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Tytuł:
Testing of a price-based system for power balancing on real-life HVAC installation in real life
Autorzy:
Radziszewska, Weronika
Bugaj, Marcin A.
Łuniewski, Mirosław
Hoogsteen, Gerwin
Chaja, Patryk
Bykuć, Sebastian
Powiązania:
https://bibliotekanauki.pl/articles/2173657.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
distributed management
heat pump
HVAC
power management
water loop
zarządzanie rozproszone
pompa ciepła
zarządzanie energią
pętla wodna
Opis:
HVAC systems use a substantial part of the whole energy usage of buildings. The optimizing of their operation can greatly affect the power use of a building, making them an interesting subject when trying to save energy. However, this should not affect the comfort of the people inside. Many approaches aim to optimize the operation of the heating and cooling system; in this paper, we present an approach to steer the heat pumps to reduce energy usage while aiming to maintain a certain level of comfort. For this purpose, we employ a market-based distributed method for power-balancing. To maintain the comfort level, the market-based distributed system assigns each device a cost-curve, parametrized with the current temperature of the room. This allows the cost to reflect the urgency of the HVAC operation. This approach was tested in a real-world environment: we use 10 heat pumps responsible for temperature control in 10 comparable-sized rooms. The test was performed for 3 months in summer. We limited the total peak power, and the algorithm balanced the consumption of the heat pumps with the available supply. The experiments showed that the system successfully managed to operate within the limit (lowering peak usage), and - to a certain point – reduce the cost without significantly deteriorating the working conditions of the occupants of the rooms. This test allowed us to estimate the minimal peak power requirement for the tested set-up that will still keep the room temperatures in or close to comfortable levels. The experiments show that a fully distributed market-based approach with parametrized cost functions can be used to limit peak usage while maintaining temperatures.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2022, 70, 2; art. no. e140690
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystallization of FeSiB Amorphous Ribbons Induced by Laser Interference Irradiation
Autorzy:
Kusinski, J.
Czyż, O.
Radziszewska, A.
Morgiel, J.
Ostrowski, R.
Strzelec, M.
Czyż, K.
Rycyk, A.
Powiązania:
https://bibliotekanauki.pl/articles/379811.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
laser interference heating
FeSiB alloy
amorphous alloy
scanning electron microscopy
transmission electron microscopy
stop FeSiB
stop amorficzny
skaningowa mikroskopia elektronowa
transmisyjna mikroskopia elektronowa
Opis:
Detailed studies on the effects of pulsed laser interference heating on surface characteristics and subsurface microstructure of amorphous Fe80Si11B9 alloy are reported. Laser interference heating, with relatively low pulsed laser energy (90 and 120 mJ), but with a variable number (from 50-500) of consecutive laser pulses permitted to get energy accumulation in heated areas. Such treatment allowed to form two- Dimensional micro-islands of laser-affected material periodically distributed in amorphous matrix. The crystallization process of amorphous FeSiB ribbons was studied by means of scanning and transmission electron microscopy. Detailed microstructural examination showed that the use of laser beam, resulted in development of nanostructure in the heated areas of the amorphous ribbon. The generation of nanocrystalline seed islands created by pulsed laser interference was observed. This key result may evidently give new knowledge concerning the differences in microstructure formed during the conventional and lased induced crystallization the amorphous alloys. Further experiments are needed to clarify the effect of pulsed laser interference crystallization on magnetic properties of these alloys.
Źródło:
Archives of Foundry Engineering; 2018, 18, 2; 27-30
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Emotions and their cognitive and adaptive functions
Autorzy:
Janocha, A.
Shpakou, A.
Sobieszczańska, M
Kałka, D.
Klimatckaia, L.
Woźniak, W.
Pilecka-Radziszewska, K.
Małyszczak, K.
Powiązania:
https://bibliotekanauki.pl/articles/1918593.pdf
Data publikacji:
2018-06-18
Wydawca:
Uniwersytet Medyczny w Białymstoku
Tematy:
Classification of emotions
adaptation
cognition.
Opis:
Emotions appeared very early in phylogenetic and ontogenetic development. The word emotion originates from the Latin verb movere. However, attempts to distinguish and name the concept represented by the phrase emotion reach back to the beginnings of human language. The compound and subjective nature of emotions stress an essential aspect of this phenomenon, which leads to changes in physiological, psychological, and behavioral issues. World literature dedicates significant attention to the mutual associations between the cognitive and adaptive processes and emotions. Emotions help to estimate the adaptational meaning of stimuli. Its cognitive aspect is, however, just as significant. The review of the literature presented herein is an attempt to classify and evaluate particular emotions, both positive and negative, and the influence they have on physical and mental health. Paul Ekman, the author of one of the more esteemed classification attempts, has distinguished six basic emotions: anger, disgust, fear, happiness, sadness, and surprise. These universal emotions are recognized based on emotional facial expressions, the automatic reactions that unfold within microseconds. Robert Plutchik, on the other hand, devised his „emotion wheel” upon which he organized eight basic emotions by grouping them in pairs comprising a combination of positive and negative emotions. He is also the author of one of the best framed emotional combination theories. In this respect, emotions play a crucial role as compound model reactions to everyday situations such as a long-lasting effort ensuring survival and individual development.
Źródło:
Progress in Health Sciences; 2018, 8(1); 178-184
2083-1617
Pojawia się w:
Progress in Health Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
European integration influence on the development of human capital of small and medium enterprises in Poland
Autorzy:
Kacprzak, M.
Król, A.
Radziszewska, M.
Powiązania:
https://bibliotekanauki.pl/articles/29431706.pdf
Data publikacji:
2018
Wydawca:
Szkoła Główna Gospodarstwa Wiejskiego w Warszawie. Wydawnictwo Szkoły Głównej Gospodarstwa Wiejskiego w Warszawie
Źródło:
Zeszyty Naukowe Szkoły Głównej Gospodarstwa Wiejskiego w Warszawie. Problemy Rolnictwa Światowego; 2018, 18[33], 4
2081-6960
Pojawia się w:
Zeszyty Naukowe Szkoły Głównej Gospodarstwa Wiejskiego w Warszawie. Problemy Rolnictwa Światowego
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure, Chemical and Phase Composition of Clad Layers of Inconel 625 and Inconel 686
Autorzy:
Solecka, M.
Kopia, A.
Petrzak, P.
Radziszewska, A.
Powiązania:
https://bibliotekanauki.pl/articles/351519.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Inconel 625
Inconel 686
SEM
EDS
TEM
Opis:
The article presents the investigation results of microstructural, chemical composition changes after clad layers of Inconel 625 and Inconel 686 alloys weld overlaid on boiler tubes. The boiler tubes made of 16Mo3 steel were cladded in the Boiler Factory SEFAKO S.A. using CMT technique. The microstructure and chemical composition of coatings were analysed using light microscopy, scanning and transmission electron microscopy. The value of the partition coefficient k was determined for Inconel 625 and Inconel 686 clad layers. The value was calculated by dividing the average content (% wt.) of Ni, Cr, Mo, Fe, Nb and W.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 513-518
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Modification of the Structure and Properties of FeSiB Amorphous Ribbon by Interference Pulsed Laser Heating
Autorzy:
Czyż, O.
Kusiński, J.
Radziszewska, A.
Ostrowski, R.
Morgiel, J.
Kanak, J.
Kąc, M.
Powiązania:
https://bibliotekanauki.pl/articles/355908.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
laser heating
FeSiB
crystallization
magnetic properties
structure
Opis:
Paper describes the results of Fe80Si11B9 amorphous ribbon investigation after pulsed laser interference heating and conventional annealing. As a result of interference heating periodically placed laser heated microareas were obtained. Structure characterisation by scanning and transmission electron microscopy showed in case of laser heated samples presence of crystalline nanostructure in amorphous matrix. Microscopy observations showed significant difference in material structure after laser heating – nanograin structure, and material after annealing – dendritic structure. Magnetic force microscopy investigation showed expanded magnetic structure in laser heated microareas, while amorphous matrix did not give magnetic signal. Change of magnetic properties was examined by magnetic hysteresis loop measurement, which showed that the laser heating did not have a significant influence on soft magnetic properties.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 2001-2007
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Przyjazny dla środowiska recykling podkładów kolejowych
Autorzy:
Wojciechowski, A.
Doliński, A.
Radziszewska-Wolińska, J. M.
Wołosiak, M.
Powiązania:
https://bibliotekanauki.pl/articles/215104.pdf
Data publikacji:
2018
Wydawca:
Instytut Kolejnictwa
Tematy:
rozkład termiczny
odpady
zamknięty obieg materiałowy
GZO
olej kreozotowy
podkłady kolejowe
Opis:
Surowce mineralne i naturalne surowce energetyczne powinny być w większym stopniu zastępowane przez surowce wtórne pozyskane z odpadów poużytkowych i poprodukcyjnych, których ilość nieustannie wzrasta. Postulaty te są podstawą programu Wspólnoty: Zero Waste for Europe. Koncepcja gospodarki o obiegu zamkniętym powinna być również wdrożona w sektorze kolejowym w celu zapewnienia właściwego zagospodarowania odpadów oraz zapewnienia oszczędności energii i odzysku materiałów. W artykule przedstawiono kierunki działań technologicznych, mające zapewnić rozwój jednocześnie chroniąc środowisko i zasoby naturalne. Procesowi recyklingu powinny podlegać między innymi wyeksploatowane drewniane podkłady kolejowe impregnowane olejem kreozotowym powodujące największe problemy środowiskowe. Opisano zasady stosowania i wymagania dotyczące drewnianych elementów nawierzchni kolejowej nasycanych olejem kreozotowym. Przedstawiono także czynniki utrudniające kompleksowe podejście do recyklingu tych wyrobów. Scharakteryzowano procesy termicznego rozkładu odpadów organicznych metodą termolizy oraz właściwości pozyskanych produktów z wyeksploatowanych drewnianych podkładów kolejowych.
Źródło:
Problemy Kolejnictwa; 2018, 181; 63-70
0552-2145
2544-9451
Pojawia się w:
Problemy Kolejnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Quality Assessment of E-Commerce Service in the Context of Customer Expiriences
Autorzy:
Radziszewska, A.
Powiązania:
https://bibliotekanauki.pl/articles/2064961.pdf
Data publikacji:
2018
Wydawca:
STE GROUP
Tematy:
e-service quality
e-commerce
quality assessment
customer experiences
Opis:
With rapid growth of the Internet, companies adopted the new information and communication technology to offer e-services to their customers. This paper addresses e-service quality issue in the electronic marketplace. Service quality of e-retailers has been recognized as an important factor in determining success of e-commerce ventures. The objective of this research is to develop a theoretical, comprehensive, and measurable framework for assessing the quality of e-commerce services and to indicate factors, which are significant for customers satisfaction and high quality online shopping experiences. This paper reviewed the most recognized evaluation criteria, which are used in different e-commerce websites, and proposes a general comprehensive framework for evaluating the quality of any e-commerce service regarding to two main areas: website features and customer service in e-commerce platform. The detailed list of quality attributes in both assessment areas was derived from the reviewed literature. The survey and analysis described in this paper enable a better understanding of the influence these quality attributes on the main quality assessment categories. The results provide an important foundation for the understanding of quality in e-commerce services that will allow to assess the strengths and weaknesses of each e-commerce service. This paper concludes by discussing the findings of this study and highlighting areas for the future research.
Źródło:
Multidisciplinary Aspects of Production Engineering; 2018, 1, 1; 635--640
2545-2827
Pojawia się w:
Multidisciplinary Aspects of Production Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of microstructure and mechanical properties of laser-welded stainless steels
Charakterystyka struktury i właściwości mechanicznych złączy spawanych wiązką laserową stali nierdzewnych
Autorzy:
Koclęga, D.
Radziszewska, A.
Kąc, S.
Zowczak, W.
Dębowska, A.
Jędrusik, M.
Petrzak, P.
Powiązania:
https://bibliotekanauki.pl/articles/264238.pdf
Data publikacji:
2016
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
laser welding
stainless steel
microstructure
chemical composition
hardness
spawanie wiązką lasera
stal nierdzewna
mikrostruktura
skład chemiczny
twardość
Opis:
This work presents the laser welding of dissimilar X12CrCoWVNbN12-2-2 and X10CrNi18-10 steels. This system is of interest, as laser welding offers new flexibility in the joining of metals and laser welds (LWs) and are usually of high quality; they are obtained only after the optimization of process parameters. The aim of the work was to investigate the microstructure, chemical composition, and hardness changes of laser-welded steels. After laser welding, two zones were generated in the processed materials: a fusion zone and a heat-affected zone. Due to solidification, a refinement of the microstructure occurred in the fusion zone. Examinations of the chemical composition of particular melted areas showed the occurrence of Nb-rich precipitations. The laser welding of steels led to increased hardness in the fusion zone (about 240–530 HV0.3).
W pracy przedstawiono wyniki badań różnorodnych złączy spawanych wiązką laserową stali X12CrCoWVNbN12-2-2 i X10CrNi18-10. Zastosowanie wiązki laserowej jest wysoce użyteczne ze względu na nowe możliwości procesu wytwarzania i zwykle wysoką jakość złączy po optymalizacji procesu. Celem pracy była ocena mikrostruktury, składu chemicznego i zmian twardości w złączach spawanych wiązką lasera. Po procesie spawania zaobserwowano dwa główne obszary, tj. linię wtopienia i strefę wpływu ciepła. Podczas krystalizacji w obszarze przy linii wtopienia zaobserwowano rozdrobnienie struktury. Szczegółowa analiza składu chemicznego ujawniła występowania wydzieleń bogatych w Nb w obszarze metalu stopionego. Zaobserwowano, że spawanie laserowe prowadzi do wzrostu twardości w obszarze przy linii wtopienia.
Źródło:
Metallurgy and Foundry Engineering; 2016, 42, 4; 213-224
1230-2325
2300-8377
Pojawia się w:
Metallurgy and Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Erosive Wear of Inconel 625 Alloy Coatings Deposited by CMT Method
Autorzy:
Solecka, M.
Kopyściański, M.
Kusiński, J.
Kopia, A.
Radziszewska, A.
Powiązania:
https://bibliotekanauki.pl/articles/357042.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Inconel 625
erosion wear
solid particles erosion
alloys
Opis:
The article presents the investigation results concerning the determination of the characteristics of erosive wear caused by the impact of Al2O3 solid particles on the surface of Inconel 625 alloy after plastic working and the same material after weld cladding process using the CMT method. Erosion wear tests were performed at two temperatures: 20°C and 650°C. The erosion tests were conducted using the standard ASTM G76. A jet with a specified abrasive waight was directed to the surface of the tested material at an α impingement angle varied in the range of 30-90° at a velocity imparted to the abrasive by the medium, which was compressed air. The eroded surface was examined using a scanning electron microscope (SEM), while the depths of craters caused by the erosion tests were measured with an optical profilometer. The predominant mechanisms of the formation of mass losses during solid particle erosion were microcutting and microfissuring.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2B; 1201-1206
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fractography and Porosity Analysis of Cr and Cr-Mo PM Steels
Autorzy:
Kulecki, P.
Lichańska, E.
Radziszewska, A.
Sułkowski, M.
Powiązania:
https://bibliotekanauki.pl/articles/351712.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintered steels
alloying elements
porosity
fractography
mechanical properties
Opis:
The aim of the study was to evaluate the effect of processing variables on the porosity and fractography of Cr and Cr-Mo PM steels. The measurements were performed on sintered steels made from commercial Höganäs pre-alloyed powders: Astaloy CrA, Astaloy CrL and Astaloy CrM with two different carbon concentrations (0.2% and 0.6%) added in the form of ultra fine graphite powder grade C-UF. Following mixing in Turbula mixer for 30 minutes, green compacts were single-action pressed at 660 MPa according to PN-EN ISO 2740 standard. Sintering was carried out in a laboratory horizontal tube furnace at 1120°C and 1250°C for 60 minutes, in an atmosphere containing 5%H2 and 95%N2. After sintering, the samples were tempered at 200°C for 60 minutes in air. For porosity evaluation computer software was employed. Hitachi S-3500M SEM equipped with EDS (made by Noran) was employed for fracture analysis. The steel based on Astaloy CrM pre-alloyed powder is characterized by fine pores and good mechanical properties. When sintered at 1250°C, it had area of pores approx. 7.12 μm2, ultimate tensile strength (UTS) about 679 MPa and elongation about 4%. The steels were characterized by ductile/cleavage and ductile fractures.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 3; 1613-1622
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High-temperature corrosion of Ni-base alloys by waste incineration ashes
Autorzy:
Solecka, M.
Kusiński, J.
Kopia, A.
Rozmus-Górnikowska, M.
Radziszewska, A.
Powiązania:
https://bibliotekanauki.pl/articles/1112555.pdf
Data publikacji:
2016-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bh
68.47.Gh
68.37.Hk
61.05.cp
Opis:
Ni-Cr-Mo alloys, e.g. Inconel 625 and 686, exhibit high-temperature corrosion, oxidation and wear resistance. For this reason, these alloys are typically used as a coating material in different environments as effective solid-state diffusion barriers between the corrosive atmosphere and the base metal. To perform: the Ni-base weld overlays, without introducing too much Fe, a new welding technique called cold metal transfer was used. High-temperature corrosion of boiler parts during incineration of waste was investigated. Boiler tubes were coated with Inconel 625 and Inconel 686 nickel alloys and, after subjecting them to waste incineration ashes, they were examined by scanning electron microscopy with energy dispersive X-ray spectrometer to reveal different corrosion mechanisms and their causes. Results indicate a strong dependence of the boiler steel corrosion on anions in the incineration waste ash. X-ray diffraction characteristics of the scale showed that surface corrosion processes induce the formation of CrO₂, NiO. The presence of iron in the clad weld surface is conductive to the formation of the Fe₂O₃ oxide.
Źródło:
Acta Physica Polonica A; 2016, 130, 4; 1045-1048
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Chemical Composition of Fe-Cr Alloy Tempered in High Temperature and Atmosphere Containing Ar-SO2
Autorzy:
Radziszewska, A.
Kranzmann, A.
Dörfel, I.
Mosquera Feijoo, M.
Solecka, M.
Powiązania:
https://bibliotekanauki.pl/articles/354072.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
microstructure
high-temperature corrosion
X20Cr13 steel
Opis:
The paper presents the microstructure, chemical and phase composition of thin scale, obtained as a result of high-temperature corrosion of X20Cr13 stainless steel. Samples were exposed to gas atmosphere of the following composition: 0.25 vol.% of SO2 and 99.75 vol.% of Ar at 600 °C for 5 h. As a consequence, thin compact scale was formed on steel surface. This scale consisted of three different zones. An amorphous zone was formed close to steel surface. Then, nanocrystalline zone could be observed. Finally, larger grains were formed during the corrosion process. The analysis of the chemical composition revealed higher concentration of chromium near steel surface. In contrast, to chromium, the content of iron, increased near the scale surface. It was found out that the (Cr, Mn, Fe)5O12 phase appeared in the thin scale.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 3; 1607-1612
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Porous SiO2/HAp Coatings on Cp-Titanium Grade 1 Surfaces Produced by Electrophoretic Deposition
Autorzy:
Moskalewicz, T.
Babkiewicz, A.
Dubiel, B.
Kot, M.
Radziszewska, A.
Łukaszczyk, A.
Powiązania:
https://bibliotekanauki.pl/articles/356668.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
porous coating
corrosion resistance
electrophoretic deposition
Opis:
Porous hydroxyapatite doped SiO2 coatings were electrophoretically deposited (EPD) on commercially pure titanium. The influence of EPD parameters on coatings quality was investigated. Microstructural observation was done using transmission and scanning electron microscopy as well as X-ray diffractometry. The coatings consisted of spherical micro and nanocrystalline hydroxyapatite (HAp) as well as amorphous SiO2 nanoparticles. The coatings exhibited open porosity with pore diameter up to 1 μm and due to presence of nanoparticles high surface development. It was found that application of SiO2/HAp coating increase corrosion resistance of titanium in Ringer’s solution.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 4; 2177-2182
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Deposition Of Oxide And Intermetallic Thin Films By Pulsed Laser (PLD) And Electron Beam (PED) Methods
Osadzanie tlenkowych oraz międzymetalicznych cienkich filmów z wykorzystaniem lasera impulsowego (PLD) i wiązki elektronowej (PED)
Autorzy:
Kusiński, J.
Kopia, A.
Cieniek, Ł.
Kąc, S.
Radziszewska, A.
Powiązania:
https://bibliotekanauki.pl/articles/352325.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
PLD
PED
thin film
structure
doped oxides
cienki film
struktura
osadzanie
Opis:
In this work the pulsed laser deposition (PLD) and the pulsed electron beam deposition (PED) techniques were used for fabrication of Mo-Bi2O3, La1-xSrxCoO3, La1-xCaxCoO3 and Al-Mg thin films. An influence of ablation process basic parameters on the coatings structure and properties was discussed. Two types of laser ablation systems were applied: one equipped with a KrF excimer and second with a Q-switched Nd:YAG. Films were deposited on Si and MgO substrates. Scanning (SEM) and transmission (TEM) electron microscopy, atomic force microscopy (AFM) as well as X-ray diffraction (XRD) were used for structural analysis. Investigations focused on structure and chemical composition showed that smooth and dense thin films with nanocrystalline structure, preserving the composition of the bulk target, could be obtained by the both PLD and PED techniques. Research study showed that by a proper selection of PLD and PED process parameters it was possible to deposit films with significantly decreased amount and size of undesirably nanoparticulates.
Osadzanie laserem impulsowym (PLD) oraz osadzanie impulsową wiązka elektronową (PED) wykorzystane zostało do wytwarzania cienkich filmów typu: Mo-Bi2O3, La1-xSrxCoO3, La1-xCaxCoO3 and Al-Mg oraz Al-Mg. Dyskutowano wpływ podstawowych parametrów procesu ablacji na strukturę i właściwości uzyskiwanych powłok. Wykorzystane zostały dwa typy systemów do ablacji; jeden z ekscymerowym laserem KrF i drugi na bazie lasera Nd:YAG z modulatorem dobroci (Q-Switch). Filmy osadzano na podłożu Si i MgO. Skaningowa (SEM) i transmisyjna (TEM) mikroskopia elektronowa, mikroskopia sił atomowych (AFM), oraz dyfrakcja rentgenowska (XRD) wykorzystana została do analizy strukturalnej. Badania skoncentrowane na strukturze i składzie chemicznym wykazały jednorodną i zwartą budowę cienkich nanokrystalicznych filmów uzyskanych metodami PLD i PED utrzymujących skład odparowywanych tarcz. Wykazano doświadczalnie, że odpowiednie dobranie parametrów procesu pozwala otrzymywać filmy o istotnym zminimalizowaniu ilości i wymiarów niekorzystnych nanocząstek w powłoce.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 3; 2173-2182
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł

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