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Tytuł:
Positronium time-of-flight Measurements of Mesoporous Silica Films
Autorzy:
Kuang, Peng
Zhang, Xiao
He, Chun
Cao, Xing
Wang, Bao
Powiązania:
https://bibliotekanauki.pl/articles/1029796.pdf
Data publikacji:
2018-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
61.05.-a
68.47.Mn
Opis:
Mesoporous silica films were synthesized with various concentrations of cetyltrimethylammonium bromide (CTAB) in precursor sols through the method of electro-assisted self-assembly (EASA). Oriented pore channels were observed in the films prepared with more CTAB in the precursor sols. Positronium time-of-flight (Ps-TOF) measurements were performed for the silica films with different porous structures. It is demonstrated that the Ps emission intensity and energies are well correlated to the apparent porosity, pore interconnectivity and possibly pore channel orientation. The results indicate that Ps-TOF can be a useful technique for probing the structures of porous films.
Źródło:
Acta Physica Polonica A; 2018, 133, 1; 3-6
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Selected Properties of ZnO Coating on Mg-Based Alloy for Biomedical Application
Autorzy:
Kania, A.
Pilarczyk, W.
Babilas, R.
Powiązania:
https://bibliotekanauki.pl/articles/1029768.pdf
Data publikacji:
2018-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
68.55.-a
61.05.cp
68.37.Ps
82.45.Bb
Opis:
Magnesium and its alloys are interesting materials for biodegradable implant applications. Magnesium alloys have very good strength properties, they are lightweight, but their main disadvantage is a low corrosion resistance in the physiological environment. Various modifications of a Mg alloys surface by deposition of different coatings are used to prevent untimely dissolution. The article presents the investigation results of a thin ZnO coating deposited on a MgCa2Zn1Gd3 alloy by means of the magnetron sputtering method. The studies include: scanning electron microscope observation of the ZnO surface, X-ray phase analysis, surface roughness measurement in atomic force microscopy, the microhardness test and potentiodynamic corrosion resistance test in the Ringer solution at 37°C. It was found that the ZnO coating is compact and continuous. It increases the hardness of the MgCa2Zn1Gd3 alloy and also improves its corrosion resistance. The corrosion potential is shifted slightly towards the positive values from -1.52 V to -1.50 V for the alloy with the ZnO coating.
Źródło:
Acta Physica Polonica A; 2018, 133, 2; 222-224
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Macroscopic and Microscopic Study of a CePdIn Compound
Autorzy:
Klicpera, M.
Javorský, P.
Puente-Orench, I.
Hoser, A.
Powiązania:
https://bibliotekanauki.pl/articles/1030269.pdf
Data publikacji:
2017-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.F-
71.27.+a
72.15.Eb
Opis:
The magnetization and electrical resistivity measurements on a CePdIn single crystal as well as its preparation and structural characterization are presented. The negative paramagnetic Curie temperatures indicate antiferromagnetic ground state, the anisotropy of the paramagnetic Curie temperature amounts 22.7 K. No ferromagnetic correlations were indicated. Powder neutron diffraction experiment performed at temperatures down to 0.4 K did not lead to observation of any magnetic peak in diffraction patterns. We estimate the magnetic moment on Ce atoms to be significantly lower than 0.5 μ_{B}. The temperature development of lattice parameters documents the standard thermal expansion of the unit cell; no signs of structural phase transition were observed.
Źródło:
Acta Physica Polonica A; 2017, 131, 4; 970-972
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure of Melt-Spun Co₂MnAl Heusler Alloy
Autorzy:
Piovarči, S.
Diko, P.
Kavečanský, V.
Ryba, T.
Vargová, Z.
Varga, R.
Powiązania:
https://bibliotekanauki.pl/articles/1032646.pdf
Data publikacji:
2017-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
68.55.-a
75.50.Cc
61.05.cp
Opis:
The growth-related microstructure and texture of the Co₂MnAl-type Heusler alloy in the form of a melt-spun ribbon was studied by electron microscopy, electron backscattered diffraction and X-ray diffraction. It is shown that melt spinning produces a single-phase disordered Heusler alloy. The fine grain structure at the wheel side of the ribbon exhibits no texture, while dominant columnar grain structure formed on the free surface side exhibits the ⟨111⟩ fibre texture with a declination by about 10 degrees in the spinning direction. The dendritic growth of columnar crystals causes inhomogeneity of the chemical composition on a micrometre scale with a higher Co and Al concentration in the centre of dendritic arms and a higher concentration of Mn at the dendrite arm boundaries.
Źródło:
Acta Physica Polonica A; 2017, 131, 4; 881-883
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Comparative Study of the Microstructure and Phase Composition of Nanoausferritic Ductile Iron Alloy Using SEM, TEM, Magnetometer, and X-Ray Diffraction Methods
Autorzy:
Skołek, E.
Giętka, T.
Świątnicki, W.
Myszka, D.
Powiązania:
https://bibliotekanauki.pl/articles/1033075.pdf
Data publikacji:
2017-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.-a
06.60.Mr
81.05.Bx
81.07.Bc
81.40.-z
81.40.Ef
81.40.Gh
Opis:
In this paper the microstructure and phase composition of ausferritic ductile iron alloy were investigated by scanning electron microscopy, transmission electron microscopy and X-ray diffraction methods. In order to obtain the nanoausferritic microstructure in the alloy, the austempering heat treatment was performed at relatively low temperature. As a result, a specific kind of microstructure, containing nanocrystalline ausferrite and retained austenite blocks, was obtained in each heat-treated sample. The volume fractions of phases were determined using different methods: MicroMeter software for scanning electron micrographs, stereological analysis for transmission electron micrographs, quantitative analysis of the X-ray diffraction spectra and magnetometer measurements. All methods revealed a high amount of retained austenite which varied as a function of the austempering treatment parameters. It was shown that the quantitative phase composition measured by X-ray diffraction and magnetometer, in all samples investigated, differs significantly from the stereological measurements and image analysis performed through the MicroMeter software. The possible reasons of the observed differences were discussed.
Źródło:
Acta Physica Polonica A; 2017, 131, 5; 1319-1323
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Gold Nanolayer Properties Using X-Ray Reflectometry and Spectroscopic Ellipsometry Methods
Autorzy:
Stabrawa, I.
Banaś, D.
Dworecki, K.
Kubala-Kukuś, A.
Braziewicz, J.
Majewska, U.
Wudarczyk-Moćko, J.
Pajek, M.
Góźdź, S.
Powiązania:
https://bibliotekanauki.pl/articles/1398825.pdf
Data publikacji:
2016-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cm
62.23.St
68.55.-a
81.07.-b
Opis:
X-ray reflectometry and spectroscopic ellipsometry methods were applied for determination of physical properties of gold nonolayers. The nanolayers were prepared by sputtering of gold on different substrates: borosilicate glass, polished crystalline quartz and crystalline silicon. With X-ray reflectometry technique roughness of the substrates and density, thickness and roughness of gold layers were determined. The results showed decrease in density of the gold layers due to their nanometer thickness and that roughness of the underlayer affects roughness of the gold layer. In addition, thicknesses of the gold layers measured with spectroscopic ellipsometry turned out to be in agreement, within the experimental uncertainty, with results of the X-ray reflectometry method.
Źródło:
Acta Physica Polonica A; 2016, 129, 2; 233-236
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Requirement for and Use of Coated P92 Steel for Enhanced Structural Integrity at High Temperature
Autorzy:
Hoey, T.
Chen, R.
McCartney, D.
Sun, W.
Mansfield, J.
Barnard, P.
Foster, J.
Powiązania:
https://bibliotekanauki.pl/articles/1402066.pdf
Data publikacji:
2015-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
81.15.Pq
68.37.-d
61.05.-a
64.75.-g
Opis:
To achieve climate change targets and to improve the efficiency of fossil fuel power plant the temperature and pressure of operation must be increased. With steam temperatures predicted to rise by 50-100 K in the next 30 years, this presents a number of material challenges, not least for the ferritic steels used for steam pipework. Currently the best in class ferritic steel for power plant steam pipework is P92, a 9-12% Cr advanced martensitic steel that was developed for its superior high temperature creep resistance. This paper will give a brief overview of P92 microstructure, composition and metallurgy and identify experimentally and computationally some key features of the material. As well as failure by creep, P92 at high temperature also suffers from steam oxidation damage. Recent literature suggests that coatings applied to P92 are a very promising solution. A short review of previous work on steam oxidation resistant coatings for P92 is included. A novel Co-Cr-C coating that has not previously been explored for this application is described. Experimental and computational characterisation is included.
Źródło:
Acta Physica Polonica A; 2015, 128, 4; 514-519
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
XRD Analysis of Synthetic Diamond Powders Irradiated with Electrons
Autorzy:
Shishonok, E.
Luhin, V.
Koltunowicz, T.
Powiązania:
https://bibliotekanauki.pl/articles/1402231.pdf
Data publikacji:
2015-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.-a
61.43.Gt
61.50.-f
61.80.Fe
Opis:
Powders of synthetic diamond with low strength were sorted on sets with a different grain size. The synthetic diamond sets had various crushing strengths and morphology. They were irradiated with high energy electrons (6.5 MeV, D=2×10¹⁹ cm¯²) and analyzed using X-ray diffraction (Cu K_α) before and after irradiation. As established from nonlinearity of the a(Θ)=f{R(Θ)} dependences and observed extra splittings in X-ray diffraction patterns (in addition to α₁-α₂ doublets), crystal lattice of synthetic diamond from different sets was variously distorted. Irradiation led to decreasing distortions more significantly, the higher the initial strength of the set was. The made conclusions coincide well with our previous results on synthetic diamond powders which were irradiated under various softer conditions with direct measurements of synthetic diamond crushing strength without X-ray diffraction analysis. X-ray diffraction allows to presort synthetic diamond of critically low relative mechanical strength as well as evaluate resistance of diamond crystal lattice against heavy irradiation and other external impacts.
Źródło:
Acta Physica Polonica A; 2015, 128, 5; 912-914
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characteristics of Ba-Doped PbS Thin Films Prepared by the SILAR Method
Autorzy:
Gülen, Y.
Powiązania:
https://bibliotekanauki.pl/articles/1205230.pdf
Data publikacji:
2014-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.-a
61.05.cp
68.55.Ln
Opis:
In this material production research, undoped and Ba-doped nanostructured PbS films are fabricated on glass surfaces by SILAR method. The structural, optical and morphological properties of the films are examined via scanning electron microscopy, UV-vis spectrophotometry and X-ray diffraction analysis. Scanning electron microscopy analysis revealed that Ba-doping concentration influences the size of the thin film's nanoparticles. X-ray diffraction results showed that all of the thin films are in a face centered cubic structure. Optical studies, in the room temperature, revealed that the optical band gap of the films increases as Ba-doping concentration is increased. The intercept values on the energy axis in the range of 1.86 eV and 2.12 eV for 1% and 8% Ba-doped PbS films respectively. As a result, it is concluded that the structural, optical and morphological properties of the fabricated thin films are directly depend on the Ba doping ratio.
Źródło:
Acta Physica Polonica A; 2014, 126, 3; 763-767
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Focused Ion Beam Imaging of Defects in Multicrystalline Si for Photovoltaic Application
Autorzy:
Miyamura, Y.
Sekiguchi, T.
Chen, J.
Li, J.
Watanabe, K.
Kumagai, K.
Ogura, A.
Powiązania:
https://bibliotekanauki.pl/articles/1198415.pdf
Data publikacji:
2014-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.-a
61.85.+p
61.72.Ff
Opis:
We demonstrate the imaging of the extended defects in Si materials using a focused ion beam instrument. Since Ga-ion beam has small penetration depth and high channeling character compared with electron beam, the secondary electron signal of focused ion beam is more sensitive to the surface morphology and crystallinity. We have tried to use this secondary electron imaging of focused ion beam for observation of various extended defects in Si materials for photovoltaic and semiconductor devices. As for the texture of multicrystalline Si, some grains are imaged darker than the others. It suggests that the crystal orientation gives different channeling effect on the primary Ga-ion beam, resulting in the different secondary electron yield. The grain boundaries and lineage in multicrystalline Si are shown as bright lines and patterns in the image. Although it may reflect the surface morphologies, these contrasts may be attributed to the channeling contrast due to lattice displacement or distortion. The contrast mechanism of FIB imaging is discussed.
Źródło:
Acta Physica Polonica A; 2014, 125, 4; 991-993
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetic Study of $α^{\prime\prime}$ and $γ^{\prime\prime}$-Phases of Iron Nitride Thin Films
Autorzy:
Frątczak, E.
Prieto, J.
Moneta, M.
Powiązania:
https://bibliotekanauki.pl/articles/1368214.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.15.Hi
68.55.-a
61.05.Qr
Opis:
Most of the Fe-nitride phases have been studied in much detail. Nevertheless, there is still a debate about the most efficient, exact and controlled way of obtaining thin films of the desired iron nitride phases. Thin films of iron nitrides were deposited by Molecular Beam Epitaxy in Ultra High Vacuum. By changing the growth parameters we tried to obtain the α"-phase in its purest form. We worked also on iron mononitride, FeN (γ"-FeN) which is known to exist in different phases. The stoichiometry of the samples was determined by means of resonant Rutherford Backscattering Spectroscopy. The samples were studied by room temperature Conversion Electron Mössbauer Spectroscopy. We achieved as much as 24% of pure α"-phase and provide evidence of the existence of γ"-FeN with vacancies and of the transformation of nonmagnetic γ"-phase into magnetic ε-phase after time exposure.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 214-215
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Semi-Empirical Modelling of Glass Forming Ranges for Y-Co-Si System
Autorzy:
Śniadecki, Z.
Narojczyk, J.
Idzikowski, B.
Powiązania:
https://bibliotekanauki.pl/articles/1366620.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
05.70.-a
61.43.Dq
81.30.Bx
Opis:
Glass forming abilities of a ternary Y-Co-Si system were determined on the basis of combined semi-empirical Miedema's and geometric models. The enthalpy of amorphous and solid solution phases formation, along with the mismatch entropy and GFA parameter, were analysed to indicate compositions with the highest ability for the amorphization. The large atomic radii difference between constituents, especially Y and Si, is the deciding factor of GFA. Compositions ranged between $Y_{33}Si_{67}$ and $Y_{45}Si_{55}$ are the best glass formers.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 62-63
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Low Temperature Crystal Structure Behaviour of Complex Yttrium Aluminium Oxides YAlO_3 and Y_3Al_5O_{12}
Autorzy:
Senyshyn, A.
Vasylechko, L.
Powiązania:
https://bibliotekanauki.pl/articles/1399474.pdf
Data publikacji:
2013-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
61.05.F-
65.40.De
65.60.+a
63.70.+h
Opis:
Crystal structures of two yttrium aluminium oxides, namely $YAlO_3$ and $Y_3Al_5O_{12}$, were investigated in the temperature range 3.4-300 K by high-resolution neutron powder diffraction. Neither traces of phase transformations nor discontinuous changes of physical properties were observed. Thermal expansion of yttrium aluminium oxides was evaluated in terms of 1st order Grüneisen approximation, where the Debye temperatures and the Grüneisen parameters have been estimated for both compositions. Anomalies in the thermal expansion of yttrium aluminium perovskite have been observed and modelled using the Einstein oscillator with negative Grüneisen parameter. Extended bond length analysis revealed significant thermally-driven modifications of the aluminium-oxygen framework.
Źródło:
Acta Physica Polonica A; 2013, 124, 2; 329-335
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase Transformations in Pyrochlores Irradiated with Swift Heavy Ions: Influence of Composition and Chemical Bonding
Autorzy:
Sattonnay, G.
Thomé, L.
Sellami, N.
Monnet, I.
Grygiel, C.
Legros, C.
Tetot, R.
Powiązania:
https://bibliotekanauki.pl/articles/1400452.pdf
Data publikacji:
2013-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.80.-x
61.82.Ms
61.05.cp
05.10.-a
Opis:
$Gd_2Ti_2O_7$ and $Gd_2Zr_2O_7$ pyrochlores were irradiated with swift heavy ions in order to investigate the effects of the chemical composition on the structural changes induced by high electronic excitation. The XRD results show that the structural modifications induced by irradiation with 93 MeV Xe ions are strongly dependent on the sample composition: $Gd_2Ti_2O_7$ is readily amorphized, whereas $Gd_2Zr_2O_7$ is transformed into a radiation-resistant anion-deficient fluorite structure. Atomistic simulations with the second-moment tight-binding QEq model allow us to calculate the lattice properties of both $Gd_2Ti_2O_7$ and $Gd_2Zr_2O_7$, and also to quantify the degree of covalency and ionicity in these compounds. These calculations clearly show that $Gd_2Ti_2O_7$ is more covalent than $Gd_2Zr_2O_7$, thus confirming that the amorphization resistance can be related to the covalent character of insulators.
Źródło:
Acta Physica Polonica A; 2013, 123, 5; 862-866
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of Glass Transition and Crystallization Behavior in $Ga_{15}Se_{85 - x}Pb_x$ (0 ≤ x ≤ 6) Chalcogenide Glasses
Autorzy:
Khan, Z.
Khan, S.
Alvi, M.
Powiązania:
https://bibliotekanauki.pl/articles/1400308.pdf
Data publikacji:
2013-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
61.05.cp
64.70.p
64.70.dg
65.60.+a
Opis:
There has been a growing interest in the synthesis and characterization of amorphous chalcogenide glasses due to their importance in preparing electronic memories, grating, switching devices and their optical applications as good IR transmitting materials. The study of the glass transformations and crystallization processes in the amorphous systems is interesting not only from the fundamental aspect of establishing the reaction mechanism of crystal nucleation and growth, but also from a technological point of view. The present research work is concentrated on the study of glass transition and crystallization behavior in $Ga_{15}Se_{85 - x}Pb_x$ with x=0, 3, and 6 chalcogenide glasses by differential scanning calorimetry. Their amorphous nature has been verified by X-ray diffraction. The differential scanning calorimetry experiments were performed at different continuous heating rates (5 to 25 K/min). The glass transition temperature (T_{g}) and crystallization temperature $(T_{c})$ of these glasses has been determined from differential scanning calorimetry thermograms. The dependence of $T_{g}$ and $T_{c}$ on the heating rate (β) has been used for the determination of different crystallization parameters such as the activation energy of crystallization (Δ $E_{c}$), the activation energy for structural relaxation (Δ $E_{t}$) and the order parameter (n). The results of crystallization were discussed on the basis of different models such as Kissinger's approach and modification for non-isothermal crystallization in addition to Johnson, Mehl, Ozawa and Avrami.
Źródło:
Acta Physica Polonica A; 2013, 123, 1; 80-86
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 23

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