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    Wyświetlanie 1-11 z 11
    Tytuł:
    Rapid Synthesis of Gold Nano-Particles Using Pulse Waved Potential in a Non-Aqueous Electrolyte
    Autorzy:
    Jang, J. G.
    Lee, J.-O.
    Lee, C. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/352529.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    gold
    nanoparticle
    nonaqueous electrolyte
    pulse wave
    catalyst
    Opis:
    Rapid synthesis of gold nanoparticles (AuNPs) by pulsed electrodeposition was investigated in the non-aqueous electrolyte, 1-ethyl-3-methyl-imidazoliumbis(trifluoro- methanesulfonyl)imide ([EMIM]TFSI) with gold trichloride (AuCl3). To aid the dissolution of AuCl3, 1-ethyl-3-methyl-imidazolium chloride ([EMIM]Cl) was used as a supporting electrolyte in [EMIM]TFSI. Cyclicvoltammetry experiments revealed a cathodic reaction corresponding to the reduction of gold at −0.4 V vs. Pt-QRE. To confirmthe electrodeposition process, potentiostatic electrodeposition of gold in the non-aqueous electrolyte was conducted at −0.4 V for 1 h at room temperature. To synthesize AuNPs, pulsed electrodeposition was conducted with controlled duty factor, pulse duration, and overpotential. The composition, particle-size distribution, and morphology of the AuNPs were confirmed by field-emission scanning electron microscopy (FE-SEM), energy-dispersive spectroscopy (EDS), and transmission electron microscopy (TEM). The electrodeposited AuNPs were uniformly distributed on the platinum electrode surface without any impurities arising from the non-aqueous electrolyte. The size distribution of AuNPs could be also controlled by the electrodeposition conditions.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1389-1392
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Oxide Formation In Metal Injection Molding Of 316L Stainless Steel
    Tworzenie tlenków podczas wtryskiwania proszku stali nierdzewnej 316L
    Autorzy:
    Jang, J. M.
    Lee, W.
    Ko, S.-H.
    Han, C.
    Choi, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/351352.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    powder injection molding
    sintering
    316L stainless steel
    sintering atmosphere
    micro parts
    wtryskiwanie proszku
    spiekanie
    stal nierdzewna 316L
    mikro-część
    Opis:
    The effects of sintering condition and powder size on the microstructure of MIMed parts were investigated using water-atomized 316L stainless steel powder. The 316L stainless steel feedstock was injected into micro mold with micro features of various shapes and dimensions. The green parts were debound and pre-sintered at 800°C in hydrogen atmosphere and then sintered at 1300°C and 1350°C in argon atmosphere of 5torr and 760torr, respectively. The oxide particles were formed and distributed homogeneously inside the sample except for the outermost region regardless of sintering condition and powder size. The width of layer without oxide particles are increased with decrease of sintering atmosphere pressure and powder size. The fine oxides act as the obstacle on grain growth and the high sintering temperature causes severe grain growth in micro features due to larger amount of heat gain than that in macro ones.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1281-1285
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of Antireflection Structures as a Protective Layer of Solar Cells with Nanoporous Silica Films and Nanoimprinted Moth-Eye Structure
    Autorzy:
    Kim, K.
    Han, J.
    Jang, J.
    Choi, C.
    Choi, S.
    Kim, C.
    Kye, H.
    Cheong, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1492625.pdf
    Data publikacji:
    2011-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.46.-w
    68.37.-d
    68.55.-a
    78.20.-e
    Opis:
    The antireflection structures are fabricated by sol-gel process as a protective layer of solar cells and by hot embossing process with anodized aluminum oxide membrane template on polycarbonate film. The optical properties and morphology of the antireflection structures are analyzed by UV-visible spectroscopy and field emission scanning electron microscopy, respectively. The total conversion efficiency of a polycrystalline Si solar cell module with the protective layer, sol-gel-derived nanoporous antireflection structure, is increased by 2.6% and 5.7% for one-side antireflection coated prismatic matt glass and both-side antireflection coated prismatic matt glass, respectively.
    Źródło:
    Acta Physica Polonica A; 2011, 120, 6A; A-047-A-049
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of SiC Particles On Sinterability Of Al-Zn-Mg-Cu P/M Alloy
    Wpływ cząstek SiC na spiekalność proszku stopowego Al-Zn-Mg-Cu
    Autorzy:
    Rudianto, H.
    Jang, G. J.
    Yang, S. S.
    Kim, Y. J.
    Dlouhy, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/351304.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    metal matrix composites
    powder metallurgy
    sintering
    heat treatment
    kompozyty metalowe
    metalurgia proszków
    spiekanie
    obróbka cieplna
    Opis:
    Premix Al-5.5Zn-2.5Mg-0.5Cu alloy powder was analyzed as matrix in this research. Gas atomized powder Al-9Si with 20% volume fraction of SiC particles was used as reinforcement and added into the alloy with varied concentration. Mix powders were compacted by dual action press with compaction pressure of 700 MPa. High volume fraction of SiC particles gave lower green density due to resistance of SiC particles to plastic deformation during compaction process and resulted voids between particles and this might reduce sinterability of this mix powder. Sintering was carried out under ultra high purity nitrogen gas from 565°-580°C for 1 hour. High content of premix Al-5.5Zn-2.5Mg-0.5Cu alloy powder gave better sintering density and reached up to 98% relative. Void between particles, oxide layer on aluminum powder and lower wettability between matrix and reinforcement particles lead to uncompleted liquid phase sintering, and resulted on lower sintering density and mechanical properties on powder with high content of SiC particles. Mix powder with wt90% of Alumix 431D and wt10% of Al-9Si-vf20SiC powder gave higher tensile strength compare to another mix powder for 270 MPa. From chemical compositions, sintering precipitates might form after sintering such as MgZn2, CuAl2 and Mg2Si. X-ray diffraction, DSC-TGA, and SEM were used to characterize these materials.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1383-1385
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Pre-Sintering on the Diffusion Treatment of HRE for Coercivity Enhancement of a NdFeB Sintered Magnet
    Autorzy:
    Lee, M. W.
    Lee, J. K.
    Jang, T. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/355250.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    grain boundary diffusion process
    GBDP
    NdFeB magnet
    coercivity
    pre-sintering
    Opis:
    We investigated the effect of pre-sintering process on the penetration behavior of Dy in a NdFeB sintered magnet which was grain boundary diffusion treated with Cu/Al mixed Dy source. The pre-sintering of a magnet was performed at 900°C in vacuum and then the pre-sintered body was dipped in the solutions of DyH2, DyH2 + Cu, and DyH2 + Al, respectively. The dipped pre-sintered body were then fully sintered 4 hours at 1060°C followed by a subsequent annealing. The pre-sintering apparently improved the diffusivity of Dy atoms. The penetration of Dy into the magnet extended almost to 2,000 μm from the surface, about four times deeper than that of the normally sintered and diffusion treated one, when the DyH2 + Al solution was used as a Dy source. However, the resulting increase of coercivity was about 4 kOe, somewhat lower than that of the normally treated one, mostly due to excessive oxide formation that hindered to make a continuous Nd-rich grain boundary phase and a core-shell type structure.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 2; 597-601
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Aluminum Oxide Formation On Fecral Catalyst Support By Electro-Chemical Coating
    Powstawanie tlenku glinu na nośniku katalizatora FeCrAl przez osadzanie elektrochemiczne
    Autorzy:
    Yang, H. S.
    Jang, D. H.
    Lee, K. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/355942.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    FeCrAl
    catalyst support
    aluminum oxide formation
    PEO
    plasma electrolytic oxidation
    electrochemical coating
    nośnik katalizatora
    tlenek glinu
    plazmowe utlenianie elektrolityczne
    elektrochemiczne osadzanie
    Opis:
    FeCrAl is comprised essentially of Fe, Cr, Al and generally considered as metallic substrates for catalyst support because of its advantage in the high-temperature corrosion resistance, high mechanical strength, and ductility. Oxidation film and its adhesion on FeCrAl surface with aluminum are important for catalyst life. Therefore various appropriate surface treatments such as thermal oxidation, Sol, PVD, CVD has studied. In this research, PEO (plasma electrolytic oxidation) process was applied to form the aluminum oxide on FeCrAl surface, and the formed oxide particle according to process conditions such as electric energy and oxidation time were investigated. Microstructure and aluminum oxide particle on FeCrAl surface after PEO process was observed by FE-SEM and EDS with element mapping analysis. The study presents possibility of aluminum oxide formation by electro-chemical coating process without any pretreatment of FeCrAl.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1503-1506
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Point-Contact Spectroscopy of Superconducting $MgCNi_3$ Single Crystals
    Autorzy:
    Pribulová, Z.
    Szabó, P.
    Kačmarčík, J.
    Samuely, P.
    Jang, D.
    Lee, H.
    Lee, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1813611.pdf
    Data publikacji:
    2008-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    74.50.+r
    Opis:
    The first point-contact spectroscopy measurements on $MgCNi_3$ single crystals of very good quality are presented. The measurements have been performed in the temperature range from 1.5 K up to 10 K and at magnetic fields up to 6 T. The superconducting energy gap Δ of the system is found to be scattered between 1 and 1.2 meV which gives the 2Δ/k $T_c$ ratio between BCS weak-coupling value of ~3.5 and a strong coupling of about 4.2. The excess current evaluated in magnetic field indicates the presence of a single energy gap.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 1; 215-218
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Magnetic Properties of NdFeB Sintered Magnets Diffusion-Treated with Cu/Al Mixed Dyco Alloy-Powder
    Autorzy:
    Lee, M.-W.
    Bae, K.-H.
    Lee, S.-R.
    Kim, H.-J.
    Jang, T.-S.
    Powiązania:
    https://bibliotekanauki.pl/articles/353351.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B sintered magnets
    grain boundary diffusion process
    low melting point element
    DyCo alloy-powder diffusion
    Opis:
    We investigated the microstructural and magnetic property changes of DyCo, Cu + DyCo, and Al + DyCo diffusion-treated NdFeB sintered magnets. The coercivity of all diffusion treated magnet was increased at 880ºC of 1st post annealing(PA), by 6.1 kOe in Cu and 7.0 kOe in Al mixed DyCo coated magnets, whereas this increment was found to be relatively low (3.9 kOe) in the magnet coated with DyCo only. The diffusivity and diffusion depth of Dy were increased in those magnets which were treated with Cu or Al mixed DyCo, mainly due to comparatively easy diffusion path provided by Cu and Al because of their solubility with Ndrich grain boundary phase. The formation of Cu/Al-rich grain boundary phase might have enhanced the diffusivity of Dy-atoms. Moreover, relatively a large number of Dy atoms reached into the magnet and mostly segregated at the interface of Nd2 Fe14 B and grain boundary phases covering Nd2 Fe14 B grains so that the core-shell type structures were developed. The formation of highly anisotropic (Nd, Dy)2Fe14B phase layer, which acted as the shell in the core-shell type structure so as to prevent the reverse domain movement, was the cause of enhancing the coercivity of diffusion treated NdFeB magnets. Segregation of cobalt in Nd-rich TJP followed by the formation of Co-rich phase was beneficial for the coercivity enhancement, resulting in the stabilization of the metastable c-Nd2O3 phase.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1263-1266
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    AC Microcalorimetry of Superconducting $MgCNi_3$ Single Crystals
    Autorzy:
    Kačmarčík, J.
    Pribulová, Z.
    Samuely, P.
    Marcenat, C.
    Klein, T.
    Jang, D.
    Lee, H.
    Lee, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1813689.pdf
    Data publikacji:
    2008-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    74.70.Ad
    74.25.Bt
    Opis:
    The low-temperature specific heat of single-crystal samples of superconducting $MgCNi_3$ with typical dimensions 200 μm were measured for the first time. A computer controlled ac microcalorimeter using an optical fiber and an infrared light-emitting diode as the heat source was used down to 2 K at magnetic fields up to 8 T. The specific heat data suggest a moderate coupling in $MgCNi_3$.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 1; 363-366
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of DyMn Alloy-Powder Addition On Microstructure And Magnetic Properties Of NdFeB Sintered Magnets
    Wpływ dodatku proszku DyMn na mikrostrukturę i właściwości magnetyczne spiekanych magnesów NdFeB
    Autorzy:
    Lee, M.-W.
    Dhakal, D. R.
    Kim, T. H.
    Lee, S. R.
    Kim, H. J.
    Jang, T. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/357010.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B sintered magnets
    DyMn-alloy powder
    coercivity
    low melting point element
    magnesy spiekane
    proszek DyMn
    koercja
    elementy o niskiej temperaturze topnienia
    Opis:
    Micostructural change and corresponding effect on coercivity of a NdFeB sintered magnet mixed with small amount of DyMn powder was investigated. In the sintered magnet mixed with the DyMn alloy-powder Dy-rich shell was formed at outer layer of the main grains, while Mn was mostly concentrated at Nd-rich triple junction phase (TJP), lowering melting temperature of the Nd-rich phase that eventually improved the microstructural characteristics of the gain boundary phase. The coercivity of a magnet increased more than 3.5 kOe by the mixing of the DyMn alloy-powder.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1407-1409
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Self-Consolidation and Surface Modification of Mechanical Alloyed Ti-25.0 at.% Al Powder Mixture by Using an Electro-Discharge Technique
    Autorzy:
    Chang, S. Y.
    Jang, H. S.
    Yoon, Y. H.
    Kim, Y. H.
    Kim, J. Y.
    Lee, Y. K.
    Lee, W. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354212.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    sintering
    mechanical alloying
    powder consolidation
    intermetallic compounds
    titanium aluminides
    Opis:
    Electrical discharges using a capacitance of 450 μF at 0.5, 1.0, and 1.5 kJ input energies were applied in a N2 atmosphere to obtain the mechanical alloyed Ti3Al powder without applying any external pressure. A solid bulk of nanostructured Ti3Al was obtained as short as 160 μsec by the Electrical discharge. At the same time, the surface has been modified into the form of Ti and Al nitrides due to the diffusion process of nitrogen to the surface. The input energy was found to be the most important parameter to affect the formation of a solid core and surface chemistry of the compact.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1293-1297
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-11 z 11

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