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Tytuł:
Effects of Third-generation LED LCU on Nanomechanical Properties of Orthodontic Adhesives
Autorzy:
Bilgic, F.
Altan, H.
Akinci Sözer, Ö.
Arslanoglu, Z.
Kale, E.
Özarslan, S.
Powiązania:
https://bibliotekanauki.pl/articles/1031919.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.-x
62.20.Qp
Opis:
The aim of this study was to compare the hardness and elastic modulus of orthodontic adhesives cured with different light-curing units, based on light-emitting diodes. Standardized samples of orthodontic adhesives, Transbond™ XT, Opal® Bond™ and Light Bond™ were prepared in cylinder blocks and cured for three seconds with Valo Ortho LED (Ultradent Products, South Jordan, Utah) and Valo LED High-Power Mode. After grinding and polishing, specimens were stored in distilled water at 37°C for one day. Specimens were investigated using nanoindenter. Employment of Valo Ortho unit has resulted in significantly higher elastic modules for Transbond™ XT (p=0.041). The highest nanohardness and elastic modules were measured for Transbond™ XT cured with Valo Ortho (9.47 GPa; 81.85 GPa, respectively) and lowest for Opal® Bond™ for both Valo Ortho (0.44 GPa; 14.52 GPa, respectively) and Valo High-Power groups (0.44 GPa; 11.84 GPa, respectively).
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 697-701
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nanomechanical properties of different dental restorative materials
Autorzy:
Altan, H.
Bilgic, F.
Arslanoglu, Z.
Kale, E.
Köroğlu Kale, A.
Altan, A.
Sahin, O.
Powiązania:
https://bibliotekanauki.pl/articles/1068227.pdf
Data publikacji:
2016-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.-x
62.20.Qp
Opis:
The aim of this study is to determine the hardness and roughness of glass ionomer cement, glass carbomer, and compomer by nanoindentation. Three different dental restorative materials: glass ionomer cement, glass carbomer cement, and compomer were used. Disc specimens (10 mm × 1 mm) were prepared from each material using teflon mold. All specimens were light cured according to the manufacturer's instructions. The specimens were then mounted in polyacrilic resin. After grinding and polishing the specimens were stored in distilled water at 37°C for 1 day. The specimens were investigated using nanoindenter. The highest nanohardness was measured for glass ionomer cement and the lowest for glass carbomer. Regarding roughness, glass ionomer cement and compomer showed the highest mean values. Glass ionomer cement and compomer exhibited similar nanomechanical properties. Glass carbomer had superior ability to be polished up.
Źródło:
Acta Physica Polonica A; 2016, 130, 1; 394-396
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effects of Austempering and Induction Hardening on the Wear Properties of Camshaft Made of Ductile Cast Iron
Autorzy:
Karaca, B.
Şimşir, M.
Powiązania:
https://bibliotekanauki.pl/articles/1032072.pdf
Data publikacji:
2017-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
46.55.+d
62.20.Qp
Opis:
The aim of this study is to investigate the effects of heat austempering and induction hardening on the wear properties of GGG60 ductile cast iron for camshaft production. For this purpose, camshafts have been produced by sand mould casting method. Fe-Si-Mg alloy has been used for inoculation process to achieve iron nodulization. The casting has been done between 1410-1420°C. The casted camshafts have been austenitized at two different temperatures (800 and 900°C) and time intervals (60 and 90 min) under controlled furnace atmosphere. The austenitized camshafts have been quenched into the molten salt bath at 360°C, held there for 90 min and then cooled in air. This way, austempering heat treatment has been applied. After that, surface hardening process was conducted using induction hardening machine with medium frequency. Microstructure of camshafts has been examined by optical methods and mechanical tests have been performed. Results show that austempering heat treatment increases the wear resistance of camshaft, compared to as-cast condition. Wear resistance of the camshaft increases with increasing austenitizing temperature, time and with induction hardening. The lowest weight loss of 0.62 mg has been obtained for the induction hardened camshaft austenitized at 900°C for 90 min.
Źródło:
Acta Physica Polonica A; 2017, 131, 3; 448-452
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Physicomechanical Properties of Nanostructured (TiHfZrNbVTa)N Coatings after Implantation of High Fluences of N⁺ (10¹⁸ cm¯²)
Autorzy:
Pogrebnjak, A.
Bondar, O.
Borba, S.
Piotrowska, K.
Boiko, O.
Powiązania:
https://bibliotekanauki.pl/articles/1030134.pdf
Data publikacji:
2017-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
Opis:
New classes of high-entropy alloys, which consist of at least 5 main elements with atomic concentrations 5-35 at.%, are under great interest in modern material science. It is also very important to explore the limits of resistance of high-entropy alloy nitrides to implantation by high-energy atoms. Structure and properties of nanostructured multicomponent (TiHfZrNbVTa)N coatings were investigated before and after ion implantation. We used the Rutherford backscattering, scanning electron microscopy with energy dispersive X-ray spectroscopy, high resolution transmission electron microscopy and scanning transmission electron microscopy with local microanalysis, X-ray diffraction and nanoindentation for investigations. Due to the high-fluence ion implantation (N⁺, the fluence was 10¹⁸ cm¯²) a multiphase structure was formed in the surface layer of the coating. This structure consisted of amorphous, nanocrystalline and initial nanostructured phases with small sizes of nanograins. Two phases were formed in the depth of the coating: fcc and hcp (with a small volume fraction). Nitrogen concentration reached 90 at.% near the surface and decreased with the depth. Nanohardness of the as-deposited coatings varied from 27 to 34 GPa depending on the deposition conditions. However, hardness decreased to a value of 12 GPa of the depth of the projected range after ion implantation and increased to 23 GPa for deeper layers.
Źródło:
Acta Physica Polonica A; 2017, 132, 2; 217-221
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Characterization of Boro-Titanized AISI 1040 Steel
Autorzy:
Kon, O.
Pazarlıoğlu, S.
Durmaz, M.
Sen, U.
Sen, S.
Powiązania:
https://bibliotekanauki.pl/articles/1401328.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.65.Lp
62.20.Qp
Opis:
In this study, boro-titanizing treatment was applied to AISI 1040 steel. In the coating treatment, steel samples were pre-boronized in a slurry salt bath consisting of borax, boric acid and ferro-silicon at 900°C for 2 h, then titanized by thermo-reactive deposition technique (TRD) in a powder mixture consisting of ferro-titanium, ammonium chloride, alumina and naphthalene at 1000°C for 1-4 h. The coated samples were characterized by X-ray diffraction analysis (XRD), scanning electron microscope (SEM), glow discharge optical emission spectroscopy (GDOES) and micro-hardness tests. Coated layer formed on the pre-boronized AISI 1040 steel was compact and homogeneous. X-ray studies showed that the phases formed on the steel surfaces are TiB₂, TiC, TiN and Fe₂B. The depth of the coating layer ranged from 3.41± 0.47 μm to 6.59± 0.51 μm, depending on treatment time. A higher treatment time resulted in a thicker boro-titanized layer. The average hardness of the coating layer was 4527± 284 $HV_{0.005}$.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1211-1213
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Research of Superhard (Zr-Ti-Cr-Nb)N Coatings
Autorzy:
Bondar, O.
Postolnyi, B.
Kravchenko, Yu.
Shypylenko, A.
Sobol, O.
Beresnev, V.
Kuzmenko, A.
Zukowski, P.
Powiązania:
https://bibliotekanauki.pl/articles/1402215.pdf
Data publikacji:
2015-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
Opis:
This work presents the results of (Zr-Ti-Cr-Nb)N superhard coatings research. The samples were fabricated by the vacuum-arc deposition method (Arc-PVD). Structure, composition and properties of these coatings were studied. The study of coatings was carried out using scanning electron microscopy, energy dispersive spectroscopy, and X-ray diffraction. Hardness measurements and adhesion tests were performed. The coatings thickness was up to 6.2 μ m, nanocrystallites sizes ranged from 4 to 7.3 nm. Values of hardness and cohesive strength were H=43.7 GPa and $L_{C}$=62.06 N, respectively. The optimal conditions for coating deposition were found.
Źródło:
Acta Physica Polonica A; 2015, 128, 5; 867-870
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Properties of Fe-Ni-Al-Si Alloys Produced by Powder Metallurgy
Autorzy:
Novák, P.
Mejzlíková, L.
Hošek, V.
Martínek, M.
Marek, I.
Michalcová, A.
Powiązania:
https://bibliotekanauki.pl/articles/1418514.pdf
Data publikacji:
2012-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Dk
62.20.Qp
Opis:
Reactive sintering powder metallurgy is a simple alternative to conventional melting and powder metallurgy processes. During this process, pressed powder mixture of pure metals or other precursors is transformed into bulk intermediary phases by thermally activated in situ reaction. This process was previously tested on Fe-Al and Fe-Al-Si alloys. Positive effect of silicon on the reactive sintering behaviour was determined, leading to the development of novel carbon-free high-silicon FeAl20Si20 alloy (given in wt%). In this work, the effect of nickel on the pressureless reactive sintering of Fe-Al-Si pressed powder mixtures was studied. To explain the nickel influence, differential thermal analysis was utilized. Microstructure, phase composition and porosity of the FeAl20Si20Nix (x = 0, 5, 10, 20 wt%) alloys was described. Hardness, wear resistance, high-temperature oxidation resistance and thermal stability were evaluated as functions of nickel content. Results showed that porosity decreases with growing nickel content down to less than 3 vol.%. Oxidation rate of these alloys is more than 10 times lower than that of original FeAl20Si20 alloy. Thermal stability and abrasive wear resistance of these alloys is also superior to Fe-Al and Fe-Al-Si materials.
Źródło:
Acta Physica Polonica A; 2012, 122, 3; 524-527
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nanomechanical comparison of commonly used dental crown cements to a newly developed one
Autorzy:
Kale, E.
Arslanoğlu, Z.
Altan, H.
Bılgıç, F.
Tuzlali, M.
Köroğlu, A.
Özarslan, S.
Powiązania:
https://bibliotekanauki.pl/articles/1054940.pdf
Data publikacji:
2017-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.-x
62.20.Qp
62.20.de
Opis:
The main goal of nanoindentation tests is to obtain elastic modulus and hardness of the specimen material from load-displacement measurements. With this study, it was aimed to establish a quantitative relationship between the nanomechanical properties of commonly used dental cements in comparison to a newly developed crown cement and to predict its performance potential. Nanomechanical properties of polycarboxylate cement (PCC), glass-ionomer cement (GIC), dual-cure self-adhesive cement (SAC) and a newly developed glass-carbomer cement (GCC) were investigated by nanoindentation tests. All samples were fabricated according to their respective manufacturer's instructions. Available damage on the surface due to manipulation was removed by grinding with 1200, 2400 and 4000 grit sandpaper, and then polishing on 6, 3, and 1 μm diamond-lap-wheel was performed. Nano-mechanical measurements were done using nanoindenter machine with resolution less than 1 nN and displacement resolution of 0.04 nm. Berkovich diamond indenter tip was used for the nanoindentation tests. For each indentation, a set of nanoindentation tests at least on 6 different locations per specimen surface were performed to obtain more representative mean results. Indentation test load-displacement curves were analysed using Oliver-Pharr method, and one-way ANOVA or Kruskal-Wallis test, following Kolmogorov-Smirnov and Shapiro-Wilk, was used to compare the results. Nanohardness (H_{nano}) values were 0.52± 0.25, 0.45± 0.18, 1.03± 0.82 and 0.43± 0.18 GPa for GIC, GCC, PCC, and SAC, respectively. Reduced elastic modulus (E_{r}) values were 9.51± 6.17, 11.77± 5.04, 27.37± 20.61, 10.33± 5.08 GPa for GIC, GCC, PCC, and SAC, respectively. There was no statistical difference between the tested materials. PCC was the hardest, and GIC was the least hard material, whereas the newly developed GCC was the second, in terms of H_{nano}, before SAC. PCC also had the highest E_{r} mean, compared to the other dental crown cements, suggesting lower elastic properties. SAC was more elastic than GCC and less elastic than GIC. GCC had the second highest E_{r}, standing closer to SAC and GIC. Within the limitations of the current study, it can be concluded that the newly developed glass-carbomer cement is comparable to the other tested commonly used dental crown cements, regarding H_{nano} and E_{r}.
Źródło:
Acta Physica Polonica A; 2017, 132, 3; 954-958
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of rare earth element on the mechanical properties of ZE41 magnesium alloys produced by mechanical alloying
Autorzy:
Sahin, O.
Haluk Ertsak, F.
Oztekin, K.
Ozarslan, S.
Powiązania:
https://bibliotekanauki.pl/articles/1065306.pdf
Data publikacji:
2016-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.-x
62.20.Fe
62.20.Qp
Opis:
In this work, we have intended to synthesize ZE41 Magnesium alloys having varying content of Ce of 0.3, 0.6 and 0.9 wt.% and to investigate mechanical properties of these alloys. Alloys were produced by mechanical alloying under argon atmosphere. Structural, and mechanical properties of these alloys were investigated by means of XRD, SEM and nanoindenter analysis. From the XRD data it is found that as the Ce content increases, the crystallite size also increases. On the other hand, the hardness of the alloys decreases with the increasing Ce content. Indentation results show that the measured hardness displays a peak load dependence. Load-independent hardness was calculated by Hays-Kendall approach. As a results, it was found that Ce-doping modifies the microstructure and hardness of the alloy.
Źródło:
Acta Physica Polonica A; 2016, 130, 1; 289-292
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Vickers and Knoop Indentation Microhardness Study of β-SiAlON Ceramic
Autorzy:
Güder, H.
Şahin, E.
Şahin, O.
Göçmez, H.
Duran, C.
Ali Çetinkara, H.
Powiązania:
https://bibliotekanauki.pl/articles/1492772.pdf
Data publikacji:
2011-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.-x
62.20.Qp
62.20.de
Opis:
In this paper, analysis and interpretation of mechanical property measurements of β-SiAlON ceramic were reported. Indentation microhardness of β-SiAlON ceramic was measured using the Knoop and Vickers indenters. The analysis of the Vickers indentation microhardness data reveals the reverse indentation size effect that is the apparent microhardness increases with increasing applied indentation test load. However, the Knoop indentation microhardness data exhibit indentation size effect that is the apparent microhardness increases with decreasing applied test load. The experimental Knoop microhardness data was analyzed using Meyer's law, elastic-plastic deformation model, proportional specimen resistance model, and Hays-Kendall's model. As a result, modified proportional specimen resistance model is found to be the most effective one for the load-independent $(H_{LI})$ microhardness determination of the SiAlON ceramic. It was seen that different models used to analyze the data obtained from the Vickers indentation do not give the same intrinsic hardness value. We also present the calculation of the Young modulus, E, of the β-SiAlON ceramic.
Źródło:
Acta Physica Polonica A; 2011, 120, 6; 1026-1033
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microhardness and the Young Modulus of Thin, MBE-Grown, (Sn,Mn)Te Layers Containing up to 8% of Mn
Autorzy:
Adamiak, S.
Zięba, M.
Minikayev, R.
Reszka, A.
Taliashvili, B.
Szuszkiewicz, W.
Powiązania:
https://bibliotekanauki.pl/articles/1033220.pdf
Data publikacji:
2017-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.de
62.20.Qp
68.60.Bs
Opis:
The thin layers of (Sn,Mn)Te solid solution were grown by molecular beam epitaxy onto (111)-oriented BaF₂ substrates and characterized by scanning electron microscopy, atomic force microscopy, energy dispersive X-ray spectrometry, and X-ray diffraction methods. The epitaxial character of the growth was confirmed. All the layers exhibited a regular (fcc) structure of the rock-salt type and were (111)-oriented, their thickness was close to about 1 μm. The layers contained up to 8% of Mn. The microhardness and the Young modulus values were determined by the nanoindentation measurements. The Berkovich type of the intender was applied, the maximum applied load was equal to 1 mN. The results of measurements demonstrated a lack of the composition dependence of the Young modulus value. A slight increase of the microhardness value with an increasing Mn content in the (Sn,Mn)Te solid solution was observed.
Źródło:
Acta Physica Polonica A; 2017, 132, 2; 347-350
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Powder Metallurgy Preparation of Co-Based Alloys for Biomedical Applications
Autorzy:
Marek, I.
Novák, P.
Mlynár, J.
Vojtěch, D.
Kubatík, T.
Málek, J.
Powiązania:
https://bibliotekanauki.pl/articles/1402090.pdf
Data publikacji:
2015-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.Qp
62.20.F-
64.70.kd
Opis:
Co-based alloys represent very important group of materials used for medical applications. Currently, fabrication of these materials is preferentially done by casting or forming. Production by powder metallurgy techniques is less common. However, powder metallurgy fabrication of these alloys brings advantages such as reduced machining, possibility of alloying by high-melting elements, preparation of nanocrystalline materials with enhanced mechanical properties or producing of porous alloys with improved ability to integrate into issues. In this work, our attention was focused on fundamental preparation of an CoCrMo alloy by two methods of powder metallurgy. In the first method, pure metallic powders were mixed, pressed and sintered in vacuum furnace. The second applied technology consisted of mechanical alloying using planetary ball mill and compaction by spark plasma sintering technique. A series of samples was prepared under various conditions by these procedures. Dependence of microstructure, phase composition and mechanical properties of prepared samples on fabrication conditions (milling parameters, sintering temperature etc.) was studied. Obtained results were compared with properties of commercial cast cobalt alloy used for medical applications.
Źródło:
Acta Physica Polonica A; 2015, 128, 4; 597-601
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Properties of Multilayer Nanostructured Coatings TiN/MoN Depending on Deposition Conditions
Autorzy:
Pogrebnjak, A.
Abadias, G.
Bondar, O.
Postolnyi, B.
Lisovenko, M.
Kyrychenko, O.
Andreev, A.
Beresnev, V.
Kolesnikov, D.
Opielak, M.
Powiązania:
https://bibliotekanauki.pl/articles/1365941.pdf
Data publikacji:
2014-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
62.25.-g
Opis:
This work presents the results of TiN/MoN coatings studying. These multilayer nanostructured coatings demonstrate dependence on depositions conditions on nanometer level. The influence of nanosized monolayer thickness on structure changing and properties of nanocomposite multilayer coatings TiN/MoN was found. Multilayer TiN/MoN coatings of the total thickness from 6.8 to 8.2 μm were obtained using C-PVD method. Thicknesses of monolayers were 2, 10, 20, 40 nm. The structure of samples was studied using X-ray diffraction (Bruker D-8 Advance) in Cu $K_{α}$ radiation, high resolution transmission electron microscopy with diffraction CFEI EO Techai F200, scanning electron microscopy with energy dispersive X-ray spectroscopy (JEOL-7001F), and microhardness measurements in dependence on indenter load. Scratch tests (friction, wear, etc.) were also provided using Rockwell-C diamond indenter (CSM Revetest Instruments) with a tip radius of 200 μm. Friction and wear behavior were evaluated using ball-on-plate sliding test on a UMT-3MT tribometer (CETR, USA). With decreasing monolayer thickness the hardness value increases, and the size of nanograins reduces. The values obtained for the friction coefficient of the multilayer system is much smaller than in nanostructured coatings of TiN (nc) or MoN (nc). Annealing showed formation of a (Ti,Mo)N solid solution and small growth of nanocrystals.
Źródło:
Acta Physica Polonica A; 2014, 125, 6; 1280-1283
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Deposition Parameters and Thermal Annealing on the Structure and Properties of Nitride Coatings (TiHfZrVNb)N
Autorzy:
Pogrebnjak, A.
Abadias, G.
Chartier, P.
Bondar, O.
Yakuschenko, I.
Takeda, Y.
Krause-Rehberg, R.
Kolesnikov, D.
Beresnev, V.
Partyka, J.
Powiązania:
https://bibliotekanauki.pl/articles/1365973.pdf
Data publikacji:
2014-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
62.25.-g
Opis:
Results of structure, phase composition, physical and mechanical properties and tribological properties investigations of nitride high-entropy coatings (TiZrHfVNb)N are presented in the paper. Proton microbeam (μ-PIXE), X-ray diffraction method, including method of X-ray strains measurements, energy dispersive X-ray spectroscopy and scanning electron microscopy analysis, microhardness testing and nanoindentation were used. Thermal annealing (t=600°C) influence on defect profiles, structure and element distribution in the coatings was investigated. It was found that thermal treatment of coatings leads to changing of defect profiles and to element redistribution. Also we can say that it influences less on grain size changing. Investigated (TiZrHfVNb)N coatings demonstrate high values of hardness and excellent wear resistance.
Źródło:
Acta Physica Polonica A; 2014, 125, 6; 1296-1298
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical Properties of Boronized AISI 316, AISI 1040, AISI 1045 and AISI 4140 Steels
Autorzy:
Calik, A.
Sahin, O.
Ucar, N.
Powiązania:
https://bibliotekanauki.pl/articles/1808113.pdf
Data publikacji:
2009-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.-x
62.20.Qp
68.35.Fx
Opis:
In this study, some mechanical properties of borided and unborided four steels were investigated. Boronizing of steels was performed by powder pack method at 1210 K for 4 h. The hardness of borides, boride layer thickness and room temperature tensile properties were measured and it was observed that hardness and tensile properties strongly depend on chemical composition of steels. In addition, the effect of a notch on impact behavior was examined by conducting the Charpy tests on borided and unborided steels. The greatest notch toughness was found for a steel AISI 316 with a microstructure consisting of different C, Ni and Cr chemical composition compared to AISI 1040, 1045 and 4140 steels.
Źródło:
Acta Physica Polonica A; 2009, 115, 3; 694-698
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Thermal Treatment on the Structure and Mechanical Properties of Coatings Based on (Ti, Hf, Nb, Si)N
Autorzy:
Pogrebnjak, A.
Komarov, F.
Sobol, O.
Kaverina, A.
Shypylenko, A.
Karwat, C.
Powiązania:
https://bibliotekanauki.pl/articles/1198976.pdf
Data publikacji:
2014-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
62.25.-g
Opis:
Current paper presents the results of investigating of nanostructured cathode arc vacuum evaporation coatings, based on (Ti, Hf, Nb, Si)N. Several methods of the structural and elemental analysis were used: proton microbeam, nano- and micro-electron beam, X-ray diffraction analysis. To determine tribological properties (scratch resistance, adhesive and cohesive strength) of the coatings, scratch testing were conducting. Influence of thermal annealing at temperatures 300, 500, 800, 1000C on elemental composition, microstructure, residual stress, phase composition, profiles of atomic distribution in the coatings were investigated.
Źródło:
Acta Physica Polonica A; 2014, 125, 6; 1312-1315
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Multicomponent (Ti-Zr-Hf-V-Nb)N Nanostructure Coatings Fabrication, High Hardness and Wear Resistance
Autorzy:
Pogrebnjak, A.
Beresnev, V.
Kolesnikov, D.
Bondar, O.
Takeda, Y.
Oyoshi, K.
Kaverin, M.
Sobol, O.
Krause-Rehberg, R.
Karwat, C.
Powiązania:
https://bibliotekanauki.pl/articles/1400429.pdf
Data publikacji:
2013-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
62.25.-g
Opis:
First results in the field of synthesis and research of the multicomponent (Ti-Zr-Hf-V-Nb)N nanostructured coatings are presented in the paper. Influence of processes of spinodal segregation and mass-transfer on single-layered or multilayered crystal boundary (second phase) forming were explored. Superhard nanostructured coatings were investigated before and after annealing at the temperature 600°C using unique methods (slow positron beam, proton microbeam particle induced X-ray emission-μ, Rutherford backscattering-analysis, scanning electron microscopy with energy dispersive X-ray spectroscopy, X-ray diffraction analysis was performed using DRON-4 and nanoindentor). Diffraction spectra were taken point-by-point, with a scanning step 2Θp=0.05 to 0.1°. We detected that positron trapping by defects was observed on the nanograins boundaries and interfaces (vacancies and nanopores which are the part of triple and larger grain's boundary junction). The 3D distribution maps of elements obtained by the proton microbeam (particle induced X-ray emission-μ) together with the results obtained by slow positron microbeam gave us comprehensive information about physical basis of the processes, connected with diffusion and spinodal segregation in superhard coatings.
Źródło:
Acta Physica Polonica A; 2013, 123, 5; 816-818
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Nanoscale TiN/MoN Multilayered Systems, Fabricated Using Arc Evaporation
Autorzy:
Pogrebnjak, A.
Bondar, O.
Abadias, G.
Eyidi, D.
Beresnev, V.
Sobol, O.
Postolnyi, B.
Zukowski, P.
Powiązania:
https://bibliotekanauki.pl/articles/1402193.pdf
Data publikacji:
2015-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
62.25.-g
Opis:
Using the vacuum-arc evaporation method we fabricated periodic multilayered TiN/MoN structures with different bilayer periods λ ranging from 8 to 100 nm. We found that molybdenum nitride and titanium nitride layers grown on steel show local partial epitaxy and columnar growth across interfaces. A molybdenum-titanium carbide interlayer was evidenced between the substrate and the multilayer. Molybdenum nitride and titanium nitride layers contain small (5÷30 nm) grains and are well crystallized with (100) preferred orientation. They were identified as stoichiometric fcc TiN and cubic γ-M₂N. Non-cubic molybdenum nitride phases were also detected. The hardness of the obtained structures achieved great values and maximal hardness was 31÷41.8 GPa for the multilayered structure with a 8 nm period. Hardness of the obtained coatings is 25÷45% higher in comparison with the initial single-layer nitride coatings, plasticity index of multilayered structure is 0.075.
Źródło:
Acta Physica Polonica A; 2015, 128, 5; 836-840
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Multilayered Nano-Microcomposite Ti-Al-N/TiN/$Al_2O_3$ Coatings. Their Structure and Properties
Autorzy:
Pogrebnjak, A.
Shpak, A.
Kirik, G.
Erdybaeva, N.
Il'yashenko, M.
Dem'yanenko, A.
Kunitskii, Yu.
Kaverina, A.
Baidak, V.
Makhmudov, N.
Zukowski, P.
Komarov, F.
Beresnev, V.
Ruzimov, Sh.
Shypylenko, A.
Powiązania:
https://bibliotekanauki.pl/articles/1503960.pdf
Data publikacji:
2011-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
62.25.-q
Opis:
This paper presents the first results on formation and study of structure and properties of micro- and nanocomposite combined coatings. By means of modeling the deposition processes (deposition conditions, current density-discharge, plasma composition and density, voltage) we formed the three-layer nanocomposite coatings of Ti-Al-N/Ti-N/$Al_2O_3$. The coating composition, structure and properties were studied using physical and nuclear-physical methods. The Rutherford proton and helium ion backscattering, scanning electron microscopy with microanalysis, grazing incidence X-ray diffraction, as well as nanohardness tests (hardness) were used. Measurements of wear resistance and corrosion resistance in NaCl, HCl and $H_2SO_4$ solutions were also performed. For testing mechanical properties such characteristics of layered structures as hardness H, elastic modulus E: $H^3//E^2$ etc. were measured. It is demonstrated that the formed three-layer nanocomposite coatings have hardness of 32 to 36 GPa and elastic modulus of 328 ± 18 to 364 ± 14 GPa. Its wear resistance (cylinder-surface friction) increased by factor of 17 to 25 in comparison with the substrate (stainless steel). The layers thickness was in the range of 56-120 μm.
Źródło:
Acta Physica Polonica A; 2011, 120, 1; 94-99
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Properties of Nano- and Microcomposite Coating Based on Ti-Si-N/WC-Co-Cr
Autorzy:
Pogrebnjak, A.
Shpak, A.
Beresnev, V.
Il'yashenko, M.
Komarov, F.
Shypylenko, A.
Kaverin, M.
Zukovski, P.
Kunitskyi, Y.
Kolesnikov, D.
Kolisnichenko, O.
Makhmudov, N.
Powiązania:
https://bibliotekanauki.pl/articles/1503969.pdf
Data publikacji:
2011-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.46.-w
62.20.Qp
62.25.-g
Opis:
Using the two technologies: plasma-detonation and vacuum-arc deposition, we fabricated two types of coatings: Ti-Si-N/WC-Co-Cr/steel and Ti-Si-N/steel. We found that the top coating of Ti-Si-N was nanostructured one with 12 to 15 nm grain sizes and H = 40 to 38 GPa hardness. A thick coating which was deposited using the pulsed plasma jet, demonstrated 11 to 15.3 GPa hardness, an elastic modulus (E) changing within 176 to 240 GPa, and tungsten carbide grain dimensions varying from 150 to 350 nm to several microns. An X-ray diffraction analysis shows that the coating has the following phase composition: TiN, (Ti,Si)N solid solution, WC, $W_2C$ tungsten carbides. An element analysis was performed using energy dispersive spectroscopy (microanalysis) and scanning electron microscopy, as well as the Rutherford backscattering of $\text{}^4He^{+}$ ion and the Auger electron spectroscopy. Surface morphology and structure were analyzed using scanning electron microscopy and scanning tunnel microscopy. Tests friction and resistance (cylinder-plane) demonstrated essential resistance to abrasive wear and corrosion in the solution. The decrease of grain dimensions ≤ 10 nm occurring in the top Ti-Si-N coating layer increased the sample hardness to 42 ± 2.7 GPa under $Ti_{72}-Si_8-N_{20}$ at.% concentration.
Źródło:
Acta Physica Polonica A; 2011, 120, 1; 100-104
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Structural Properties of Fe-Ti-B Based Alloys Produced by Mechanical Alloying
Autorzy:
Kon, O.
Sen, U.
Powiązania:
https://bibliotekanauki.pl/articles/1401329.pdf
Data publikacji:
2015-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ev
06.30.Dr
62.20.Qp
Opis:
In the present study, the production of Fe-Ti-B based alloys was realized and their structure and properties were investigated. Mechanical alloying proceeds by the continual cold welding and fracturing of the constituent mixture of Ti+4B+5Fe powder when subjected to the large compressive forces of a high speed mill. The powder charge together with 7 mm diameter steel balls were loaded into a tool steel grinding container at approximately 350 RPM for 20 h. The samples were shaped as cylinder of Ø15×8 mm dimensions by uniaxial pressing at 450 MPa. Then, the green body materials were produced by sintering at 1100°C for 1-4 h in argon atmosphere. The morphology of composite materials was investigated by optical microscopy and scanning electron microscopy and phase analysis was realized by x-ray diffraction analysis. The bulk densities of the materials were measured using by Archimedes method. Also, the micro-hardness of the samples was measured by Vickers indentation technique. As a result, Fe, iron boride (FeB, Fe₂B) and titanium boride (TiB₂) phases were detected in the phase analysis of the Fe-Ti-B based materials. The hardness of the materials was measured between 1107 $HV_{0.05}$ and 1551 $HV_{0.05}$, depending on sintering time. The densities of the samples were determined between 4.205 g/cm³ and 4.219 g/cm³.
Źródło:
Acta Physica Polonica A; 2015, 127, 4; 1214-1217
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Comparison of Hardness and Wear Behaviour οf Boronized and Carburized AISI 8620 Steels
Autorzy:
Calik, A.
Duzgun, A.
Ekinci, A.
Karakas, S.
Ucar, N.
Powiązania:
https://bibliotekanauki.pl/articles/1585043.pdf
Data publikacji:
2009-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
62.20.-x
62.20.M-
62.20.Qp
68.35.Fx
Opis:
In this study, the hardness and wear behaviour of carburized and boronized AISI 8620 steels have been studied. The boronizing treatment increased the hardness of AISI 8620 steels from 395 $HV_{0.1}$ to a maximal 1610 $HV_{0.1}$ compared to the carburized steels and also significantly improved its wear behaviour. From obtained results, it can be concluded that boronizing is very effective surface hardening method for improving the wear properties of AISI 8620 steels.
Źródło:
Acta Physica Polonica A; 2009, 116, 6; 1029-1032
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Parameters on Dry Sliding of Chopped Bamboo Reinforced Epoxy Composites Based on the Taguchi Method
Autorzy:
Ozsoy, N.
Ozsoy, M.
Mimaroglu, A.
Powiązania:
https://bibliotekanauki.pl/articles/1191719.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Qk
07.05.Fb
62.20.Qp
Opis:
Chopped bamboo-reinforced epoxy composites were fabricated and tested to investigate their tribological properties. Three different weight fractions of 6%, 8% and 10% were used as reinforcement in the composites. Wear behaviour of composites was investigated by pin on disc wear testing device. To analyse the results the design of experiments (DOE) approach by using the Taguchi method was employed. Three different parameters (load, sliding speed, weight fractions) with three levels were chosen in design of experiments. Signal to noise ratio and analysis of variance (ANOVA) were used to investigate the influence of parameters on the wear rate and the coefficient of friction. According to the results, load was the most effective parameter for both wear rate and coefficient of friction.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 687-689
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Boriding of binary Ni-Ti and ternary Ni-Ti-Cu shape memory alloys
Autorzy:
Ucar, N.
Turku, N.
Ozdemir, A.
Calik, A.
Powiązania:
https://bibliotekanauki.pl/articles/1065676.pdf
Data publikacji:
2016-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Dk
61.72.-y
62.20.Qp
Opis:
In this work, the boriding of binary (Ni-Ti) and ternary (Ni-Ti-Cu) shape memory alloys was carried out in a solid medium at 1173 K for 8 h using the powder pack method with Ekabor-Ni powders. Characterization of boride layer formed on the surface of alloys was identified by optical microscopy and scanning electron microscopy. TiB₂, NiB₂ and SiC phases in the boride layer of borided binary (Ni-Ti) and ternary (Ni-Ti-Cu) shape memory alloys was confirmed by X-ray diffraction analysis. The microhardness and thickness of the boride layers were measured. The obtained hardness values show a hardness anomaly due to porosity and structural defects with increase of Cu content, while a decrease in the value of hardness moving from the boride layer to main structure was observed.
Źródło:
Acta Physica Polonica A; 2016, 130, 1; 492-495
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Properties of Me/Si Structures Prepared by Means of Self-Ion Assisted Deposition
Autorzy:
Tashlykov, I.
Żukowski, P.
Mikhalkovich, O.
Baraishuk, S.
Powiązania:
https://bibliotekanauki.pl/articles/1198974.pdf
Data publikacji:
2014-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.72.uf
82.80.-d
62.20.Qp
Opis:
In this paper a composite structure, topography, wettability and nanohardness of a (100) Si surface modified by means of ion-assisted deposition of metal (Me) coatings in conditions of a self-irradiation are discussed.
Źródło:
Acta Physica Polonica A; 2014, 125, 6; 1306-1308
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł

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