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Wyświetlanie 1-15 z 66
Tytuł:
Formation And Stabilization Of Silver Nanoparticles In Ethanol By Phosphinic Acid
Redukcja i stabilizacja nanocząstek srebra w etanolu przez kwas fosforowy
Autorzy:
Kim, J.-K.
Shim, H.-M.
Park, M. J.
Koo, K.-K.
Powiązania:
https://bibliotekanauki.pl/articles/356073.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silver
nanoparticle
kinetic analysis
phosphinic acid
reduction
srebro
nanocząstki
analiza kinetyczna
kwas fosforowy
redukcja
Opis:
Although phosphinic acid (H3PO2) has a powerful reduction potential, the reduction of silver ions by phosphinic acid salt has not yet been reported. In this work, colloidal silver has successfully synthesized by reducing silver ions in ethanol with phosphinic acid as a reducing agent. The effects of [AgNO3]/[H3PO2] ratios and reaction temperature were considered. Spherical silver nanoparticles with cubic structure were successfully prepared and their diameters were measured to be 8.5±0.9 nm − 11.3±0.2 nm. Half-life analysis showed that the reduction of silver ions proceeded with the reaction order of 1.30 on concentration of phosphinic acid and activation energy of 120.7 kJ/mol.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1293-1296
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation of Tungsten/Ammonium Perchlorate Composites and Their Reaction Kinetics
Autorzy:
Shim, H.-M.
Lee, E.-A.
Kim, J.-K.
Kim, H.-S.
Koo, K.-K.
Powiązania:
https://bibliotekanauki.pl/articles/358373.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
ammonium perchlorate
composite
thermal decomposition
Opis:
The reaction kinetics of tungsten nanoparticles/ammonium perchlorate (W/AP) composites, produced by a spray drying technique, were analyzed and compared with those of neat AP particles and aluminum nanoparticles/AP (Al/AP) composites. The W was found to raise the onset temperature of the thermal decomposition of AP by increasing the activation energy, whereas Al conversely lowered the onset temperature of AP due to the decreased activation energy. From the master plots of kinetic models with the experimental data, the Prout-Tompkins model and the 1-D diffusion controlled model were found to describe the low-temperature decomposition (LTD) and high-temperature decomposition (HTD), respectively, giving remarkable agreement with experimental curves for all heating rates. The presence of W was found to increase the HTD zone width compared with that of neat AP particles and Al/AP composites. Analysis of the average activation energy and pre-exponential factor showed that W increases the energy barrier and the frequency of occurrence of the reaction compared with that of neat AP particles at the LTD state, whereas W decreases both of them at the HTD state. The effect of Al was also shown to be similar to that of W, but the magnitudes of the variation in activation energy and the pre-exponential factor were relatively small.
Źródło:
Central European Journal of Energetic Materials; 2015, 12, 4; 703-722
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Carbon Nanotubes On The Properties Of Spark Plasma Sintered ZrO2/CNT Composites
Wpływ nanorurek węglowych na właściwości spiekanych metodą sps kompozytów ZrO2/CNT
Autorzy:
Shim, D. H.
Jung, S. S.
Kim, H. S.
Cho, H.
Kim, J. K.
Kim, T. G.
Yoon, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/351266.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
CNT
ZrO2
composite
SPS
kompozyty
Opis:
Zirconia matrix ZrO2/CNT composite materials reinforced with multiwall carbon nanotubes were fabricated using a spark plasma sintering technique. The effects of the amount of CNTs addition, sintering temperature and sintering pressure on the properties of the resulting ZrO2/CNT composites were examined. 0 to 9 vol. % CNTs were dispersed in zirconia powder, and the resulting mixture was sintered. The electrical conductivity, hardness, flexural strength, and density were measured to characterize the composites. The friction and wear properties of the composites were also tested. The flexural strength and friction coefficient of the composites were improved with up to 6 vol.% of CNT addition and the flexural strength showed a close relationship with the relative density of the composite. The electrical conductivity increased with increasing proportion of the CNTs, but the efficiency was reduced at more than 6 vol.% CNTs.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1315-1318
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis Of The Extrusion Process Of A Square Tube Multi-Channel Heat Pipe
Analiza procesu wytłaczania wielokanałowych ciepłowodów o kwadratowym przekroju
Autorzy:
Kim, K. S.
Kim, J. Y.
Powiązania:
https://bibliotekanauki.pl/articles/353935.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum hot extrusion
FE simulation
stress analysis
extrusion experiment
aluminium wytłaczane na gorąco
symulacja FE
analiza naprężeń
wytłaczanie
Opis:
Heat pipes have been recently in use for cooling purposes in various fields, including electronic circuit boards and vehicle parts that generate large amounts of heat. In order to minimize the loss of heat transferred, there is a need to maximize the contact area of the working fluid. This study produced a square tube multi-channel heat pipe to replace the existing circular pipe type to maximize the internal surface area thereof. This expands the surface, allowing the working fluid to come into contact with a wider area and enhancing thermal radiation performance. A mold for the production for such a product was designed, and finite element simulation was performed to determine whether production is possible.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1463-1466
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and Optical Properties of Hydrothermally Synthesized ZnO and $Zn_{0.99}O:Eu^{3+}$ Powders
Autorzy:
Park, K.
Hakeem, D.
Kim, J.
Kim, Y.
Kim, S.
Powiązania:
https://bibliotekanauki.pl/articles/1398243.pdf
Data publikacji:
2018-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.55.-m
78.55.Hx
78.55.Et
Opis:
The structural and optical properties of the ZnO and $Zn_{0.99}O:Eu^{3+}$ powders synthesized by the hydrothermal method at two different temperatures (150°C and 250°C) were studied. The ZnO and $Zn_{0.99}O:0.01Eu^{3+}$ powders synthesized at 150 and 250°C showed rod- and flower-like morphologies, respectively. The as-synthesized and annealed ZnO and $Zn_{0.99}O:0.01Eu^{3+}$ powders formed the wurtzite crystal structure and P6₃mc space group. The crystallite size of the as-synthesized and annealed ZnO powders increased by the incorporation of $Eu^{3+}. The photoluminescence properties of annealed $Zn_{0.99}O:0.01Eu^{3+}$ powders were substantially improved by controlling the synthesis temperature. The annealed $Zn_{0.99}O:0.01Eu^{3+}$ powders synthesized at 250°C displayed much stronger emission intensity than those at 150°C.
Źródło:
Acta Physica Polonica A; 2018, 133, 4; 902-906
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Loading Time of a Load Plate and Sample Size on the Measurement of Physical Properties of Resilient Materials
Autorzy:
Kim, K.-W.
Yeon, J.-O.
Yang, K.-S.
Kim, M.-J.
Powiązania:
https://bibliotekanauki.pl/articles/178069.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
resilient materials
dynamic stiffness
compressibility
long-term deformation
Opis:
This study investigates several factors that have not been specified in the standard for dynamic stiffness, compressibility, and long-term deformation; these factors can be used to evaluate the acoustic and physical performances of resilient materials. The study is intended to provide basic data for deriving the factors that need to be additionally reviewed through the standards. Since magnitude of dynamic stiffness changes with an increase in loading time, it is necessary to examine the setting of the loading time for a load plate under test conditions. Samples of size 300×300 mm, rather than 200×200 mm, yielded more reliable results for compressibility measurement. Since the test to infer long-term deformation of resilient materials after a period of 10 years in some samples showed variation characteristics different from those specified in the standards, it is recommended that the test method should be reviewed through ongoing research.
Źródło:
Archives of Acoustics; 2015, 40, 2; 159-167
0137-5075
Pojawia się w:
Archives of Acoustics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on the Microstructure and Tensile Deformation Behavior of Oxide Dispersion Strengthened Alloys Manufactured by Complex Milling Process
Autorzy:
Kim, Y.-K.
Kim, J.-H.
Gwon, J.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352535.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
oxide dispersion strengthening
microstructure
tensile deformation behavior
Opis:
This study attempted to manufacture an ODS alloy by combining multiple milling processes in mechanical alloying stage to achieve high strength and fracture elongation. The complex milling process of this study conducted planetary ball milling, cryogenic ball milling and drum ball milling in sequential order, and then the microstructure and tensile deformation behavior were investigated after additional heat treatment. The oxide particles distributed within the microstructure were fine oxide particles of 5~20 nm and coarse oxide particles of 100~200 nm, and the oxide particles were confirmed to be composed of Cr, Ti, Y and O. Results of tensile tests at room temperature measured yield strength, tensile strength and elongation as 1320 MPa, 2245 MPa and 4.2%, respectively, before heat treatment, and 1161 MPa, 2020 MPa and 5.5% after heat treatment. This results indicate that the ODS alloy of this study gained very high strengths compared to other known ODS alloys, allowing greater plastic zones.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1335-1340
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of Fe-TiB2 Nanocomposites by Spark-Plasma Sintering of a (FeB, TiH2) Powder Mixture
Autorzy:
Huynh, X.-K.
Kim, B.-W.
Kim, J.-S.
Powiązania:
https://bibliotekanauki.pl/articles/351368.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-TiB2 nanocomposite
mechanical activation
spark plasma sintering
self-propagating high-temperature synthesis reaction
Opis:
Fe-40wt% TiB2 nanocomposites were fabricated by mechanical activation and spark-plasma sintering of a powder mixture of iron boride (FeB) and titanium hydride (TiH2). The powder mixture of (FeB, TiH2) was prepared by high-energy ball milling in a planetary ball mill at 700 rpm for 3 h followed by spark-plasma sintering (SPS) at various conditions. Analysis of the change in relative sintered density and densification rate during sintering showed that a self-propagating high-temperature synthesis reaction occurs to form TiB2 from FeB and Ti. A sintered body with relative density higher than 98% was obtained after sintering at 1150°C for 5 and 15 min. The microstructural observation of sintered compacts with the use of FE-SEM and TEM revealed that ultrafine particulates with approximately 5 nm were evenly distributed in an Fe-matrix. A hardness value of 83 HRC was obtained, which is equivalent to that of conventional WC-20 Co systems.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1043-1047
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Mechanical Activation on the in situ Formation of TiB2 Particulates in the Powder Mixture of TiH2 and FeB
Autorzy:
Huynh, X.-K.
Kim, B.-W.
Kim, J. S.
Powiązania:
https://bibliotekanauki.pl/articles/355844.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
mechanical activation
in situ formation
TiB2 particulate
Fe-matrix
specific ball-milling energy
Opis:
The in situ formation of TiB2 particulates via an interface reaction between Ti and FeB powders was studied. The effects of mechanical activation by high-energy milling on the decomposition of TiH2 and the interface reactions between Ti and FeB powders to form TiB2 were investigated. Powder mixtures were fabricated using planetary ball-milling under various milling conditions. The specific ball-milling energy was calculated from the measured electrical power consumption during milling process. High specific milling energy (152.6 kJ/g) resulted in a size reduction and homogeneous dispersion of constituent powders. This resulted in a decrease in the decomposition temperature of TiH2 and an increase in the formation reaction of TiB2 particulates in the Fe matrix, resulting in a homogeneous microstructure of nanoscale TiB2 evenly distributed within the Fe matrix. In contrast, the powder mixture milled with low specific milling energy (36.5 kJ/g) showed an inhomogeneous microstructure composed of relatively large Fe-Fe2 B particles surrounded by a thin layer of Fe-TiB2 within a finely dispersed Fe-TiB2 matrix region.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1393-1398
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Additive Element on the Properties of Mechanically Alloyed Fe-Y2O3 Alloys
Autorzy:
Ahn, J.-H.
Kim, T. K.
Ahn, J.
Powiązania:
https://bibliotekanauki.pl/articles/356561.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
mechanical alloying
ODS alloy
nanoparticles
oxide dispersion strengthening
high-energy ball milling
Opis:
In the present work, we have examined the effect of Ti on the properties of Fe-Y2O3 alloys. The result showed that the addition of Ti was effective for improving mechanical properties. This is due to the reduction of oxides by Ti during mechanical alloying and hot-consolidation. In particular, iron oxides are effectively reduced by the addition of Ti. Compared to the pristine Fe-Y2O3 alloys, titanium-added alloys exhibited fine and uniform microstructures, resulting in at least 60% higher tensile strength.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1043-1046
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Growth and Characterization of Indium-Doped Zinc Oxide Thin Films Prepared by Sol-Gel Method
Autorzy:
Kim, M.
Yim, K.
Kim, S.
Nam, G.
Lee, D.
Kim, Jin
Kim, Jong
Leem, J.
Powiązania:
https://bibliotekanauki.pl/articles/1491351.pdf
Data publikacji:
2012-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Dz
81.20.Fw
78.66.Hf
Opis:
Indium-doped ZnO thin films were deposited by sol-gel spin-coating method with various In content. The effects of In content on the structural and optical properties of the indium-doped ZnO thin films were investigated by scanning electron microscopy, X-ray diffraction, and UV-visible spectroscopy. The particle-like surface morphology and the crystallinity of the indium-doped ZnO thin films were affected by change in the In content, especially at the In content of 3 at.%. The values of direct band gap were decreased with increase in the In content. The width of localized states in the optical band gap of the indium-doped ZnO thin films were changed with In content and the Urbach energy $(E_{U})$ was changed inversely with optical band gap of the indium-doped ZnO thin films.
Źródło:
Acta Physica Polonica A; 2012, 121, 1; 217-220
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of Image Processing to Predict Compressive Behavior of Aluminum Foam
Autorzy:
Kim, S.
Chung, H. J.
Rhee, K.
Powiązania:
https://bibliotekanauki.pl/articles/357032.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum foam
compute tomography (CT) image
finite element method (FEM)
Opis:
An image processing technique was used to model the internal structure of aluminum foam in finite element analysis in order to predict the compressive behavior of the material. Finite element analysis and experimental tests were performed on aluminum foam with densities of 0.2, 0.25, and 0.3 g/cm3. It was found that although the compressive strength predicted from the finite element analysis was higher than that determined experimentally, the predicted compressive stress-strain curves exhibited a tendency similar to those determined from experiments for both densities. However, the behavior of the predicted compressive stress-strain curves was different from the experimental one as the applied strain increased. The difference between predicted and experimental stress-strain curves in a high strain range was due to contact between broken aluminum foam walls by the large deformation.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 635-640
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Causal relationship between supply chain dynamic capabilities, technological innovation, and operational performance
Autorzy:
Ju, K.-J.
Park, B.
Kim, T.
Powiązania:
https://bibliotekanauki.pl/articles/407389.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
supply chain management
dynamic capabilities
supply chain dynamic capabilities
technological innovation
operational performance
Opis:
The aim of this study is to empirically examine the impact of supply chain dynamic capabilities on operational performance, and the mediating effect of technological innovation between dynamic capabilities and operational performance. This study is based on empirical data collected from a survey of 206 small- and medium-size firms in Korea. Structural equation modeling is used to test the research questions. The results show that supply chain dynamic capabilities positively influence technological innovation and operational performance of an enterprise. Additionally, structural equation analyses reveal that technological innovation plays a role as a partial mediator of the relationship between supply chain dynamic capabilities and operational performance. In a dynamic and ever-changing environment, the enforcement of dynamic capabilities in a sustainable supply chain is important for the innovation of technology and the improvement of operational performance. Further investigation is required to understand the differences by industries, characteristics of enterprises, and positions in a supply chain.
Źródło:
Management and Production Engineering Review; 2016, 7, 4; 6-15
2080-8208
2082-1344
Pojawia się w:
Management and Production Engineering Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
ZnO Nanorods on Nanofibrous ZnO Seed Layers by Hydrothermal Method and Their Annealing Effects
Autorzy:
Yim, K.
Jeon, S.
Kim, M.
Kim, S.
Nam, G.
Lee, D.
Kim, Jin
Kim, Jong
Leem, J.
Powiązania:
https://bibliotekanauki.pl/articles/1491348.pdf
Data publikacji:
2012-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Dz
81.15.Lm
78.55.Et
Opis:
ZnO nanorods were grown by using the hydrothermal method on p-type Si (100) substrates with nanofibrous ZnO seed layers. Before the ZnO nanorods growth, nanofibrous ZnO seed layers were spin-coated onto the Si substrates. The structural and optical properties of ZnO nanorods were characterized by scanning electron microscopy, X-ray diffraction, and photoluminescence. The fibrous ZnO nanorods is possible due to the surface morphology of the nanofibrous ZnO seed layers. To investigate annealing effects of the ZnO nanorods, the post-annealing process was carried out at various temperatures ranging from 300 to 700C under argon conditions. The structural and optical properties of the ZnO nanorods were also affected by the post-annealing treatment.
Źródło:
Acta Physica Polonica A; 2012, 121, 1; 214-216
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 66

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