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    Wyświetlanie 1-5 z 5
    Tytuł:
    Crystal structure and Mössbauer effect in multiferroic 0.5BiFeO3-0.5Pb(Fe0.5Ta0.5)O3 solid solution
    Autorzy:
    Stoch, A.
    Maurin, J.
    Stoch, P.
    Kulawik, J.
    Szwagierczak, D.
    Powiązania:
    https://bibliotekanauki.pl/articles/146870.pdf
    Data publikacji:
    2017
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    BiFeO3
    crystal structure
    hyperfine interactions
    multiferroics
    solid solution
    Opis:
    Multiferroic 0.5BiFeO3-0.5Pb(Fe0.5Ta0.5)O3 solid solution is a material that exhibits ferroelectric and antiferromagnetic orderings in ambient temperature. The solid solution was obtained as a result of a conventional reaction in a solid state. The obtained material is a dense, fine-grained sinter whose surface was observed by scanning electron microscopy (SEM) and stoichiometry was confirmed by energy dispersive X-ray spectroscopic (EDS) analysis. According to the X-ray powder diffraction (XRD) measurements, the main phase is R3c space group with admixture of Pm-3m regular phase. Small contribution of pyrochlore-like phase was also observed. Mössbauer spectroscopy suggested random distribution of Fe3+/Ta5+ cations in the B sites of ABO3 compound. Reduction of the magnetic hyperfine field with an increase in the substitution of Ta5+ in Fe3+ neighbourhood was also observed.
    Źródło:
    Nukleonika; 2017, 62, 2; 177-181
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Struktura a nieelastyczne rozpraszanie neutronów przez kryształy molekularne z wiązaniami wodorowymi
    Structure and inelastic neutron scattering by the molecular crystals with the hydrogen bonds
    Autorzy:
    Rok, M.
    Bator, G.
    Sobczyk, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/171492.pdf
    Data publikacji:
    2017
    Wydawca:
    Polskie Towarzystwo Chemiczne
    Tematy:
    kompleksy molekularne
    wiązanie wodorowe
    struktura krystaliczna
    rozpraszanie neutronów
    dynamika cząsteczek w fazie stałej
    molecular complexes
    hydrogen bonds
    crystal structure
    neutron scattering
    molecular dynamics in the solid state
    Opis:
    The molecular crystals, which are built of organic or organic-inorganic molecules, are characterized by the weak intermolecular interactions. From the viewpoint of the potential applications in electronics or optoelectronics the electric properties of the crystals are essential. In turn these properties are related to their crystal structure as well as the dynamics of the molecules in the solid state. The existence of the hydrogen bonds in the crystal structures, conventional and unconventional, is crucial from the viewpoint of the electric properties of the crystals. The dynamics of methyl groups present in the structure can be a measure of the molecular interactions in the crystals. In this work the dynamical properties, first of all taking into account the research results concerning the neutron scattering, will be discussed. The neutron technique is very effective as regards the methyl group dynamics investigations. The relationship between a formation of the conventional and unconventional hydrogen bonds and a tunneling of the methyl groups at low temperature will be discussed. The method of the interpretation of the INS spectra will be described taking into account the theoretical model, the parameters of which are fitted to the experimental data. The examples will regard the following molecular crystals: p-N,N’-1,10-tetraacethyldiaminodurene (TADD) (Figs. 2 and 4), 2,3,5,6-tetramethylpyrazine with chloranilic acid (TMP·CLA) (Figs. 5, 6 and 7), 2,3,5,6- tetramethylpyrazine with bromanilic acid (TMP·BRA) (Figs. 5 and 6) and the crystal of 3,4,7,8-tetramethylphenantroline (Me4phen) and its complex with picric acid (Me4phen·PIC) (Figs. 8 and 9). In this paper we have shown that the surrounding of the methyl group and its interactions with the adjacent molecules has a stronger effect than the changes in the electronic charge density in the molecule.
    Źródło:
    Wiadomości Chemiczne; 2017, 71, 7-8; 533-557
    0043-5104
    2300-0295
    Pojawia się w:
    Wiadomości Chemiczne
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Formation of Transition Phases on Interface between Monocrystalline Fe and Cu Due to Mutual Solid-State Diffusion
    Autorzy:
    Perek-Nowak, M.
    Boczkal, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/351905.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    copper single crystals
    iron single crystal
    transition phase
    solid-state diffusion
    Opis:
    Interdiffusion between Fe (Armco) and Cu single crystals of similar orientation (around [110]) annealed at temperatures of 873 and 973K in air for 0.5 up to 4 h is studied. Formation of three phases different in their chemical composition has been observed: 1) oxide layer on Cu border (porous), 2) a layer rich in copper, iron and oxygen, 3) a layer of iron and oxygen with only small addition of Cu. All reactions of interface formation occurred in solid state. It was noted that oxygen plays an important role in development of new phases. Strong Kirkendall effect is observed due to large difference in diffusion coefficients of copper atoms to iron, DCu→Fe=300exp(-67800/RT) and iron atoms to copper DCu→Fe=0.091exp(-46140/RT).
    Źródło:
    Archives of Metallurgy and Materials; 2016, 61, 2A; 581-586
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Crystal structure and spectroscopic properties of 4-acetaminopyridine and its protonated form
    Autorzy:
    Koleva, B.B.
    Nikolova, R.
    Tchapkanov, A.
    Kolev, T.
    Mayer-Figge, H.
    Spiteller, M.
    Sheldrick, W.S.
    Powiązania:
    https://bibliotekanauki.pl/articles/778733.pdf
    Data publikacji:
    2009
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    4-acetyloaminopirydyna
    struktura kryształów
    spektroskopia IR
    spektroskopia UV
    4-acetaminopyridine
    protonated form
    crystal structure
    solid-state linear polarized IR spectroscopy
    UV spectroscopy
    quantum chemical calculations
    1H and 13C NMR
    ESI-MS
    TGA and DSC
    Opis:
    4-Acetaminopyridine dihydrate and its protonated form, stabilized as the hydrochloride salt have been synthesized and spectroscopic elucidated in solution and in the solid-state by means of the inear-polarized solid state IR-spectroscopy (IR-LD), UV-spectroscopy, TGA, DSC, and the positive and negative ESI MS. Quantum chemical calculations were used to obtain the electronic structure, vibrational data and the electronic spectra. The spectroscopic and theoretical data are compared with the structure of the first compound obtained by single crystal X-ray diffraction. The effect of Npy protonation on the optical and magnetic properties of a 4-acetaminopyridine is discussed.
    Źródło:
    Polish Journal of Chemical Technology; 2009, 11, 3; 35-40
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Nonlinear and linear pressure determination in a two-layer structure: solid crystal - water at GHz frequencies
    Autorzy:
    Filipczyński, L.
    Wójcik, J.
    Kujawska, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/332574.pdf
    Data publikacji:
    2003
    Wydawca:
    Polskie Towarzystwo Akustyczne
    Tematy:
    pressure determination
    solid crystal
    water
    GHz frequencies
    Opis:
    Determination of acoustic pressures at the frequency of 1 GHz by means of PVDF hydrophones is not possible due to their limited frequency response. Moreover, the size of their active electrodes is by about 3 orders of magnitude greater than the resolution in the acoustic microscopes at such a high frequency. Therefore the authors solved this problem at first in a microscope with the working frequency of 34 MHz using both the numerical and experimental methods. A numerical procedure of nonlinear propagation and transducer power measurements were applied giving in effect the same quantitative results. Therefore the identical numerical procedure was used for the l GHz microscope working in the reflection mode. Many pressure field quantities of the microscope were shown, e.g. the pressure values, distributions of the first, second, third and fourth pressure harmonics in and outside of the focus, pulse distortions and their spectra, the resolutions achieved etc. The obtained information on nonlinear propagation effects in microscopy was previously lacking.
    Źródło:
    Hydroacoustics; 2003, 6; 143-150
    1642-1817
    Pojawia się w:
    Hydroacoustics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-5 z 5

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