field generated by the e-beam column in a defined position and at a defined magnification.
Źródło:
Metrology and Measurement Systems; 2020, 27, 1; 141-149
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Auditory ossicles in Scanning Electron Microscopy
Autorzy:
Wiatr, Agnieszka
Składzień, Jacek
Wiatr, Maciej
Powiązania:
https://bibliotekanauki.pl/articles/1397399.pdf
Data publikacji:
2020-05-12
Wydawca:
Index Copernicus International
Tematy:
middle ear surgery
ossicular chain
Scanning Electron Microscope
Opis:
Introduction: Knowledge about the physiology of a healthy middle ear is essential for understanding the activity and mechanics of the ear as well as the basics of ossiculoplasty. Trauma of the epithelial lining of the tympanic cavity as well as the ossicular chain may be the result of chronic inflammation and surgery. Depending on the observed changes of the middle ear lining, there are several types of distinguished chronic inflammatory changes: simple, with cholesteatoma, with the formation of inflammatory granulation tissue, in course of specific diseases. Purpose: The aim of the article is presentation of the microstructure and vasculature of the ossicular chain in the Scanning Electron Microscope. Particular attention is drawn to the anatomical aspects of the structure and connections of auditory ossicles as vital elements for reconstruction of the conduction system of the middle ear. Material and method: The analysis covered auditory ossicles standardly removed in accordance with the methodology of the investigated surgical procedures. The preparations were evaluated in a scanning electron microscope. Results: The exposure of bone surface promotes deep erosion. The advanced process of destruction of bone surface in the case of chronic otitis media correlates with a significant degree of damage to both the lining covering the auditory ossicles and that surrounding articular surfaces. Conclusions: (1) The ossicles in the image of the Scanning Electron Microscope are covered with lining. It passes from the surface of the ossicles to the vascular bundles, forming vascular sheaths; (2) Damage to lining continuity on the surface of the auditory ossicles promotes the rapid destruction of bone tissue in the inflammatory process; (3) The dimensions of the individual ossicles are respectively: malleus – 8.36 +/- 0.01, incus – 8.14 +/- 0.0, stapes – 3.23 +/- 0.01 mm. Behavior of the anatomical length of ossicular chain during tympanoplasty appears to be essential to maintaining adequate vibration amplitude of the conductive system of the middle ear.
Źródło:
Polish Journal of Otolaryngology; 2020, 74, 4; 1-7
0030-6657
2300-8423
Pojawia się w:
Polish Journal of Otolaryngology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Badanie powierzchni folii celulozowych bez nadruku i z nadrukiem farbami biodegradowalnymi przy użyciu profilometru, mikroskopu konfokalnego i mikroskopu skaningowego
Examination of the surface of cellulose films with and without printing, made with biodegradable inks by means of a profilometer, confocal and scanning microscops
Autorzy:
Nowak, W.
Podsiadło, H.
Powiązania:
https://bibliotekanauki.pl/articles/128541.pdf
Data publikacji:
2017
Wydawca:
Centralny Ośrodek Badawczo-Rozwojowy Przemysłu Poligraficznego
Tematy:
folie celulozowe
folie biodegradowalne
starzenie promieniowaniem
farba kompostowalna
mikroskop konfokalny
mikroskop skaningowy
profilometr
cellulose films
biodegradable films
confocal microscope
scanning microscope
profilometer
Opis:
The article presents the visual effects of solar and UV-VIS radiation with appropriate intensity and aging time on three types of cellulose foils with and without overprint. The print was made with biodegradable AquaBio and compostable GeckoFrontalEco inks. Photographs of the film surface were taken using a confocal and scanning microscope, and their profile was determined using a profilometer.
Źródło:
Acta Poligraphica; 2017, 10; 43-54
2299-9981
Pojawia się w:
Acta Poligraphica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Badanie struktury skrzydła motyla przy użyciu skaningowego mikroskopu elektronowego w kształceniu studentów kierunku inżynierii materiałowej
Researching the Butterfly Wing Structure Using Scanning Electron Microscope in Education of Materials Engineering Students
Autorzy:
KRZEMIŃSKI, PIOTR
PRACH, PIOTR
JEDZINIAK, KAROLINA
KILMAN, KLAUDIA
Powiązania:
https://bibliotekanauki.pl/articles/457269.pdf
Data publikacji:
2019
Wydawca:
Uniwersytet Rzeszowski
Tematy:
skaningowy mikroskop elektronowy wymiarowanie struktur mikrometrycznych
scanning electron microscope dimensioning of micrometric structures
Opis:
W artykule omówiono wyniki obrazowania struktury skrzydła motyla wraz z wymiarowaniem jego struktury w skali mikrometrycznej na skaningowym mikroskopie elektronowym.
The article presents results of butterfly wing structure imaging complete with measuring dimensions of said structures on scanning electron microscope.
Źródło:
Edukacja-Technika-Informatyka; 2019, 10, 3; 257-261
2080-9069
Pojawia się w:
Edukacja-Technika-Informatyka
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Biosynthesis, characterisation, free radical scavenging activity and anti-bacterial effect of plant-mediated zinc oxide nanoparticles using Pithecellobium dulce and Lagenaria siceraria Leaf Extract
Autorzy:
Prakash, M. Jeevan
Kalyanasundharam, S.
Powiązania:
https://bibliotekanauki.pl/articles/1193960.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
2-2-diphenyl-1-picrylhydrazyl
DPPH
Energy Dispersive Xray
Lagenaria siceraria
Pithecellobium dulce
Scanning Electron Microscopy
Transmission Electron Microscope
X-Ray
ZnO
by FTIR Spectroscopy
gram-positive and gram negative bacterial
Opis:
The study involved synthesis of Zinc Oxide nanoparticles using biological and chemical reducing agents. The aim was to compare the yield, nature and antimicrobial activity of nanoparticles. Nanoparticles synthesized by the two methods were characterized by FTIR Spectroscopy, Scanning Electron Microscopy (SEM), Energy Dispersive Xray (EDAX), Transmission Electron Microscope (TEM) and X-ray diffraction (XRD). In biological method, Pithecellobium dulce and Lagenaria siceraria leaf extract; and in chemical method, sodium hydroxide was used as reducing agents. Antibacterial study was carried out on gram-positive and gram negative bacterial strains by disc diffusion method. The biologically synthesized ZnO Nanoparticles showed better antimicrobial activities with respect to the activities of synthetic drugs than chemical method. Antioxidant potential of synthesized nanoparticles was assessed through 2,2–diphenyl-1-picrylhydrazyl (DPPH) method.
Źródło:
World Scientific News; 2015, 18; 60-77
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Calcium (Ca2+) expression and intensity in cumulus-oocyte complex (COCs) in Kacang goat after vitrification
Autorzy:
Widjiati, W.
Faizah, Z.
Darsini, N.
Hendrawan, V.F.
Karima, H.N.
Chotimah, C.
Sumitro, S.B.
Yustinasari, L.R.
Kasman, A.A.M.N.
Ntoruru, J.M.
Luqman, E.M.
Powiązania:
https://bibliotekanauki.pl/articles/16539072.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czasopisma i Monografie PAN
Tematy:
Calcium (Ca2+)
confocal laser scanning microscope
cumulus-oocyte complex (COCs)
food production
Kacang goat
Opis:
The process of vitrification of the cumulus-oocyte complex (COCs) often results in cold shock. When warming, heat shock occurs which can disrupt the balance of intracellular calcium (Ca2+) intensity. Drastic changes in temperature cause Reactive Oxygen Species (ROS), affecting changes on Ca2+ in COCs. The role of calcium is needed for oocyte activation in the fertilization process. The purpose of this study was to measure the expression of Ca2+ and the intensity of Ca2+ in COCs after vitrification. The study was divided into 2 groups, the control group (C) of fresh COCs, and the treatment group (T) of COCs after vitrification. After vitrification for 24 hours, then thawing, the expression of Ca2+ was examined using the Immunocytochemistry (ICC) method and the intensity of calcium (Ca2+) with a Confocal Laser Scanning Microscope (CLSM). The research data obtained were analyzed statistically by T-Test. The results showed that the expression of Ca2+ in the control group (12.00±0.00) was different from the treatment group (0.35±0.79). The intensity of Ca2+ in the control group (1059.43±489.59) was different from the treatment group (568.21±84.31). The conclusion of this study is that cryopreservation affects calcium in COCs; there were differences in the expression and the intensity of Ca2+ between fresh COCs and COCs after vitrification. Ca2+ intensity of COCs after vitrification was concentrated in the nucleus, while in fresh COCs it was concentrated in the cytoplasm.
Źródło:
Polish Journal of Veterinary Sciences; 2022, 25, 1; 19-26
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Chronic suppurative otitis media with cholesteatoma and chronic otitis media with granulation investigated by scanning electron microscope based on an analysis of 140 patients
Autorzy:
Wiatr, Agnieszka
Job, Katarzyna
Składzień, Jacek
Wiatr, Maciej
Powiązania:
https://bibliotekanauki.pl/articles/1397266.pdf
Data publikacji:
2021
Wydawca:
Index Copernicus International
Tematy:
bone defects
chronic otitis media
inflammatory granulation
scanning electron microscope
structure of cholesteatoma
Opis:
Introduction: Chronic purulent cholesteatoma of the middle ear, as well as to a lesser extent chronic granulomatous otitis media, lead to destruction of bone structures within the middle ear space. The above process is controlled by the OPG/RANKL/RANK system. Aim: The aim of the study is a comparative analysis of surgical material obtained from patients with diagnosed chronić cholesteatoma and chronic otitis media with inflammatory granulation in the assessment of the Scanning Electron Microscope (SEM). Material and methods: An analysis of 140 patients operated on due to chronic otitis media was performed. Forty patients who had been diagnosed with chronic cholesteatoma of the middle ear and chronic granulomatous otitis media were selected for a detailed analysis in the SEM. The final study under SEM included 20 patients. Results: The regular structure of cholesteatoma depicted in the SEM concerned 5 patients. In the remaining 7 patients, the system was irregular and even chaotic. The lack of regularity can also be observed in the case of granulation tissue, which in the SEM image presented itself as an irregular tissue mass without detectable regularities. Conclusions: (1) The regular pattern of the cholesteatoma matrix cells observed in some patients with chronic cholesteatoma of the middle ear reduces the molecular permeability of inflammatory cytokines, concurrently limiting the destructive activity on bone structures; (2) the presence of inflammatory granulation tissue in the middle ear is accompanied by an influx of leukocytes: neutrophils and lymphocytes, which are the source of pro-inflammatory cytokines, the growth of which activates the processes leading to the damage of bone tissue and the development of inflammation; (3) no specimen of acquired cholesteatoma revealed the presence of commensal organisms from Demodex species on the surface of the exfoliated human epithelium.
Źródło:
Polish Journal of Otolaryngology; 2021, 75, 3; 21-27
0030-6657
2300-8423
Pojawia się w:
Polish Journal of Otolaryngology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Confocal microscopy for investigations of agricultural materials
Autorzy:
Konstankiewicz, K.
Krol, A.
Pukos, A.
Powiązania:
https://bibliotekanauki.pl/articles/25302.pdf
Data publikacji:
1995
Wydawca:
Polska Akademia Nauk. Instytut Agrofizyki PAN
Tematy:
microstructure
potato tissue
image transmission
computer image analysis
tandem scanning reflected light microscope
agricultural material
confocal microscopy
tomograph image
Źródło:
International Agrophysics; 1995, 09, 4
0236-8722
Pojawia się w:
International Agrophysics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystallization of the Structural Components of Multiple Remelted AlSi9Cu3 Alloy
Autorzy:
Matejka, M.
Bolibruchova, D.
Kuriš, M.
Powiązania:
https://bibliotekanauki.pl/articles/1837683.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al-Si-Cu
remelting
returnable material
structural components
scanning electron microscope
Opis:
At present, Al-Si-Cu based alloys (with a typical representative AlSi9Cu3 alloy) represent more than half of the castings used in various industries (automotive, aerospace and electrical engineering). These are most often sub-eutectic (exceptionally eutectic) alloys with a content of 6 to 13 wt. % Si and 1 to 5 wt. % Cu. The aim of the paper is to point out the importance of the evaluation of input raw materials that determines the overall properties of the casting and the costs invested in its production. A negative impact on performance can be expected when using an alloy made up of a high proportion of recycled material, despite its economic benefits. Experimental alloys were evaluated based on the results of crystallization process and a combination of scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), and deep etching. The effect of remelting and increasing the remelted returnable material in the batch was manifested especially in the crystallization of iron-rich phases. The negative effect of remelting on the structural components was manifested after the fourth remelting. Gradual increase of remelted returnable material in the batch causes harmful changes in the crystallization process.
Źródło:
Archives of Foundry Engineering; 2021, 21, 2; 41-45
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Determination of acceleration of different dynamic microobjects by the television scanning optical microscope
Autorzy:
Prudyus, I.
Matiieshyn, Y.
Powiązania:
https://bibliotekanauki.pl/articles/114123.pdf
Data publikacji:
2015
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
television scanning optical microscope
microscope field of view
acceleration of movement
Opis:
The acceleration of the dynamic microobjects (MO) movement, the motion of which is accelerated uniformly or non-uniformly is an important task for television measuring systems. Most existing measuring systems usually have a small range of acceleration with a short period of growth. Such period of growth of the acceleration is characteristic for many dynamic MO. Better instruments to determine the non-uniform velocity of the various objects are based on various laser devices. These instruments are contactless and high-speed enough. In the paper the basics of the television scanning optical microscope (TSOM) are presented. In the Chapter 2 the schematic diagram of the TSOM and its main functionalities are pointed out. In the Chapter 3 an adaptation of the TSOM for movement acceleration of microobjects is discussed. Modified structural and functional diagram of the instrument is presented.
Źródło:
Measurement Automation Monitoring; 2015, 61, 8; 410-412
2450-2855
Pojawia się w:
Measurement Automation Monitoring
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Determination of Accumulated Electrons at PET Surface Using Mirror Effect Phenomena in SEM
Autorzy:
Abood, Tareq H.
Hadi, Hasan A.
Mohi, Ali T.
Powiązania:
https://bibliotekanauki.pl/articles/1192591.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Polyethylene Terephthalate
scanning electron microscope
Magnification Factor Method
Disappearing Method
Opis:
An experimental-theoretical investigation have been presented to exploring phenomena of mirror effect. The Polyethylene Terephthalate (PET) material is chosen to be a case study throughout this work. Where the scanning electron microscope (SEM) is used for executing the experiments. Attention has been focused on determination of the number of electrons that accumulated at PET surface, since it is regarded to be the most important factor for producing mirror effect images. Thus two different procedures are produced to achieve such a task namely Magnification Factor Method and Disappearing Method. Results obtained from these two approaches have clearly shown that mirror effects can accurately be used as an excellent tool to determine dielectric constant of insulator.
Źródło:
World Scientific News; 2016, 55; 27-37
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Digital analysis of geo-referenced concrete Scanning Electron Microscope (SEM) images
Autorzy:
Ahamad, Mohd Sanusi S.
Maizul, Elly Nur Myaisara
Powiązania:
https://bibliotekanauki.pl/articles/1838090.pdf
Data publikacji:
2020
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
scanning electron microscope
geo-referenced imagery
digital image analysis
image mapping
mikroskop skaningowy
cyfrowa analiza obrazu
mapowanie obrazu
Opis:
The microstructural evaluation of complex cementitious materials has been made possible by the microscopic imaging tools such as Scanning Electron Microscope (SEM) and X-Ray Microanalysis. Particularly, the application of concrete SEM imaging and digital image analysis have become common in the analysis and mapping of concrete technology. In this study, six samples of two-dimensional (2D) SEM images were spatially resampled to produce Geo-referenced SEM sample images. Subsequently, they were analyzed and the intensity histogram plot was produced to facilitate visual interpretation. The consecutive digital image analysis performed was the enhancement and noise removal process using two filtering methods i.e. median and adaptive box filter. The filtered resampled images, then undergone the unsupervised K-Means classification process to collectively separate each individual pixel corresponds to the spectral data. By spatial segmentation of K-Means algorithms, the cluster groups generated were carefully reviewed before proceeding to the final analysis. From the resulting data, the mapping of the spatial distribution of k-cluster and the quantification of micro-cracks (voids) were performed. The results of the SEM images (1st - 4th sample) showed a higher percentage of k-cluster data indicating a good correlation with the major elemental composition of EDX analysis, namely Oxide (O), Silicon (Si) and Carbon (C). Meanwhile, the subjective visual assessment of the image (5th and 6th sample) has confirmed the micro-crack developments on the concrete SEM images upon which the crack density was 3.02 % and 1.30 %, respectively.
Źródło:
Civil and Environmental Engineering Reports; 2020, 30, 2; 67-79
2080-5187
2450-8594
Pojawia się w:
Civil and Environmental Engineering Reports
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Diversity of the floral nectaries surface of four Crataegus L. species
Zroznicowanie powierzchni nektarnikow kwiatowych czterech gatunkow z rodzaju Crataegus L.
Autorzy:
Chwil, M
Konarska, A
Weryszko-Chmielewska, E
Powiązania:
https://bibliotekanauki.pl/articles/26759.pdf
Data publikacji:
2006
Wydawca:
Polskie Towarzystwo Botaniczne
Tematy:
scanning electron microscope
nectary surface
Crataegus crus-galli
stoma
cuticle
Crataegus curvisepala
diversity
floral nectary
epidermis
Crataegus coccinea
nectary
Crataegus
Crataegus prunifolia
Rosaceae
Opis:
The performed studies focused on the surface structure of floral nectaries of four species from the following genus: C. coccinea L , C. crus-galli L, C. curvisepala Lindm and C. prunifolia (Poiret) Pers. The observations of the epidermis area were made in a scanning electron microscope (SEM). A nectary appears to be shaped like a slightly curved disk situated between the pistil style and the basal part of the stamens filaments. The nectary area of the studied species differed substantially as regards the cuticle sculpture and stomata number. The nectary secretion in Crataegus flowers proceeds through the stomata located below a level of the other epidermis cells, in the deep indents of the secretory tissue. The highest stomata number in 1 mm² nectary epidermis was recorded in C. crus-galli, C. coccínea, C. prunifolia and finally, C. curvisepala. Analyzing the nectary cuticular structure in respect of its increasing complexity (absence or presence of stripes), the investigated taxons can be ordered as following: Crataegus curvisepala, C. coccinea, C. crus-galli and C. prunifolia.
Przeprowadzone badania dotyczyły budowy powierzchni nektarników kwiatowych czterech gatunków z rodzaju Crataegus: C. coccínea L., C. crus-galli L., C. curvisepala Lindm. i C. prunifolia (Poiret) Pers. Obserwacje epidermy przeprowadzono w skaningowym mikroskopie elektronowym (SEM). Nektarnik ma kształt lekko wygiętego dysku leżącego między szyjką słupka, a nasadową częścią nitek pręcikowia. Powierzchnia epidermy nektarników badanych gatunków różniła się znacznie urzeźbieniem kuty kuli i liczbą aparatów szparkowych. Sekrecja nektaru w kwiatach Crataegus odbywała się przez aparaty szparkowe, które były położone poniżej poziomu pozostałych komórek skórki, w głębokich obniżeniach tkanki wydzielniczej. Największą liczbę szparek w mm² epidermy nektarnika stwierdzono u C. crus-galli, a następnie C. coccínea, C. prunifolia i C. curvisepala. Analizując kutykularną strukturę nektarników pod względem wzrastającego stopnia skomplikowania budowy (brak lub obecność prążków) badane taksony można uporządkować następująco: Crataegus curvisepala, C. coccínea, C. crus-galli i C. prunifolia.
Źródło:
Acta Agrobotanica; 2006, 59, 1
0065-0951
2300-357X
Pojawia się w:
Acta Agrobotanica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Efekty ekstrakcji pyłku kwiatowego nadkrytycznym dwutlenkiem węgla®
The effects of supercritical carbon dioxide treatment on bee pollen®
Autorzy:
Bakier, S.
Bajko, E.
Powiązania:
https://bibliotekanauki.pl/articles/227616.pdf
Data publikacji:
2017
Wydawca:
Wyższa Szkoła Menedżerska w Warszawie
Tematy:
ekstrakcja w nadkrytycznym CO2
pyłek kwiatowy
GC-MS
skaningowy mikroskop elektronowy
supercritical CO2 fluid extraction
bee pollen
scanning electron microscope
Opis:
W artykule przedstawiono wyniki badań ekstrakcji pyłku kwiatowego w postaci obnóży za pomocą ditlenku węgla w stanie nadkrytycznym. Badano wpływ sposobu przygotowania surowca na wydajność ekstrakcji oraz strukturę pojedynczych ziaren pyłku. Proces ekstrakcji realizowano przy ciśnieniu 35 MPa, w temperaturze 40°C przy przepływie CO2 wynoszącym 80 g/min przez 90 minut. Uzyskane wydajności ekstrakcji wynosiły od 0,86% ±0,25% do 1,52% ±0,2% masy obnóży przed ekstrakcją. Skład chemiczny uzyskanych ekstraktów identyfikowano za pomocą techniki chromatografii gazowej z detektorem masowym (GC-MS). Analiza GC-MS wykazała, że prawie 82 % ekstraktu stanowią związki o charakterze lipidowym, w tym 14,07 % nienasycone kwasy tłuszczowe. Badania z użyciem skaningowego mikroskopu elektronowego wykazały, że w wyniku działania nadkrytycznego ditlenku węgla nastąpiło zniszczenie zewnętrznych osłon ziaren pyłkowych.
This article presents the results of studies on the extraction of components from bee pollen by supercritical dioxide carbon. The influence of the method of bee pollen preparation and process conditions on the extraction yield and the structure of bee pollen grains was investigated. The extraction was performed at the pressure 35 MPa, temperature 40°C, CO2 flow rate 80 g/min for 90 min. The obtained extraction yields ranged from 0,86% ±0,25% to 1,52% ± 0,2% mass of bee pollen. The chemical compounds of the extracts obtained from supercritical carbon dioxide extraction were identified by using gas chromatography-mass spectrometry (GC-MS). GC-MS analysis of the extract showed that lipids accounted for approximately 82 %, including 14,07 % unsaturated fatty acids. Scanning electron microscopy studies revealed that supercritical dioxide carbon treatment was an effective way to break cell wall of bee pollen.
Źródło:
Postępy Techniki Przetwórstwa Spożywczego; 2017, 1; 66-70
0867-793X
2719-3691
Pojawia się w:
Postępy Techniki Przetwórstwa Spożywczego
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of Aspect Ratio and Loading on the Mechanical Properties of Prosopis Juliflora Fibre-reinforced Phenol Formaldehyde Composites
Właściwości mechaniczne żywic fenolowo-formaldehydowych wzmocnionych włóknami Prosopis Juliflora.
Autorzy:
Sujin Jose, A.
Athijayamani, A.
Ramanathan, K.
Sidhardhan, S.
Powiązania:
https://bibliotekanauki.pl/articles/232126.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Tematy:
prosopis juliflora fibres
composite
mechanical properties
scanning electron microscope
theoretical models
włókna prosopis juliflora
właściwości mechaniczne kompozytów
elektronowy mikroskop skaningowy
modele teoretyczne
Opis:
In this paper, an attempt was made to use Prosopis juliflora fibres (PJFs) as a reinforcing agent for phenol formaldehyde (PF) composites. Mechanical properties of the composites were studied for various fibre aspect ratios (FAR) and fibre loadings (FL). A scanning electron microscope (SEM) was used to study the fractured surface of the composites. The peak range of mechanical properties was identified for composites with a FAR of 136 and fibre loading of 23.53 wt%. This study shows that the optimum FAR and fibre loading for PJFs were found to be 136 and 23.53 wt% in order to achieve good reinforcement with better mechanical properties in the PF resin matrix. Experimental results were observed to be in very good agreement with the theoretical.
W pracy podjęto próbę wykorzystania włókien Prosopis juliflora jako środka wzmacniającego żywice fenolowo-formaldehydowe. Przy użyciu elektronowego mikroskopu skaningowego zbadano powierzchnie przełomu kompozytów. Dla różnych wartości wydłużenia włókien (46, 136 i 227 mm) i udziału procentowego włókien w matrycy (4.88, 10.34, 16.51, 23.53 i 31.58 wt%) zbadano właściwości mechaniczne kompozytów. Na podstawie badań stwierdzono, że optymalne wydłużenie i zawartość włókien w matrycy to odpowiednio 136 mm i 23,53 wt%. Wyniki eksperymentalne charakteryzowały się dobrą korelacją z wynikami teoretycznymi.
Źródło:
Fibres & Textiles in Eastern Europe; 2017, 4 (124); 59-64
1230-3666
2300-7354
Pojawia się w:
Fibres & Textiles in Eastern Europe
Dostawca treści:
Biblioteka Nauki
Artykuł
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