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Wyświetlanie 1-10 z 71
Tytuł:
Identification of sandstone-related rocks composition using the X-ray analysis
Autorzy:
Kosuth, M.
Powiązania:
https://bibliotekanauki.pl/articles/344037.pdf
Data publikacji:
2013
Wydawca:
nakł. Maciej Pawlikowski
Tematy:
X-ray analysis
mineral composition
sandstones
siltstones
calcite
dolomite
Opis:
The article presents knowledge based on investigation of sandstones or siltstones composition from the Paleogene flysch terrains in North-East Slovakia. Samples of frequently crumbling clastic rocks were commonly considered to be close to sandstones, composed by predominant quartz. The set of such samples, belonging to Dukla Unit Sandstones were analyzed using the XRD analyses. Beside of quartz the diffraction patterns gave the evidence in significant carbonate share with some minor to minute feldspars, mica and chlorite contents. Among majority of analyzed samples we distinguish three groups of sandstones: (1) with the abundant calcite admixture, (2) the sandstones which contain meaning dolomite portion. The group (3) is representing the samples is formed the same by quartz as by both of carbonates, each of them could form important up to prevailed mineral component. Comparison of analyzed samples mineral composition shows remarkable trend of higher calcite and dolomite contents in younger clastic sediments.
Źródło:
Auxiliary Sciences in Archaeology, Preservation of Relics and Environmental Engineering; 2013, 16; 1-7
1689-6742
Pojawia się w:
Auxiliary Sciences in Archaeology, Preservation of Relics and Environmental Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure, physical properties and fractal character of surface topography of CVD coatings
Autorzy:
Kwaśny, W.
Powiązania:
https://bibliotekanauki.pl/articles/100107.pdf
Data publikacji:
2011
Wydawca:
Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
Tematy:
CVD coatings
fractal geometry
multifractal geometry
X-ray analysis
Opis:
The aim of the presented study is to establish a methodology elaboration, giving a possibility to predict properties of coatings reached in CVD process on tool materials, based on fractal quantities describing their surface. Coatings' topography and its structure which has an impact on a shape of analysed objects' surface were characterised in a comprehensive way. Influence of a type of process and conditions of deposition over structure and shape of topography as well as mechanical and operational properties of the acquired coatings were determined.
Źródło:
Journal of Machine Engineering; 2011, 11, No. 1-2; 134-151
1895-7595
2391-8071
Pojawia się w:
Journal of Machine Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Ceramic Coating on Mechanical Properties of Stainless Steel
Autorzy:
Czekaj, D.
Lisińska-Czekaj, A.
Krzysztofowicz, K.
Powiązania:
https://bibliotekanauki.pl/articles/353220.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
X-ray analysis
microhardness
sol-gel ceramic coating
Opis:
Crystal structure and phase composition of stainless steel substrates (AISI 304 type) was studied and it was found that they adopted the cubic symmetry. The calculated elementary cell parameter for the mayor Fe-Ni phase (weight fraction 99%) was a = 3.593 Å, whereas the mean grain size was = 2932 Å. Morphology of the stainless steel substrate surface was studied with profilometry. Mechanical properties of the stainless steel substrates and stainless steel substrates coated with ceramic layer of barium strontium titanate were studied with microhardness tester. For measurements performed according to the Vickers method the average microhardness was found HV = 189 or HV = 186 for the “in-line” and “mapping” measurement pattern, respectively. The sol-gel method was used to coat the surface of the stainless steel substrate with a thin ceramic layer of the chemical composition Ba0.6 Sr0.4 TiO3 . It was found that the stainless steel substrate covered with sol-gel deposited ceramic coating exhibited the average hardness within the range HV = 217 up to HV = 235 for loading force F = 98 mN and F = 0.98 N, respectively. The Knopp method was also used and it was found that the stainless steel substrate with Ba0.6 Sr0.4 TiO3 coating exhibited hardness HK = 386.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 911-916
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
N-N Bond Lengths and Initiation Reactivity of Nitramines
Autorzy:
Zeman, Svatopluk
Atalar, Taner
Růžička, Aleš
Powiązania:
https://bibliotekanauki.pl/articles/358441.pdf
Data publikacji:
2020
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
bond length
impact sensitivity
nitramines
reactivity
thermal decomposition
X-ray analysis
Opis:
For the 16 selected nitramines, it is shown that an increase in the energy content of these molecules (represented by enthalpies of formation) is connected with an increase in the lengths of the longest N–N bonds in the molecules. These lengths are directly proportional to the activation energies of the low-temperature thermal decomposition of the pure nitramines in all states of matter for this reaction. Raising the energy content also leads to reductions in the rate constants of thermal decomposition. Both of these facts are in contrast to expectations and also with similar published findings concerning thermal decomposition of nitramines in solution, which can be explained by the solvation effect and termination of the emerging aza-radicals in solutions. The calculated dissociation energies of the weakest N–N bonds yielded a relatively good reciprocal conformity with the lengths of the longest N–N bonds of the nitramines studied, especially when using the UB3LYP/6-31G* method. The relationship between the impact sensitivity of these nitramines and the lengths of their longest N–N bond is not completely clear. Such lengths cannot be a measure of impact reactivity, because the longest N–N bond might be stabilized in some cases by suitable intermolecular interactions with adjacent molecules in the crystal lattice.
Źródło:
Central European Journal of Energetic Materials; 2020, 17, 2; 169-200
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of X-ray fluorescence techniques for the determination of hazardous and essential trace elements in environmental and biological materials
Autorzy:
Bamford, S.
Wegrzynek, D.
Chinea-Cano, E.
Markowicz, A.
Powiązania:
https://bibliotekanauki.pl/articles/147255.pdf
Data publikacji:
2004
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
biological material
environmental materials
X-ray fluorescence analysis
Opis:
The utilization of X-ray fluorescence technique for the determination of trace element concentrations in environmental and biological samples is presented. The analytical methods used include energy dispersive X-ray fluorescence with polarizing secondary targets, total reflection X-ray fluorescence, direct in-situ X-ray fluorescence, and micro-beam X-ray fluorescence spectrometry. These methods were applied to analysis of different samples including soil, water, plant material and airborne particulate matter collected on polycarbonate filters. The performance and achieved detection limits of elements for different techniques, established by measuring appropriate reference standards, are presented. Also described is the utilization of micro-beam X-ray fluorescence technique for studying element distribution in heterogeneous samples and investigating the 2D- and 3D-morphology of minute samples by means of computerized X-ray absorption and X-ray fluorescence tomography. The different X-ray techniques have their unique advantages. The micro-beam X-ray fluorescence set-up has an advantage of producing very well collimated primary X-ray beam (about 15 mm in diameter), in front of which the analyzed sample can be precisely positioned, providing local information about the sample composition. The energy dispersive X-ray fluorescence with secondary targets offers rapid analysis of broad range of elements (Na–U) combined with a simple sample preparation method. Total reflection X-ray fluorescence technique, characterized by the lowest detection limits of elements, has its leading edge in analysis of liquid samples, and dealing with particle size effects in air particulates collected on filter papers. In-situ X-ray fluorescence spectrometers are truly portable and enable on the spot, in field analysis. It is shown that the combination of several XRF methods
Źródło:
Nukleonika; 2004, 49, 3; 87-95
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wpływ procesu redukcji na właściwości strukturalne i mechaniczne szkieł tlenkowych z grupy (Pb,Bi)-(Si,Ge)-O
Influence of reduction process on the structural and mechanical properties of (Pb,Bi)-(Si,Ge)-O oxide glasses
Autorzy:
Bochentyn, B.
Powiązania:
https://bibliotekanauki.pl/articles/134776.pdf
Data publikacji:
2015
Wydawca:
ADVSEO
Tematy:
szkła tlenkowe
skaningowa mikroskopia elektronowa
analiza rentgenowska
oxide glass
reduction
Scanning Electron Microscopy
Energy Dispersive X-Ray Analysis
Opis:
The effect of the reduction process in H2 at 380 °C on the microstructure and elemental composition of a glass Bi0.4Pb0.2Si0.4Ox has been investigated. It has been shown that after reduction a clearly separated top layer with a thickness of approx. 50 µm was formed on the surface of the sample. This layer is depleted of oxygen and has higher electrical conductivity than the interior of the glass. It has also been found that some granules of metallic bismuth with a diameter of tens to hundreds of nanometers were formed on the surface of the glass. Furthermore, depletion of lead was observed in these samples in relation to the initial stoichiometry of the glass prior to trial reduction.
Źródło:
Technical Issues; 2015, 2; 3-8
2392-3954
Pojawia się w:
Technical Issues
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Metallurgical analysis of the causes of failure of the hardening furnace conveyor belt
Autorzy:
Merda, A.
Klimaszewska, K.
Sroka, M.
Golański, G.
Powiązania:
https://bibliotekanauki.pl/articles/378641.pdf
Data publikacji:
2019
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
microstructure
X-ray phase analysis
precipitates
failure
mikrostruktura
rentgenowska analiza fazowa
osady
niepowodzenie
Opis:
Purpose: The aim of the tests was to analyze the microstructure and mechanical properties of a section of the hardening furnace conveyor belt serviced at the temperature of 880-920°C in the carburizing atmosphere, in the context of determining the probable causes of its failure. Design/methodology/approach: The scope of performed tests included: chemical composition analysis of the steel and particles, microstructure investigated using optical and scanning electron microscopy, X-ray phase analysis. Findings: The analysis of the chemical composition showed that the examined material was austenitic steel X15CrNiSi25-21 (S310). Performed metallurgical tests showed that after the service the examined steel was characterized by austenitic structure with numerous precipitates of diverse morphology. In the structure the sigma phase particles and probably the M23C6 carbides precipitates were observed. The continuous grid of precipitates on the boundaries of grains (mainly the sigma phase) and the influence of the cyclic changing heat loads (or thermo-mechanical loads) were the main causes of failure of the analysed detail. Research limitations/implications: The aim of the work was to determine the probable causes of damage of the material used for a conveyor belt of a hardening furnace. Practical implications: The results of investigation and analysis of the metallographic of het-resisting austenitic steel X15CrNiSi25-21 (S310) after service at the temperature of 880-920°C are presented. Originality/value: The paper presents the results of research on the microstructure and mechanical properties of the section of hardening furnace conveyor belt made of creepresisting austenitic steel. The aim of the performed tests was to determine the probable causes of damage of the analysed detail.
Źródło:
Archives of Materials Science and Engineering; 2019, 98, 2; 68-73
1897-2764
Pojawia się w:
Archives of Materials Science and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Zmiany struktury zaczynu cementowego pod wpływem roztworu powodującego dekalcyfikację
Changes of the cement paste structure under decalcification
Autorzy:
Słomka-Słupik, B.
Zybura, A.
Powiązania:
https://bibliotekanauki.pl/articles/362852.pdf
Data publikacji:
2009
Wydawca:
Instytut Fizyki Budowli Katarzyna i Piotr Klemm
Tematy:
dekalcyfikacja zaczynu cementowego
chlorek amonu
analiza rentgenowska
SEM-BSE
analiza obrazu
decalcification of the cement paste
ammonium chloride
X-ray analysis
image analysis
Opis:
Przedstawiono zmiany struktury zaczynu z cementu portlandzkiego zwykłego zachodzące wskutek działania chlorku amonu, który wchodzi w skład ścieków zakładów koksochemicznych. Działanie agresywne nasyconego roztworu NH4Cl trwało 25 dób. Badania rentgenowskie składu fazowego wskazały zanikanie portlandytu przy brzegu próbki. Wywołane ubytkiem portlandytu nieciągłości struktury określono na podstawie obserwacji zgładu w elektronowym mikroskopie skaningowym (SEM) oraz stosując metodę analizy obrazu.
The changes of ordinary Portland cement paste structure caused by interaction with ammonium chloride solution, which is present in coke sewage, are described. The aggressive immersion of specimen lasted for 25 days into saturated solution of NH4Cl. The X-ray examinations of phase composition pointed at portlandite decrease and its disappearance at the edge of the specimen. Discontinuities of the cement paste matrix caused by the portlandite amount changes determined from the polished section observations into scanning electron microscope using backscattered electrons with application of image analysis.
Źródło:
Fizyka Budowli w Teorii i Praktyce; 2009, T. 4; 163-168
1734-4891
Pojawia się w:
Fizyka Budowli w Teorii i Praktyce
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical behaviour and phase transition mechanisms of a shape memory alloy by means of a novel analytical model
Autorzy:
Carpinteri, A.
Di Cocco, V.
Fortese, G.
Ronchei, C.
Scorza, D.
Vantadori, S.
Zanichelli, A.
Iacoviello, F.
Natali, S.
Powiązania:
https://bibliotekanauki.pl/articles/386617.pdf
Data publikacji:
2018
Wydawca:
Politechnika Białostocka. Oficyna Wydawnicza Politechniki Białostockiej
Tematy:
fatigue behaviour
phase transition mechanisms
shape memory alloy
tensile cyclic test
x-ray diffraction analysis
Opis:
The aim of the present paper is to examine both the fatigue behaviour and the phase transition mechanisms of an equiatomic pseudo-elastic NiTi Shape Memory Alloy through cyclic tests (up to 100 loading cycles). More precisely, miniaturised dog-bone specimens are tested by using a customised testing machine and the contents of both austenite and martensite phase are experimentally measured by means of X-Ray diffraction (XRD) analyses. On the basis of such experimental results in terms of martensite content, an analytical model is here formulated to correlate the stress-strain relationship to the phase transition mechanisms. Finally, a validation of the present model by means of experimental data pertaining the stress-strain relationship is performed.
Źródło:
Acta Mechanica et Automatica; 2018, 12, 2; 105-108
1898-4088
2300-5319
Pojawia się w:
Acta Mechanica et Automatica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analiza nieorganicznych i organicznych pozostałości po wystrzale z broni palnej.
Analysis of inorganic and organic remains after firearms discharge.
Autorzy:
Łasińska, Anna
Powiązania:
https://bibliotekanauki.pl/articles/501767.pdf
Data publikacji:
2017-03-15
Wydawca:
Agencja Bezpieczeństwa Wewnętrznego
Tematy:
skaningowa mikroskopia elektronowa,
SEM,
mikroanaliza rentgenowska,
EDS,
pozostałości po wystrzale z broni palnej,
GSR,
spektroskopia Ramana.
scanning electron microscopy,
X-ray analysis,
EDX,
gunshot residue,
Raman spectroscopy.
Opis:
W publikacji przedstawiono rezultaty pilotażowych badań metodą skaningowej mikroskopii elektronowej sprzężonej z mikroanalizą rentgenowską oraz spektroskopii Ramana. Wykazano możliwość identyfikacji składników nieorganicznych oraz niektórych związków organicznych zawartych w pozostałościach powystrzałowych, a także wprowadzono nowy element badawczy w postaci mapowania zmian intensywności pasm niektórych grup funkcyjnych substancji organicznych obecnych w pojedynczym ziarnie. Celem badań jest stopniowe i systematyczne opracowywanie metodyki analizy chemicznej cząstek powystrzałowych pochodzących z amunicji zawierającej ołów oraz z amunicji bezołowiowej, a także opracowanie procedur badawczych dotyczących oznaczania pozostałości po użyciu z broni palnej, w tym typowanie rodzaju materiałów dowodowych i materiału porównawczego oraz wdrożenie ich do rutynowej praktyki opiniodawczej w Biurze Badań Kryminalistycznych ABW. Wskazane jest także opracowanie własnych kryteriów interpretacji wyników badań pozostałości powystrzałowych w celu powiązania osoby podejrzanej z użyciem broni palnej. Należy zaznaczyć, że zrealizowany eksperyment jest jedynie wstępem do podjęcia dalszych, bardziej zaawansowanych badań, prowadzących do identyfikacji, klasyfikacji oraz dyskryminacji mikrośladów pochodzących z przestępstw z udziałem broni.
The paper describes the results of the Raman spectroscopy and scanning electron microscopy equipped with X-ray in the primary analysis of gunshot residues. It demonstrates the ability to identify inorganic components and the organic compounds contained in the gunshot residue, and also introduces a new element of the research in the form of mapping changes in the intensity of bands of some functional groups of organic substances to be found in a single grain. The aim of the research is a gradual and systematical elaboration of the methodology of chemical analysis of gunshot residue particles, originating from ammunition containing lead and unleaded ammunition. Further aim is to develop the testing procedures remains with use of firearms and their implementation in consultative routine practice in the Forensic Laboratory ABW, choosing the type of evidence and comparative materials. In order to relate the person suspected to fact of using firearms, it is advisable to elaborate individual criteria of interpreting the results of gunshot residues study. It should be noted that the conducted experiment determines only a prelude for conducting more advanced researches which lead to the identification, classification and discrimination of microtraces originated from crime use of firearms.
Źródło:
Przegląd Bezpieczeństwa Wewnętrznego; 2017, 9, 16; 157-189
2080-1335
2720-0841
Pojawia się w:
Przegląd Bezpieczeństwa Wewnętrznego
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-10 z 71

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