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    Wyświetlanie 1-14 z 14
    Tytuł:
    AFM/STM Modification of Thin Sb Films on 6H-SiC(0001)
    Autorzy:
    Mazur, P.
    Zuber, S.
    Grodzicki, M.
    Ciszewski, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1195467.pdf
    Data publikacji:
    2014-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Dz
    68.37.Ps
    68.37.Ef
    68.37.-d
    81.10.Bk
    81.07.-b
    Opis:
    Atomic force microscopy and scanning tunneling microscopy have been used for nanometer scale modifications of Sb films deposited on 6H-SiC(0001) surface. The films are grown in situ by vapor deposition under ultrahigh vacuum. The growth follows the Volmer-Weber mode. Ultrathin (up to 3 nm on average) Sb films which consist of no coalesced islands can be modified by moving the island over the substrate surface by the AFM tip. Thicker films, which are firmer due to the coalescence, can be modified by the field and/or current produced by STM tip. Final result of the modifications is adsorbate free 6H-SiC(0001) surface restitution over the modified area.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 5; 1131-1133
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Sb Layers on p-GaN: UPS, XPS and LEED Study
    Autorzy:
    Grodzicki, M.
    Mazur, P.
    Pers, J.
    Zuber, S.
    Ciszewski, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1376064.pdf
    Data publikacji:
    2014-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Dz
    68.37.Ps
    68.37.Ef
    68.37.-d
    81.10.Bk
    81.07.-b
    Opis:
    The electronic structure of p-type GaN(0001) surfaces and its modification by antimony adsorption, and properties of Sb/GaN(0001) interface, are presented in this report. The studies were carried out in situ by ultraviolet photoelectron spectroscopy, X-ray photoelectron spectroscopy, and low-energy electron diffraction. Thin Sb layers were deposited under ultrahigh vacuum conditions onto the substrate at room temperature. Electron affinity of clean p-GaN surface amounted to 3.0 eV. A small amount of Sb on GaN(0001) surface reduced the electron affinity to 1.9 eV. The work function of the Sb layer was equal to 4.4 eV. For the Schottky barrier height of the Sb/GaN interface, the value of 2.50 eV was obtained.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 5; 1128-1130
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Requirement for and Use of Coated P92 Steel for Enhanced Structural Integrity at High Temperature
    Autorzy:
    Hoey, T.
    Chen, R.
    McCartney, D.
    Sun, W.
    Mansfield, J.
    Barnard, P.
    Foster, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402066.pdf
    Data publikacji:
    2015-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.15.Pq
    68.37.-d
    61.05.-a
    64.75.-g
    Opis:
    To achieve climate change targets and to improve the efficiency of fossil fuel power plant the temperature and pressure of operation must be increased. With steam temperatures predicted to rise by 50-100 K in the next 30 years, this presents a number of material challenges, not least for the ferritic steels used for steam pipework. Currently the best in class ferritic steel for power plant steam pipework is P92, a 9-12% Cr advanced martensitic steel that was developed for its superior high temperature creep resistance. This paper will give a brief overview of P92 microstructure, composition and metallurgy and identify experimentally and computationally some key features of the material. As well as failure by creep, P92 at high temperature also suffers from steam oxidation damage. Recent literature suggests that coatings applied to P92 are a very promising solution. A short review of previous work on steam oxidation resistant coatings for P92 is included. A novel Co-Cr-C coating that has not previously been explored for this application is described. Experimental and computational characterisation is included.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 4; 514-519
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of Magnetosomes After Exposure to the Effect of the Sonication and Ultracentrifugation
    Autorzy:
    Molčan, M.
    Hashim, A.
    Kováč, J.
    Rajňák, M.
    Kopčanský, P.
    Makowski, M.
    Gojzewski, H.
    Molokáč, M.
    Hvizdák, L.
    Timko, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1368025.pdf
    Data publikacji:
    2014-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.07.-b
    75.60.-d
    87.50.Y-
    68.37.-d
    Opis:
    Magnetosomes are intracellular organelles of widespread aquatic microorganisms called Magnetotactic bacteria. At present they are under investigation especially in biomedical applications. This ability depends on the presence of intracellular magnetosomes which are composed of two parts: first, nanometer-sized magnetite $(Fe_{3}O_{4})$ or greigite $(Fe_{3}S_{4})$ crystals (magnetosome crystal), depending on the bacterial species; and second, the bilayer membrane surrounding the crystal (magnetosome membrane). The magnetosomes were prepared by biomineralization process of magnetotactic bacteria Magnetospirillum Magnetotacticum sp. AMB-1. The isolated magnetosome chains (sample M) were centrifugated at speed of 100000 rpm for 4 hours (sample UM) and sonicated at power of 120 W for 3 hours (sample SM), respectively. The prepared suspensions were investigated with respect to morphological, structural and magnetic properties. The results from scanning electron microscopy showed that isolated chains of magnetosomes were partially broken to smaller ones after ultracentrifugation. On the other hand the application of the sonication process caused the formation of individual magnetosomes (unordered in chain). These results were confirmed by coercivity and magnetization saturation measurements.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 1; 198-199
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of Ca Content on the Structure and Properties οf (Co,Ca)O Thin Films Deposited by PLD Technique
    Autorzy:
    Cieniek, L.
    Kac, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1537944.pdf
    Data publikacji:
    2010-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.Fg
    81.15.-z
    81.15.Aa
    68.55.-a
    68.60.Bs
    68.37.-d
    68.55.jd
    Opis:
    In this paper the results of investigations of pure and Ca-doped CoO thin films deposited by PLD technique are presented. The studies carried out for variable Ca content allowed to establish optimal conditions for good quality oxide films preparation. The microstructure, chemical/phase composition and morphology of obtained thin films were examined by means of diverse techniques (SEM, EDS, XPS and XRD). For estimation of deposited Ca-doped CoO films quality the nanohardness and scratch tests (adhesion) were performed. Obtained results confirm that using PLD technique it is possible to carry stoichiometric composition of (Co,Ca)O from target to single crystal substrate and allow to conclude that the calcium dopant concentration (chemical composition) influence on the morphology and measured properties of deposited (Co,Ca)O films.
    Źródło:
    Acta Physica Polonica A; 2010, 117, 5; 803-807
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Borax Pentahydrate Addition to Acid Bath on the Microstructure and Corrosion Resistance of Zn-Co Coating
    Autorzy:
    Karahan, İ.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402495.pdf
    Data publikacji:
    2015-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.37.-d
    68.55.-a
    81.65.Kn
    Opis:
    In this work, the Zn-Co coatings were synthesized on AISI 4140 steel and aluminum plates by using potentiostatic electrodeposition technique in sulphate-based acidic baths with 0, 20, 40 and 60 gl¯¹ of borax pentahydrate, as additive. The effect of borax pentahydrate on the microstructure of the samples was observed using scanning electron microscopy and X-ray diffractometer. The deposition process was investigated by cyclic voltammetry. The effect of borax pentahydrate on the corrosion resistance of the samples was studied by potentiodynamic polarization technique. The results have demonstrated, that the addition of borax pentahydrate was in favor of the growth of grains. The morphology of pyramidal islands on the surface was changed to a more flat structure. The results have also demonstrated that the effect of borax pentahydrate was not monotonous. With increasing concentration, the corrosion potential was at minimum and the charge transfer resistance $R_{t}$ was at maximum for the sample obtained from the bath with 60 gl¯¹ of borax pentahydate, indicating that this sample showed the best corrosion resistance. It was found that current density first decreased and than increased, due to adsorption of a complex of borax pentahydrate and/or changes in the morphology, however, the initial deposition potential was not affected. The addition of borax pentahydrate to the bath led to formation of the best Zn-Co deposits, composed of coalesced globular fine grains, smaller than ≈2 μm in diameter. In addition, all of the studied Zn-Co deposits consisted of η phases. It is suggested that Zn-Co deposits produced in the bath containing 60 gl¯¹ of borax pentahydrate probably offer sacrificial protection to the steel substrate.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 2B; B-432-B-435
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structural Characterization of $La_{1-x}Sr_xCoO_3$ Thin Films Deposited by Pulsed Electron Deposition Method
    Autorzy:
    Cieniek, Ł.
    Kopia, A.
    Cyza, A.
    Kowalski, K.
    Kusiński, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398370.pdf
    Data publikacji:
    2016-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.-z
    81.10.Bk
    81.07.Bc
    68.55.-a
    68.55.J-
    68.55.Nq
    68.37.-d
    Opis:
    The aim of the presented research was to investigate the influence of strontium dopant on the structure and composition of $La_{1-x}Sr_{x}CoO_3$ (x=0, 0.1, 0.2) perovskite thin films. Pure and Sr doped LaCoO₃ thin films were grown by pulsed electron deposition technique on crystalline epi-polished Si/MgO substrates. Numerous analytical techniques (scanning electron microscopy, atomic force microscopy, X-ray photoelectron spectroscopy, and X-ray diffraction) were applied to characterize their phase/chemical composition, structure and surface morphology. X-ray diffraction analysis showed the presence of pure LaCoO₃ perovskite phase in the undoped thin film. For Sr doped thin films $La_{0.8}Sr_{0.2}CoO_3$ (x=0.2), $La_{0.9}Sr_{0.1}CoO_3$ (x=0.1) small contents of La₂ O₃ and LaSrCoO₄ phases were noticed. The crystallite sizes, calculated from the Williamson-Hall plots, were about 18 nm for all analyzed films. According to scanning electron microscopy/atomic force microscopy observations, obtained thin films were free from defects and cracks. Atomic force microscopy (tapping mode) analysis revealed the differences in the shape and quantity of surface crystallites for all thin films as a result of Sr doping and different deposition parameters. Atomic force microscopy technique also allowed measurement of roughness parameters for analyzed samples. X-ray photoelectron spectroscopy analyses of chemical states of elements of thin films showed that their chemical state was stable across the film thickness and even at the interface with the MgO substrate. X-ray photoelectron spectroscopy analysis also allowed to evaluate chemical states and atomic concentration of La, Co, and Sr elements within cross-sections of deposited thin films.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 4; 1121-1123
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Phase Composition of the Surface Zone of Nitrided Cast Steels and Their Mechanical Properties
    Autorzy:
    Brzózka, K.
    Budzynowski, T.
    Górka, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/1506569.pdf
    Data publikacji:
    2011-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.66.Dk
    81.65.Lp
    81.40.-z
    76.80.+y
    61.05.cp
    68.37.-d
    81.40.Pq
    Opis:
    Conversion electron Mössbauer spectroscopy and structural X-ray diffractometry have been used to study nitrides formation in the surface layer of cast steels subjected previously to low-temperature nitriding. It has been found that creation of iron-nitrogen phases strongly depends on sample composition. Nitrides: $γ^\prime-Fe_{4}N$ and $\epsilon-Fe_{2-3}N$ arise in the course of the nitriding procedure in most investigated cast steels. Moreover, considerable changes in their microstructure and tribological properties occur. The depth profile of nitrides has been derived for selected cast steel.
    Źródło:
    Acta Physica Polonica A; 2011, 119, 1; 28-32
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of Preparation Technique on the Properties of In:CdS Thin Films
    Autorzy:
    Dhanam, M.
    Kavitha, B.
    Maheswari, B.
    Jesna, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1505169.pdf
    Data publikacji:
    2011-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.-z
    78.66.Hf
    61.05.cp
    68.37.-d
    Opis:
    This paper presents the results of the structural, morphological and optical analysis of In:CdS thin films prepared by chemical bath deposition and successive ionic layer adsorption and reaction techniques. X-ray diffraction patterns showed the hexagonal phase of cadmium sulfide and it has been found that the amount of atomic percentage of indium increases the intensity of the preferential orientation (002) plane in chemical bath deposition In:CdS thin films. Compositional analysis confirmed the replacement of Cd ions by In ions and morphological analysis confirmed the lesser grain size and dense morphology in chemical bath deposition In:CdS thin films. Increase in In concentration in successive ionic layer adsorption and reaction In:CdS thin films leads to an increase in the optical transmission up to 80% and the higher band gap and therefore the results of this investigation enabled to understand the significance of preparation technique.
    Źródło:
    Acta Physica Polonica A; 2011, 119, 6; 885-889
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure Development in Multilayer $TiB_x // TiSi_y C_z$ Coatings during Post-Deposition Heat Treatment
    Autorzy:
    Twardowska, A.
    Rajchel, B.
    Morgiel, J.
    Mędala-Wójcik, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398372.pdf
    Data publikacji:
    2016-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.15.Cd
    81.20.-n
    42.62.-b
    61.43.Dq
    68.37.-d
    68.37.Lp
    68.65.Ac
    64.70.Kb
    Opis:
    Multilayer amorphous $TiB_{x} // TiSi_{y}C_{z}$ coatings were formed by duplex treatment: dual beam ion beam assisted deposition and pulsed laser deposition. Post-deposition heating was applied to activate crystallization in the coating. In situ transmission electron microscopy heating experiments were conducted in the temperature range 20-600°C. Crystallization of TiB₂ phase in $TiB_{x}$ layers begun at 450°C, while $TiSi_{y}C_{z}$ layers retained nearly amorphous up to 600°C.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 4; 1124-1126
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The influence of selected organic compounds on the corrosion of historical glass based on their state of preservation
    Autorzy:
    Greiner-Wronowa, E.
    Świt, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1058515.pdf
    Data publikacji:
    2016-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    89.90.+n
    61.43.Fs
    07.60.Pb
    68.37.-d
    68.37.Hk
    81.70.-q
    07.07.Df
    07.75.+h
    81.40.Np
    Opis:
    The aim of this study was to investigate the influence of selected organic compounds such as acetic acid and formaldehyde on the historical glass objects of corrosion processes. This is a very important problem for the field of conservation and restoration of glass of art. Glass objects exhibited in museum display cases can be suffered by evaporating organic compounds which undergo to reaction with leached glass elements to create corrosion deposit on their surface. The proposed method called glass sensors has been used to identify results of impact of various external factors on the tested glass. Due to aggressive environment for the objects there created corrosion phenomena. Glass sensor were prepared as reproduced XVIII-cent. materials. The current studies were carried out by modern physico-chemical methods such as optical, metallography, scanning electron microscopy, inductively coupled plasma mass spectrometry and the Fourier transform infrared spectrometry. These techniques allow to determine the composition of the corrosion layers as well as their structure. The issues raised in this work have been studied following an interdisciplinary approach. The information obtained by using different techniques provides a valuable source of knowledge about the chemical reactions taking place on the surface of the glass. The results derived from this work are useful for the design and implementation of exhibition recommendations and better planning of conservation tasks.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 6; 1406-1414
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparison of Five-Layered ZrO₂ and Single-Layered Ce, Eu, and Dy-Doped ZrO₂ Thin Films Prepared by Sol-Gel Spin Coating Method
    Autorzy:
    Çiçek Bezir, N.
    Evcin, A.
    Kayali, R.
    Özen, M.
    Esen, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031178.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.37.-d
    68.55-a
    68.60-p
    78.20.-e
    81.10.Dn
    71.20.Be
    Opis:
    In order to investigate the influence of the number of layers on the properties of ZrO₂ thin films, we prepared one pure ZrO₂ film sample with five layers and Ce, Eu, and Dy-doped ZrO₂ samples with single layer, by spin-coating sol gel-method. The crystal structures of thin films were determined using X-ray diffraction, morphology of the samples was analyzed by scanning electron microscopy, and the optical properties of the samples were determined by ultraviolet/visible absorbance measurements. The results of these measurements have shown that the concentration of the dopants and the thickness of thin film layers play a vital role in the physical, chemical, and optical properties of the pure and doped ZrO₂ thin films.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 612-616
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparison of Pure and Doped TiO₂ Thin Films Prepared by Sol-Gel Spin-Coating Method
    Autorzy:
    Çiçek Bezir, N.
    Evcin, A.
    Kayali, R.
    Özen, M.
    Balyaci, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031525.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.37.-d
    68.55.-a
    68.60.-p
    78.20.-e
    81.10.Dn
    71.20.Be
    Opis:
    In this study, using spin-coating sol-gel method we fabricated TiO₂ thin films, doped with different concentrations (1, 2, and 3 mole %) of Ce, Dy, and Eu. Characterization of the prepared samples was performed by means of the X-ray diffraction, scanning electron microscopy, ultraviolet visible absorption, and differential thermal and thermo gravimetric analysis. X-ray diffraction measurements have shown that in Eu and Dy-doped samples crystal structure consists of mixed rutile and the dominant anatase phases, however the Ce doped samples consist of anatase phase only. Scanning electron microscopy images have revealed that while average thin film thickness of the Dy-doped samples decreases with increasing concentration of Dy, the average film thicknesses of samples doped with Ce and Eu increases with increasing concentrations of these dopants. Ultraviolet visible absorption spectroscopy measurements have shown that while absorbances of the samples doped by 1 and 2 mole % of the dopants have nearly similar properties, these properties differ from each other for 3 mole % of the dopants. Finally, differential thermal and thermo gravimetric analyses have shown that the chemical reactions and weight losses of the samples have occurred at the expected temperatures.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 620-624
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structures in Multicomponent Polymer Films: Their Formation, Observation and Applications in Electronics and Biotechnology
    Autorzy:
    Budkowski, A.
    Bernasik, A.
    Moons, E.
    Lekka, M.
    Zemła, J.
    Jaczewska, J.
    Haberko, J.
    Raczkowska, J.
    Rysz, J.
    Awsiuk, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1808304.pdf
    Data publikacji:
    2009-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.16.Dn
    61.25.H-
    68.37.-d
    82.80.Ms
    85.60.-q
    85.65.+h
    82.37.Rs
    Opis:
    Several strategies to form multicomponent films of functional polymers, with micron, submicron and nanometer structures, intended for plastic electronics and biotechnology are presented. These approaches are based on film deposition from polymer solution onto a rotating substrate (spin-casting), a method implemented already on manufacturing lines. Film structures are determined with compositional (nanometer) depth profiling and (submicron) imaging modes of dynamic secondary ion mass spectrometry, near-field scanning optical microscopy (with submicron resolution) and scanning probe microscopy (revealing nanometer features). Self-organization of spin-cast polymer mixtures is discussed in detail, since it offers a one-step process to deposit and align simultaneously domains, rich in different polymers, forming various device elements: (i) Surface segregation drives self-stratification of nanometer lamellae for solar cells and anisotropic conductors. (ii) Cohesion energy density controls morphological transition from lamellar (optimal for encapsulated transistors) to lateral structures (suggested for light emitting diodes with variable color). (iii) Selective adhesion to substrate microtemplates, patterned chemically, orders lateral structures for plastic circuitries. (iv) Submicron imprints of water droplets (breath figures) decorate selectively micron-sized domains, and can be used in devices with hierarchic structure. In addition, selective protein adsorption to regular polymer micropatterns, formed with soft lithography after spin-casting, suggests applications in protein chip technology. An approach to reduce lateral blend film structures to submicron scale is also presented, based on (annealed) films of multicomponent nanoparticles.
    Źródło:
    Acta Physica Polonica A; 2009, 115, 2; 435-440
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-14 z 14

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