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Wyszukujesz frazę "81.65.LP" wg kryterium: Temat


Tytuł:
Changing Properties of Metal Surface Layers during Thermo-Chemical Treatment
Autorzy:
Wróblewski, G.
Skalski, K.
Piekarski, R.
Powiązania:
https://bibliotekanauki.pl/articles/2011035.pdf
Data publikacji:
1999-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
81.65.Ya
Opis:
In this article a two-stage technology for constituting surface layers is proposed. First, the material is subjected to initial hardening by burnishing and next to a nitriding process. The surface layer after such processing should have considerably better strength properties compared to those created through a conventional nitriding process. A description of the state of the surface layer after these stages of the proposed process is obtained by defining suitable energy states for the materials. These states are expressed by residual strain and stress function and also by the functions of external work during the burnishing process and thermal energy given in the nitriding process. Methods of identifying the above functions through experimental research on the residual stress state and selected parameters of the surface layer, and also through numerical analysis of the coupled processes, are also proposed. The main part of the work consists in the mathematical description of complex deformation phenomena occurring in the material during the proposed process. In the given description, coupled stress fields appear as a result of the additivity of elastic, plastic, thermal, diffusional, and phase strains.
Źródło:
Acta Physica Polonica A; 1999, 96, 2; 311-317
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure Development in Multilayer $TiB_x // TiSi_y C_z$ Coatings during Post-Deposition Heat Treatment
Autorzy:
Twardowska, A.
Rajchel, B.
Morgiel, J.
Mędala-Wójcik, M.
Powiązania:
https://bibliotekanauki.pl/articles/1398372.pdf
Data publikacji:
2016-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.15.Cd
81.20.-n
42.62.-b
61.43.Dq
68.37.-d
68.37.Lp
68.65.Ac
64.70.Kb
Opis:
Multilayer amorphous $TiB_{x} // TiSi_{y}C_{z}$ coatings were formed by duplex treatment: dual beam ion beam assisted deposition and pulsed laser deposition. Post-deposition heating was applied to activate crystallization in the coating. In situ transmission electron microscopy heating experiments were conducted in the temperature range 20-600°C. Crystallization of TiB₂ phase in $TiB_{x}$ layers begun at 450°C, while $TiSi_{y}C_{z}$ layers retained nearly amorphous up to 600°C.
Źródło:
Acta Physica Polonica A; 2016, 130, 4; 1124-1126
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The law of growth of nitrided layer in 31CrMoV9 steel
Autorzy:
Syla, N.
Aliaj, F.
Dalipi, B.
Powiązania:
https://bibliotekanauki.pl/articles/1068250.pdf
Data publikacji:
2016-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
81.65.Lp
Opis:
The law of growth of nitrided layers produced by gaseous nitriding of 31CrMoV9 alloy steel at different process parameters is described. 31CrMoV9 steel specimens were subjected to nitriding process in ammonia gas at three different temperatures: 510, 550 and 590°C, and for each temperature four different nitriding times were used. This way twelve specimens were produced. Nitrided specimens were investigated with optical microscopy, electron probe micro-analysis and x-ray diffraction. The nitrogen depth concentration profiles, deduced from electron probe micro-analysis, in conjunction with results of optical microscopy, were used to determine the thickness of the nitrided layers, i.e. the diffusion depth of nitrogen. From the dependence of the nitrided layer thickness on process parameters (temperature and time) it was possible to deduce the law that governs the growth of the nitrided layer for 31CrMoV9 alloy steel. Through this law, then, it is possible to predetermine the layer thickness for every real process parameter in nitriding of 31CrMoV9 steel, which is very important for technological applications.
Źródło:
Acta Physica Polonica A; 2016, 130, 1; 83-86
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of the Silanization Processes on the Properties οf Oxidized Multiwalled Carbon Nanotubes
Autorzy:
Scheibe, B.
Borowiak-Palen, E.
Kalenczuk, R.
Powiązania:
https://bibliotekanauki.pl/articles/1807640.pdf
Data publikacji:
2009-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Mq
81.07.De
61.48.De
65.80.-g
68.37.Lp
Opis:
This paper presents the results of the research on the effect of the two different silanization methods on the thermal and structural properties of oxidized multiwalled carbon nanotubes. As-purified material was oxidized in the mixture of nitric and sulfuric acids. An oxidized material was divided into two parts which underwent two silanization treatments by 3-aminopropyltriethoxysilane (APTES). The first experiment (I) was performed at room temperature in acetone (pH 7) for 30 min. The second experiment (II) involved a hydrolysis of APTES at 40°C in water (pH 4) for 3 h. The functionalization extent of the samples at each step of the preparation was investigated by the Raman spectroscopy. The presence of the functional groups on the nanotubes surface have been studied via the Fourier transform infrared spectroscopy (FT-IR). The quantity of the external moieties introduced on multiwalled carbon nanotubes surface after oxidation process was estimated by the Boehms titration method. The high resolution transmission electron microscopy analysis allowed us to observe the changes of the morphology of the investigated carbon nanotubes. The influence of the silanization processes on the thermal stability of multiwalled carbon nanotubes was thoroughly studied by thermogravimetry analysis. There was observed a significant increase of the thermal stability of the multiwalled carbon nanotubes samples upon silanization treatment in respect of pristine and oxidized multiwalled carbon nanotubes.
Źródło:
Acta Physica Polonica A; 2009, 116, S; S-150-S-155
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment and Pulse Plasma Process on Surface Properties of Steels
Autorzy:
Özbek, Y.
Powiązania:
https://bibliotekanauki.pl/articles/1032518.pdf
Data publikacji:
2017-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
Opis:
The aim of this study was to examine the effect of heat treatment and pulse plasma treatment on surface properties of AISI 1050 steel used in this work. Firstly, the heat treatment was applied to samples for 2 h at 860°C. The quenching media were selected as water and oil and air cooling was applied. The tempering process was applied at different temperatures like 600°C, 500°C, 400°C and 100°C. Having completed the heat treatment, the pulse plasma process was applied to all samples. The surfaces were investigated with optic microscope, scanning electron microscopy, and X-ray diffraction analyses. The hardness testing was done for all samples from surface to center. The mechanical properties were improved after pulse plasma treatment.
Źródło:
Acta Physica Polonica A; 2017, 131, 1; 182-185
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Influence of the Au Nanoparticles Dimension on the Photocatalytic Performances of $TiO_2-Au$ Porous Composites
Autorzy:
Melinte, G.
Baia, M.
Georgescu, D.
Baia, L.
Iancu, V.
Diamandescu, L.
Popescu, T.
Cotet, L.
Barbu-Tudoran, L.
Danciu, V.
Simon, S.
Powiązania:
https://bibliotekanauki.pl/articles/1491327.pdf
Data publikacji:
2012-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Rm
81.07.Wx
82.80.Ej
68.37.Lp
82.65.+r
82.50.Hp
Opis:
The influence of Au nanoparticles dimension on the photocatalytic performances of the $TiO_2$ aerogels-Au composites was evaluated. Structural and morphological peculiarities of the $TiO_2$ aerogel, unloaded and loaded with 5 and 22 nm Au nanoparticles, were studied by transmission electron microscopy technique, X-ray diffraction and $N_2$-sorption measurements. UV-Vis diffuse reflectance measurements were performed to determine the band gap energies. The photocatalytic activity was evaluated by monitoring the salicylic acid photodegradation. It was found that the Au nanoparticles promote the anatase phase crystallization and produce the decrease of the specific surface area and band gap energy values. The porous composite with the smallest Au nanoparticles dimension exhibits the best photocatalytic performances.
Źródło:
Acta Physica Polonica A; 2012, 121, 1; 208-210
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Characterization of Boro-Titanized AISI 1040 Steel
Autorzy:
Kon, O.
Pazarlıoğlu, S.
Durmaz, M.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1401328.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
62.20.Qp
Opis:
In this study, boro-titanizing treatment was applied to AISI 1040 steel. In the coating treatment, steel samples were pre-boronized in a slurry salt bath consisting of borax, boric acid and ferro-silicon at 900°C for 2 h, then titanized by thermo-reactive deposition technique (TRD) in a powder mixture consisting of ferro-titanium, ammonium chloride, alumina and naphthalene at 1000°C for 1-4 h. The coated samples were characterized by X-ray diffraction analysis (XRD), scanning electron microscope (SEM), glow discharge optical emission spectroscopy (GDOES) and micro-hardness tests. Coated layer formed on the pre-boronized AISI 1040 steel was compact and homogeneous. X-ray studies showed that the phases formed on the steel surfaces are TiB₂, TiC, TiN and Fe₂B. The depth of the coating layer ranged from 3.41± 0.47 μm to 6.59± 0.51 μm, depending on treatment time. A higher treatment time resulted in a thicker boro-titanized layer. The average hardness of the coating layer was 4527± 284 $HV_{0.005}$.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1211-1213
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of Fe-Nb-B Base Hardfacing of Steel
Autorzy:
Kilinc, B.
Cegil, O.
Abakay, E.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1311693.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Kn
68.55.J-
81.65.Lp
Opis:
Recently hardfacing by welding has become a commonly used technique for improvement of material performance in extreme (high temperature, impact/abrasion, erosion, etc.) conditions. In the present study, three different alloy compositions of the Fe-Nb-B were used for hardfacing of the AISI 1020 steel by tungsten inert gas welding process and analyzed. The coatings were produced from a mixture of ferrous niobium, ferrous boron and iron powders in the range of - 45 μm particle size with different ratio. The coatings' thickness was set to 2-3 mm on the substrate. Microstructure, phase analysis and hardness of the manufactured hardfacing alloys were characterized. Deposition results indicate good quality thick coating and porosity free of the hardfacings. X-ray diffraction analyses showed that the alloyed layers include iron borides, FeNbB and iron phases. It was shown that surface alloyed layer has composite structure including steel matrix and well distributed boride phases.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 656-658
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Corrosion Behavior of Nitride and Cr-Al-N Coatings Formed on AISI D2 Steel
Autorzy:
Kılınc, B.
Demirkiran, S.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1399749.pdf
Data publikacji:
2013-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Kn
68.55.J-
81.65.Lp
Opis:
In the present work, the corrosion behavior of Cr-Al-N coating formed on the pre-nitrided AISI D2 cold work tool steel by thermo-reactive diffusion technique in the powder mixture consisting of ferro-chromium, aluminum, ammonium chloride and alumina at 1000C for 2 h was investigated. The phases formed in the coating layers were $Cr_2N$, $(Cr,Fe)_2N_{1-x}$, $AlN$, and $Fe_2N$ which were confirmed by X-ray diffraction analysis. The uncoated, nitrided, and Cr-Al-N coated specimens were placed in corrosive media (3.5 wt% salt solution). A standard saturated calomel electrode was used as a reference and graphite as a counter or auxiliary electrode. The effectiveness of the coatings in preventing corrosion was tested in the NaCl solution by electrochemical impedance studies using the Nyquist plots and potentiodynamic studies as well. Conclusively, the application of nitride and Cr-Al-N layers on AISI D2 steel increased its surface hardness and corrosion resistance. The corrosion resistance of Cr-Al-N coatings is higher than that of uncoated and nitrided steels.
Źródło:
Acta Physica Polonica A; 2013, 123, 2; 268-270
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Properties of Cr-Al-N Based Coatings Formed on AISI D2 Steel by Thermo-Reactive Diffusion Technique
Autorzy:
Kılınc, B.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1399772.pdf
Data publikacji:
2013-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.15.-z
62.20.Qp
68.55.J-
81.65.Lp
Opis:
In this study, chromium aluminum nitride coating was applied on pre-nitrided AISI D2 steel by the thermo-reactive deposition technique in a powder mixture consisting of ferrochromium, aluminum, ammonium chloride, and alumina at 1000C for 2 h. Steels were gas nitrided for the purpose to enrich the surfaces with nitrogen of the steels in a nitrogen and ammonia atmosphere at 560C for 8 h. The effect of aluminum content in the powder mixture on the Cr-Al-N layer properties was investigated. The coated samples were characterized by X-ray diffraction analysis, scanning electron microscope, and micro-hardness tests. Chromium aluminum nitride layer formed on the pre-nitrided AISI D2 steel was compact and homogeneous. Electron dispersive spectrometer results showed that coating layer includes chromium, aluminum, and nitrogen. X-ray studies showed that the phases formed in the coating layers on the steel surfaces are $Cr_2N$, $(Cr,Fe)_2N_{1-x}$, $AlN$, and $Fe_2N$. The depth of the Cr-Al-N layer ranged from 10.01 ± 1.2 to 13.2 ± 1.7 μm, depending on the aluminum content. The hardness of the coated layers produced on AISI D2 steel are changing from 1743 ± 150 $HV_{0.01}$ to 2067 ± 160 $HV_{0.01}$ depending on bath compositions.
Źródło:
Acta Physica Polonica A; 2013, 123, 2; 271-273
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wear Behavior of TiAlN and CrAlN Coatings Deposited by TRD Process on AISI D2 Steel
Autorzy:
Kılınc, B.
Cegil, O.
Sen, S.
Sen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1219208.pdf
Data publikacji:
2014-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.15.-z
46.55.+d
81.65.Lp
Opis:
The wear properties of uncoated, chromium aluminum nitride (CrAlN) and titanium aluminum nitride (TiAlN) coated AISI D2 steel were investigated and compared using ball-on-disc method at 0.3 m/s sliding speed and under the loads of 2.5 N, 5 N, and 10 N against $Si_3N_4$ ball as a counter material. Steel samples were nitrided at 575C for 8 h in the first step of the coating process, and then titanium aluminum nitride coating and chromium aluminum nitride were performed by thermoreactive deposition (TRD) process at 1000C for 2 h. Coated samples were characterized by X-ray diffraction analysis, scanning electron microscopy, microhardness, and ball on disk wear tests. The results of friction coefficient and wear rate of the tested materials showed that the TiAlN coating presents the lowest results.
Źródło:
Acta Physica Polonica A; 2014, 125, 2; 362-364
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Detection of Shallow Dislocations on 4H-SiC Substrate by Etching Method
Autorzy:
Ishikawa, Y.
Yao, Y.
Sato, K.
Sugawara, Y.
Danno, K.
Suzuki, H.
Bessho, T.
Kawai, Y.
Shibata, N.
Powiązania:
https://bibliotekanauki.pl/articles/1492539.pdf
Data publikacji:
2011-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.72.uj
81.65.Cf
68.37.Lp
Opis:
Correlation between dislocation types in epitaxial 4H-SiC and etch pit types on the 4H-SiC wafer surface were investigated by etch pit method and transmission electron microscope. Shallow dislocation on the wafer was found to form round pit without core. The shallow dislocation was estimated half-loop type in wafer and this estimation explains that step-flow growth converts half-loop dislocation into complex dislocation composed by threading dislocation and basal plane dislocation.
Źródło:
Acta Physica Polonica A; 2011, 120, 6A; A-025-A-027
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Properties of Co and CoFe Electrodes Forming a Magnetic Tunnel Junction
Autorzy:
Gładczuk, L.
Pankowski, P.
Paszkowicz, W.
Dłużewski, P.
Wójcik, M.
Przysłupski, P.
Powiązania:
https://bibliotekanauki.pl/articles/2047237.pdf
Data publikacji:
2007-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.15.Hi
68.65.Ac
61.10.Nz
76.60.Lz
68.37.Lp
Opis:
The M$\text{}_{1}$/MgO/M$\text{}_{2}$ trilayer tunnel magnetoresistance systems are studied by means of X-ray diffraction, NMR, and transmission electron microscopy techniques. As M$\text{}_{1}$ and M$\text{}_{2}$ electrodes we used Co, Fe, and CoFe layers. The growth mechanism and structural quality of both electrodes and of the epitaxial MgO barrier forming the magnetic tunnel junctions are experimentally examined. It is shown that the crystallographic coherence of magnetic tunnel junctions across the MgO barrier is significantly disturbed by imperfect crystal structure of magnetic electrodes. The NMR results indicate a difference in short-range order between bottom and top electrodes.
Źródło:
Acta Physica Polonica A; 2007, 111, 1; 135-140
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology and Selected Properties of Core/Shell ZnTe-Based Nanowire Structures Containing ZnO
Autorzy:
Gas, K.
Janik, E.
Zaleszczyk, W.
Pasternak, I.
Dynowska, E.
Fronc, K.
Kolkovsky, V.
Kret, S.
Morhange, J. F.
Reszka, A.
Wiater, M.
Caliebe, W.
Karczewski, G.
Kowalski, B. J.
Szuszkiewicz, W.
Wojtowicz, T.
Powiązania:
https://bibliotekanauki.pl/articles/2047950.pdf
Data publikacji:
2011-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
68.37.Hk
68.37.Lp
68.65.La
81.07.Vb
Opis:
We report on an approach to fabricate ZnTe-based core/shell radial heterostructures containing ZnO, as well as on some of their physical properties. The molecular beam epitaxy grown ZnTe nanowires constituted the core of the investigated structures and the ZnO shells were obtained by thermal oxidation of ZnTe NWs. The influence of the parameters characterizing the oxidation process on selected properties of core/shell NWs were examined. Scanning electron microscopy revealed changes of the NWs morphology for various conditions of the oxidation process. X-ray diffraction, high resolution transmission electron microscopy, and Raman scattering measurements were applied to reveal the presence of ZnTe single crystal core and polycrystalline ZnO-shell of investigated structure.
Źródło:
Acta Physica Polonica A; 2011, 119, 5; 612-614
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Cathodic Electrolytic Plasma Hardening of Steel and Cast Iron Based Automotive Camshafts
Autorzy:
Dayanç, A.
Karaca, B.
Kumruoğlu, L.
Powiązania:
https://bibliotekanauki.pl/articles/1030309.pdf
Data publikacji:
2017-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
82.45.Hk
81.40.Pq
Opis:
Cathodic electrolytic plasma hardening is a novel thermochemical surface modification and hardening process, used to increase wear resistance and surface hardness of metallic components in a local area of interest. The heating efficiency is related with the plasma nozzle design, applied current and electrolyte. The nozzle design is also a critical factor for the hardening of complex shapes, such as gears and camshafts. In this work, lobes of camshafts, fabricated from several cast iron and steel grades were hardened by cathodic electrolytic plasma hardening in aqueous carbonate electrolyte, using a specific plasma nozzle. The camshafts were attached to CNC lathe for turning them in the horizontal axis. In order to optimise heating and to achieve the ideal flowing and wetting by the electrolyte of the lobe case, the ceramic ellipse-shaped nozzle outlet was designed. As a result of preliminary studies, external surface of lobes was heated and subsequently quenched by electrolyte. The hardness of processed surface was in the range of 50-60 HRc for the different camshafts. No distortion was observed on the surface of lobes. Hardness depth was measured to be from 0.1 mm to 5 mm for several lobes.
Źródło:
Acta Physica Polonica A; 2017, 131, 3; 374-378
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł

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