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Wyświetlanie 1-15 z 19
Tytuł:
Synthesis And Electrochemical Characteristics Of Mechanically Alloyed Anode Materials SnS2 For Li/SnS2 Cells
Synteza mechaniczna i charakterystyka elektrochemiczna materiałów anodowych SnS2 dla ogniw Li/SnS2
Autorzy:
Hong, J. H.
Liu, X. J.
Park, D. K.
Kim, K. W.
Ahn, H. J.
Ahn, I. S.
Powiązania:
https://bibliotekanauki.pl/articles/356903.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
MA
Li/SnS2 cell
PCA
wet milling process and electrochemical characteristics
ogniwa Li/SnS2
charakterystyka elektromechaniczna
Opis:
With the increasing demand for efficient and economic energy storage, tin disulfide (SnS2), as one of the most attractive anode candidates for the next generation high-energy rechargeable Li-ion battery, have been paid more and more attention because of its high theoretical energy density and cost effectiveness. In this study, a new, simple and effective process, mechanical alloying (MA), has been developed for preparing fine anode material tin disulfides, in which ammonium chloride (AC), referred to as process control agents (PCAs), were used to prevent excessive cold-welding and accelerate the synthesis rates to some extent. Meanwhile, in order to decrease the mean size of SnS2 powder particles and improve the contact areas between the active materials, wet milling process was also conducted with normal hexane (NH) as a solvent PCA. The prepared powders were both characterized by X-ray diffraction, Field emission-scanning electron microscopeand particle size analyzer. Finally, electrochemical measurements for Li/SnS2 cells were takenat room temperature, using a two-electrode cell assembled in an argon-filled glove box and the electrolyte of 1M LiPF6 in a mixture of ethylene carbonate(EC)/dimethylcarbonate (DMC)/ethylene methyl carbonate (EMC) (volume ratio of 1:1:1).
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1191-1194
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Characterization of Metallic Fuel Slugs Prepared by Modified Injection Casting
Autorzy:
Mun, S.-U.
Kim, K.-H.
Oh, S.-J.
Park, J.-Y.
Hong, S.-I.
Powiązania:
https://bibliotekanauki.pl/articles/351428.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sodium-cooled fast reactor
metallic fuel slug
U-Zr alloy
surface characterization
injection casting
Opis:
Metallic fuel slugs containing rare-earth (RE) elements have high reactivity with quartz (SiO2) molds, and a reaction layer with a considerable thickness is formed at the surface of metallic fuel slugs. The surface characterization of metallic fuel slugs is essential for safety while operating a fast reactor at elevated temperature. Hence, it is necessary to evaluate the surface characteristics of the fuel slugs so that chemical interaction between fuel slug and cladding can be minimized in the reactor. When the Si element causes a eutectic reaction with the cladding, it deteriorates the metallic fuel slugs. Thus, it is necessary to examine the characteristics of the surface reaction layer to prevent the reaction of the metallic fuel slugs. In this study, we investigated the metallurgical characteristics of the surface reaction layer of fabricated U-10wt.%Zr-Xwt.%RE (X = 0, 5, 10) fuel slugs using injection casting. The results showed that the thickness of the surface reaction layer increased as the RE content of the metallic fuel slugs increased. The surface reaction layer of the metallic fuel slug was mainly formed by RE, Zr and the Si, which diffused in the quartz mold.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1049-1053
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Solvent Extraction of Co, Ni and Mn from NCM Sulfate Leaching Solution of Li(NCM)O2 Secondary Battery Scraps
Autorzy:
Hong, H. S.
Kim, D. W.
Choi, H. L.
Ryu, S.-S.
Powiązania:
https://bibliotekanauki.pl/articles/355577.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
waste recycling
NCM-system lithium ion battery
reduction
leaching
Opis:
As a part of the study on recycling Li(NCM)O2 lithium-ion battery scraps, solvent extraction experiments were performed using different extraction agents such as PC88A, Cyanex272 and D2EHPA to separate Co, Ni and Mn from the leaching solution. When the ratio of Mn to Ni was about 0.4 in the leaching solution, the separation factor for Co and Mn was found to be less than 10 so that the separation of Co and Ni was insufficient. When solvent extraction was done using the solution with the lower Mn/Ni ratio of 0.05 where Mn was removed by potassium permanganate and chlorine dioxide, more than 99% of Mn could be extracted through five courses of extraction using 30vol% D2EHPA while the extraction rates of Co and Ni were around 17% and 11%, respectively. In the case that Mn was removed from the solution, the extraction rate of Co was higher than 99% whereas less than 7% Ni was extracted using Cyanex272 suggesting that Co and Ni elements were effectively separated.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1011-1014
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Reduction of Thermal Conductivity Through Complex Microstructure by Dispersion of Carbon Nanofiber in p-Type Bi0.5Sb1.5Te3 Alloys
Autorzy:
Sharief, P.
Madavali, B.
Sohn, Y.
Han, J. H.
Song, G.
Hong, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/2049341.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bismuth telluride
carbon nano fiber
grain size
Thermal conductivity
ZT
Opis:
The influence of nano dispersion on the thermoelectric properties of Bi2Te3 was actively investigating to wide-spread thermoelectric applications. Herein this report, we have systematically controlled the microstructure of Bi0.5Sb1.5Te3 (BST) alloys through the incorporation of carbon nanofiber (CNF), and studied their effect on thermoelectric properties, and mechanical properties. The BST/x-CNF (x-0, 0.05, 0.1, 0.2 wt.%) composites powder was fabricated using high energy ball milling, and subsequently consolidated the powder using spark plasma sintering. The identification of CNF in bulk composites was analyzed in Raman spectroscopy and corresponding CNF peaks were recognized. The BST matrix grain size was greatly reduced with CNF dispersion and consistently decreased along CNF percentage. The electrical conductivity was reduced and Seebeck coefficient varied in small-scale by embedding CNF. The thermal conductivity was progressively diminished, obtained lattice thermal conductivity was lowest compared to bare sample due to induced phonon scattering at interfaces of secondary phases as well as highly dense fine grain boundaries. The peak ZT of 0.95 achieved for 0.1 wt.% dispersed BST/CNF composites. The Vickers hardness value of 101.8 Hv was obtained for the BST/CNF composites.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 3; 803-808
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure And Thermoelectric Properties Of TAGS-90 Compounds Fabricated By Mechanical Milling Process
Mikrostruktura i właściwości termoelektryczne związków TAGS-90 wytworzonych przez mielenie
Autorzy:
Kim, H.-S.
Babu, M.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/353404.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TAGS-90
thermoelectric properties
high-energy milling
SPS
właściwości termoelektryczne
mielenie wysokoenergetyczne
Opis:
TAGS-90 compound powder was directly prepared from the elements by high-energy ball milling (HEBM) and subsequently consolidated by a spark plasma sintering (SPS). Effect of milling time on the microstructure and thermoelectric properties of the samples were investigated. The particle size of fabricated powders were decreased with increasing milling time, finally fine particles with ~1μm size was obtained at 90 min. The SPS samples exhibited higher relative densities (>99%) with fine grain size. X-ray diffraction analysis (XRD) and energy dispersion analysis (EDS) results revealed that all the samples were single phase of GeTe with exact composition. The electrical conductivity of samples were decreased with milling time, whereas Seebeck coefficient increased over the temperature range of RT~450°C. The highest power factor was 1.12×10-3 W/mK2 obtained for the sample with 90 min milling at 450°C.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1231-1234
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Joining Of Green Body And Dense Substrate For Indium Tin Oxide Under Uniaxial Pressure In An Open Condition
Łączenie zielonej masy i gęstego podłoża z tlenku cyny indu w warunkach jednoosiowego ściskania w stanie otwartym
Autorzy:
Moon, G.-S.
Chung, T.-J.
Yang, S. H.
Hong, G.-S.
Oh, K.-S.
Powiązania:
https://bibliotekanauki.pl/articles/355654.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
transparent conducting oxide
indium tin oxide
green body
joining
tlenek indu
zielona masa
łączenie
Opis:
The green body and dense substrate of indium tin oxide was joined by uniaxially pressing at 0.3 MPa at 1300°C to test the restoring of the eroded part of transparent conducting oxide target. The green body was sintered to 98% of theoretical density under the suppression of shrinkage along the boundary below 5%. The boundary between two parts was free of pore but could be recognized from the difference in grain sizes. The joined part had the virtually same density with the substrate, but the grain size was less than one fifth compared with that of substrate.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1209-1212
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Interface Engineering in Heteroepitaxy
Autorzy:
Hong, S. K.
Chen, Y.
Ko, H. J.
Yao, T.
Powiązania:
https://bibliotekanauki.pl/articles/2035571.pdf
Data publikacji:
2002
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
68.35.-p
68.35.Dv
81.15.-z
81.15.Hi
81.10.Aj
Opis:
We report the importance of interface engineering in heteroepitaxy with examples of plasma-assisted molecular beam epitaxial ZnO growths on (0001) sapphire substrates and on (0001) GaN/sapphire templates, whose interfaces are engineered to improve and to control properties of ZnO films. The growth of rocksalt structure MgO buffer on Al$\text{}_{2}$O$\text{}_{3}$ (0001) is developed for ZnO epitaxy. By employing the MgO buffer layer, the formation of 30$\text{}^{o}$ rotated mixed domains is prohibited and two-dimensional layer-by-layer growth of ZnO on sapphire substrate is achieved. High-resolution X-ray diffraction reveals the superior improvement in a crystal quality of ZnO films with an MgO buffer. Polarity of wurtzite structure ZnO films on Ga-polar GaN/sapphire templates is controlled by changing interface structures. By forming a single crystalline, monoclinic Ga$\text{}_{2}$O$\text{}_{3}$ interfacial layer between GaN and ZnO through O-plasma pre-exposure on the Ga-polar GaN surface, O-polar ZnO films are grown. By forming the ZnO/GaN heterointerface without an interfacial layer through the Zn pre-exposure on the Ga-polar GaN surface, Zn-polar ZnO films are grown.
Źródło:
Acta Physica Polonica A; 2002, 102, 4-5; 541-554
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Improved Mechanical Properties of Al-Si Alloys by Adding an Extrusion Process to Conventional Processing Method
Autorzy:
Han, J. Y.
Femi, O. E.
Kilicaslan, F.
Jeong, C. U.
Baeg, C. H.
Hong, S. J.
Koo, J. M.
Powiązania:
https://bibliotekanauki.pl/articles/355114.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al-Si alloys
extrusion
mechanical properties
Opis:
In this study, the mechanical properties of Al-Si alloys was improved by selecting higher Si content and avoiding distortion in Al-Si matrix by adding an extrusion process such that the fabrication processes casting and extrusion were in sequence. Cast billets were extruded at ratios 4:1 and 10:1 to obtained two extruded bars with different processing parameters. The as-extruded samples were characterized and investigated for microstructure and mechanical properties. Optical Microscope was used to examined phase morphologies and microstructures of the extruded Al-Si bars. Mechanical properties were conducted on each sample to study the effectiveness of the additional extrusion process in high Si content Al-Si alloys. The result shows that by increasing the extrusion ratio, the size of the primary Si particle reduces leading to a higher density, better tensile and yield strength compared to the cast billet.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1179-1183
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication Of Zn4Sb3 Alloys By A Combination Of Gas-Atomization And Spark Plasma Sintering Processes
Wytwarzanie i konsolidacja proszków stopowych zn4sb3 przez kombinację procesów atomizacji gazowej i spiekania
Autorzy:
Dharmaiah, P.
Kim, H.-S.
Lee, L. H.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/355894.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gas atomization
microstructure
spark plasma sintering (SPS)
X-ray diffraction
atomizacja gazowa
mikrostruktura
SPS
spiekanie plazmowe
analiza rentgenowska (XRD)
Opis:
In this study, single phase polycrystalline Zn4Sb3 as well as 11 at.% Zn-rich Zn4Sb3 alloy having ε-Zn4Sb3 (majority phase) and Zn (minority phase) phases bulk samples produced by gas-atomization and subsequently consolidated by spark plasma sintering (SPS) process. The crystal structures were analyzed by X-ray diffraction (XRD) and cross-sectional microstructure were observed by the scanning electron microscopy (SEM). The internal grain microstructure of 11at.% Zn-rich Zn4Sb3 powders shows lamellar structure. Relative density, Vickers hardness and crack lengths were measured to investigate the effect of sintering temperature of Zn4Sb3 samples which are sintered at 653, 673 and 693 K. Relative density of the single phase bulk Zn4Sb3 sample reached to 99.2% of its theoretical density. The micro Vickers hardness of three different sintering temperatures were found around 2.17 – 2.236 GPa.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1417-1421
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ethnobotany of Acorus in China
Autorzy:
Shu, H.
Zhang, S.
Lei, Q.
Zhou, J.
Ji, Y.
Luo, B.
Hong, L.
Li, F.
Liu, B.
Long, C.
Powiązania:
https://bibliotekanauki.pl/articles/59160.pdf
Data publikacji:
2018
Wydawca:
Polskie Towarzystwo Botaniczne
Opis:
In China, species in the genus Acorus are used for many different purposes, viz., in traditional medicine, for rituals, and as ornamental plants. Acorus calamus (sweet flag) has been a symbolic plant in Chinese culture for many centuries and is used as a ceremonial object in festivals throughout the country. For other Acorus species in China, ethnobotanical records are few. During field investigations from 2006 to 2017, we interviewed 573 individuals representing ethnic groups such as the Miao, Yao, Buyi, Shui, Tujia, Dong, She, Maonan, Zhuang, Yi, and Han people. Various ethnobotanical approaches were adopted in the field surveys, including key informant interviews, semistructured interviews, participatory observation, direct observation, etc. The results have revealed a rich treasure trove of traditional knowledge on Acorus in China. Two species (A. macrospadiceus and A. gramineus) were used by ethnic groups as spices to add flavor to meat. Through the study found that all the species of Acorus had medicinal value, especially A. tatarinowii, deafness, blindness, and digestive disorders were among the conditions commonly treated using these plants. Traditional knowledge of the cultural, ethnomedicinal, and food values of Acorus, based on our recent literature surveys and field investigations in China is presented here. A better understanding of Acorus is vital for conserving the plants and the traditional knowledge associated with them.
Źródło:
Acta Societatis Botanicorum Poloniae; 2018, 87, 2
0001-6977
2083-9480
Pojawia się w:
Acta Societatis Botanicorum Poloniae
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Trace Elements (Co, Cr) on the Microstructure and Physical Properties of Al-Si-Cu-Mg-Fe Extruded Alloy
Autorzy:
Ahn, S. S.
Sharief, P.
Lee, C. H.
Son, H. T.
Kim, Y. H.
Kim, Y. C.
Hong, S.
Hong, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/352787.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al-Si alloy
microstructure
extrusion
coefficient of thermal expansion
trace elements
Opis:
Trace elements Co, Cr were added to investigate their influence on the microstructure and physical properties of Al-Si extruded alloy. The Co, Cr elements were randomly distributed in the matrix, forms intermetallic phase and their existence wereconfirmed by XRD, EDS and SEM analysis. With addition of trace elements, the microstructure was modified, Si particle size was reduced and the growth rate of β-(Al5 FeSi) phase limited. Compared to parent alloy, hardness and tensile strength were enhanced while the linear coefficient of thermal expansion (CTE) was significantly reduced by 42.4% and 16.05% with Co and Cr addition respectively. It is considered that the low CTE occurs with addition of Co was due to the formation of intermetallic compound having low coefficient of thermal expansion. The results suggested that Co acts as an effective element in improving the mechanical properties of Al-Si alloy.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 857-862
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Ti Powder Addition On The Fabrication Of TiO2 Nanopowders
Wpływ dodatku nanoproszku Ti na zagęszczanie i spiekanie nanoproszków TiO2
Autorzy:
Raihanuzzaman, R. M.
Park, H. Y.
Ghomashchi, R.
Kwon, T. H.
Son, H.-T.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/353186.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2 nanopowder
magnetic pulsed compaction
densification
sintering
nanoproszek Ti
magnetyczne zagęszczanie impulsowe
zagęszczanie
spiekanie
Opis:
Sintered samples of Ti added TiO2 nanopowders were fabricated by combined application of magnetic pulsed compaction (MPC) and sintering. The effect of Ti nano powder on density, shrinkage and hardness of the samples were investigated as part of the study. The optimum processing conditions were found to be around 0.5 GPa MPC pressure and 1450°C sintering temperature, illustrating maximum density, hardness and minimum shrinkage. High pressure compaction using MPC was found to enhance density with increasing MPC pressure up to 0.9 GPa, and significantly reduce the total shrinkage (about 16% in this case) in the sintered bulks compared to other general processes (about 18%). While sintered samples blended with micro Ti showed presence of microstructural cracks, the samples with 1-2% nano Ti had less or no cracks on them. Overall, the inclusion of nano Ti indicated improvement in mechanical properties of TiO2 nanopowders sintered preforms as opposed to micro Ti-added TiO2.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1473-1477
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Surfactant Addition on Bi2Te3 Nanostructures Synthesized by Hydrothermal Method
Autorzy:
Dharmaiah, P.
Lee, C. H.
Madavali, B.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/351609.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bismuth telluride
hydrothermal synthesis
spark plasma sintering
thermoelectric materials
X-ray diffraction
Opis:
In the present work, we have prepared Bi2Te3 nanostructures with different morphologies such as nano-spherical, nanoplates and nanoflakes obtained using various surfactant additions (EG, PVP, and EDTA) by a hydrothermal method. The shape of the nanoparticles can be controlled by addition of surfactants. The samples were characterized by x-ray diffraction (XRD) and scanning electron microscopy (SEM). It is found that the minority BiOCl phase disappears after maintained pH at 10 with EG as surfactant. SEM bulk microstructure reveals that the sample consists of fine and coarse grains. Temperature dependence of thermoelectric properties of the nanostructured bulk sample was investigated in the range of 300-450K. The presence of nanograins in the bulk sample exhibits a reduction of thermal conductivity and less effect on electrical conductivity. As a result, a figure of merit of the sintered bulk sample reached 0.2 at 400 K. A maximum micro Vickers hardness of 102 Hv was obtained for the nanostructured sample, which was higher than the other reported results.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1005-1010
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Milling Time Parameter on the Microstructure and the Thermoelectric Properties of n-Type Bi2Te2.7Se0.3 Alloys
Autorzy:
Sharief, P.
Madavali, B.
Koo, J. M.
Kim, H. J.
Hong, S.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/354418.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
milling time
microstructure
thermoelectric properties
ZT
Opis:
Nanostructured thermoelectric materials receiving great attention for its high thermoelectric performance. In this research, nanostructured n-type Bi2 Te2.7 Se0.3 alloys have prepared using high energy ball milling and followed by spark plasma sintering. Also, we have varied ball milling time to investigate milling time parameter on the thermoelectric properties of n-type Bi2 Te2.7 Se0.3 powder. The powders were discrete at 10 min milling and later particles tend to agglomerate at higher milling time due to cold welding. The bulk fracture surface display multi-scale grains where small grains intersperse in between large grains. The maximum Seebeck coefficient value was obtained at 20-min milling time due to their lower carrier density. The κ values were decreased with increasing milling time due to the decreasing trend observed in their κL values. The highest ZT of 0.7 at 350 K was observed for 30-min milling time which was ascribed to its lower thermal conductivity. The Vickers hardness values also greatly improved due to their fine microstructure.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 585-590
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Heat-Treatment On Microstructure And Magnetic Properties Of Nanocrystallized Mn-Zn Ferrite Powders
Wpływ obróbki cieplnej na mikrostrukturę i właściwości magnetyczne nanokrystalicznych proszków ferrytu Mn-Zn
Autorzy:
Lee, W. H.
Hong, C. S.
Chang, S. Y.
Powiązania:
https://bibliotekanauki.pl/articles/351552.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high energy ball milling
nanosized particles
crystallite size
magnetic properties
frezowanie kulowe
nanocząstki
wielkości krystalitów
właściwości magnetyczne
Opis:
The initial ferrite powders were subjected to high energy ball milling at 300rpm for 3h, and subsequently heat-treated at 573-1273K for 1h. Based on the observation of microstructure and measurement of magnetic properties, the heat-treatment effect was investigated. The size of initial powders was approximately 70μm. After milling, the powders with approximately 230nm in size were obtained, which were composed of the nano-sized particles of approximately 15nm in size. The milled powders became larger to approximately 550nm after heat-treatment at 973K. In addition, the size of particles increased to approximately 120nm with increasing temperature up to 973K. The coercivity of initial powders was almost unchanged after milling, whereas the saturation magnetization increased. As the heat-treatment temperature increased, the saturation magnetization gradually increased and the maximum coercivity was obtained at 773K.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1347-1350
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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