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Wyświetlanie 1-15 z 32
Tytuł:
Effect of Heat Treatment on Microstructure and Impact Toughness of Ti-6Al-4V Manufactured by Selective Laser Melting Process
Autorzy:
Lee, K.-A.
Kim, Y.-K.
Yu, J.-H.
Park, S.-H.
Kim, M.-C.
Powiązania:
https://bibliotekanauki.pl/articles/354570.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
selective laser melting
Ti-6Al-4V
microstructure
impact toughness
heat treatment
Opis:
This study manufactured Ti-6Al-4V alloy using one of the powder bed fusion 3D-printing processes, selective laser melting, and investigated the effect of heat treatment (650°C/3hrs) on microstructure and impact toughness of the material. Initial microstructural observation identified prior-β grain along the building direction before and after heat treatment. In addition, the material formed a fully martensite structure before heat treatment, and after heat treatment, α and β phase were formed simultaneously. Charpy impact tests were conducted. The average impact energy measured as 6.0 J before heat treatment, and after heat treatment, the average impact energy increased by approximately 20% to 7.3 J. Fracture surface observation after the impact test showed that both alloys had brittle characteristics on macro levels, but showed ductile fracture characteristics and dimples at micro levels.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1341-1346
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects Of Environmental Factors On The Dispersion Behavior Of Iron Oxide In Aqueous Solutions With Poly Acrylic Acid
Wpływ parametrów charakteryzujących wodne roztwory poli(kwasu akrylowego) na dyspersję tlenku żelaza
Autorzy:
Lee, E.-H.
Kim, K.-M.
Maeng, W.-Y.
Hur, D.-H.
Powiązania:
https://bibliotekanauki.pl/articles/354513.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
polyacrylic acid
dispersion stability
magnetite
nanoparticles
suspension
poli(kwas akrylowy)
stabilność dyspersji
magnetyt
nanocząstki
zawiesina
Opis:
After preparing aqueous suspensions from magnetite particles with a poly-acrylic acid, we investigated the effects of several experimental parameters. We characterized the stability of the suspensions using visual inspection, sedimentation, adsorption, and thermal stability of the dispersant. The dispersion stability is affected by the solution pH, the concentrations of magnetite particles, the molecular weight, the concentration of the dispersants, and the temperature. The stability of the suspensions increased as the concentration of the dispersant and the temperature increased. In terms of the molecular weights of the dispersant, the suspensions with dispersant of low-molecular weight (1800) were more stable than those of high-molecular weight (250000) at room temperature. However, at high temperature the suspensions with high-molecular weight showed stability. The adsorption efficiency of the dispersant was very low. The dispersant of high-molecular weight showed a higher thermal integrity than that of low-molecular weight. From this work, we obtained the optimum conditions for stable aqueous suspensions of magnetite particles.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1561-1564
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Recovery Of Valuable Metals In Tin-Based Anodic Slimes By Carbothermic Reaction
Odzysk cennych metali ze szlamów anodowych na bazie Sn metodą reakcji karbotermicznej
Autorzy:
Han, C.
Kim, Y.-M.
Son, S. H.
Choi, H.
Kim, T. B.
Kim, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/352796.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
tin
anodic slime
carbothermic reduction
carbon
recovery
cyna
szlam anodowy
reakcja karbotermiczna
węgiel
odzysk metali
Opis:
This study investigated the recovery of anodic slimes by carbothermic reaction in the temperature range of 973~1,273K and amount of carbon as a function of time. Tin anodic slime samples were collected from the bottom of the electrolytic cells during the electro-refining of tin. The anodic slimes are consisted of high concentrated tin, silver, copper and lead oxides. The kinetics of reduction were determined by means of the weight-loss measurement technique. In order to understand in detail of carbothermic reaction, thermodynamic calculation was carried out and compared with experiments. From thermodynamic calculation and experiment, it was confirmed that Sn-based anodic slime could be reduced by controlling temperature and amount of carbon. However, any tendency between the reduction temperature and carbon content for the reduction reaction was not observed.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1213-1216
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Different Mechanical Milling Processes On Morphology And Microstructural Changes Of Nano And Micron Al-Powders
Wpływ różnych procesów mielenia na morfologię i mikrostrukturę nanometrycznych i mikronowych proszków Al
Autorzy:
Kim, H.-S.
Madavali, B.
Eom, T.-J.
Kim, C.- M.
Koo, J.-M.
Lee, T. H.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/355715.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al alloys
high-energy ball milling
low energy ball milling
plastic deformation
stopy Al
wysokoenergetyczne mielenie kulkowe
mielenie energooszczędne
odkształcenia plastyczne
Opis:
In this research, effect of the various mechanical milling process on morphology and microstructural changes of nano and micron Al-powders was studied. The milling of Al-powders was performed by both high energy and low energy ball milling process. The influence of milling (pulverizing) energy on the structural changes of Al-powders was studied. Al-nanoparticles were agglomerated during the MA and its size was increased with increasing milling while micron Al-powder gets flattened shape during high energy ball milling due to severe plastic deformation. Meanwhile, structural evolution during high energy ball milling of the nano powder occurred faster than that of the micron powder. A slight shift in the position of X-ray diffraction peaks was observed in nano Al-powders but it was un-altered in macro Al-powders. The variation in lattice parameters was observed only for nano Al powders during the high energy ball milling due to lattice distortion.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1235-1239
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Acid Dissolution Conditions on Recovery of Valuable Metals from Used Plasma Display Panel Scrap
Autorzy:
Kim, C.- M.
Dharmaiah, P.
Kim, H.-S.
Koo, J.-M.
Yoon, J.-S.
Hong, S.-H.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/355713.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high energy ball milling
waste plasma display panels
dissolution
recovery
Opis:
The objective of this particular study was to recover valuable metals from waste plasma display panels using high energy ball milling with subsequent acid dissolution. Dissolution of milled (PDP) powder was studied in HCl, HNO3, and H2SO4 acidic solutions. The effects of dissolution acid, temperature, time, and PDP scrap powder to acid ratio on the leaching process were investigated and the most favorable conditions were found: (1) valuable metals (In, Ag, Mg) were recovered from PDP powder in a mixture of concentrated hydrochloric acid (HCl:H2O = 50:50); (2) the optimal dissolution temperature and time for the valuable metals were found to be 60°C and 30 min, respectively; (3) the ideal PDP scrap powder to acid solution ratio was found to be 1:10. The proposed method was applied to the recovery of magnesium, silver, and indium with satisfactory results.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1173-1177
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxidation Behavior of Steel with Cr Content and Water Flow Rate
Autorzy:
Kim, D.-J.
Kim, K. M.
Shin, J. H.
Cheong, Y. M.
Lee, E. H.
Lee, G. G.
Kim, S. W.
Kim, H. P.
Choi, M. J.
Lim, Y. S.
Hwang, S. S.
Powiązania:
https://bibliotekanauki.pl/articles/351548.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
steel
flow accelerated corrosion
Cr content
flow rate
surface oxides
Opis:
Fast water flow facilitates ferrous ion transport leading to flow accelerated corrosion (FAC) of carbon steel and the possibility of a large accident through a failure of a secondary pipe in a nuclear power plant. Ion transport is directly linked to oxide properties such as the thickness, chemical composition and porosity. This work deals with a precise observation of the cross section of the corroded specimen focusing on an oxide passivity and its thickness using SEM (scanning electron microscope) and TEM (transmission electron microscope) as well as an apparent weight loss and a surface observation for the specimens corroded using a rotating cylindrical electrode autoclave system in pure water of pH 7 at 150°C having dissolved oxygen below 1 ppb within a flow rate range of 0 to 10 m/s. The Cr content in steel was changed from 0.02 to 2.4 wt%. Increasing the Cr content in the alloy, the FAC rate and oxide thickness decreased. The oxide porosity tends to decrease with the Cr content and immersion time owing to the development of Cr containing oxide. The oxidation behavior is not changed with the immersion time.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1383-1387
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
CO Oxidation Properties Of Selective Dissoluted Metallic Glass Composites
Utlenianie wybranych rozcieńczonych kompozytów szkieł metalicznych
Autorzy:
Kim, S. Y.
Lee, M. H.
Kim, T. S.
Kim, B. S.
Powiązania:
https://bibliotekanauki.pl/articles/355092.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
CO oxidation
metallic glasses
porous metal
catalyst materials
utlenianie
szkło metaliczne
metale porowate
materiał katalityczny
Opis:
Porous metallic materials have been widely used in many fields including aerospace, atomic energy, electro chemistry and environmental protection. Their unique structures make them very useful as lightweight structural materials, fluid filters, porous electrodes and catalyst supports. In this study, we fabricated Ni-based porous metallic glasses having uniformly dispersed micro meter pores by the sequential processes of ball-milling and chemical dissolution method. We investigated the application of our porous metal supported for Pt catalyst. The oxidation test was performed in an atmosphere of 1% CO and 3% O2. Microstructure observation was performed by using a scanning electron microscope. Oxidation properties and BET (Brunauer, Emmett, and Teller) were analyzed to understand porous structure developments. The results indicated that CO Oxidation reaction was dependent on the specific surface area.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1227-1229
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation of Different Cu Nanopowders and Stability of Cu Fluids Produced by Electrical Explosion of Wire in Liquid
Autorzy:
Nguyen, M.-T.
Kim, J.-H.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/355217.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Cu nanopowder
Cu nanofluids
electrical explosion of wire
stability of nanofluids
Opis:
In this study, copper nanoparticles and nanofluids were synthesized by electrical explosion of wire (EEW) in liquid media such as water, ethanol, and acetone. The effect of the different conditions on the properties of the as-synthesized Cu powders and nanofluids were investigated. X-ray diffraction (XRD) analysis was employed to measure the phase of the as-synthesized powder. Only pure Cu phase appeared in case of acetone condition, but CuO and CuO2 phases could be observed in the others. The EEWed particle size was broadened from under 50 to 100 nm. The results showed that acetone was the best condition for achieving smaller particles, preventing the oxidation of the Cu particles and good stability of the nanofluids.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1453-1457
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Characterization of Si Oxide Coated Nano Ceria by Hydrolysis, and Hydrothermal Treatment at Low Temperature
Autorzy:
Kong, M.
Kim, H. W.
Powiązania:
https://bibliotekanauki.pl/articles/354290.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nano-particle
water glass
hydro-reaction
coating method
Opis:
The purpose of this work was to the application of Si oxide coatings. This study deals with the preparation of ceria (CeO2) nanoparticles coating with SiO2 by water glass and hydrolysis reaction. First, the low temperature hydro-reactions were carried out at 30~100°C. Second, Silicon oxide-coated Nano compounds were obtained by the catalyzing synthesis. CeO2 Nano-powders have been successfully synthesized by means of the hydrothermal method, in a low temperature range of 100~200°C. In order to investigate the structure and morphology of the Nano-powders, scanning electron microscopy (SEM) and X-ray diffraction (XRD) were employed. The XRD results revealed the amorphous nature of silica nanoparticles. To analyze the quantity and properties of the compounds coated with Si oxide, transmission electron microscopy (TEM) in conjunction with electron dispersive spectroscopy was used. Finally, it is suggested that the simple growth process is more favorable mechanism than the solution/aggregation process.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1125-1129
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sintering and Microstructures of SUS 316L Powder Produced by 3D Printing Process
Autorzy:
Kim, W. J.
Nguyen, H.-H.
Kim, H. Y.
Nguyen, M.-T.
Park, H. S.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/356018.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
3D printing
selective laser sintering
SUS 316L
flake powder
Opis:
Selective laser sintering (SLS) is a type of laminating sintering technique, using CO2 laser with (metal, polymer, and ceramic) powders. In this result, the flake SUS 316L was used to achieve a high porous product, and compare to spherical type. After SLS, the porosity of flake-type sample with 34% was quite higher than that of the spherical-type one that had only 11%. The surface roughness of the flake SLS sample were also investigated in both inner and surface parts. The results show that the deviation of the roughness of the surface part is about 64.40μm, while that of the internal one was about 117.65μm, which presents the containing of high porosity in the uneven surfaces. With the process using spherical powder, the sample was quite dense, however, some initial particles still remained as a result of less energy received at the beneath of the processing layer.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1215-1218
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of Grain Boundary Morphologies on Stress Corrosion Cracking of Alloy 600
Autorzy:
Kim, H. P.
Choi, M. J.
Kim, S. W.
Kim, D. J.
Lim, Y. S.
Hwang, S. S.
Powiązania:
https://bibliotekanauki.pl/articles/352569.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
alloy 600
NaOH
stress corrosion cracking
grain boundary morphologies
Opis:
Effects of grain boundary morphologies on stress corrosion cracking (SCC) of Alloy 600 have been studied in 40% NaOH at 315°C using C-ring specimens. The configuration of the grain boundary and the intergranular carbide density were controlled by heat treatment. SCC tests were performed at +150 mV above the corrosion potential. The specimen with a serrated grain boundary showed higher SCC resistance than that with a straight grain boundary. This appears to be caused by the fact that the specimen with the serrated grain boundary has longer SCC path. SCC resistance also increased with intergranular carbide density probably due to enhanced relaxation of stress at intergranular carbide.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1415-1419
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Characterization of Ni-CNT Composites by Electrical Explosion of Wire in Different Liquids
Autorzy:
Thuyet-Nguyen, M.
Maithili-Biswas, Maithili-Biswas
Kim, W. J.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/958201.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nickel-Carbon nanotubes composite
carbon nanotubes
electrical explosion of wire
nano-colloid
magnetic properties
Opis:
In this study, Ni-CNT powders and colloids were synthesized via the Electrical explosion of wire (EEW) in different liquid conditions. The influence of ambient solvents (D.I. Water, ethanol, methanol, acetone and ethylene-glycol) on characteristics of the as-synthesized Ni-CNT was investigated. The morphology and size were observed by field emission scanning electron microscopy (FE-SEM). The Ni particles were spherical or near spherical shape. The phase of the composite powders analyzed via X-ray diffraction demonstrate the presence of CNTs in composite powders is not affect the structure of Ni. However, the phase of the composites was changed based on the changing of liquid conditions. Stability of colloids was investigated by Turbiscan technique. Magnetic properties were also investigated by Vibrating sample magnetometer (VSM) at room temperature. The as-synthesized composite powders revealed a ferromagnetic characteristic material.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1219-1223
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure And Thermoelectric Properties Of TAGS-90 Compounds Fabricated By Mechanical Milling Process
Mikrostruktura i właściwości termoelektryczne związków TAGS-90 wytworzonych przez mielenie
Autorzy:
Kim, H.-S.
Babu, M.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/353404.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TAGS-90
thermoelectric properties
high-energy milling
SPS
właściwości termoelektryczne
mielenie wysokoenergetyczne
Opis:
TAGS-90 compound powder was directly prepared from the elements by high-energy ball milling (HEBM) and subsequently consolidated by a spark plasma sintering (SPS). Effect of milling time on the microstructure and thermoelectric properties of the samples were investigated. The particle size of fabricated powders were decreased with increasing milling time, finally fine particles with ~1μm size was obtained at 90 min. The SPS samples exhibited higher relative densities (>99%) with fine grain size. X-ray diffraction analysis (XRD) and energy dispersion analysis (EDS) results revealed that all the samples were single phase of GeTe with exact composition. The electrical conductivity of samples were decreased with milling time, whereas Seebeck coefficient increased over the temperature range of RT~450°C. The highest power factor was 1.12×10-3 W/mK2 obtained for the sample with 90 min milling at 450°C.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1231-1234
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Ga2O3 Nanoparticles Dispersion on Microstructure and Thermoelectric Properties of p-Type BiSbTe Based Alloys
Autorzy:
Kim, E.-B.
Koo, J.-M.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/351366.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
thermoelectric properties
Bi0.5Sb1.5Te3 alloys
Seebeck coefficient
mechanical alloying
spark plasma sintering
Opis:
In this study, p-type Bi0.5Sb1.5Te3 based nanocomposites with addition of different weight percentages of Ga2O3 nanoparticles are fabricated by mechanical milling and spark plasma sintering. The fracture surfaces of all Bi0.5Sb1.5Te3 nanocomposites exhibited similar grain distribution on the entire fracture surface. The Vickers hardness is improved for the Bi0.5Sb1.5Te3 nanocomposites with 6 wt% added Ga2O3 due to exhibiting fine microstructure, and dispersion strengthening mechanism. The Seebeck coefficient of Bi0.5Sb1.5Te3 nanocomposites are significantly improved owing to the decrease in carrier concentration. The electrical conductivity is decreased rapidly upon the addition of Ga2O3 nanoparticle due to increasing carrier scattering at newly formed interfaces. The peak power factor of 3.24 W/mK2 is achieved for the base Bi0.5Sb1.5Te3 sintered bulk. TheBi0.5Sb1.5Te3 nanocomposites show low power factor than base sample due to low electrical conductivity.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 993-997
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation And Stabilization Of Silver Nanoparticles In Ethanol By Phosphinic Acid
Redukcja i stabilizacja nanocząstek srebra w etanolu przez kwas fosforowy
Autorzy:
Kim, J.-K.
Shim, H.-M.
Park, M. J.
Koo, K.-K.
Powiązania:
https://bibliotekanauki.pl/articles/356073.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silver
nanoparticle
kinetic analysis
phosphinic acid
reduction
srebro
nanocząstki
analiza kinetyczna
kwas fosforowy
redukcja
Opis:
Although phosphinic acid (H3PO2) has a powerful reduction potential, the reduction of silver ions by phosphinic acid salt has not yet been reported. In this work, colloidal silver has successfully synthesized by reducing silver ions in ethanol with phosphinic acid as a reducing agent. The effects of [AgNO3]/[H3PO2] ratios and reaction temperature were considered. Spherical silver nanoparticles with cubic structure were successfully prepared and their diameters were measured to be 8.5±0.9 nm − 11.3±0.2 nm. Half-life analysis showed that the reduction of silver ions proceeded with the reaction order of 1.30 on concentration of phosphinic acid and activation energy of 120.7 kJ/mol.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1293-1296
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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