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Wyświetlanie 1-15 z 56
Tytuł:
Positron Annihilation Study of Structural Relaxation and Crystallization in Metallic Glasses Fe$\text{}_{78-x}$Co$\text{}_{x}$Si$\text{}_{9}$B$\text{}_{13}$
Autorzy:
Filipecki, J.
Powiązania:
https://bibliotekanauki.pl/articles/1929084.pdf
Data publikacji:
1993-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
Opis:
Results of measurements of positron lifetimes and X-ray diffraction in the annealed metallic glasses Fe$\text{}_{78-x}$Co$\text{}_{x}$Si$\text{}_{9}$B$\text{}_{13}$ (x = 0, 20, 40, 60, 78) before and after the process of crystallization are presented. From the results it follows that the annealing process below the crystallization temperature causes changes in concentrations of positron-trapping areas and can be consistently described as the result of two contributions: topological and chemical short range ordering. The process of crystallization causes precipitation of α-Fe and β-Co crystalline phases and also formation of microvoids in the investigated samples.
Źródło:
Acta Physica Polonica A; 1993, 83, 3; 303-306
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Structural Changes in Metallic Glass Fe$\text{}_{18}$Co$\text{}_{60}$Si$\text{}_{9}$B$\text{}_{13}$
Autorzy:
Jakubczyk, E.
Filipecki, J.
Mandecki, Z.
Jakubczyk, M.
Powiązania:
https://bibliotekanauki.pl/articles/1933512.pdf
Data publikacji:
1995-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
Opis:
Structural changes accompanying the isothermal annealing of the metallic glass Fe$\text{}_{18}$Co$\text{}_{60}$Si$\text{}_{9}$B$\text{}_{13}$ were investigated by X-ray diffraction, positron annihilation as well as by electrical resistivity and the Hall resistivity measurements. It has been found out that at the temperature of 673 K the complete crystallization did not occur, but only a few nuclei of the α-Fe phase, which did not grow, were formed.
Źródło:
Acta Physica Polonica A; 1995, 88, 1; 163-169
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of the Annealed Metallic Glass Fe$\text{}_{28}$Co$\text{}_{50}$Si$\text{}_{9}$B$\text{}_{13}$ by the X-Ray and Electrical Resistance Methods
Autorzy:
Jakubczyk, E.
Mandecki, Z.
Powiązania:
https://bibliotekanauki.pl/articles/1861253.pdf
Data publikacji:
1994-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
Opis:
In this paper results of investigations of the X-ray diffraction and the electrical resistance of the metallic glass Fe$\text{}_{2}$8Co$\text{}_{50}$Si$\text{}_{9}$B$\text{}_{13}$ are presented. These investigations were performed for isothermally annealed samples during 4 hours in the temperature range from 573 to 823 K. As a result of annealing, the samples were obtained in a crystalline state. The second series of the investigations was performed for samples annealed at a constant temperature of 673 K but in different time intervals.
Źródło:
Acta Physica Polonica A; 1994, 85, 1; 215-218
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Effect of Annealing the Fe$\text{}_{78}$Si$\text{}_{9}$B$\text{}_{13}$ Amorphous Alloy Using the EELS Method and the Hall Effect
Autorzy:
Kołodziej, H. B.
Jakubczyk, E.
Mandecki, Z.
Całusiński, B.
Powiązania:
https://bibliotekanauki.pl/articles/1929095.pdf
Data publikacji:
1993-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
Opis:
The effect of structural relaxation on the electronic structure of Fe$\text{}_{78}$Si$\text{}_{9}$B$\text{}_{13}$ metallic glass was investigated by means of the Hall effect, electrical conductivity and EELS methods. The effect of the structural relaxations was observed by four-hour annealing of the samples in argon atmosphere at temperatures 573, 673, 723, 773 K. The most distinct changes in the measured quantities were observed for samples annealed at 773 K. The differences in EELS spectrum, a decrease in the electrical and the Hall resistance are specific to these samples. X-ray diffractometry confirmed that the samples annealed at this temperature show recrystallization.
Źródło:
Acta Physica Polonica A; 1993, 83, 3; 327-331
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High Temperature Structure and Properties of Grain Boundaries - Insights Obtained from Atomic Level Simulations
Autorzy:
Keblinski, P.
Powiązania:
https://bibliotekanauki.pl/articles/2035461.pdf
Data publikacji:
2002-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
61.72.Mm
Opis:
Molecular-dynamics simulations of grain boundaries in Si and fcc metals reveal that high-energy boundaries are disordered, even at low temperatures, with their local atomic structure very similar to that of bulk amorphous material. By contrast, low energy grain boundaries are crystalline all the way up to the melting point. Upon heating intergranular"confined amorphous" structures of high-energy grain boundaries exhibit reversible transition into universal, highly confined, liquid-like structure. High-temp erature properties, such as the grain boundary diffusion therefore involve liquid-like mechanisms, with activation energies related to the diffusion process in the melt. By contrast to Si and fcc metals, high-energy diamond grain boundaries are more ordered structurally, but contain coordination disorder resulting from ability of carbon to change its hybridization from s p$\text{}^{3}$ to sp$\text{}^{2}$ character. Based on the insights obtained from our simulation of individual grain boundaries we were able to design nanocrystalline 3D microstructures, which allow to study grain boundary diffusion creep process by molecular-dynamics simulations. In order to prevent grain growth and thus to enable steady-state diffusion creep to be observed on a time scale accessible to molecular-dynamics simulations (of typically 10$\text{}^{-9}$ s), our input microstructures were tailored to (i) have a uniform grain shape and a uniform grain size of nm dimensions and (ii) contain only high-energy grain boundaries that, consistently with our studies of individual, bicrystalline grain boundaries, exhibit rather fast, liquid-like self-diffusion at high temperatures. Our simulations reveal that under relatively high tensile stresses these microstructures, indeed, exhibit steady-state diffusion creep that is homogeneous with a strain rate that agrees quantitatively with that given by the Coble-creep formula.
Źródło:
Acta Physica Polonica A; 2002, 102, 1; 123-134
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of Third Generation Synchrotron Source to Studies of Non-Crystalline Materials: In-Se Amorphous Films
Autorzy:
Burian, A.
Jabłońska, A.
Burian, A. M.
Le Bolloc'h, D.
Metzger, H.
Proux, O.
Hazemann, J. L.
Mosset, A.
Raoux, D.
Powiązania:
https://bibliotekanauki.pl/articles/2030649.pdf
Data publikacji:
2002-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.10.-i
61.43.Dq
Opis:
The local structure of vacuum evaporated In-Se amorphous films, containing 50, 60, and 66 at.% Se, was studied using differential anomalous X-ray scattering and extended X-ray absorption fine structure. Both intensity and absorption spectra were measured in the vicinity of the absorption K-edge of Se. The differential anomalous X-ray scattering data were converted to real space by the inverse Fourier transform yielding the differential radial distribution functions. The obtained results provide evidence for the presence of Se-In spatial correlations for In$\text{}_{50}$Se$\text{}_{50}$ and Se-In and Se-Se correlations for In$\text{}_{40}$Se$\text{}_{60}$ and In$\text{}_{34}$Se$\text{}_{66}$ within the first coordination sphere.
Źródło:
Acta Physica Polonica A; 2002, 101, 5; 701-708
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Structural Stability of Soft Magnetic Fe-Co-Zr-W-B Metallic Glasses Investigated by the in-situ X-ray Diffraction
Autorzy:
Michalik, S.
Bednarcik, J.
Pawlik, P.
Matija, R.
Sovak, P.
Powiązania:
https://bibliotekanauki.pl/articles/1366893.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
61.43.Dq
Opis:
The atomic structure of as-prepared $Fe_{61}Co_{(14-x)}Zr_{5}W_{x}B_{20}$ (x=1, 2 and 4) ribbon samples and their thermal stability were investigated by in-situ high-energy X-ray diffraction experiments. It was observed that higher W concentration causes the tiny shift of the main peak of the reduced atomic pair distribution function to higher values of interatomic distances and increases the coefficient of volume thermal expansion. The crystallization process occurs in two steps and is qualitatively the same for all studied specimens. Firstly the $Fe_{23}B_{6}$ phase is created and later is transformed to other types of borides together with the creation of a Fe-based phase.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 66-67
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermopower and hardness characterization of structural relaxation and crystallization in FINEMET type amorphous precursor alloy
Autorzy:
Bán, K.
Szabó, A.
Ipach, R.
Szabó, B.
Powiązania:
https://bibliotekanauki.pl/articles/1053037.pdf
Data publikacji:
2017-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
72.15.Jf
Opis:
In this paper, the thermopower (U) and hardness (HV) of FINEMET type glasses are studied during structural relaxation and beyond the crystallization onset. In this multicomponent alloy (Fe_{73.5-x}Si_{13.5}B_{9}Nb_{x}Cu_{1}) both property changes are more complex than that in binary Fe-B glasses. The phenomenon of relaxation and the crystallization onset can be successfully distinguished in both property changes. Simultaneously with the hardness increase, a slope increase in the thermopower versus temperature dependences was observed if crystallization started. The character of both property changes does alter drastically at the beginning of amorphous-nanocrystalline transformation. Similar trends were measured on samples undergoing traditional isothermal and pulse heat treatments.
Źródło:
Acta Physica Polonica A; 2017, 131, 4; 702-704
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermopower Monitoring of Relaxation and Devitrification in Fe-Based Glassy Alloys
Autorzy:
Lovas, A.
Kravcak, J.
Szabó, A.
Powiązania:
https://bibliotekanauki.pl/articles/1200307.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
72.15.Jf
Opis:
The change of thermopower is investigated in Fe-based glassy alloys during structural relaxation and amorphous-crystalline transformation. It was found, that thermopower shifts to negative direction until solely the relaxation proceeds. This negative shift is composition independent. The net shape of thermopower curves is composed from the thermopower of the individual constituent crystalline phases after the crystallization process.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 78-79
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Plastic Deformation on Nanocrystallization of Finemet Alloy
Autorzy:
Csach, K.
Miškuf, J.
Juríková, A.
Janák, G.
Powiązania:
https://bibliotekanauki.pl/articles/1534051.pdf
Data publikacji:
2010-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
62.20.Hg
Opis:
The Finemet alloy prepared by the crystallization of an amorphous precursor is a basic model material for study of magnetic nanoparticle structures. Intensive plastic deformation localized in adiabatic shear bands causes the intensive heating and structural changes in the amorphous alloy. These changes influence the magnetic properties of the amorphous precursor for the Finemet crystallization.
Źródło:
Acta Physica Polonica A; 2010, 118, 5; 820-822
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Plastic Deformation on Devitrification of $Fe_{73.5}Nb_{3}Cu_{1}Si_{13.5}B_{9}$ Amorphous Alloy
Autorzy:
Csach, K.
Miškuf, J.
Juríková, A.
Powiązania:
https://bibliotekanauki.pl/articles/1367306.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
62.20.Hg
Opis:
The method of thermogravimetry in external magnetic field was modified using square wave alternate magnetic field for an estimation of the temperature dependence of the magnetization. This method was used for the study of influence of plastic deformation of the amorphous alloy $Fe_{73.5}Nb_{3}Cu_{1}Si_{13.5}B_{9}$ on the structural changes.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 98-99
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fragmentation of Co-Fe-Ta-B Soft Magnetic Amorphous Alloy
Autorzy:
Miškuf, J.
Csach, K.
Juríková, A.
Huráková, M.
Tabachnikova, E.
Powiązania:
https://bibliotekanauki.pl/articles/1387048.pdf
Data publikacji:
2015-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
62.25.Mn
Opis:
The main limitation of high-strength Co-based bulk metallic glasses for their application as structural materials is the large brittleness. Spontaneously emerging cracks in the alloy degrade the magnetic properties. We analyzed the failure characteristics of $Co_{43}Fe_{20}Ta_{5.5}B_{31.5}$ bulk soft magnetic metallic glass deformed in the compression at room temperature and the low strain rate. Under loading the amorphous structure stores high elastic energy. During the failure this energy is released and the alloy breaks into small particles or powder exhibiting a fragmentation mode.
Źródło:
Acta Physica Polonica A; 2015, 127, 2; 558-560
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural Relaxation of Ni-Si-B Amorphous Ribbon
Autorzy:
Juríková, A.
Csach, K.
Miškuf, J.
Ocelík, V.
Powiązania:
https://bibliotekanauki.pl/articles/1813536.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
62.20.Hg
Opis:
The structural relaxation of the Ni-Si-B amorphous ribbon was studied by means of differential scanning calorimetry and thermomechanical analysis. It was shown that considerable length changes associated with reversible structural relaxation were revealed after a previous creep applied at higher temperatures.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 99-102
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure Refinement of Amorphous Cd-As by Analysis of Partial Radial Distribution Functions
Autorzy:
Burian, A.
Powiązania:
https://bibliotekanauki.pl/articles/1964102.pdf
Data publikacji:
1997-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
61.43.Bn
61.43.-j
Opis:
The anomalous wide angle X-ray scattering technique was used to determine the partial structure factors and then the partial radial distribution functions for vacuum evaporated Cd-As amorphous films containing 41 and 74% at. As. The experiments were performed using synchrotron radiation tuned near the As and Cd absorption edges. The obtained structural information about the individual Cd-Cd, Cd-As and As-As correlations shows that As and Cd remain almost tetrahedrally coordinated and suggest a certain degree of chemical disorder of the investigated samples.
Źródło:
Acta Physica Polonica A; 1997, 91, 5; 917-921
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of High Co Addition on the Properties of $Fe_{79}Zr_{9}B_{12}$ and $Fe_{76}Zr_{9}B_{15}$ Alloys
Autorzy:
Yu, W.
Long, D.
Liu, Y.
Sun, Y.
Hua, Z.
Powiązania:
https://bibliotekanauki.pl/articles/1401884.pdf
Data publikacji:
2015-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
65.60.+a
61.43.Dq
Opis:
Thermal properties, microstructure and magnetic properties of $Fe_{79}Zr_{9}B_{12},$ $Fe_{76}Zr_{9}B_{15},$ $Fe_{39.5}Co_{39.5}Zr_{9}B_{12}$ and $Fe_{38}Co_{38}Zr_{9}B_{15}$ alloys were investigated by differential thermal analysis, X-ray diffraction and vibrating sample magnetometer. High Co addition has a significant impact on the properties of alloys. High Co addition increases the main crystallization peak temperature and the crystallization activation energy. Moreover, high Co addition changes the crystallization products and influences the crystallization processes of $Fe_{79}Zr_{9}B_{12}$ and $Fe_{76}Zr_{9}B_{15}$ alloys. The specific saturation magnetization $(M_{s})$ increases and coercivity $(H_{c})$ decreases by high Co additions.
Źródło:
Acta Physica Polonica A; 2015, 128, 3; 340-342
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 56

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