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Tytuł:
Uncommon applications of statistical methods of the design of experiments in chemical technology and environment protection
Autorzy:
Lewandowski, G.
Ćwirko, J.
Powiązania:
https://bibliotekanauki.pl/articles/778597.pdf
Data publikacji:
2007
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
planowanie doświadczeń
optymalizacja
plany kompozycyjne centralne
barwniki
estryfikacja
fotoaktywność TiO2
design of experiments
optimization
central composite designs
dyes
esterification
TiO2 photoactivity
biodiesel
Opis:
The review of literature related to the applications of statistic methods of design of experiments in chemical technology and environment protection was presented in the work. The research that consists of two stages: a stage of choosing the best variables describing an experimental object and a stage of proper experimental investigation, seems particularly interesting. An interesting example of an application of statistical strategies in environmental protection is the optimization of photoactivity of TiO2/SiO2 mixture, received by a sol-gel technique. TiO2, due to its specific feature, was applied in the photocatalytic methods of removing toxic compounds from water and air. In the experiments there were used two designs - the fractional factorial design 2^5-1 (as the elimination one) and the central composite design (as the proper one). Following the data analysis from the elimination plan two variables were eliminated, which helped to simplify the research object. Among other uncommon applications of the design of experiments: the optimization of the conditions for the extraction of natural pigments used in dyeing food, the production of fatty acid methyl esters used as diesel oil substitutes (biodiesel) and the optimization of a supercritical fluid extraction methodology for the analysis of castor oil, should be mentioned.
Źródło:
Polish Journal of Chemical Technology; 2007, 9, 4; 63-67
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Zastosowanie centralnych rotatabilnych planów kompozycyjnych w optymalizacji parametrów metody ball-cratering
Application of the central composite rotatable design in the optimisation of parameters of a ball-cratering method
Autorzy:
Osuch-Słomka, E.
Ruta, R.
Powiązania:
https://bibliotekanauki.pl/articles/188540.pdf
Data publikacji:
2013
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
metoda ball-cratering
powłoka przeciwzużyciowa
centralne rotabilne plany kompozycyjne
funkcja użyteczności
ball-cratering method
antiwear coating
central composite rotatable design
utility function
Opis:
Artykuł przedstawia propozycję wykorzystania centralnych rotabilnych planów kompozycyjnych [L. 1–5] do wyznaczenia optymalnych wartości parametrów metody ball-cratering i badania zużywania ściernego powłok przeciwzużyciowych. Pokazano zestawy wartości parametrów metody ball-cratering wyznaczone jako układy planu rotatabilnego eksperymentu kompozycyjnego. Na podstawie pomiaru średnic śladów zużycia uzyskanych dla wyznaczonych zestawów wartości parametrów metody zidentyfikowano zależności maksymalnych błędów względnych średnic zewnętrznej i wewnętrznej oraz grubości pierścienia śladu zużycia jako funkcje kwadratowe parametrów metody. Wykorzystując funkcję użyteczności, wyznaczono wartości parametrów metody maksymalizujące łączną użyteczność uwzględniającą minimalizację błędu względnego i maksymalizację grubości pierścienia. Wyznaczone parametry pracy węzła tarcia zostały zastosowane do przeprowadzenia biegów tribologicznych mających na celu wyznaczenie współczynnika zużywania ściernego gradientowej powłoki przeciwzużyciowej TiN/TiCN.
This article presents an outline of a method of planning an experiment known as the central composite rotatable design (CCRD) for the optimisation of processes and as an example of its application in the optimisation of parameters of a ball-cratering method. Abrasive wear tests were performed on chosen antiwear physical vapour deposition coating with the optimum work parameters of friction node. The presented method of determining the values of the parameters has been with reference to the tested PVD gradient coating TiN/TiCN.
Źródło:
Tribologia; 2013, 6; 77-86
0208-7774
Pojawia się w:
Tribologia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Parametric optimization of rice bran oil extraction using response surface methodology
Autorzy:
Ahmad, S. W.
Javed, F.
Ahmad, S.
Akram, M.
Rehman, A.
Powiązania:
https://bibliotekanauki.pl/articles/778979.pdf
Data publikacji:
2016
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
solvent extraction
rice bran oil
response surface methodology (RSM)
central composite design (CCD)
Opis:
Use of bran oil in various edible and nonedible industries is very common. In this research work, efficient and optimized methodology for the recovery of rice bran oil has been investigated. The present statistical study includes parametric optimization, based on experimental results of rice bran oil extraction. In this study, three solvents, acetone, ethanol and solvent mixture (SM) [acetone: ethanol (1:1 v/v)] were employed in extraction investigations. Response surface methodology (RSM), an optimization technique, was exploited for this purpose. A five level central composite design (CCD) consisting four operating parameter, like temperature, stirring rate, solvent-bran ratio and contact time were examined to optimize rice bran oil extraction. Experimental results showed that oil recovery can be enhanced from 71% to 82% when temperature, solvent-bran ratio, stirring rate and contact time were kept at 55°C, 6:1, 180 rpm and 45 minutes, respectively while fixing the pH of the mixture at 7.1.
Źródło:
Polish Journal of Chemical Technology; 2016, 18, 3; 103-109
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pressure acid leaching of sphalerite concentrate. Modeling and optimization by response surface methodology
Autorzy:
Guler, E.
Powiązania:
https://bibliotekanauki.pl/articles/110475.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
pressure leaching
sphalerite concentrate
optimization
response surface methodology
central composite rotatable design
Opis:
The zinc leaching from sphalerite concentrate using oxygen under pressure in sulfuric acid solution was primarily studied and evaluated. The effects of important leaching parameters such as oxygen partial pressure, temperature, solid/liquid ratio and leaching time on leaching efficiency, Zn concentration and Fe extraction were investigated. Response surface methodology based on central composite rotatable design technique was used to optimize the leaching process parameters in order to obtain a suitable leach solution with high Zn leaching efficiency considering further processes such as precipitation of contaminating metal ions and electrolysis. The optimum leaching condition for maximum Zn leaching efficiency and Zn concentration with minimum Fe extraction was determined as follows: oxygen partial pressure of 12 bars, temperature of 150 °C, solid/liquid ratio of 0.20 and leaching time of 89.16 minutes. The achieved experimental results for Zn leaching efficiency, Zn concentration and Fe extraction under the optimum conditions were as 94%, 80 g/dm3 and 8.1% respectively. The experimental results corresponded well with the predicted results of quadratic polynomial models.
Źródło:
Physicochemical Problems of Mineral Processing; 2016, 52, 1; 479-496
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Central composite design application in oil agglomeration of talc
Autorzy:
Polowczyk, I.
Kozlecki, T.
Powiązania:
https://bibliotekanauki.pl/articles/109551.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
talc
oil agglomeration
optimization
central composite design
design of experiment
Opis:
Talc has many applications in various branches of industry. This material is an inert one with a naturally hydrophobic surface. Talc agglomeration is within the wide interest of pharmaceutical industry. Oil agglomeration experiments of talc were carried out to find out and assess the significance of experimental factors. Central composite design (CCD) was used to estimate the importance and interrelation of the agglomeration process parameters. Four experimental factors have been evaluated, i.e. concentration of cationic surfactant and oil, agitation intensity as well as time of the process. The median size of agglomerates (D50) and the polydispersity span (PDI) were used as the process responses. Logarithmic transformations of the responses provide better description of the model, than untransformed responses, with the reduced cubic model for D50 and quadratic model for PDI. This was supported by the Box-Cox plots. It was shown that there were many statistically important factors, including the concentration of cationic surfactant and stirring rate for D50, concentration of oil and stirring rate for PDI, as well as various interactions, up to third order for D50. Optimal conditions for minimum values of reagent amounts as well as mixing time and intensity for the maximum size of agglomerates but of rather narrow size distribution were found.
Źródło:
Physicochemical Problems of Mineral Processing; 2017, 53, 2; 1061-1078
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of Factors Influencing Dry Sliding Wear Behaviour of Laser Remelted Plasma Sprayed Mo Coating Using Response Surface Methodology
Autorzy:
Manjunatha, S. S.
Manjaiah, M.
Basavarajappa, S.
Powiązania:
https://bibliotekanauki.pl/articles/356714.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
laser remelting
plasma spray
central composite design (CCD)
response surface methodology (RSM)
Mo coating
Opis:
Plasma spraying is a process widely used to fabricate wear resistant coatings. However, various problems are associated with plasma spraying out of which poor bonding strength between the coating and the substrate and the high porosity in the as sprayed coatings are of major concern. In order to eliminate these problems and enhance wear performance, the laser remelting process has been used. The laser remelting of plasma sprayed Mo coatings alters the wear mechanism and improves the wear resistance. The wear mechanism and wear volume loss depend on the applied load, sliding speed and sliding distance. Hence, an effort has been made to investigate the effect of process parameters on volume loss using Response Surface Methodology (RSM) based mathematical models. The experiments were planned as per Central Composite Design (CCD). The investigations revealed that the applied load was the most dominant factor affecting the volume loss of the coating. The sliding speed, sliding distance and interaction effects were considered as the next important parameters influencing the volume loss. The investigation also reveals that, the wear volume loss depends on two wear mechanisms, one being the formations of grooves along surface tribo films and other being fracture of splats with delamination of the coating.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 217-225
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of the central composite design to optimization of petroleum hydrocarbons removal from oilfield water using advanced oxidation process
Autorzy:
Farzadkia, M.
Ghorbanian, M.
Biglari, H.
Gholami, M.
Mehrizi, E. A.
Powiązania:
https://bibliotekanauki.pl/articles/204881.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
advanced oxidation processes
optimizing
total oil hydrocarbons
central composite design
Opis:
In the last few years, RSM method has been used widely to analyze, optimize and evaluate the interaction of independent factors for chemical, biochemical, and environmental processes. This study examined and evaluated the applicability of this method to manage Oilfield Produced Water to prevent marine environment due to the presence of hard degradable compounds by ozonation process. In this study simulated oil-water sample and a homogenizer reactor was used. The main reactor used in this study was impeinger equipped with sintered glass filter through which the treated oil-water was entered to reactor in the form of discontinuous flow. After ozonation and at the end of the reaction time (60 min), the concentration of oil hydrocarbons was determined by a gas chromatography device equipped with a flame ionization detector. The performance of the central composite design (CCD) approach was evaluated by the F-Value, P-Value, R2, lack of fit test and Adequate Precision parameters to determine the influence of effective factors, including ozonation time, pH, ozone dose, and TPH concentration on the TPH removal efficiency. The mean TPH efficiency obtained from the design of the 30-step experiment resulting from surface-response method was 49.903%, with a standard deviation of 12.47. This study showed the high power of model adopted from the central composite design to predict the hydrocarbons removal from oilfield water using advanced oxidation process, and it was proved that this model can be used alone to determine the design space nature.
Źródło:
Archives of Environmental Protection; 2018, 44, 4; 22-30
2083-4772
2083-4810
Pojawia się w:
Archives of Environmental Protection
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization and optimization of spectrophotometric colour removal from dye containing wastewater by Coagulation-Flocculation
Autorzy:
Obiora-Okafo, I. A.
Onukwuli, O. D.
Powiązania:
https://bibliotekanauki.pl/articles/779809.pdf
Data publikacji:
2018
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
coagulation-flocculation
natural organic polymer
fibre-metric analysis
spectrophotometer
face-centred central composite design
Opis:
The performance of Vigna unguiculata coagulant (VUC) for colour removal from acid dye was investigated in this study. The proximate, structure and morphology of the coagulant were investigated using standard official methods, Fourier-Transform Infrared (FTIR) spectrometer and scanning electron microscopy (SEM), respectively. Response surface methodology (RSM) using face-centred central composite design (FCCD) optimized four process variables including pH, coagulant dosage, dye concentration and time. The colour removal efficiency obtained from the optimization analysis was 99.26% at process conditions of pH 2, coagulant dosage 256.09 mg/l, dye concentration 16.7 mg/l and time 540 min. The verification experiments agreed with the predicted values having a standard error value of 1.96%. Overlay contour plot established optimum areas where the predicted response variable is in an acceptable range (≥ 70%) with respect to optimum conditions. The FCCD approach was appropriate for optimizing the process giving higher removal efficiency when compared to the main effect plots.
Źródło:
Polish Journal of Chemical Technology; 2018, 20, 4; 49-59
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Parametric optimization of coal desulfurization through Alkaline leaching
Autorzy:
Rehman, F.
Ahmad, S. W.
Zafar, M. S.
Ahmad, S.
Zia-Ul-Haq, M.
Powiązania:
https://bibliotekanauki.pl/articles/779964.pdf
Data publikacji:
2018
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
Desulfurization
Alkaline leaching
Response surface methodology
ANOVA
Central Composite design
Opis:
Desulfurization of Pakistani coal has been carried out through alkaline leaching. During present experimental investigation, the effect of operating parameters like alkali concentration, time, temperature and particle size has also been analyzed, graphically represented and critically discussed. Parametric optimization of leaching process has been carried out by using response surface methodology (RSM) based on central composite design (CCD). The analysis of variance (ANOVA) was performed in order to assess the highest level interactions of variables and three way interactions were observed significant. Further, the optimum value of total sulfur removal was observed as 53% when the operatic conditions fixed at 10% W/V, 60 min, 80°C and 140 mesh for alkaline concentration, leaching time, temperature and particle size, respectively.
Źródło:
Polish Journal of Chemical Technology; 2018, 20, 3; 103-109
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Adsorption of lead ions onto chemically activated carbon from waste tire char and optimization of the process using response surface methodology
Autorzy:
Rutto, Hilary
Seidigeng, Tumisang
Malise, Lucky
Powiązania:
https://bibliotekanauki.pl/articles/204781.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
waste tire pyrolysis char
chemical activation
central composite design
CCD
adsorption capacity
numerical optimization
Opis:
Tires play an important role in the automobile industry. However, their disposal when worn out has adverse effects on the environment. The main aim of this study was to prepare activated carbon from waste tire pyrolysis char by impregnating KOH onto pyrolytic char. Adsorption studies on lead onto chemically activated carbon were carried out using response surface methodology. The effect of process parameters such as temperature (°C), adsorbent dosage (g/100 ml), pH, contact time (minutes) and initial lead concentration (mg/l) on the adsorption capacity were investigated. It was found out that the adsorption capacity increased with an increase in adsorbent dosage, contact time, pH, and decreased with an increase in lead concentration and temperature. Optimization of the process variables was done using a numerical optimization method. Fourier Transform Infrared Spectra (FTIR) analysis, X-ray Diffraction (XRD), Thermogravimetric analysis (TGA) and scanning electron microscope were used to characterize the pyrolytic carbon char before and after activation. The numerical optimization analysis results showed that the maximum adsorption capacity of 93.176 mg/g was obtained at adsorbent dosage of 0.97 g/100 ml, pH 7, contact time of 115.27 min, initial metal concentration of 100 mg/and temperature of 25°C. FTIR and TGA analysis showed the presence of oxygen containing functional groups on the surface of the activated carbon produced and that the weight loss during the activation step was negligible.
Źródło:
Archives of Environmental Protection; 2019, 45, 4; 92-103
2083-4772
2083-4810
Pojawia się w:
Archives of Environmental Protection
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Novel Media for Lipid Production of Chlorococcum oleofaciens: A RSM Approach
Autorzy:
Pauline, J. Mercy Nisha
Achary, Anant
Powiązania:
https://bibliotekanauki.pl/articles/52074455.pdf
Data publikacji:
2019
Wydawca:
Uniwersytet Jagielloński. Wydawnictwo Uniwersytetu Jagiellońskiego
Tematy:
Biomass
Central composite design
Lipid
Medium optimization
Plackett Burman Design
AM medium
Opis:
The algal medium was optimized to increase the biomass and lipid production of Chlorococcum oleofaciens. The significant variables were screened and chosen from previously reported algal culture media using Plackett Burman Design (PBD). Optimization of the significant variables were performed using central composite design. The Pareto chart for PBD revealed that the salts such as sodium bicarbonate, sodium nitrate, potassium nitrate and ferrous sulphate had enhanced the biomass and lipid production. The variables and its effect on the responses were further studied by central composite design (CCD). A new medium was formulated based on the response surface methodology. The predicted concentration of NaHCO3, NaNO3, KNO3, MgSO4.7H2O were found to be 6.75 g/L, 0.75 g/L, 1.88 g/L and 0.35 g/L respectively. The actual and the predicted total lipid yield for the optimized media was around 0.74 g/L and 0.78 g/L respectively. The optimal medium has been named as AM medium. Growth and the lipid yields of C. oleofaciens were found higher in AM medium. The specific growth rates of C. oleofaciens in AM and CFTRI media were found to be 0.14 day-1 and 0.19 day-1 respectively. The biomass produced by the optimized AM medium was found to be 2.7 times greater compared to the CFTRI medium. The lipid was extracted and GC-MS was performed which revealed that the fatty acids were predominantly of the class C15:0, C18:0, C16:0 and C12:0. It is concluded that besides lipid content, AM medium increased the cell number leading to the increase in biomass.
Źródło:
Acta Protozoologica; 2019, 58, 1; 31-41
0065-1583
1689-0027
Pojawia się w:
Acta Protozoologica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Batch and Continuous Photo-Fenton Oxidation of Reactive-Red Dye from Wastewater
Autorzy:
Hassan, Ali A.
AlJaberi, Forat Yasir
Al-Khateeb, Raid T.
Powiązania:
https://bibliotekanauki.pl/articles/2025725.pdf
Data publikacji:
2021
Wydawca:
Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:
dye
wastewater treatment
advanced oxidation process
central composite design
optimization
Opis:
This paper aims to investigate the ability of photo-Fenton technology to remove Reactive Red dye (RR-dye) from wastewater using batch and continuous operating modes. The batch mode of photo-Fenton removal of organic content was conducted under the influence of solution pH (3–10), hydrogen peroxide (25–100 ppm), irradiation time (20–90 min), ferrous sulphate (5–20 ppm), and temperature (25–60 °C). For comparison, the continuous treatment was conducted under the influence of the flow rate of the contaminated solution (10, 20, 30, 40, and 50 mL/min). The results revealed that the treatability of the batch mode was more effective compared to the continuous mode. In the batch process, the organic contaminant was completely removed compared to that of 82% obtained when the continuous system was performed. The optimization process showed that the optimal values of the operating variables in the case of the batch removal of RR-dye were 3, 78 ppm, 90 min, 20 ppm, and 60 °C for pH, hydrogen peroxide, irradiation time, ferrous sulphate, and temperature, respectively. Moreover, the reversion F-value was 21.69, the probability P value was less than 0.001, and the correlation coefficient was (R2 = 0.9455), which illustrative the significance of the model obtained for the batch process.
Źródło:
Journal of Ecological Engineering; 2022, 23, 1; 14-23
2299-8993
Pojawia się w:
Journal of Ecological Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optimization of Acetaminophen and Methylparaben Removal within Subsurface Batch Constructed Wetland Systems
Autorzy:
Mutar, Zahraa Hasan
Mohammed, Ahmed A.
Al-Baldawi, Israa Abdulwahab
Powiązania:
https://bibliotekanauki.pl/articles/2025734.pdf
Data publikacji:
2021
Wydawca:
Polskie Towarzystwo Inżynierii Ekologicznej
Tematy:
phytoremediation
ornamental plant
constructed wetland
PPCPs
central composite design
Opis:
The response surface methodology accompanied by Central Composite Design (CCD) was employed in this study to optimize the Alternanthera spp-based phytoremediation process for the individual removal of acetaminophen and methylparaben. Two operational variables, including concentration (A) (20, 60,100 mg/L) and sampling time (B) (7, 14, 21, and 35 days) were involved in the study for removal efficiency (Y) as response. CCD had required a total of 18 experiments for each compound. Analysis of variance (ANOVA) was conducted to verify the adequacy of the proposed mathematical models and revealed good agreement with the experimental data. The observed R2 values (0.9732 and 0.9870), adjusted R2 (0.9620 and 0.9816) and predicted R2 (0.9383 and 0.9721) for AC and MP, respectively, indicated that the developed models were significant at the 95% probability level. Concentration factor was found to be insignificant in the mathematical models; in contrast, sampling time was found to be of a crucial role. The removal of AC and MP were 89.23% and 64.48% under optimum conditions of A = 100 mg/L and B = 35 days respectively. The validation test confirmed the predicted results obtained by Central Composite Design, as the removals achieved under optimum conditions were 91.04% and 59.17% for AC and MP, respectively, which were in good agreement with the results proposed by the theoretical design.
Źródło:
Journal of Ecological Engineering; 2022, 23, 1; 228-239
2299-8993
Pojawia się w:
Journal of Ecological Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Production of Spindle Palm Petiole Fiber Reinforced High Density Polyethyele Composites
Autorzy:
Nneka, Ejikeugwu L.
Monday, Omotioma
Nnaemeka, Omeje B.
Uzoma, Eke R.
Powiązania:
https://bibliotekanauki.pl/articles/1839868.pdf
Data publikacji:
2021
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Spindle palm petiole fiber
Sodium hydroxide
cellulose
chemical composition
Central Composite Design
Response Surface Methodology
tensile strength
polyethylene
Opis:
The work is on the production of spindle palm petiole fiber reinforced high density polyethylene (HDPE) composites. The Spindle Palm Petiole Fiber (SPPF) and HDPE composites were produced using injection molding machine. SPPF were characterized to determine their chemical compositions. Central Composite Design (CCD) was applied as an optimization tool of RSM for cellulose and tensile strength. The chemical composition of the SPPF is cellulose (65%), hemicelluloses (17.1%) and lignin (14.1%). Surface modifications of the fiber enhanced the properties of the fiber. Quadratic model adequately described the relationship between percentage cellulose yield and variables: chemical concentration, mass/volume ratio and time. The cellulose content at optimal level is 60.3% at 3.5wt% concentration, 4g/l mass/volume ratio and time of 16hr. Also for the composite, the quadratic model described the relationship between tensile strength and temperature, fiber/polymer ratio and time. The optimum tensile strength of 42.0 Mpa was obtained at fiber/polymer ratio of 29wt%, temperature of 172 °C and time of 10 min. Water absorbed by the untreated fiber was high compared to the chemically treated fiber. The chemical treatment created a better interfacial bonding of SPPF/HDPE and this could be responsible for the observations.
Źródło:
World News of Natural Sciences; 2021, 38; 98-119
2543-5426
Pojawia się w:
World News of Natural Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study on the Pore and Fibre metric Characteristics of Natural Organic Polymer for Colour Degradation in Wastewater: Face-Centred Central Composite Design
Autorzy:
Obiora-Okafo, Ifeoma Amaoge
Onukwuli, Okechukwu Dominic
Powiązania:
https://bibliotekanauki.pl/articles/1193490.pdf
Data publikacji:
2021
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Biebrich scarlet
Coagulation-flocculation
Face-centred central composite design
Natural organic polymer
Overlaid contour plot
Vigna subterranean
Opis:
The use of natural organic polymer (NOP) coagulants in the removal of pollutants from industrial wastewater has been the subject of continuous research. The importance of applying Vigna subterranean coagulant (VSC) for colour removal from crystal Ponceau 6R dye was investigated in this study. The precursor's proximate analysis, structure, surface morphology, fibre metric, and pore size distribution were examined. The pH, coagulant dosage, dye concentration, and time were optimized using response surface methodology (RSM) and face-centred central composite design (FCCD). For the coagulant precursor, the proximate analysis gave high protein content of 18.15 %, the Fourier Infra-Red (FTIR) analysis confirmed the existence of O-H, N-H, and C=H, the SEM image revealed polymer rough surfaces, the most occurring pore size of 0.41 μm2, different fibre length between 2.11 μm -17.94 μm, and a compact net structure. As can be seen in the main effects plots, pH has the greatest impact on colour removal, followed by time. Coagulant dosages and dye concentration have less influence on the process. The colour removal efficiency obtained from the optimization analysis was 99.60% at process conditions of pH 2.11, coagulant dosage 293.32 mg/L, dye concentration 13.75 mg/L and time 533.3 min. The projected values were confirmed in the verification experiments, with a standard error of 2.10 %. Overlay contour plot established optimum areas where the predicted response variable is in an acceptable range (≥ 80%) with respect to optimum conditions. When compared to the main effect plots, the FCCD approach proves more appropriate for improving the process and yielding higher removal efficiency. As a result, protein extract from Vigna subterranean seed has the potential to be used as an effective coagulant for colour removals from industrial wastewaters.
Źródło:
World Scientific News; 2021, 159; 20-44
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 18

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