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Tytuł:
Phase Analysis of Different Liquid Ratio on Metakaolin/Dolomite Geopolymer
Autorzy:
Syauqi Sauffi, Ahmad
Wan Mastura, Wan Ibrahim
Mohd Mustafa Al Bakri, Abdullah
Ibrahim, Masdiyana
Ahmad, Romisuhani
Ahmad Zaidi, Fakhryna
Powiązania:
https://bibliotekanauki.pl/articles/2048822.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
geopolymer
metakaolin
dolomite
phase analysis
Opis:
Geopolymer is widely studied nowadays in various scope of studies. Some of the ongoing studies are the study of the various materials towards the geopolymer strength produced. Meanwhile, some of the studies focus on the mixing of the geopolymer itself. This paper discussed the phase analysis of metakaolin/dolomite geopolymer for different solid to the liquid ratio which was, 0.4, 0.6, 0.8, and 1.0, and the properties that affected the geopolymer based on the phases. The constant parameters in this study were the percentage of metakaolin and dolomite used. The metakaolin used was 80% meanwhile dolomite usage was 20%. Besides that, the molarity of NaOH used is 10M and the alkaline activator ratio used is 2.0. All the samples were tested at 28 days of curing. The results show that the 0.8 solid to the liquid ratio used gave better properties compare to other solid to liquid ratio. The phases analyzed were quartz, sillimanite, mullite, and faujasite. The 0.8 S/L ratio shows the better properties compared to others by the test of phase analysis, compressive strength morphology analysis, and functional group analysis.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 1; 247-250
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of die forging parameters on the microstructure and phase composition of Inconel 718 alloy
Wpływ warunków kucia matrycowego na mikrostrukturę oraz skład fazowy stopu Inconel 718
Autorzy:
Bunsch, A.
Kowalska, J.
Witkowska, M.
Powiązania:
https://bibliotekanauki.pl/articles/355862.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Inconel 718
microstructure
texture
phase analysis
recrystallization
Opis:
The object of the present investigation was Inconel 718 alloy. The material in the initial state and after forging at the temperatures of 1100°C and 1000°C was examined. Diffraction analyses indicate that a nickel-based γ solid solution is a dominating phase in the alloy (so-called nickel austenite). Apart from a solid solution, which constitutes the matrix, certain volume fractions of the other phase were detected e.g. δ phase and carbides. It was found that, due to thermo-mechanical-treatment at both temperatures, the phase composition of Inconel 718 was considerably changed in comparison to the initial state. On the contrary, differences in the temperature of forging did not significantly influence the alloy constitution. However, both of the temperatures of forging result in distinct texture intensity. Microstructure observations indicate that forging at 1000C° led to recrystallization by creation of the new recrystallizated grains near or on the grain boundaries of existing deformed grains. After forging at 1100°C, the microstructure was fully recrystallized at the whole volume of the material.
W pracy przedstawiono wyniki badan wykonanych na stopie niklu Inconel 718. Przebadano materiał w stanie wyjściowym i po kuciu w temperaturach 1100 i 1000°C. Wykonane badania dyfrakcyjne wskazują, ze faza dominującą w stopie jest faza γ roztwór Fe w Ni, często nazywany austenitem niklowym. Oprócz tej fazy, w stopie występują takie fazy jak δ oraz węgliki. Proces kucia w porównaniu do stanu wyjściowego wpływa na skład fazowy (następuje rozpuszczenie niektórych faz i być może przesycenie osnowy), natomiast różnica w temperaturze przeróbki plastycznej nie wpłynęła znacząco na skład fazowy. Obserwacje mikrostruktury wskazują, ze kucie w temperaturze 1100°C prowadzi do pełnej rekrystalizacji dynamicznej, zaś w temperaturze 1000°C rekrystalizacja zachodzi tylko poprzez tworzenie nowych ziarn na granicach ziarn lub w obszarach przy granicach istniejących odkształconych ziarn. Równocześnie, obserwuje się różnice w stopniu steksturowania materiału.
Źródło:
Archives of Metallurgy and Materials; 2012, 57, 4; 929-935
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of X-Ray Diffraction to Analyse Phase Composition of Aluminium Alloys for Plastic Working
Autorzy:
Pachut, K.
Żelechowski, J.
Boczkal, S.
Powiązania:
https://bibliotekanauki.pl/articles/354144.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium alloys
X-ray diffraction
qualitative phase analysis
Opis:
An attempt was made to determine phase composition of commercial aluminium alloys using X-ray diffraction. Samples for phase composition analysis were selected from the group of aluminium alloys covered by the EN 573-3:2013 standard [1]. Representative samples were taken from eight groups of alloys with different chemical composition (at least one sample from each group). The diffraction intensity was measured with a standard X-ray diffractometer in Bragg-Brentano geometry in a way that allowed identification of the weakest diffraction peaks. As a results of the performed research it has been shown that X-ray phase analysis can be used to identify the matrix of aluminium alloys, Si and crystalline intermetallic phases such as Mg2Si, Al93.38Cu6.02Fe24Si16.27, Al4.01MnSi0.74, MgZn2, Al17 (Fe3.2Mn0.8)Si2, Al65Cu20Fe15, and Cu3Mn2Al. The detectability limit of the above-mentioned phases is better than 0.5%. The research has also shown that X-ray phase analysis is applicable in the investigation of phase transformations taking place in aluminium alloys.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1315-1319
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure of Archaeological 17th Century Cast Copper Alloys
Autorzy:
Konieczny, J.
Labisz, K.
Głowik-Łazarczyk, K.
Ćwiek, J.
Wierzbicki, Ł.
Powiązania:
https://bibliotekanauki.pl/articles/382152.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metallography
archaeometallurgy
microstructure
excavations
phase analysis
metalografia
archaeometalurgia
mikrostruktura
wykopaliska
Opis:
In Poland, researchers have a very strong interest in archaeometallurgy, which, as presented in classical works, focuses on dating artefacts from the prehistoric and early medieval periods in the form of cast iron and copper castings. This study, extending the current knowledge, presents the results of a microstructure investigation into the findings from the Modern era dating back to the late Middle Ages. The investigated material was an object in the form of a heavy solid copper block weighing several kilograms that was excavated by a team of Polish archaeologists working under the direction of Ms Iwona Młodkowska-Przepiórowska during works on the marketplace in the city of Czestochowa during the summer of 2009. Pre-dating of the material indicates the period of the seventeenth century AD. The solid copper block was delivered in the form of a part shaped like a bell, named later in this work as a “kettlebell”. To determine the microstructure, the structural components, chemical composition, and homogeneity, as well as additives and impurities, investigations were carried out using light microscopy, scanning electron microscopy including analysis of the chemical composition performed in micro-areas, and qualitative X-ray phase analysis in order to investigate the phase composition. Interpretation of the analytical results of the material’s microstructure will also help modify and/or develop new methodological assumptions to investigate further archaeometallurgical exhibits, throwing new light on and expanding the area of knowledge of the use and processing of seventeenth-century metallic materials.
Źródło:
Archives of Foundry Engineering; 2017, 17, 2; 190-196
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of High-Temperature Oxidizing Conditions on AlCoCrCuNi High Entropy Alloys with and without Silicon Addition
Autorzy:
Gawel, R.
Rogal, Ł.
Przybylski, K.
Matsuda, Kenji
Powiązania:
https://bibliotekanauki.pl/articles/2106569.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high entropy alloy
high temperature oxidation
phase analysis
alloying element
Opis:
Initial investigations on oxidation behaviour and phase transformations of equimolar AlCoCrCuNi high entropy alloy with and without 1 at.% silicon addition during 24-hr exposure to air atmosphere at 1273 K was carried out in this work. After determining the oxidation kinetics of the samples by means of thermogravimetric analysis, the morphology, chemical and phase compositions of the oxidized alloys were determined by means of scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray diffraction analysis. Additional cross-section studies were performed using transmission electron microscopy combined with energy dispersive X-ray spectroscopy and selected area electron diffraction. From all these investigations, it can be concluded that minor silicon addition improves the oxidation kinetics and hinders the formation of an additional FCC structure near the surface of the material.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 2; 471--478
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Reaction Kinetics and Morphological Study of TiNb2O7 Synthesized by Solid-State Reaction
Autorzy:
Choi, S. H.
Ali, B.
Choi, K. S.
Hyun, S. K.
Sim, J. J.
Choi, W. J.
Joo, W.
Lim, J. H.
Lee, T. H.
Kim, T. S.
Park, K. T.
Powiązania:
https://bibliotekanauki.pl/articles/355326.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
solid state reaction
kinetic analysis
quantitative phase analysis
TiNb2O7 synthesis
Opis:
Although TiNb2O7 is regarded as a material with high application potential in lithium-ion batteries (LIBs) and solid-oxide fuel cells (SOFCs), it has been difficult to find suitable cost-effective conditions for synthesizing it on a commercial scale. In this study, TiNb2O7 compounds were synthesized by a solid state synthesis process. For stoichiometrically precise synthesis of the TiNb2O7 phase, the starting materials, TiO2 and Nb2O5 were taken in a 1:1 molar ratio. Activation energy and reaction kinetics of the system were investigated at various synthesis temperatures (800,1000,1200, and 1400°C) and for various holding durations (1,5,10, and 20 h). Furthermore, change in the product morphology and particle size distribution were also evaluated as a function of synthesis temperature and duration. Additionally, quantitative phase analysis was conducted using the Rietveld refinement method. It was found that increases in the synthesis temperature and holding time lead to increase in the mean particle size from 1 to 4.5 μm. The reaction rate constant for the synthesis reaction was also calculated.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1051-1056
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase Composition of Urban Soils by X-Ray Diffraction and Mössbauer Spectroscopy Analysis
Autorzy:
Kierlik, P.
Hanc-Kuczkowska, A.
Męczyński, R.
Matuła, I.
Dercz, G.
Powiązania:
https://bibliotekanauki.pl/articles/353120.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mössbauer spectroscopy
X-ray diffraction
environmental protection
qualitative phase analysis
topsoil
Opis:
The main purpose of this study was to identify the mineral composition of soil sample taken from the upper layer of topsoil. High absorption of chemical substance is a characteristic for humus-organic layer of topsoil. The source of those substance could be a pollutant emitted to the atmosphere by human activity. The research area includes Upper Silesia region, which is the most industrial region of Poland. In the present study, the phase composition of the top soil separates were analyzed by using X-raydiffraction and Mössbauer spectroscopy. X-ray diffraction analysis revealed the presence of seven mineral phases in the material magnetic separated by lower current (quartz, illite, kaolinite, Fe3+ oxides, hematite, magnetite and pyrite). In case of higher current were identified four phases (quartz, muscovite, kaolinite and K0.94 Na0.06 (AlSi3 O8 )). Mössbauer spectroscopy was used for an extensive analysis of iron-containing phases (pyrrhotite, magnetite, aluminosilicate oxides with Fe3+ and kaolinite/Fe2+ silicate).
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 1029-1032
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Iron-containing phases in metallurgical and coke dusts as well as in bog iron ore
Autorzy:
Szumiata, T.
Rachwał, M.
Magiera, T.
Brzózka, K.
Gzik-Szumiata, M.
Gawroński, M.
Górka, B.
Kyzioł-Komosińska, J.
Powiązania:
https://bibliotekanauki.pl/articles/148303.pdf
Data publikacji:
2017
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
metallurgical dusts
coke dusts
bog ore
phase analysis
Mössbauer spectrometry
magnetic susceptibility
Opis:
Several samples of dusts from steel and coke plants (collected mostly with electro filters) were subjected to the investigation of content of mineral phases in their particles. Additionally, sample of bog iron ore and metallurgical slurry was studied. Next, the magnetic susceptibility of all the samples was determined, and investigations of iron-containing phases were performed using transmission Mössbauer spectrometry. The values of mass-specific magnetic susceptibility varied in a wide range: from 59 to above 7000 × 10−8 m3kg−1. The low values are determined for bog iron ore, metallurgical slurry, and coke dusts. The extremely high was obtained for metallurgical dusts. The Mössbauer spectra and X-ray diffraction patterns point to the presence of the following phases containing iron: hematite and oxidized magnetite (in coke and metallurgical dusts as well as metallurgical slurry), traces of magnetite fi ne grains fraction (in metallurgical dusts), amorphous glassy silicates with paramagnetic Fe3+ and Fe2+ ions, traces of pyrrhotite (in coke dusts), α-Fe and nonstoichiometric wüstite (in metallurgical slurry), as well as ferrihydrite nanoparticles (in bog iron ore). For individual samples of metallurgical dusts, the relative contributions of Fe2+/3+ ions in octahedral B sites and Fe2+ ions in tetrahedral A sites in magnetite spinel structure differs considerably.
Źródło:
Nukleonika; 2017, 62, 2; 187-195
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Metallurgical analysis of the causes of failure of the hardening furnace conveyor belt
Autorzy:
Merda, A.
Klimaszewska, K.
Sroka, M.
Golański, G.
Powiązania:
https://bibliotekanauki.pl/articles/378641.pdf
Data publikacji:
2019
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
microstructure
X-ray phase analysis
precipitates
failure
mikrostruktura
rentgenowska analiza fazowa
osady
niepowodzenie
Opis:
Purpose: The aim of the tests was to analyze the microstructure and mechanical properties of a section of the hardening furnace conveyor belt serviced at the temperature of 880-920°C in the carburizing atmosphere, in the context of determining the probable causes of its failure. Design/methodology/approach: The scope of performed tests included: chemical composition analysis of the steel and particles, microstructure investigated using optical and scanning electron microscopy, X-ray phase analysis. Findings: The analysis of the chemical composition showed that the examined material was austenitic steel X15CrNiSi25-21 (S310). Performed metallurgical tests showed that after the service the examined steel was characterized by austenitic structure with numerous precipitates of diverse morphology. In the structure the sigma phase particles and probably the M23C6 carbides precipitates were observed. The continuous grid of precipitates on the boundaries of grains (mainly the sigma phase) and the influence of the cyclic changing heat loads (or thermo-mechanical loads) were the main causes of failure of the analysed detail. Research limitations/implications: The aim of the work was to determine the probable causes of damage of the material used for a conveyor belt of a hardening furnace. Practical implications: The results of investigation and analysis of the metallographic of het-resisting austenitic steel X15CrNiSi25-21 (S310) after service at the temperature of 880-920°C are presented. Originality/value: The paper presents the results of research on the microstructure and mechanical properties of the section of hardening furnace conveyor belt made of creepresisting austenitic steel. The aim of the performed tests was to determine the probable causes of damage of the analysed detail.
Źródło:
Archives of Materials Science and Engineering; 2019, 98, 2; 68-73
1897-2764
Pojawia się w:
Archives of Materials Science and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Workflow of Ground Penetrating Radar Data Analysis Based on Maximum Energy Difference Steering
Przebieg pracy z danymi radarowymi penetrującymi ziemię Analiza oparta na sterowaniu maksymalną różnicą energii
Autorzy:
Dang, Duy Hoang
Le, Cuong Van Anh
Nguyen, Thuan Van
Nguyen, Long Quoc
Huynh, Nhan Thanh
Powiązania:
https://bibliotekanauki.pl/articles/28756746.pdf
Data publikacji:
2023
Wydawca:
Polskie Towarzystwo Przeróbki Kopalin
Tematy:
ground penetrating radar
phase analysis
energy difference
radar penetrujący podłoże
analiza fazowa
różnica energii
Opis:
Ground Penetrating Radar is commonly used in civil engineering sectors. Underground anomalies (i.e., electric wires, water pipes or sinkholes) can be detected through representations of hyperbolae in the measured processed GPR image. Our work focuses on detecting the underground objects and understanding their metallic or nonmetallic characteristics. The max energy difference attribute is applied to illuminate their positions while phase analysis process can determine change of phase spectrum in the diffracted signals. For improving phase analysis, we applied a novel workflow combining conventional processed steps and a zooming step for preserving phase originality without disturbed by any unnecessary filters. We applied the workflow in model and real data for proving its effectiveness. Interpretation of two real datasets in Vietnam by our workflow can express existences of the artificial underground anomalies as well as their matter characteristics comparing to their surrounding environments.
Ground Penetrating Radar jest powszechnie stosowany w inżynierii lądowej i wodnej. Podziemne anomalie (np. przewody elektryczne, rury wodociągowe lub zapadliska) można wykryć za pomocą reprezentacji hiperbol w zmierzonym przetworzonym obrazie GPR. Nasza praca koncentruje się na wykrywaniu podziemnych obiektów i zrozumieniu ich metalicznych lub niemetalicznych wła-ściwości. Atrybut maksymalnej różnicy energii jest stosowany do oświetlania ich pozycji, podczas gdy proces analizy fazowej może określić zmianę widma fazowego w dyfrakcyjnych sygnałach. Aby usprawnić analizę fazową, zastosowaliśmy nowatorski przepływ pracy łączący konwencjonalne kroki przetwarzania i krok powiększania w celu zachowania oryginalności fazy bez zakłócania przez niepotrzebne filtry. Zastosowaliśmy przepływ pracy w modelu i rzeczywistych danych, aby udowodnić jego skuteczność. Interpretacja dwóch rzeczywistych zbiorów danych w Wietnamie za pomocą naszego przepływu pracy może wyrazić istnienie sztucznych anomalii podziemnych, a także ich charakterystykę materii w porównaniu z otaczającym je środowiskiem.
Źródło:
Inżynieria Mineralna; 2023, 1; 195--202
1640-4920
Pojawia się w:
Inżynieria Mineralna
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Joint Hydrogen Susceptibility of 304 SS Welded with Titanium
Podatność połączenia na wodorowanie w układzie plateru stal 304 SS zgrzewanym wybuchowo z tytanem
Autorzy:
Mazancová, E.
Ostroushko, D.
Saksl, K.
Niesłony, A.
Powiązania:
https://bibliotekanauki.pl/articles/356513.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
304 SS-Ti weld
fatique
hydrogen response
phase analysis
304 SS
zmęczenie
wodorowanie
analiza fazowa
Opis:
Welds of thick plates (304 SS) clad with Ti of commercial purity in as-received state and also after subsequent heat treatment and/or after hydrogen charging were investigated. Fatigue tests were carried out at amplitude of 20 Hz and in case of bimetal without hydrogen charging also at amplitude of 40 Hz. After heat treatment, charged welds showed higher threshold level than the welds without heat treatment. Energy dispersed analyses (EDA) of fracture surfaces showed that failure predominantly occurred in joint. Hydrogen induced cracking (HIC) response of bimetal samples demonstrated favourable results both after welding and after subsequent heat treatment. Short and thin cracks were observed, exclusively located in mixed zone, where approx. 16-20 at. % of Ti using EDX (energy dispersed analyser) was revealed. By application of monochromatic synchrotron radiation Ti-α , Fe-fcc, Fe-bcc and intermetallic phase Fe2Ti were detected.
Badano połączenia grubych blach platerowanych (304 ss) z Ti o czystości technicznej po zgrzaniu, jak i po częściowym procesie termicznym i/lub po wodorowaniu. Wykonano testy zmęczeniowe o amplitudzie 20 Hz a w przypadku bimetalu bez wodorowana również o amplitudzie - 40 Hz. po przeprowadzeniu wygrzewania, obciążone połączenie ujawniło wyższy poziom progu niż połączenie, w których nie wykonano obróbki termicznej. Analiza EDA powierzchni łączenia udokumentowała silny udział pęknięć na powierzchni łączenia. Wodorowanie silnie wpływa na inicjacje pękanie (HIC), w bimetalowych próbkach w stanie po platerowaniu, jak i po obróbce termicznej. Zaobserwowano, krótkie i cienkie pęknięcia, które zlokalizowane były w strefie połączenia, gdzie zaobserwowano (analiza SEM/EDX) fazy zawierające 16-20 wt.% Ti. Przez zastosowanie monochromatycznego promieniowania synchrotonowego wykryto fazy Ti- α, Fe-fcc, Fe-bcc oraz fazę międzymetaliczną typu Fe2Ti.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 4; 1605-1610
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of Thermal Stability of Intermetallic Phases Precipitates in Continuous Ingots of AlCu4MgSi Alloy
Autorzy:
Nuckowski, P. M.
Kondracki, M.
Wróbel, T.
Powiązania:
https://bibliotekanauki.pl/articles/382300.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium alloys
phase analysis
high temperature X-ray diffraction
thermal-derivative analysis
stopy aluminium
analiza fazowa
wysokotemperaturowa dyfrakcja rentgenowska
analiza termopochodna
Opis:
The article presents the results of research concerning to AlCu4MgSi alloy ingots produced using horizontal continuous casting process. The presented research was focused on the precise determination of phase composition of the precipitates formed during the solidification of ingots and the analysis of their thermal stability. In order to assess the morphology of precipitates in the AlCu4MgSi alloy, data obtained by using a computer simulation of thermodynamic phenomena were compiled with results obtained using advanced research techniques, i.e. High-temperature X-ray diffraction (HT-XRD), SEM-EDS, Thermal and derivative analysis (TDA) and Glow discharge optical emission spectroscopy (GD OES). SEM observations and analysis of chemical composition in micro-areas showed that the precipitates are mainly intermetallic θ-Al2Cu and β-Mg2Si phases, and also presence of Al19Fe4MnSi2 intermetallic phase was confirmed by X-ray diffraction studies. Based on the prepared Thermo-Calc simulation data, high-temperature X-ray diffraction measurements were conducted.
Źródło:
Archives of Foundry Engineering; 2019, 4; 99-104
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
DSC Application for Microstructure Investigations of Medieval Cu Alloys
Autorzy:
Konieczny, J.
Labisz, K.
Głowik-Łazarczyk, K.
Surma, S.
Wierzbicki, Ł.
Jurczyk, S.
Powiązania:
https://bibliotekanauki.pl/articles/381124.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
scanning calorimetry DSC
archaeometallurgy
copper alloy
excavation
phase analysis
kalorymetria skaningowa DSC
archeometalurgia
stop miedzi
wyrobisko
analiza fazowa
Opis:
Archaeometallurgical investigations presented in this work focus on analysing the microstructure as well as mechanical properties of artefacts from the17th in form of findings performed from cast iron as well as copper casts. The presented research results extend the up-to-date knowledge and present the analysis of structural compounds found in the microstructure of the artefacts from the time dating back to the late Middle Ages in the region around Czestochowa, Poland. The tested samples were found in earth in the city centre under the present marketplace. The excavation works were carried out in summer in the year 2009, and have resulted in the excavation of artefacts in form of copper block of the weight of several kg. The excavation action was led by a group of Polish archaeologists collaborating with the local authorities. The performed pre-dating of this element determines the age of the artefacts as the 17th century AD. The excavations that have been taking place since 2007 have widened the knowledge of the former Czestochowa. Historians of this town have suggested, that the found weight and traces of metallurgical activity suggest that the exposed walls were an urban weight. The weight is visible on the 18th century iconography. What was find on the Old Market indicates that there was a lush economic life before the Swedish invasion in this part of Poland. Some buildings lost their functions or were changed, others died in fires, but new places developed. To describe the microstructure, with its structural components, research was done using microscopy techniques, both of the light as well as electron microscopy (SEM), also chemical composition analysis was carried out using the EDS technique, as well as tool for phase analysis were applied in form of X-Ray Diffraction (qualitative analysis), especially for the reason to describe the phases present in the excavated material. This research will help to obtain new information in order to investigate further archaeometallurgical artefacts, extending the knowledge about middle age metallic materials its usage and manufacturing.
Źródło:
Archives of Foundry Engineering; 2018, 18, 2; 21-26
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wear resistance of aluminized steel plates
Odporność na scieranie aluminiowanych taśm stalowych
Autorzy:
Żaba, K.
Powiązania:
https://bibliotekanauki.pl/articles/352691.pdf
Data publikacji:
2011
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminiowana taśma stalowa
odporność na ścieranie
powłoki
chropowatość
aluminized steel plate
abrasion resistance
coatings
roughness
X-ray phase analysis
Opis:
The results of the abrasion resistance measurements of aluminized steel strips are presented in the hereby paper. Steel strips of DX52D+AS120 grade, before and after a heat treatment at temperatures of 200-1000 C for 1 – 5760 minutes, were tested. Tests of the abrasion resistance were carried on in a specially built device: rotating disk – sample performing a plane-rotary motion, with an application of a lubricating medium. Examinations of the abrasion resistance were also performed by means of the block-on-ring tester. Estimations of a coating mass loss, roughness and thickness changes were carried on. The obtained results are illustrated by diagrams and macro- and micro-observations. Phase analysis investigations were also performed on samples selected after the abrasibility testing. The range of the heat treatment parameters – after which the Al-Si coating increased its abrasion resistance – was estimated.
W artykule przedstawiono wyniki badan odpornosci na ścieranie aluminiowanych tasm stalowych. Badaniom poddano taśmy stalowe z gatunku DX52D+AS120 przed i po obróbce cieplnej w temperaturze 200-1000 C w czasie 1min-5760min. Wykonano badania odporności na ścieranie w specjalnie przygotowanym urzadzeniu typu obracająca się tarcza – próbka, wykonujaca ruch posuwisto-zwrotny, przy zastosowaniu środka smarujacego Zrealizowano także badania odporności na zużycie cierne za pomocą testera typu rolka-klocek. Dokonano oceny ubytku masy, zmian chropowatoąci i grubości powłoki. Wyniki badan zobrazowano za pomocą wykresów oraz makro i mikro obserwacji. Przeprowadzono także badania analizy fazowej na próbkach wytypowanych po badaniach ścieralności. Określono taki zakres parametrów obróbki cieplnej, po której następuje wzrost odporności na ścieranie powłoki Al-Si.
Źródło:
Archives of Metallurgy and Materials; 2011, 56, 4; 871-882
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Identyfikacja wydzieleń występujących w strukturze blach cienkich ze stopu magnezu AM50
Identification of precipitations in structure of AM50 magnesium alloy sheets
Autorzy:
Skupień, P.
Rozmus, R.
Powiązania:
https://bibliotekanauki.pl/articles/181554.pdf
Data publikacji:
2013
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Metalurgii Żelaza im. Stanisława Staszica
Tematy:
stop magnezu AM50
struktura
wydzielenia
blachy cienkie
analiza fazowa
AM50 magnesium alloy
structure
precipitations
sheets
phase analysis
Opis:
W pracy przedstawiono wyniki badań obejmujące identyfikację wydzieleń znajdujących się w strukturze blach cienkich ze stopu magnezu AM50 walcowanych na gorąco. Badania przeprowadzono przy użyciu wysokorozdzielczego elektronowego mikroskopu skaningowego Inspect F oraz transmisyjnego Titan 80-300. W strukturze badanego stopu zidentyfikowano trzy typy wydzieleń różniących się miedzy sobą składem chemicznym i morfologią.
This paper presents the results of tests including the identification of precipitations in the structure of hot rolled AM50 magnesium alloy sheets. The tests were carried out using high-resolution scanning electron microscope Inspect F and transmission electron microscope Titan 80-300. Three types of precipitations were identified within the structure of the tested alloy, which differed in their chemical compositions and morphologies.
Źródło:
Prace Instytutu Metalurgii Żelaza; 2013, T. 65, nr 4, 4; 18-22
0137-9941
Pojawia się w:
Prace Instytutu Metalurgii Żelaza
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 121

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