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Wyświetlanie 1-15 z 29
Tytuł:
Ordering of alfa-FeCo phase in the nanocrystalline Fe83-xCoxNb3B13Cu1 (x = 6, 25 or 41.5) alloy
Autorzy:
Zbroszczyk, J.
Młyńczyk, A.
Olszewski, J.
Ciurzyńska, W.
Wysłocki, B.
Perduta, K.
Lelątko, J.
Nabiałek, M.
Powiązania:
https://bibliotekanauki.pl/articles/148219.pdf
Data publikacji:
2007
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
nanocrystalline alloys
microstructure
ordering
Mössbauer spectroscopy
Opis:
The microstructure and ordering of alfa-FeCo phase of the nanocrystalline Fe83 xCoxNb3B13Cu1 (x = 6, 25 or 41.5) alloys were investigated. We have stated that á-FeCo phase is atomically ordered in the Fe83 xCoxNb3B13Cu1 (x = 25 or 41.5) samples crystallized by the heat treatment in a furnace. However, after flash annealing (by current or laser) that phase is disordered. Moreover, we have found that Co concentration in the crystalline alfa-FeCo phase strongly depends on Co content in the as-quenched ribbons. The annealing conditions influence also the grain diameter of the crystalline phase. In the nanocrystalline alloys obtained by a flash annealing of the amorphous ribbons finer grains are present.
Źródło:
Nukleonika; 2007, 52, supl. 1; 29-32
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hierarchical Carbon Fiber-Carbon Nanotubes by Using Electrospray Deposition Method with Preserved Tensile Properties
Autorzy:
Zakaria, Muhammad Razlan
Akil, Hazizan Md
Omar, Mohd Firdaus
Al Bakri Abdullah, Mohd Mustafa
Rahim, Shayfull Zamree Abd
Nabiałek, Marcin
Wysłocki, Jerzy J.
Powiązania:
https://bibliotekanauki.pl/articles/2174561.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
hybrid materials
carbon nanotubes
carbon fiber
Opis:
In this study, the electrospray deposition (ESD) method was used to deposit carbon nanotubes (CNT) onto the surfaces of carbon fibers (CF) in order to produce hybrid carbon fiber-carbon nanotubes (CF-CNT) which is rarely reported in the past. Extreme high-resolution field emission scanning electron microscopy (XHR-FESEM), high-resolution transmission electron microscopy (HRTEM) and x-ray photoelectron spectroscopy (XPS) were used to analyse the hybrid carbon fiber-carbon nanotube (CF-CNT). The results demonstrated that CNT was successfully and homogenously distributed on the CF surface. Hybrid CF-CNT was then prepared and compared with CF without CNT deposition in terms of their tensile properties. Statistically, the tensile strength and the tensile modulus of the hybrid CF-CNT were increased by up to 3% and 25%, respectively, as compared to the CF without CNT deposition. The results indicated that the ESD method did not cause any reduction of tensile properties of hybrid CF-CNT. Based on this finding, it can be prominently identified some new and significant information of interest to researchers and industrialists working on CF based products.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 4; 1299--1304
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase structure of the nanocrystalline Nd2Fe14B/alfa-Fe magnets with different grain
Autorzy:
Wnuk, I.
Wysłocki, J.
Przybył, A.
Powiązania:
https://bibliotekanauki.pl/articles/148342.pdf
Data publikacji:
2007
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Nd2Fe14B + alfa-Fe nanocrystalline magnets
Mössbauer spectroscopy
magnetic properties
Opis:
The effect of the contents of the magnetically hard and magnetically soft phases on the magnetic properties of Nd2Fe14B + alfa-Fe nanocrystalline magnets, as produced by the method of mechanical alloying, has been established. The phase composition of specimens was determined using X-ray diffractometry and Mössbauer spectroscopy. The Mössbauer examination showed that as the powder milling times increased, the content of the Nd2Fe14B phase increased from 42.8% (after the milling time of 10 h, with a grain size of 44.8 nm) to 66.3% (after the milling time of 48 h, with a grain size of 37.3 nm) and then decreased to 40.3% after 120 h of milling. On the other hand, the content of the magnetically soft phase alfa-Fe initially decreased (from 27.7%), reaching a minimum after the milling time of 48 h (17.4%) and then increasing to 36.9% after 120 h of milling.
Źródło:
Nukleonika; 2007, 52, supl. 1; 85-88
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of phase constitution and magnetic properties of the hard magnetic nanocrystalline Nd9.5Fe63.65B21.85Nb5 alloy ribbons
Autorzy:
Szwaja, M.
Pawlik, K.
Wysłocki, J. J.
Pawlik, P.
Gębara, P.
Powiązania:
https://bibliotekanauki.pl/articles/147840.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
magnetic properties NdFeB alloys
nanocrystalline ribbon
Nd2Fe14B
X-ray diffractometry
Opis:
In order to investigate the phase constitution of the nanocrystalline Nd9.5Fe63.65B21.85Nb5 alloy ribbons in the as-cast state and after short-time annealing Mossbauer study has been carried out. In as-cast state, ribbon samples were not fully amorphous but revealed soft magnetic properties. X-ray diffraction analysis showed the presence of hard magnetic Nd2Fe14B, metastable Nd2Fe23B3 and paramagnetic Nd1+epsilonFe4B4 phases in annealed samples. Mossbauer spectroscopy was used to determine the fractions of constituent phases formed during annealing of ribbons. Magnetic measurements were made with a vibrating sample magnetometer (VSM) and have shown that with increasing annealing temperature the remanence polarization Jr and maximum energy product (BH)max values were increasing.
Źródło:
Nukleonika; 2013, 58, 1; 159-163
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetic properties of the nanocrystalline Nd9.6Fe64.32Nb4B22.08 alloy ribbons
Właściwości magnetyczne nanokrystalicznych taśm stopu Nd9,6Fe64,32Nb4B22,08
Autorzy:
Szwaja, M.
Pawlik, P.
Wysłocki, J. J.
Gębara, P.
Powiązania:
https://bibliotekanauki.pl/articles/354465.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
dyfraktometria promieniowania X
właściwości magnetyczne stopu NdFeB
Nd2Fe14B
taśma nanokrystaliczna
X-ray diffractometry
magnetic properties NdFeB alloys
nanocrystalline ribbon
Opis:
Studies of magnetic properties and phase constitution of nanocrystalline Nd9.6Fe64.32Nb4B22.08 alloy ribbon samples are presented. In as-cast state, ribbon samples were fully amorphous and soft magnetic. Subsequent annealing resulted in an evolution of the phase constitution together with change of their magnetic properties. The main phase observed in the material is Nd2Fe14B hard magnetic phase.
W pracy badano własności magnetyczne oraz skład fazowy taśm wytworzonych ze stopu Nd9,6Fe64,32Nb4B22,08. Taśma w stanie po odlaniu ma amorficzną budowę i wykazuje miękkie właściwości magnetyczne. Wygrzewanie taśm powoduje zmiany składu fazowego wraz ze zmianą ich właściwości magnetycznych. Podstawową fazą obserwowaną w badanym materiale jest faza magnetycznie twarda Nd2Fe14B.
Źródło:
Archives of Metallurgy and Materials; 2012, 57, 1; 233-236
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetization Reversal Processes in Nanocrystalline (Pr, Dy)-(Fe, Co)-B Bulk Alloys
Autorzy:
Przybył, A.
Pawlik, K.
Pawlik, P.
Gębara, P.
Wysłocki, J.
Powiązania:
https://bibliotekanauki.pl/articles/1387335.pdf
Data publikacji:
2015-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.20.En
75.75.-c
75.75.Cd
Opis:
The aim of this paper was to study the phase constitution, magnetic properties and magnetization reversal processes in the rapidly solidified bulk (Pr,Dy)-(Fe,Co)-B alloys doped with Zr, Ti, Mn and Ni. The 3 mm outer diameter tubes samples of the $Pr₈Dy₁Fe₆₀Co₇Ni_{(6x)}MnₓB₁₄Zr₁Ti₃$ (where x = 0, 3, 6) alloys were produced by suction-casting technique. The admixture of Zr was introduced in order to improve their glass forming abilities while Dy was substituted to enhance the magnetocrystalline anisotropy of hard magnetic phase. The effect of Ni and Mn addition on the phase constitution and magnetic properties was studied in the presented work.
Źródło:
Acta Physica Polonica A; 2015, 127, 2; 579-581
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Annealing Temperature on the Phase Constitution and Magnetic Properties of the Pr₈Dy₁Fe₆₀Co₇Mn₆B₁₄Zr₁Ti₃ Alloy Ribbons
Autorzy:
Przybył, A.
Pawlik, K.
Pawlik, P.
Gębara, P.
Kaszuwara, W.
Wysłocki, J.
Filipecka, K.
Powiązania:
https://bibliotekanauki.pl/articles/1402331.pdf
Data publikacji:
2015-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.20.En
91.60.Pn
Opis:
Melt-spun ribbons were produced from the Pr₈Dy₁Fe₆₀Co₇Mn₆B₁₄Zr₁Ti₃ base alloy at the surface velocity of the cooper wheel of 30 m/s. The studies showed amorphous structure of ribbons and their soft magnetic properties. X-ray diffraction was used to determine phase constitution of all obtained samples. Annealing of ribbons caused formation of nanocomposite structure, which was a result of coexistence of hard magnetic RE₂(Fe,Co)₁₄B and soft magnetic α-Fe phases. Basic magnetic properties such as: coercivity $\text{}_{J}H_{c}$, remanence $J_{r}$ and maximum energy product $(BH)_\text{max}$ were determined from the measured hysteresis loops. The microstructure of selected specimens was observed by transmission electron microscopy technique.
Źródło:
Acta Physica Polonica A; 2015, 128, 1; 94-97
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanism of Rotational Hysteresis Energy in Sm-Fe-N Permanent Magnets
Autorzy:
Pawlik, P.
Wysłocki, J. J.
Dziliński, K.
Powiązania:
https://bibliotekanauki.pl/articles/2030425.pdf
Data publikacji:
2002-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.30.-m
75.60.-d
Opis:
Investigations were carried out on Sm-Fe-N permanent magnet produced by the reactive diffusion method with different grain sizes (from 8.6 to 0.97μm). The rotational hysteresis energy has been measured as a function of the applied field. The proposed model of rotational hysteresis energy is in good agreement with the experimental results. It is shown that the magnetization reversal process in Sm-Fe-N magnet is controlled by the nucleation of reversed domains.
Źródło:
Acta Physica Polonica A; 2002, 101, 2; 267-277
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
On Magnetization Reversal in Hard Magnetic Sm-Fe-N Permanent Magnets
Autorzy:
Pawlik, P.
Wysłocki, J. J.
Baran, M.
Powiązania:
https://bibliotekanauki.pl/articles/2029275.pdf
Data publikacji:
2001-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.-y
75.60.-d
Opis:
The investigations were carried out on Sm-Fe-N permanent magnets produced by reactive diffusion method. The magnets consist of hard magnetic phases: Sm$\text{}_{2}$Fe$\text{}_{17}$N$\text{}_{0.86}$ and SmFe$\text{}_{5}$ and soft magneticα-Fe phase. From the comparison of experimentally determined angular dependence of coercive field with appropriate theoretical predictions and from the dependence of coercive field on the external magnetic field determined from the minor hysteresis loops, it was stated that magnetization reversal process in Sm-Fe-N magnets is controlled by the nucleation of reversed domains process.
Źródło:
Acta Physica Polonica A; 2001, 100, 6; 905-913
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Glass forming abilities and crystallization process in amorphous Pr-Fe-Co-Zr-Nb-B alloys of various B content
Autorzy:
Pawlik, K.
Pawlik, P.
Kaszuwara, W.
Wysłocki, J.
Powiązania:
https://bibliotekanauki.pl/articles/1054842.pdf
Data publikacji:
2017-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
64.70.dg
61.05.cp
75.20.En
75.50.Vv
Opis:
The influence of boron contents on the glass forming abilities and magnetic properties of melt-spun ribbon samples produced from Pr₉Fe_{50+x}Co₁₃Zr₁Nb₄B_{23-x} (x=0, 2, 5, 8) alloys, were investigated. For all compositions, the rapidly solidified samples were fully amorphous, which was confirmed by X-ray diffractometry and the Mössbauer spectroscopy. Differential scanning calorimetry and differential thermal analysis studies revealed good glass forming abilities for all investigated specimens and allowed to determine thermal stability parameters of the amorphous phase. For all alloy ribbons, very large supercooled liquid region before crystallization ΔT_x reaching 100 K was measured. The Kissinger plots were constructed to determine the activation energies for crystallization. Annealing of specimens at temperatures ranging from 923 K to 1033 K for 5 min resulted in significant change of the phase constitution. The X-ray diffractometry studies have shown presence of hard magnetic Pr₂(Fe,Co)₁₄B and paramagnetic Pr_{1+x}Fe₄B₄ phases. Furthermore, with the increase of B contents in the alloy composition crystallization of α-Fe phase occurs at wider range of the annealing temperature. Anomaly of both thermal and magnetic properties was observed for the Pr₉Fe₅₂Co₁₃Zr₁Nb₄B₂₁ alloy ribbons.
Źródło:
Acta Physica Polonica A; 2017, 131, 4; 979-981
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetization Reversal Processes in Pr-Fe-B-type Nanocrystalline Magnets
Autorzy:
Pawlik, K.
Pawlik, P.
Kaszuwara, W.
Wysłocki, J.
Powiązania:
https://bibliotekanauki.pl/articles/1368000.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Vv
75.60.Ej
75.50.Bb
75.50.Tt
75.50.Ww
Opis:
The magnetization reversal processes in magnets derived from rapidly solidified $Pr_{9}Fe_{52}Co_{13}Zr_{1}Nb_{4}B_{21}$ alloy samples were studied by analysis of minor hysteresis loops and recoil curves. The studies were carried out on suction-cast 1 mm diameter rod, 1 mm thick plate, 3 mm outer diameter (o.d.) tube and melt-spun ribbon samples subjected to annealing at 983 K for 5 min. The X-ray diffraction analysis has shown multiphase constitution of the samples. Structural and magnetic studies indicated that the initial state of microstructure and phase composition affects the magnetization reversal processes in annealed samples due to a variation of microstructure in samples of various shapes. Magnetic studies allowed estimation of the mean values of nucleation and pinning fields that control the magnetization reversal processes.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 186-187
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetization Reversal Processes in the Nanocrystalline Fe-Co-Zr-Ti-Pr-B Magnets
Autorzy:
Pawlik, K.
Pawlik, P.
Wysłocki, J.
Kaszuwara, W.
Powiązania:
https://bibliotekanauki.pl/articles/1813515.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ww
75.50.Kj
71.20.Eh
Opis:
Magnetization reversal processes in the magnets derived from the $Fe_{60}Co_{13}Zr_1Ti_3Pr_9B_{14}$ alloy were investigated. It was shown that the processing technique affects the magnetization reversal processes. For the nanocrystalline ribbon samples pinning of the domain walls arises at low external magnetic fields while nucleation of reversed domains occurs at higher fields. However, the nucleation fields are lower than the pinning fields for the nanocrystalline rod and tube samples produced by suction-casting technique.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 39-42
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase composition investigations of the Nd-Fe alloys processed by various methods
Autorzy:
Pawlik, K.
Wysłocki, J.
Olszewski, J.
Bodak, O.
Pawlik, P.
Powiązania:
https://bibliotekanauki.pl/articles/147201.pdf
Data publikacji:
2004
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Nd-Fe binary system
intermetallic compounds
Mössbauer spectroscopy
phase composition
Opis:
Abstract In the paper, the phase composition changes for the series of Nd10+xFe90 x (x = 0; 0.5; 1; 1.5; 2; 2.5; 3; 3.5; 4) binary alloys, produced by long time annealing and rapid solidification methods were investigated. X-ray diffractometry and Mössbauer spectroscopy were used to determine the phase composition of the alloys. These structural investigations revealed the existence of two crystalline phases in the long time annealed samples: bcc á-Fe and rhombohedral Nd2Fe17 of the Th2Zn17-type structure. Furthermore, the single phase region was observed for the Nd concentration above 12 at.%. For the rapidly solidified ribbon samples, a low volume fraction of the alfa-Fe and the crystalline phase of hexagonal symmetry were detected.
Źródło:
Nukleonika; 2004, 49,suppl.3; 27-31
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Bulk Glass Forming Ability and Magnetic Properties of $Pr_9Fe_{50 + x}Co_{13}Zr_1Nb_4B_{23 - x}$ (x = 0, 2, 5, 8) Alloys
Autorzy:
Pawlik, K.
Pawlik, P.
Wysłocki, J.
Powiązania:
https://bibliotekanauki.pl/articles/1534352.pdf
Data publikacji:
2010-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ww
75.50.Kj
71.20.Eh
Opis:
In the present study the rapidly quenched $Pr_9Fe_{50 + x}Co_{13}Zr_1Nb_4B_{23 - x}$ (x = 0, 2, 5, 8) alloy samples produced in a form of 100 $mm^2$ plate of various thicknesses were investigated. The X-ray diffraction revealed changes in the phase constitution of as-cast samples depending on the alloy composition and plate thickness. The presence of hard magnetic $Pr_2(Fe,Co)_{14}B$ phase was observed in 0.5 mm thick plates of the x = 8 alloy, while fully glassy structure was shown in 0.5 mm thick plates of the x = 0 alloy. It was shown in the present paper that magnetic properties of annealed samples originated from different microstructure of as-cast samples.
Źródło:
Acta Physica Polonica A; 2010, 118, 5; 900-902
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nanocrystallization studies of rapidly quenched Fe85.4-xCoxZr6.8-yNbyB6.8Cu1 (x = 0 or 42.7, y = 0 or 1) alloys
Autorzy:
Olszewski, J.
Zbroszczyk, J.
Ciurzyńska, W.
Fukunaga, H.
Wysłocki, B.
Perduta, K.
Łukiewska, A.
Młyńczyk, A.
Lelątko, J.
Świerczek, J.
Powiązania:
https://bibliotekanauki.pl/articles/148787.pdf
Data publikacji:
2003
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Mössbauer spectra
nanocrystalline Fe-Co alloys
Opis:
The microstructure of amorphous and nanocrystalline Fe42.7Co42.7Zr6.8-xNbxB6.8Cu1 (x = 0 or 1) alloys was investigated. We have stated that the nanocrystalline samples consist of the crystalline alfa-FeCo grains about 8 nm in diameter embedded in an amorphous matrix which is rich in cobalt. From Mössbauer spectroscopy studies we have found that the crystalline alfa-FeCo phase in the nanocrystalline samples obtained by the conventional annealing is atomically ordered. Moreover, the order degree depends on the annealing time. As for the samples partially crystallized during rapid quenching, the crystalline alfa-FeCo phase is atomically disordered.
Źródło:
Nukleonika; 2003, 48,suppl.1; 49-52
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 29

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