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    Wyświetlanie 1-9 z 9
    Tytuł:
    Effect of Vacuum Hot-Press Process on The Sintered Characteristics and Mechanical Properties of A High-Density Cr-31.2 Mass% Ti Alloy
    Autorzy:
    Chang, S.-H.
    Li, C.-L.
    Huang, K.-T.
    Yang, T.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356911.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Cr-31.2 mass% Ti alloy
    vacuum hot-press sintering
    relative density
    TRS
    electrical conductivity
    Opis:
    In this study, two different compositions of submicron-structured titanium (760 nm) and micron-structured chromium (4.66 μm) powders were mixed to fabricate Cr-31.2 mass% Ti alloys by vacuum hot-press sintering. The research imposed various hot-press sintering pressures (20, 35 and 50 MPa), while the sintering temperature maintained at 1250°C for 1h. The experimental results showed that the optimum parameters of the hot-press sintered Cr-31.2 mass% Ti alloys were 1250°C at 50 MPa for 1h. Also, the relative density reached 99.94%, the closed porosity decreased to 0.04% and the hardness and transverse rupture strength (TRS) values increased to 81.90 HRA and 448.53 MPa, respectively. Moreover, the electrical conductivity is enhanced to 1.58 × 104 S·cm-1 However, the grain growth generated during the high-temperature and high-pressure of the hot-press sintering process resulted in the grain coarsening phenomenon of the Cr-31.2 mass% Ti alloys after 1250°C hot-press sintering at 50 MPa for 1h. In addition, the Cr-31.2 mass% Ti alloys were fabricated with the submicron-structured titanium (760 nm) and chromium (588 nm) powders showed more effective compaction than the micron-structured titanium (760 nm) and chromium (4.66 μm) powders did. The closed porosity decreases to 0.02% and the hardness values increase to 83.23 HRA. However, the agglomeration phenomenon of the Cr phase and brittleness of the TiCr2 Laves phases easily led to a slight decrease in TRS (400.54 MPa).
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 4; 1715-1723
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Compact High Current Vacuum Diode Based on a Ceramic-Metal Welding Interface
    Autorzy:
    Xun, T.
    Zhang, J.
    Yang, H.
    Wang, Y.
    Liu, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1807886.pdf
    Data publikacji:
    2009-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    52.59.Mv
    73.20.-r
    84.70.+p
    Opis:
    For one kind of high current diodes composed of a ceramic-metal welding vacuum interface, the electrical design was presented. For compactness, a radial type insulator and a cone-column anode crust were adopted. The shielding methods around cathode and anode region were applied to mitigate the influence of welding solder to vacuum flashover. Finite Element Analysis (FEA) simulation results indicated that by adjusting the anode outline and shielding shape, the electric fields along the ceramic were well distributed. High voltage test was conducted on a long-pulse accelerator and experimental results confirm the theoretic design: the diode can stably hold on 400 kV and 200 ns voltage pulse.
    Źródło:
    Acta Physica Polonica A; 2009, 115, 6; 1013-1015
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Analysis of the breakthrough phenomena during heavy metal elution from a column packed with municipal waste incineration ash
    Autorzy:
    Zhang, W.
    Yang, Y.
    Suganuma, H.
    Kato, S.
    Suzuki, S.
    Kojima, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/206904.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    calcium compounds
    dissolution
    heavy metals
    leaching
    particle size
    związki wapnia
    rozpuszczanie
    metale ciężkie
    ługowanie
    wielkość cząstek
    Opis:
    At some point during acid leaching column tests of heavy metals from municipal waste incineration ash, sudden and rapid elution of harmful elements was observed which was called the breakthrough (BT) phenomena. The mechanism was elucidated from the results of measurement of elemental and particle size distribution in the column and batch leaching tests as follows. At the first stage of experimental runs, CaCO3 was dissolved in acidic solution and pH profile along the bed is formed. Some of the minor elements of Zn and Al dissolved by acid at the upper part of the column are precipitated at bottom of the column, leading to the reduction of flow rate of the leachate solution. After leachate pH becomes low by the termination of dissolution of Ca, these deposits are dissolved and thus, the flow rate increases. Most of the trace elements behave as such, which causes the increase of harmful element concentrations in the eluate. Some drastic concentration increase of harmful elements in leachate may occur even after the long period of pseudo stable dissolution behavior in the land-fill site.
    Źródło:
    Environment Protection Engineering; 2018, 44, 3; 63-78
    0324-8828
    Pojawia się w:
    Environment Protection Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Impact Toughness of Offshore Steel
    Autorzy:
    Cheng, T.-C.
    Yu, C.
    Yang, T.-C.
    Huang, C.-Y.
    Lin, H.-C.
    Shiue, R.-K.
    Powiązania:
    https://bibliotekanauki.pl/articles/351264.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    low-temperature impact toughness
    prior austenite grain size
    hardenability
    bainite
    Opis:
    This study focused on the effects of microstructures on the low-temperature impact toughness of directly water-quenched offshore steel. Martensite dominated the microstructure directly below the quenched surface. In contrast, mainly lower bainite, martensite, and low amount of ferrite were observed in the central region of the quenched specimen. The ductile to brittle transition temperature of tempered martensite was significantly lower than that of a bainite-dominated microstructure. It is found that low-angle boundaries within the bainite packets greatly impair the low-temperature impact toughness of the steel. The absence of high-angle boundaries in the lower bainite packets significantly deteriorates the low-temperature impact energy of offshore steel.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 1; 167-172
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis, Crystal Structure, and Properties of a Novel, Highly Sensitive Energetic, Coordination Compound: Iron (II) Carbohydrazide Perchlorate
    Autorzy:
    Liu, R.
    Zhou, Z.
    Qi, S.
    Yang, L.
    Wu, B.
    Huang, H.
    Zhang, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/358343.pdf
    Data publikacji:
    2013
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    iron (II) carbohydrazide perchlorate
    energetic material
    high
    sensitivity
    DFT
    energy gap
    Opis:
    A single crystal of iron (II) carbohydrazide perchlorate [FeII (CHZ)3](ClO4)2 (FeCP), a novel, lead-free, energetic coordination compound, was synthesized and its structure determined by X-ray single crystal diffraction for the frst time. The crystal belongs to the monoclinic system P2(1)/n space group, with a = 1.0066(2) nm, b = 0.8458(2) nm, c = 2.1194(4) nm, β = 100.693(3)° and Z = 4. The central Fe(II) ion is coordinated to three bidentate carbohydrazide units through the carbonyl oxygen atom and an amino nitrogen atom, forming a six-coordinated, non-centrosymmetric complex cation. The thermal analyses by differential scanning calorimetry and thermogravimetry show that the onset temperature of thermal decomposition (152.7 °C) and the critical temperature of thermal explosion of FeCP (161.2 °C) are both much lower than those of other transition metal carbohydrazide perchlorate compounds, and also those of some other primary explosives in service. FeCP has a high enthalpy of combustion, as measured by oxygen bomb calorimetry. The impact, friction and fame sensitivity tests indicate that FeCP is extremely sensitive and hazardous. Unexpected explosions occurred even during the operational processes. In order to explore the intrinsic cause of these explosions, theoretical calculations of the orbital energies were performed based on DTF. These results reveal that the impact sensitivity is positively correlated with the energy gap between HOMO and LUMO: the smaller energy gap results in the higher impact sensitivity.
    Źródło:
    Central European Journal of Energetic Materials; 2013, 10, 1; 17-36
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Joining Of Green Body And Dense Substrate For Indium Tin Oxide Under Uniaxial Pressure In An Open Condition
    Łączenie zielonej masy i gęstego podłoża z tlenku cyny indu w warunkach jednoosiowego ściskania w stanie otwartym
    Autorzy:
    Moon, G.-S.
    Chung, T.-J.
    Yang, S. H.
    Hong, G.-S.
    Oh, K.-S.
    Powiązania:
    https://bibliotekanauki.pl/articles/355654.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    transparent conducting oxide
    indium tin oxide
    green body
    joining
    tlenek indu
    zielona masa
    łączenie
    Opis:
    The green body and dense substrate of indium tin oxide was joined by uniaxially pressing at 0.3 MPa at 1300°C to test the restoring of the eroded part of transparent conducting oxide target. The green body was sintered to 98% of theoretical density under the suppression of shrinkage along the boundary below 5%. The boundary between two parts was free of pore but could be recognized from the difference in grain sizes. The joined part had the virtually same density with the substrate, but the grain size was less than one fifth compared with that of substrate.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1209-1212
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Comprehensive Study of the Electrostatic Discharge Sensitivity and Chargeability of Tris(carbohydrazide)zinc Perchlorate
    Autorzy:
    Li, Z.
    Zeng, D.
    Zhou, Z.
    Zhou, M.
    Zhang, T.
    Huang, H.
    Zhang, J.
    Yang, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/358298.pdf
    Data publikacji:
    2014
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    primary explosive
    tris(carbohydrazide)zinc perchlorate
    electrostatic discharge sensitivity
    chargeability
    Opis:
    Most primary explosives are non-conductors, easily accumulate charge when contacting with and separating from other materials, and are sensitive to electrostatic discharge (ESD). In order to reduce the number of accidents caused by ESD initiation of primary explosives, studies on their electrostatic hazards are necessary. This work presents comprehensive experimental results of electrostatic discharge sensitivity and chargeability of tris(carbohydrazide)zinc perchlorate (ZnCP) under different conditions. The influences of the testing conditions, of devices, particle size, ambient temperature and relative humidity on the electrostatic discharge sensitivity and chargeability have been investigated in detail, and the quantitative regression equations obtained.
    Źródło:
    Central European Journal of Energetic Materials; 2014, 11, 4; 553-573
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Mitigation scratch on fused silica optics using CO2 laser
    Autorzy:
    Liu, C.-M.
    Yan, Z.-H.
    Yang, L.
    Jiang, Y.
    Zu, X.-T.
    Wang, H.-J.
    Liao, W.
    Yuan, X.-D.
    Zheng, W.-G.
    Powiązania:
    https://bibliotekanauki.pl/articles/174978.pdf
    Data publikacji:
    2016
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    mitigation
    scratch
    fused silica
    CO2 laser
    Opis:
    The scratch on a fused silica surface was treated as a chain of connected damage sites and mitigated one after another using CO2 laser irradiation. The optical microscopy image shows that a scratch with the width of about 30 μm and length of several millimeters can be completely mitigated without the formation of debris and bubbles. The mitigated scratch can survive under raster scan laser irradiation with the fluency increased up to 11.0J/cm2 at 3ns and 351nm. On the contrary, the substrate without CO2 laser mitigation is seriously damaged under this irradiation. The light modulation induced by mitigation is much smaller when the scratch is mitigated before being damaged. The light modulation is about 2 when the distance to the mitigated sample is larger than 20cm. The birefringence induced by residual stress in the mitigated scratch is measured. The retardance of the mitigated scratch before being damaged is not visible. Therefore, residual stress in this mitigated scratch before being damaged should be not a critical potential risk in laser damage.
    Źródło:
    Optica Applicata; 2016, 46, 3; 387-397
    0078-5466
    1899-7015
    Pojawia się w:
    Optica Applicata
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Photoexcitation Spectroscopy and Material Alteration with Free-Electron Laser
    Autorzy:
    Sturmann, J.
    Albridge, R. G.
    Barnes, A. V.
    Gilligan, J.
    Graham, M. T.
    Mckinley, J. T.
    Ueda, A.
    Wang, W.
    Yang, X.
    Tolk, N. H.
    Davidson, J. L.
    Margaritondo, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1963341.pdf
    Data publikacji:
    1997-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    79.20.La
    79.20.Ds
    63.20.-e
    79.60.Jv
    73.20.At
    Opis:
    As synchrotron radiation sources have been used for many experiments in the ultraviolet and X-ray regimes, the free-electron laser is an excellent source for a wide array of infrared-photon projects and applications. The free-electron laser delivers a beam of powerful tunable pulsed radiation which provides the opportunity for spatial and temporal localization of the energy delivered at any desired wavelength within the 2-10 μ regime. One application discussed employs the free-electron laser for spectroscopy as a probe of electronic and vibrational structures. Another application uses the free-electron laser beam as a tool for altering materials in a fundamentally new way.
    Źródło:
    Acta Physica Polonica A; 1997, 91, 4; 689-696
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-9 z 9

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