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Tytuł:
The Investigation of Ground Granulated Blast Furnace Slag Geopolymer at High Temperature by Using Electron Backscatter Diffraction Analysis
Autorzy:
Aziz, Ikmal Hakem
Mohd Mustafa Al Bakri, Abdullah
Salleh, Mohd Arif Anuar Mohd
Yoriya, Sorachon
Rafiza, Abd Razak
Mohamed, Rosnita
Baltatu, Madalina Simona
Powiązania:
https://bibliotekanauki.pl/articles/2048835.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
geopolymer
ground granulated blast furnace slag
electron backscatter diffraction
Opis:
This paper elucidated the potential of electron backscatter diffraction analysis for ground granulated blast furnace slag geopolymers at 1000°C heating temperature. The specimen was prepared through the mechanical ground with sandpaper and diamond pad before polished with diamond suspension. By using advanced technique electron backscatter diffraction, the microstructure analysis and elemental distribution were mapped. The details on the crystalline minerals, including gehlenite, mayenite, tobermorite and calcite were easily traced. Moreover, the experimental Kikuchi diffraction patterns were utilized to generate a self-consistent reference for the electron backscatter diffraction pattern matching. From the electron backscatter diffraction, the locally varying crystal orientation in slag geopolymers sample of monoclinic crystal observed in hedenbergite, orthorhombic crystal in tobermorite and hexagonal crystal in calcite at 1000°C heating temperature.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 1; 227-231
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Crystalographic Texture on Cavitation Wear Resistance of As-Cast CuZn10 Alloy
Autorzy:
Jasionowski, R.
Polkowski, W.
Zasada, D.
Powiązania:
https://bibliotekanauki.pl/articles/355595.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
texture
cavitation
cavitation erosion
electron backscatter diffraction
EBSD
CuZn10 alloy
Opis:
Analysis of a crystallographic texture (a preferred orientation) effect on cavitation wear resistance of the as-cast CuZn10 alloy, has been conducted in the present paper. The experiment was conducted on the CuZn10 alloy samples with <101>//ND or <111>//ND preferred orientations (where the ND denotes direction that is perpendicular to the exposed surface). The cavitation resistance examinations have been carried out on three different laboratory stands (namely, vibration, jet-impact and flow stands) that are characterized by a various intensity and a way of cavitation’s excitement. Obtained results point towards a higher cavitation resistance of the CuZn10 alloy with the <111>//ND preferred orientation.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 935-940
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
An SEM/EBSD study of shear bands formation in Al-0.23%wt.Zr alloy deformed in plane strain compression
Krystalograficzne aspekty formowania się pasm ścinania w stopie Al-0.23%wag. Zr odkształcanym w próbie nieswobodnego ściskania
Autorzy:
Paul, H.
Uliasz, P.
Miszczyk, M.
Skuza, W.
Knych, T.
Powiązania:
https://bibliotekanauki.pl/articles/350874.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
pasmo ścinania
tekstura
mikrostruktura
dyfrakcja elektronów
niska temperatura odkształcenia
shear bands
texture
microstructure
electron diffraction
low temperature deformation
Opis:
The crystal lattice rotations induced by shear bands formation have been examined in order to investigate the influence of grain boundaries on slip propagation and the resulting texture evolution. The issue was analysed on Al-0.23wt.%Zr alloy as a representative of face centered cubic metals with medium-to-high stacking fault energy. After solidification, the microstructure of the alloy was composed of flat, twin-oriented, large grains. The samples were cut-off from the as-cast ingot in such a way that the twinning planes were situated almost parallel to the compression plane. The samples were then deformed at 77K in channel-die up to strains of 0.69. To correlate the substructure with the slip patterns, the deformed specimens were examined by SEM equipped with a field emission gun and electron backscattered diffraction facilities. Microtexture measurements showed that strictly defined crystal lattice re-orientations occurred in the sample volumes situated within the area of the broad macroscopic shear bands (MSB), although the grains initially had quite different crystallographic orientations. Independently of the grain orientation, their crystal lattice rotated in such a way that one of the f111g slip planes became nearly parallel to the plane of maximum shear. This facilitates the slip propagation across the grain boundaries along the shear direction without any visible variation in the slip plane. A natural consequence of this rotation is the formation of specific MSB microtextures which facilitates slip propagation across grain boundaries.
W pracy analizowano wpływ rotacji sieci krystalicznej wywołanej pojawieniem się pasm ścinania na propagacje poślizgu poprzez granice ziaren oraz na ewolucje tekstury. Badania prowadzono na próbkach stopu Al-0.23%wag.Zr, jako reprezentatywnym dla grupy metali o średniej i dużej energii błędu ułożenia. W stanie wyjściowym w mikrostrukturze stopu dominowały duże, silnie spłaszczone ziarna, bliźniaczo względem siebie zorientowane. Z odlanego wlewka wycinano próbki w ten sposób, ze płaszczyzny zblizniaczenia usytuowane były równolegle do płaszczyzny ściskania. Badania zachowania umocnieniowego analizowano w próbie nieswobodnego ściskania prowadzonej w temperaturze 77K. Próbki odkształcano do zakresu -50% zgniotu. Analizę zmian strukturalnych prowadzono w oparciu o pomiary orientacji lokalnych w SEM wyposażonym w działo o emisji polowej. Wyniki pomiarów orientacji lokalnych pokazują, że w obszarach zajmowanych przez makroskopowe pasma ścinania występuje ścisle zdefiniowana tendencja rotacji sieci krystalicznej, pomimo, że początkowe ziarna posiadały silnie zróznicowana orientacje. Niezależnie od orientacji poszczególnych ziaren, w obszarze makroskopowych pasm ścinania ich sieć krystaliczna rotuje w taki sposób, ze w każdym ziarnie jedna z płaszczyzn {111}zmierza do nałożenia się z płaszczyzną maksymalnych naprężeń ścinających. Umożliwia to propagacje poślizgu poprzez granice ziaren wzdłuż kierunku ścinania bez widocznej zmiany w kierunku poślizgu. Naturalna konsekwencja takiej rotacji jest uformowanie się specyficznej tekstury 'wnętrza' makroskopowych pasm ścinania.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 1; 145-150
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The effect of aluminum content on the microstructure and cavitation wear of feal intermetallic alloys
Autorzy:
Jasionowski, R.
Zasada, D.
Polkowski, W.
Powiązania:
https://bibliotekanauki.pl/articles/386821.pdf
Data publikacji:
2014
Wydawca:
Politechnika Białostocka. Oficyna Wydawnicza Politechniki Białostockiej
Tematy:
intermetallic alloys
cavitation
cavitation wear
Electron Backscattered Diffraction (EBSD)
stopy międzymetaliczne
kawitacja
EBSD
Opis:
Intermetallic-based alloys (so called intermetallics) of the Fe-Al binary system are modern construction materials, which in re- cent decades have found application in many branches of the power, chemical and automotive industries. High resistance of FeAl based alloys to cavitational erosion results first of all from their high hardness in the as-cast state, large compressive stresses in the material, as well as homogeneous structure. In the present paper, the effect of aluminum content on the microstructure, texture and strain imple- mented upon cavitation wear of FeAl intermetallic alloys, have been analyzed by field emission gun scanning electron microscopy (FEG SEM) and electron backscatter diffraction (EBSD) analysis. Obtained results of structural characterization indicates that with increasing aluminium content effects of orientation randomization (weakening of <100>//ND casting texture), grain refinement and rising of mechani- cal strenght (and so cavitational resistance) take place.
Źródło:
Acta Mechanica et Automatica; 2014, 8, 1; 49-52
1898-4088
2300-5319
Pojawia się w:
Acta Mechanica et Automatica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Local Strain Distribution of Cold-Rolled Alloy 690 on Primary Water Stress Corrosion Crack Growth Behavior
Autorzy:
Kim, S.-W.
Ahn, T.-Y.
Lim, Y.-S.
Hwang, S.-S.
Powiązania:
https://bibliotekanauki.pl/articles/354997.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
alloy 690
crack growth
electron backscatter diffraction
local strain distributions
stress corrosion cracking
Opis:
This work aims to study the stress corrosion crack growth behavior of cold-rolled Alloy 690 in the primary water of a pressurized water reactor. Compared with Alloy 600, which shows typical intergranular cracking along high angle grain boundaries, the cold-rolled Alloy 690, with its heterogeneous microstructure, revealed an abnormal crack growth behavior in mixed mode, that is, in transgranular cracking near a banded region, and in intergranular cracking in a matrix region. From local strain distribution analysis based on local mis-orientation, measured along the crack path using the electron back scattered diffraction method, it was suggested that the abnormal behavior was attributable to a heterogeneity of local strain distribution. In the cold-rolled Alloy 690, the stress corrosion crack grew through a highly strained area formed by a prior cold-rolling process in a direction perpendicular to the maximum principal stress applied during a subsequent stress corrosion cracking test.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1243-1248
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Changes in Structure of CuCr0.6 Alloy After Repetitive Corrugation Process
Autorzy:
Jung, T.
Kwaśny, W.
Rdzawski, Z.
Głuchowski, W.
Matus, K.
Pawlyta, M.
Szindler, M.
Powiązania:
https://bibliotekanauki.pl/articles/356417.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
CuCr0.6 alloy
severe plastic deformation
repetitive corrugation and straightening
electron backscatter diffraction
transmission electron microscopy
Opis:
This paper presents the study of repetitive corrugation process influence on the strengthening of annealed alloy. Based on the results of mechanical properties of deformed sample, it has been found that the microhardness, ultimate tensile strength, yield strength and apparent elastic limit are significantly increased in relation to annealed sample. Examination on transmission electron microscopy confirmed the effect of intensive plastic deformation on structure fragmentation in the nanometric scale. This work confirmed the possibility of using the repetitive corrugation process to increase mechanical properties of CuCr0.6 alloy.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 4; 2441-2448
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Natural ageing effects on microstructure and properties of rail fastening elements SKL-12
Autorzy:
Labisz, Krzysztof
Konieczny, Jarosław
Powiązania:
https://bibliotekanauki.pl/articles/197042.pdf
Data publikacji:
2020
Wydawca:
Politechnika Śląska. Wydawnictwo Politechniki Śląskiej
Tematy:
microstructure
rail fastening system
sleepers
mechanical properties
rail steel
electron diffraction
mikrostruktura
system przytwierdzeń szyn
podkłady
właściwości mechaniczne
stal szynowa
dyfrakcja elektronów
Opis:
Rail transport is presently one of the most supported means of transport in Europe; it existed from the end of the 18th century. However, some issues especially concerning materials and its exploitation are still actual and are a matter of scientific projects or developments. In this paper, analyses concerning the characterisation of used track infrastructure elements in form of sleepers of the popular rail fastening system SKL 12 were performed. Specifically, the main objective of the work was the characteristics of the material microstructure and properties after long-term usage and natural ageing, reaching over a few decades. In this paper was conducted investigations concerning the non-used and used fasteners by reason of classic material research methods. The analysis was carried out based on the results obtained through research using mainly light, scanning electron microscopy (SEM) and transmission electron microscopy (TEM), as well as electron diffraction for the lattice structure determination, EDS chemical microanalysis and Rockwell hardness testing were also carried out in terms of identification of the chemical analysis changes that occurred after long-term application. The main reason was to characterise the long-term usage for the microstructure changes on the surface layer of the used fasteners compared to newly produced material.
Źródło:
Zeszyty Naukowe. Transport / Politechnika Śląska; 2020, 106; 85-96
0209-3324
2450-1549
Pojawia się w:
Zeszyty Naukowe. Transport / Politechnika Śląska
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Change In Microstructure and Mechanical Properties Of Four-Layer Stack ARB Processed Complex Aluminum Sheet with Annealing
Autorzy:
Jo, Sang-Hyeon
Lee, Seong-Hee
Powiązania:
https://bibliotekanauki.pl/articles/2049296.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
accumulative roll bonding
heterogeneous microstructure
aluminum alloy
electron back scatter diffraction
annealing
Opis:
The four-layer stack accumulative roll bonding (ARB) process using AA1050, AA5052 and AA6061 alloy sheets is performed up to 2 cycles without a lubricant at room temperature. The sample fabricated by the ARB is a multi-layer complex aluminum alloy sheet in which the AA1050, AA5052 and AA6061 alloys are alternately stacked to each other. The changes of microstructure and mechanical properties with annealing for the-ARBed aluminum sheet are investigated in detail. The as-ARBed sheet shows an ultrafine grained structure, however the grain diameter is some different depending on the kind of aluminum alloys. The complex aluminum alloy still shows ultrafine structure up to annealing temperature of 250℃, but above 275℃ it exhibits a heterogeneous structure containing both the ultrafine grains and the coarse grains due to an occurrence of discontinuous recrystallization. This change in microstructure with annealing also has an effect on the change of the mechanical properties of the sample. Especially, the specimen annealed at 300℃ represents abnormal values for the strength coefficient K and work hardening exponent n value.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 3; 765-770
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Destruction Mechanism of Z10400 Zn-based Alloy Subjected to Cavitational Erosion
Autorzy:
Jasionowski, R.
Zasada, D.
Polkowski, W.
Powiązania:
https://bibliotekanauki.pl/articles/380734.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
zinc alloy
cavitation wear
Electron Backscattered Diffraction (EBSD)
stop cynku
zużycie kawitacyjne
dyfrakcja elektronów wstecznie rozproszonych
Opis:
Z10400 zinc-based alloy has a very good casting properties and high resistance to corrosion. These two advantages make that Z10400 zinc-based alloy is commonly used for cathodic protection of hulls of ships. Cathodic anodes made of Z10400 zinc-based alloy in the propeller and flap rudder areas are also additionally exposed to the cavitation erosion. The aim of this work was to determine the cavitation erosion resistance of Z10400 zinc-based alloy, which is applied as protectors in cathodic protection of hulls of ships. The examination of cavitational erosion was carried out on a jet-impact measuring device. Study of the mechanism of the destruction of Z10400 alloy based on analysis was performed with scanning electron microscope Quanta 3d FEG and electron back scattered diffraction (EBSD) method.
Źródło:
Archives of Foundry Engineering; 2013, 13, 2 spec.; 48-52
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
EBSD Strain Analysis of CuZn10 Alloy in As-cast State and After Plastic Working and Annealing During Cavitational Wear
Autorzy:
Jasionowski, R.
Zasada, D.
Polkowski, W.
Powiązania:
https://bibliotekanauki.pl/articles/381392.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Electron Backscattered Diffraction (EBSD)
cavitation wear
strain analysis
dyfrakcja elektronów wstecznie rozproszonych
zużycie kawitacyjne
analiza odkształceń
Opis:
Electron backscatter diffraction (EBSD) system in conjunction with scanning electron microscope (SEM) allows performing full material characterization which include analysis of individual grain orientations, crystal orientation, global and local texture, phase identification and distribution or microstrain mapping. EBSD technique may be also applied for assessing lattice strain introduced during local plastic deformation due to its close relationship with development of dislocation substructure. The aim of this study was analysis of surface deformation by EBSD method of CuZn10 alloy in as-cast state and after plastic working and annealing, with different grain size at the beginning of the cavitation destruction process. The local changes of plastic deformation inside each grain were expressed by Grain Orientation Spread (GOS) and Kernel Average Misorientation (KAM) parameters.
Źródło:
Archives of Foundry Engineering; 2013, 13, 2 spec.; 53-60
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Mechanical Properties of AA1050/ AA6061/AA1050 Multi-Layer Sheet Fabricated by Cold Roll Bonding Process
Autorzy:
Lee, S.-H.
Powiązania:
https://bibliotekanauki.pl/articles/353150.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cold roll bonding process
AA1050/AA6061/AA1050 complex sheet
mechanical properties
electron backscatter diffraction
microstructure
Opis:
A cold roll-bonding process was applied to fabricate an AA1050/AA6061/AA1050 multi-layer sheet. Three Al sheets in which an AA6061 sheet is inserted inside two AA1050 sheets of 2 mm thickness, 40 mm width and 300 mm length were stacked up after surface treatment, and the material was then reduced to a thickness of 1.0 mm by multi-pass cold rolling. The AA1050/AA6061/AA1050 laminate complex sheet fabricated by roll bonding was then hardened by a natural aging (T4) and an artificial aging (T6) treatments. The microstructures of the as-roll bonded and the age-hardened Al complex sheets were revealed by optical microscope and electron back scatter diffraction analysis, and the mechanical properties were investigated by tensile and hardness testing. The strength of the as-roll bonded complex sheet was found to increase by 2.6 times, compared to that value of the starting material. Both AA1050 and AA6061 showed a typical recrystallization structure in which the grains were equiaxed after heat treatment. However, the grain size was smaller in AA6061 than in AA1050.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1489-1492
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization Of An Equal Channel Angular Pressed Al-Zn-In Alloy
Charakterytyka stopu Al-Zn-In otrzymanego metodą przeciskania w kanale kątowym
Autorzy:
Banjongprasert, C.
Jak-Ra, A.
Domrong, C.
Patakham, U.
Pongsaksawad, W.
Chairuangsri, T.
Powiązania:
https://bibliotekanauki.pl/articles/352220.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum alloys
equal channel angular pressing
severe plastic deformation
electron backscatter diffraction
stopy aluminium
przeciskanie przez kanał kątowy
odkształcenie plastyczne duże
dyfrakcja elektronów wstecznie rozproszonych
Opis:
Equal channel angular pressing (ECAP) is a technique that creates a high accumulated strain in metals and results in ultrafine-grained structure. In this study, Al-5Zn-0.02In was processed by ECAP at a room temperature using route Bc through an ECAP die (press angle of Φ = 100° and Ψ = 20°). The samples were subjected to ECAP with 1, 2, 3 and 4 passes. The processed specimens were characterized using electron backscatter diffraction (EBSD). The results confirmed the grain refinement of the alloy after ECAP to an average grain size less than 5 μm after 4-pass ECAP. The microhardness test shows that the hardness increased with the number of passes. The hardness of the cross-sectional area of the sample was similar to that tested along the pressing direction.
Metoda przeciskania w kanale kątowym (ang. Equal channel angular pressing; ECAP) prowadzi do powstania bardzo wysokich naprężeń, w wyniku czego otrzymuje się ziarna o bardzo drobnej strukturze. W niniejszej pracy, stop Al-5Zn-0,02In wytwarzano metodą ECAP w temperaturze pokojowej, wykorzystując ścieżkę Bc przez matrycę ECAP (kąty krzywizny: Φ = 100° i Ψ = 20°). Próbki poddano ECAP z 1, 2, 3 i 4 przejściami. Otrzymane próbki badano metodą dyfrakcji elektronów wstecznie rozproszonych (ang. electron back scatter diffraction; EBSD). W stopie otrzymanym metodą ECAP z 4 przejściami, średnia wielkość ziaren wynosiła mniej niż 5 μm. Badania mikrotwardości wykazały, że twardość zwiększała się wraz z liczbą przejść. Twardość zmierzona w poprzek próbki byłą porównywalna do tej mierzonej wzdłuż osi nacisku.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2A; 887-890
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ultrasonic-assisted synthesis of reactive carboxymethyl cellulose stabilized nano zero-valent iron and its application for removal of Cr6+ and Cu2+ ions
Autorzy:
Ayob, A.
Santiagoo, R.
Amneera, W. A.
Ismail, N.
Abdullah, A. Z.
Powiązania:
https://bibliotekanauki.pl/articles/207403.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
high resolution transmission
electron microscopy
light scattering
transmission electron microscopy X ray diffraction
zero-valent iron
wysoka rozdzielczość transmisyjna
mikroskopia elektronowa
dyfrakcja rentgenowska
żelazo
Opis:
Carboxymethyl cellulose (CMC) was used in the chemical reduction using sodium borohydride to yield dispersive nano zero-valent iron (nZVI) particles as reactive and stable adsorbents. CMC- -stabilized nZVI particles were characterized via UV-visible light spectroscopy, X-ray diffraction, dynamic light scattering, transmission electron microscopy, and specific surface area assisted using a probe ultrasonication dispersing tool at 50% amplitude power. High catalytic reactivity obtained in pseudo-first order reaction for Cr6+ (rate constant K1 = 0.0311 min–1) and pseudo-second order for Cu2+ (rate constant K2 = 0.0946 g·mg–1·min–1) indicated that colloidal stability of nZVI particles can be achieved with a stabilizer for the removal of toxic contaminants.
Źródło:
Environment Protection Engineering; 2016, 42, 2; 55-79
0324-8828
Pojawia się w:
Environment Protection Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of selected diffractive and microscopic methods to evaluate the physical state of drug and morphology of microspheres obtained by spray drying of furosemide with Eudragit L30 D-55.
Autorzy:
Ostróżka-Cieślik, Aneta
Sarecka-Hujar, Beata
Krzykawski, Tomasz
Karcz, Jagna
Banyś, Anna
Jankowski, Andrzej
Powiązania:
https://bibliotekanauki.pl/articles/895685.pdf
Data publikacji:
2018-06-30
Wydawca:
Polskie Towarzystwo Farmaceutyczne
Tematy:
X-ray diffraction
scanning electron microscopy
Microsphere
furosemide
laser diffraction
Eudragit L30 D-55
Opis:
In pharmaceutical technology, the analysis of physicochemical properties of raw materials, intermediates and products is part of quality control testing at each stage of designing formulations and in the routine evaluation of the final product. The aim of the study was to analyse the physical state of drug and the morphology of microspheres obtained by spray drying, where furosemide was incorporated in the polymeric matrix of Eudragit L30 D-55. The following optimal parameters of the spray drying process were established: aspirator capacity of 80%, T.in: 140 ° C, pump capacity: 10%. The laser diffraction method was used to analyse the size distribution of microspheres in the following furosemide-Eudragit L30 D-55 systems: 1:1, 1:3, 1:5. X-ray powder diffraction was applied to compare the degrees of crystallinity of the final product and the starting material. Furosemide has crystal structure both before and after spray drying, it occurs in the polymorphic forms (form I crystals). No reflection from the crystalline phase has been found on the diffraction pattern of Eudragit. This is an amorphous substance.
Źródło:
Acta Poloniae Pharmaceutica - Drug Research; 2018, 75, 3
0001-6837
2353-5288
Pojawia się w:
Acta Poloniae Pharmaceutica - Drug Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Interaction of Pb2plus and Zn2plus salts with clay minerals
Autorzy:
Kharitonova, G.V.
Manucharov, A.S.
Chizhikova, N.P.
Zemlyanukhin, V.N.
Chernomorchenko, N.I.
Powiązania:
https://bibliotekanauki.pl/articles/26503.pdf
Data publikacji:
2004
Wydawca:
Polska Akademia Nauk. Instytut Agrofizyki PAN
Tematy:
electron microscopy
X-ray diffraction
interaction
salt
zinc
lead
clay mineral
Źródło:
International Agrophysics; 2004, 18, 3
0236-8722
Pojawia się w:
International Agrophysics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cooling Characteristic and Microstructure of Ni-Si-B-Ag Alloy
Autorzy:
Wojciechowska, M.
Ziewiec, K.
Mucha, D.
Powiązania:
https://bibliotekanauki.pl/articles/356071.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous/crystalline composite
scanning electron microscopy
X-ray diffraction
thermography
melt spinning
Opis:
The aim of this work was to investigate the possibility of obtaining an amorphous/crystalline composite starting from Ni-SiB-based powder grade 1559-40 and silver powder. The alloy was produced using arc melting of 95% wt. Ni-Si-B-based powder (1559-40) and 5% wt. Ag powder. Ingot was re-melted on a copper plate and observed while cooling using a mid-wave infra-red camera. The alloy was then melt-spun in a helium atmosphere. The microstructure of the ingot as well as the melt-spun ribbon was studied using light microscopy and scanning electron microscopy with energy dispersive spectrometry. Phase identification was performed by means of X-ray diffraction. The observations confirmed an amorphous/crystalline microstructure of the ribbon where the predominant constituent of the microstructure was an amorphous phase enriched with Ni, Si, and B, while the minor constituent was an Ag-rich crystalline phase distributed in a film along the melt-spinning direction.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1357-1360
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photosensitization of TiO2 P25 with CdS Nanoparticles for Photocatalytic Applications
Autorzy:
Trenczek-Zając, A.
Banaś, J.
Świerczek, K.
Zazakowny, K.
Radecka, M.
Powiązania:
https://bibliotekanauki.pl/articles/352507.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
semiconductors
X-ray diffraction
transmission electron microscopy TEM
catalytic properties
optical properties
Opis:
A TiO2/CdS coupled system was prepared by mixing the TiO2 P25 with CdS synthesized by means of the precipitation method. It was found that the specific surface area (SSA) of both components is extremely different and equals 49.5 for TiO2 and 145.4 m2·g-1 for CdS. The comparison of particle size distribution and images obtained by means of transmission electron microscopy (TEM) showed agglomeration of nanocomposites. X-ray diffraction (XRD) patterns suggest that CdS crystallizes in a mixture of cubic and hexagonal phases. Optical reflectance spectra revealed a gradual shift of the fundamental absorption edge towards longer wavelengths with increasing CdS molar fraction, which indicates an extension of the absorption spectrum of TiO2. The photocatalytic activity in UV and UV-vis was tested with the use of methyl orange (MO). The Langmuir–Hinshelwood model described well the photodegradation process of MO. The results showed that the photocatalytic behaviour of the TiO2/CdS mixture is significantly better than that of pure nanopowders.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2A; 841-849
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Vlijanie mekhaoaktivacii dobavki mikrokremnezema na struktury i svojjstva pressovannykh materialov iz granodioritovykh shlamov sharkinskogo karera
Effect of mechanical activation supplements and fume on the structure and properties the compact granodiorite of sludge sharhinskogo career
Autorzy:
El'kina, I.
Powiązania:
https://bibliotekanauki.pl/articles/76830.pdf
Data publikacji:
2013
Wydawca:
Komisja Motoryzacji i Energetyki Rolnictwa
Tematy:
mechanical activity
sludge
granodiorite rock
structure
property
pressing
X-ray diffraction
electron microscopy
Opis:
The influence of mechanical activation process and silica fume addition to the compressed samples from sludge granodiorite rocks studied the formation of structure and properties the material. Spotted an opportunity to obtain high-quality wall materials based on recycled materials
Źródło:
Motrol. Motoryzacja i Energetyka Rolnictwa; 2013, 15, 5
1730-8658
Pojawia się w:
Motrol. Motoryzacja i Energetyka Rolnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Halloysite intercalated by potassium acetate
Autorzy:
Mariusz, Adamczyk
Katarzyna, Małycha
Karol, Kułacz
Michał, Pocheć
Kazimierz, Orzechowski
Powiązania:
https://bibliotekanauki.pl/articles/1450347.pdf
Data publikacji:
2020
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
clay minerals
electron microscopy
XRD
X-ray diffraction
TGA
thermogravimetric analysis
dielectric spectroscopy
Opis:
Halloysite was intercalated by the mechanochemical technique from dry components. The process efficiency of 50% was achieved. The obtained intercalate differed from the material acquired using an aqueous solution of potassium acetate. The material was analyzed employing electron microscopy, thermogravimetry, X-ray powder diffraction, and dielectric spectroscopy. It was found that the molecules and/or ions present in the interlayer spaces retain some possibility of movement. This property of the material is promising for potential application as low expensive absorbers of electromagnetic radiation.
Źródło:
Physicochemical Problems of Mineral Processing; 2020, 56, 6; 235-243
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Materiały dla jednowarstwowych ogniw paliwowych
Materials for single layer fuel cells
Autorzy:
Winiarz, P.
Powiązania:
https://bibliotekanauki.pl/articles/134696.pdf
Data publikacji:
2016
Wydawca:
ADVSEO
Tematy:
fuel cell
composite material
proton conductor
lanthanum niobate
scanning electron microscopy
x-ray diffraction
Opis:
A composite material, which may be further applied as a single layer fuel cell, was synthesized using solid state synthesis method. Composite consisted of two components. The first was a nanoceramic proton conductor – calcium doped lanthanum niobate. The second one was a nanoceramic semiconductor oxide composed of lithium, nickel and zinc oxides respectively. Structural and electrical investigations were performed on the received material. Scanning electron microscope images showed that the microstructure on the surface of this material is homogeneous. Energy dispersive X-Ray diffraction confirms that the components of the investigated composite are mixed together in a volume of material allowing to current flow through the percolation threshold. Open circuit voltage was changing during measurement from 0.8V to 0.6V. Moreover, the material did not change its structural properties during the current flow, hence it could be a good candidate to the production of single layer fuel cells.
Źródło:
Technical Issues; 2016, 4; 104-109
2392-3954
Pojawia się w:
Technical Issues
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Transition in SrZnO Laser Pulse Deposited Alloy
Autorzy:
Albrithen, H. A.
Elnaggar, M.
Ozga, K.
Szota, M.
Alahmed, Z. A.
Alanazi, A. Q.
Alshahrani, H.
Alfaifi, E.
Djouadi, M. A.
Labis, J. P.
Powiązania:
https://bibliotekanauki.pl/articles/355190.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
oxide materials
solid state alloys
structural phase transition
X-ray diffraction
scanning electron microscopy
Opis:
We have discovered a structural transition for the SrZnO alloy films from a wurtzite to a rock-salt structure, leading to a reduction in the (112̲0)/(0001) surface energy ratio. The films were grown by pulsed laser deposition using different SrO ratios, x. We have revealed that growth at a higher temperature, 750°C, resulted in a sharp 0002 peak at a low SrO content (5%), whereas growth at a higher SrO content (10%) resulted in a non-crystalline film with minute crystallites with a (112̲0) orientation. Generally the crystallinity decreased as the SrO content increased. No results obtained for the crystalline films showed any orientation of significant peaks besides the peak attributed to the (0001) plane, suggesting epitaxial growth. Optical measurements showed difference in transmission widows of alloys with different SrO percentage, and this was correlated to SrO influence on growth mode as indicated by scanning electron imaging. The studied SrZnO films, with SrO/(SrO + ZnO) ≤ 0.25, were grown by pulsed laser deposition using different SrO ratios, x. The effects of temperature and oxygen pressure during growth on the films’ structural properties were investigated. XRD results indicate that the film crystallinity was improved as the temperature and O2 pressure increased up to 650°C and 0.5 Torr, respectively.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 211-216
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Diageneza kredy jeziornej i gytii w osadach holoceńskich północno-zachodniej Polski
Diagenesis of lacustrine chalk and gyttja in Holocene deposits from northwestern Poland
Autorzy:
Maćkowska, R.
Powiązania:
https://bibliotekanauki.pl/articles/2063003.pdf
Data publikacji:
2011
Wydawca:
Państwowy Instytut Geologiczny – Państwowy Instytut Badawczy
Tematy:
kreda jeziorna
gytia
mikroskopia elektronowa
dyfrakcja rentgenowska
diageneza
lacustrine chalk
gyttja
electron microscopy
X-ray diffraction
diagenesis
Opis:
W artykule przedstawiono procesy diagenetyczne zachodzące w kredzie jeziornej i gytii z osadów holoceńskich północno-zachodniej Polski. Analizom poddano próbki pochodzące ze stanowisk Tarda (Pojezierze Iławskie) oraz Suliszewo (Pojezierze Choszczeńskie). Do oznaczenia składu mineralnego, oprócz metod klasycznych (analiza derywatograficzna), zastosowano nowoczesne metody badawcze. Wykorzystano między innymi analizę chemiczną w mikroobszarze (mikrosonda elektronowa), obserwacje przy pomocy mikroskopu elektronowego oraz analizę rentgenostrukturalną. W kredzie jeziornej i gytii rozpoznano efekty procesów należących do wczesnego stadium diagenezy (eodiagenezy), głównie rozpuszczania minerałów węglanowych, pirytu i kwarcu. Znaczącą rolę odegrała także pirytyzacja oraz tworzenie się wczesnych cementów węglanowych. Stwierdzono, że w badanych osadach kompakcja zachodziła tylko na niewielką skalę. Ponadto odtworzono kolejność procesów diagenetycznych. Najwcześniejszym procesem diagenetycznym w badanej kredzie jeziornej i gytii było tworzenie się cementu mikrytowego oraz pirytyzacja. W dalszej kolejności osady były poddawane procesom rozpuszczania. Dopiero potem nastąpiła kompakcja. Po odwodnieniu próbek i ich osuszeniu z wód porowych wykrystalizował gips i halit.
The aim of this paper is to present the diagenetic processes occurring within lacustrine chalk and ooze in Holocene deposits from northwestern Poland. The analysed samples came from the Tarda (Iława Lake District) and Suliszewo (Choszczno Lake District) sites. For the purpose of mineral composition determination, both modern and classic (thermal analysis) research methods were applied. Composition analysis on a microprobe (Scanning Electron Microscopy) and X-ray structural analysis (Powder X-ray Diffraction) were used. Effects of early diagenesis processes (eodiagenesis) are observed in these sediments. The most important diagenetic processes include dissolution of carbonate minerals, pyrite and quartz. An important role was also played by pyritization and formation of early carbonate cements. Compaction occurred only on a small scale. Moreover, the sequence of the diagenetic processes was reconstructed. The earliest diagenetic process that occurred within the lacustrine chalk and ooze was the formation of micritic cement and pyritization. Successively, the whole sediment was undergoing dissolution processes, followed by compaction. After dehydration and drying of the samples, gypsum and halite crystallized from the pore waters.
Źródło:
Biuletyn Państwowego Instytutu Geologicznego; 2011, 444; 149--155
0867-6143
Pojawia się w:
Biuletyn Państwowego Instytutu Geologicznego
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Amorphization and liquid state separation in Ni80-2xCuxFexP20 alloys
Amorfizacja i podział w stanie ciekłym w stopach Ni80-2xCuxFexP20
Autorzy:
Ziewiec, K.
Prusik, K.
Różycka, M.
Powiązania:
https://bibliotekanauki.pl/articles/263952.pdf
Data publikacji:
2014
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
amorphous materials
amorphization
X-ray diffraction
transmission electron microscopy
materiały amorficzne
amorfizacja
dyfrakcja rentgenowska
transmisyjna mikroskopia elektronowa
Opis:
The aim of the work is to study the ability and potential of glass formation in Ni-Fe-Cu-P alloys. A series of alloys were produced in arc furnace (i.e. Ni70Fe5Cu5P20, Ni60Fe10Cu10P20, Ni50Fe15Cu15P20, Ni40Fe20Cu20P20, Ni30Fe25Cu25P20, Ni20Fe30Cu30P20). The primary microstructure of the ingots was studied. The ribbons in as-melt-spun state were characterized by X-ray diffraction (XRD). The Ni70Fe5Cu5P2, Ni60Fe10Cu10P20 melt-spun alloys were found to be amorphous. For higher copper and iron concentrations a crystalline structure was obtained after melt spinning. This correlated with the tendency for the formation of the Fe-based phases enriched in P and Cu-based poorly alloyed phases which resulted in the formation of crystalline microstructure in melt-spun ribbons. For higher concentration of Fe and Cu, microstructures of the alloys contained constituents resultant from a tendency for separation in the liquid state. It is observed that the formation of the crystal line melt-spun ribbons is caused by the attraction of phosphorus by iron and the formation of copper-based fcc phase.
Celem pracy było zbadanie podatności na zeszklenie oraz możliwości wytworzenia struktury szklistej w stopach wieloskładnikowych Ni-Fe-Cu-P. W piecu łukowym wytworzono serię stopów (tzn.: Ni70Fe5Cu5P20, Ni60Fe10Cu10P20, Ni50Fe15Cu15P20, Ni40Fe20Cu20P20, Ni30Fe25Cu25P20, Ni20Fe30Cu30P20). Badano strukturę pierwotną wlewków. Taśmy w stanie po odlewaniu na wirujący bęben badano za pomocą dyfrakcji rentgenowskiej. Stwierdzono, że stopy Ni70Fe5Cu5P20, Ni60Fe10Cu10P20 odlewane na wirujący bęben były amorficzne. Dla stopów o wyższych zawartościach miedzi i żelaza po odlewaniu na wirujący walec otrzymano strukturę krystaliczną. Fakt ten można powiązać z tendencją do tworzenia faz na osnowie żelaza wzbogaconych w fosfor oraz zubożonych w pozostałe składniki stopowe faz na osnowie miedzi,które przyczyniły się do tworzenia w odlewanych taśmach mikrostruktury krystalicznej. Dla wyższych zawartości żelaza i miedzi, mikrostruktury stopów zawierały składniki fazowe powstające w efekcie tendencji stopów do podziału fazowego w stanie ciekłym. Zaobserwowano, że tworze nie krystalicznych taśm jest spowodowane przez przyciąganie fosforu przez żelazo oraz tworzenie bogatej w miedź fazy o strukturze regularnej ściennie centrowanej.
Źródło:
Metallurgy and Foundry Engineering; 2014, 40, 1; 45-54
1230-2325
2300-8377
Pojawia się w:
Metallurgy and Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Infrared studies and spectral properties of photochromic high silica glasses
Autorzy:
Girsova, M A
Golovina, G F
Drozdova, I.A.
Polyakova, I G
Antropova, T V
Powiązania:
https://bibliotekanauki.pl/articles/174765.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
silica porous glass
photochromic high silica glass
transmission electron microscopy TEM
X-ray diffraction (XRD)
UV–VIS–IR transmission spectra
Opis:
The structure of photochromic high silica glasses (PHSGs) was studied by UV–VIS–NIR and IR spectroscopy, transmission electron microscopy (TEM) and X-ray diffraction (XRD) techniques. PHSG plates were obtained by impregnation of silica porous glasses at first with AgNO3 aqueous solution (in or without the presence of the sensitizers, such as Cu(NO3)2 or Ce(NO3)3), next in the mixed halide salt (NH4Cl, KBr, KI) solution. Then a part of the samples was sintered at temperatures from 850 to 900 °C up to closing of the pores. The results of TEM study have shown that the PHSG plates have two-phase structure with inclusions of the size of 10–100 nm. According to XRD data, the PHSGs contain the AgBr phase. IR spectra confirmed the presence of AgI, AgCl, CeO2, CuCl2, CuCl phases in PHSGs.
Źródło:
Optica Applicata; 2014, 44, 2; 337-344
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterisation of Mg-Zn-Ca-Y powders manufactured by mechanical milling
Autorzy:
Lesz, S.
Tański, T.
Hrapkowicz, B.
Karolus, M.
Popis, J.
Wiechniak, K.
Powiązania:
https://bibliotekanauki.pl/articles/1818808.pdf
Data publikacji:
2020
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
Mg-based alloys
scanning electron microscopy
X-ray diffraction analysis
mechanical alloying
stopy magnezu
skaningowa mikroskopia elektronowa
rentgenowska analiza dyfrakcyjna
mechaniczna synteza
Opis:
Purpose: This paper explains mechanical synthesis which uses powders or material chunks in order to obtain phases and alloys. It is based on an example of magnesium powders with various additives, such as zinc, calcium and yttrium. Design/methodology/approach: The following experimental techniques were used: X-ray diffraction (XRD) method, scanning electron microscopy (SEM), determining particle size distributions with laser measuring, Vickers microhardness. Findings: The particle-size of a powder and microhardness value depend on the milling time. Research limitations/implications: Magnesium gained its largest application area by creating alloys in combination with other elements. Magnesium alloys used in various industry contain various elements e.g. rare-earth elements (REE). Magnesium alloys are generally made by casting processes. Consequently, the search for new methods of obtaining materials such as mechanical alloying (MA) offers new opportunities. The MA allows for the production of materials with completely new physico-chemical properties. Originality/value: Thanks to powder engineering it is possible to manufacture materials with specific chemical composition. These materials are characterized by very high purity, specified porosity, fine-grain structure, complicated designs. These are impossible to obtain with traditional methods. Moreover it is possible to refine the process even further minimalizing the need for finishing or machining, making the material losses very small or negligible. Furthermore material manufactured in such a way can be thermally or chemically processed without any problems.
Źródło:
Journal of Achievements in Materials and Manufacturing Engineering; 2020, 103, 2; 49--59
1734-8412
Pojawia się w:
Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-25 z 35

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