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Wyświetlanie 1-15 z 27
Tytuł:
Fabrication of Mo-Si-B Intermetallic Compound Powders Under Different Heat Treatment Conditions
Autorzy:
Park, J. H.
Lee, S.
Kim, D.
Kim, Y.
Yang, S. H.
Lee, S. H.
Powiązania:
https://bibliotekanauki.pl/articles/353369.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mo-Si-B alloys
intermetallic compounds
reitveld refinement
T2 phase
A15 phase
Opis:
In this research, we investigated the effects of reduction atmospheres on the creation of the Mo-Si-B intermetallic compounds (IMC) during the heat treatments. For outstanding anti-oxidation and elevated mechanical strength at the ultrahigh temperature, we fabricated the uniformly dispersed IMC powders such as Mo5SiB2 (T2) and Mo3Si (A15) phases using the two steps of chemical reactions. Especially, in the second procedure, we studied the influence of the atmospheres (e.g. vacuum, argon, and hydrogen) on the synthesis of IMCs during the reduction. Furthermore, the newly produced IMCs were observed by SEM, XRD, and EDS to identify the phase of the compounds. We also calculated an amount of IMCs in the reduced powders depending on the atmosphere using the Reitveld refinement method. Consequently, it is found that hydrogen atmosphere was suitable for fabrication of IMC without other IMC phases.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1509-1512
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Compression Properties of Fe-Cr-B Alloy Manufactured using Laser Metal Deposition
Autorzy:
Joo, Y.-A.
Yoon, T.-S.
Park, S.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352075.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-Cr-B composite
laser Metal Deposition
bulk type
microstructure
compressive properties
Opis:
Fe-Cr-B alloy is a material with precipitation of boride inside Fe matrix, and it features outstanding hardness and wear resistance properties. However, Fe-Cr-B alloy is a difficult material to process, making it difficult to use as a bulk type structure material which requires delicate shapes. This study attempted to manufacture Fe-Cr-B alloy using a 3D printing process, laser metal deposition. This study also investigated the microstructure, hardness and compression properties of the manufactured alloy. Phase analysis results is confirmed that α-Fe phase as matrix and (Cr, Fe)2B phase as reinforcement phase. In the case of (Cr, Fe)2B phase, differences were observed according to the sample location. While long, coarse, unidirectional needle-type boride phases (~11 μm thickness) were observed in the center area of the sample, relatively finer boride phases (~6 μm thickness) in random directions were observed in other areas. At room temperature compression test results confirmed that the sample had a compression strength is approximately 2.1 GPa, proving that the sample is a material with extremely high strength. Observation of the compression fracture surface identified intergranular fractures in areas with needle-type boride, and transgranular fractures in areas with random borides. Based on this results, this study also reviewed the deformation behavior of LMD Fe-Cr-B alloy in relation to its microstructures.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1459-1462
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Characterization of Metallic Fuel Slugs Prepared by Modified Injection Casting
Autorzy:
Mun, S.-U.
Kim, K.-H.
Oh, S.-J.
Park, J.-Y.
Hong, S.-I.
Powiązania:
https://bibliotekanauki.pl/articles/351428.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sodium-cooled fast reactor
metallic fuel slug
U-Zr alloy
surface characterization
injection casting
Opis:
Metallic fuel slugs containing rare-earth (RE) elements have high reactivity with quartz (SiO2) molds, and a reaction layer with a considerable thickness is formed at the surface of metallic fuel slugs. The surface characterization of metallic fuel slugs is essential for safety while operating a fast reactor at elevated temperature. Hence, it is necessary to evaluate the surface characteristics of the fuel slugs so that chemical interaction between fuel slug and cladding can be minimized in the reactor. When the Si element causes a eutectic reaction with the cladding, it deteriorates the metallic fuel slugs. Thus, it is necessary to examine the characteristics of the surface reaction layer to prevent the reaction of the metallic fuel slugs. In this study, we investigated the metallurgical characteristics of the surface reaction layer of fabricated U-10wt.%Zr-Xwt.%RE (X = 0, 5, 10) fuel slugs using injection casting. The results showed that the thickness of the surface reaction layer increased as the RE content of the metallic fuel slugs increased. The surface reaction layer of the metallic fuel slug was mainly formed by RE, Zr and the Si, which diffused in the quartz mold.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1049-1053
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The High Temperature Oxidation Stability of STS434L/Silicon Oxide Compacts
Autorzy:
Park, J. W.
Ko, B. H.
Jung, W. Y.
Park, D. K.
Ahn, I. S.
Powiązania:
https://bibliotekanauki.pl/articles/352481.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high-temperature oxidation stability
metallic oxide
densification
Opis:
In order to improve the high-temperature oxidation stability, a study of 434L sintered stainless steel was focused on the effect of addition of metallic oxides to form stable oxide film on the inner particle surface. In this paper, oxidation behavior of 434L compacted parts in accordance with the addition of metallic oxides were discussed with high temperature oxidative reaction, and sintering behavior analysis under 950°C. Oxidation weight gains of 434 L have increased as a form of parabolic laws. The hightemperature oxidation resistance was improved by the mixed addition of amorphous SiO2 and silica up to 2wt.%. The oxidation rate was decreased and kept constant after 60 hours. It was caused by the restraint succeeding oxidation due to the stable oxide formation of Cr2SiO4 phases on the particle surface to prevent densification and inhibition the external diffusion of Cr. High-temperature stability was confirmed by the electrical resistivity maintains the constant value of 1.3×10-2 Ω ·cm when the silica added less than 2w/o to 1w/o A-SiO2 added 434L.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 307-313
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Carbon Co-Deposition During Gas Reduction of Water-Atomized Fe-Cr-Mo Powder
Autorzy:
Ali, B.
Choi, S. H.
Seo, S. J.
Maeng, D. Y.
Lee, C. G.
Kim, T. S.
Park, K. T.
Powiązania:
https://bibliotekanauki.pl/articles/352709.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
water atomization
Fe-based powder
oxide reduction
powder metallurgy
sinter-hardening alloys
Opis:
The water atomization of iron powder with a composition of Fe-3Cr-0.5Mo (wt.%) at 1600°C and 150 bar creates an oxide layer, which in this study was reduced using a mixture of methane (CH4) and argon (Ar) gas. The lowest oxygen content was achieved with a 100 cc/min flow rate of CH4, but this also resulted in a co-deposition of carbon due to the cracking of CH4. This carbon can be used directly to create high-quality, sinter hardenable steel, thereby eliminating the need for an additional mixing step prior to sintering. An exponential relationship was found to exist between the CH4 gas flow rate and carbon content of the powder, meaning that its composition can be easily controlled to suit a variety of different applications.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1119-1124
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Fe Content on the Microstructure and Mechanical Properties of Ti-Al-Mo-V-Cr-Fe Alloys
Autorzy:
Bae, K.-C.
Oak, J.-J.
Kim, Y. H.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/351896.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti alloy
near-β titanium alloy
aircraft applications
structural material
landing gear
Opis:
To investigate the effect of Fe content on the correlation between the microstructure and mechanical properties in near-b titanium alloys, the Ti-5Al-5Mo-5V-1Cr-xFe alloy system has been characterized in this study. As the Fe content increased, the number of nucleation sites and the volume fraction of the α phase decreased. We observed a significant difference in the shape and size of the α phase in the matrix before and after Fe addition. In addition, these morphological deformations were accompanied by a change in the shape of the α phase, which became increasingly discontinuous, and changed into globular-type α phase in the matrix. These phenomena affected the microstructure and mechanical properties of Ti alloys. Specimen #2 exhibited a high ultimate tensile strength (1071 MPa), which decreased with further addition of Fe.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1105-1108
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Hafnium and Zirconium to Glass Forming Ability, Thermal Stability, Plasticity Deformation and Crystallization of Ni-Free Pentabasic Ti-Based Bulk Metallic Glasses
Autorzy:
Oak, J.-J.
Kim, Y. H.
Bae, K.-C.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/352087.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti-based alloy
metallic glass
Ti fiber
glass formability
plastic deformation
Opis:
The newly designed Ti-based bulk metallic glass (BMG) in which case of fracture behavior was observed 1990MPa to compressive strength with a wide plastic deformation around 7% after process of elastic deformation. This phenomenon can be compared with those of Ti-based alloys and other Ti-based BMGs and indicates high potential to be applied in use. It was evaluated the Ti-based BMG for thermal stability that the reduced glass parameters, ΔTx, Trg and γ, are 79K, 0.50 and 0.38, respectively. In addition, it reveals high activation energies for crystallization in which are estimated to Ex1 = 291.77 ±9.71 kJ/mol, Ex2 = 588.77 ±28.88 kJ/mol and Ex3 = 330.26 ±3.61 kJ/mol on kissinger plotting in this study.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1081-1087
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on Microstructure and Impact Toughness of Ti-6Al-4V Manufactured by Selective Laser Melting Process
Autorzy:
Lee, K.-A.
Kim, Y.-K.
Yu, J.-H.
Park, S.-H.
Kim, M.-C.
Powiązania:
https://bibliotekanauki.pl/articles/354570.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
selective laser melting
Ti-6Al-4V
microstructure
impact toughness
heat treatment
Opis:
This study manufactured Ti-6Al-4V alloy using one of the powder bed fusion 3D-printing processes, selective laser melting, and investigated the effect of heat treatment (650°C/3hrs) on microstructure and impact toughness of the material. Initial microstructural observation identified prior-β grain along the building direction before and after heat treatment. In addition, the material formed a fully martensite structure before heat treatment, and after heat treatment, α and β phase were formed simultaneously. Charpy impact tests were conducted. The average impact energy measured as 6.0 J before heat treatment, and after heat treatment, the average impact energy increased by approximately 20% to 7.3 J. Fracture surface observation after the impact test showed that both alloys had brittle characteristics on macro levels, but showed ductile fracture characteristics and dimples at micro levels.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1341-1346
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of a Spherical Titanium Powder by Combined Combustion Synthesis and DC Plasma Treatment
Autorzy:
Choi, S. H.
Ali, B.
Hyun, S. K.
Sim, J. J.
Choi, W. J.
Joo, W.
Lim, J. H.
Lee, Y. J.
Kim, T. S.
Park, K. T.
Powiązania:
https://bibliotekanauki.pl/articles/356067.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
combustion synthesis
DC plasma treatment
titanium powder
3D printing process
combustion parameters
Opis:
Combustion synthesis is capable of producing many types of refractory and ceramic materials, as well as metals, with a relatively lower cost and shorter time frame than other solid state synthetic techniques. TiO2 with Mg as reductant were dry mixed and hand compacted into a 60 mm diameter mold and then combusted under an Ar atmosphere. Depending on the reaction parameters (Mg concentration 2 ≤ α ≤ 4), the thermocouples registered temperatures between 1160°C and 1710°C . 3 mol of Mg gave the optimum results with combustion temperature (Tc) and combustion velocity (Uc) values of 1372°C and 0.26 cm/s respectively. Furthermore, this ratio also had the lowest oxygen concentration in this study (0.8 wt%). After combustion, DC plasma treatment was carried out to spheroidize the Ti powder for use in 3D printing. The characterization of the final product was performed using X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, and N/O analysis.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1057-1062
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of High-Strength Gray Cast Iron Using Permanent Magnet Scrap
Autorzy:
Park, S.-Y.
Kim, J. H.
Seo, S. J.
On, J. S.
Lim, K. M.
Powiązania:
https://bibliotekanauki.pl/articles/352204.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gray cast iron
rare earth element
Nd-Fe-B magnet scrap
graphite formation
microstructure
Opis:
In this study, we have developed the manufacturing technology for high strength gray cast irons by using the spent permanent magnet scraps. The cast specimen inoculated by using a spent magnet scraps showed the excellent tensile strength up to 306MPa. This tensile strength value is 50MPa higher than that of the specimen cast without inoculation, and is similar to that of the specimen inoculated by using the expensive misch-metal. These superior mechanical properties are attributed to complex sulfides created during solidification that promote the formation and growth of Type-A graphite. It is therefore concluded that spent magnets scrap can provide an efficient and cost-effective inoculation agent for the fabrication of high-performance gray cast iron.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1113-1117
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High Temperature Oxidation Property of SiC Coating Layer Fabricated by Aerosol Deposition Process
Autorzy:
Ham, G.-S.
Kim, S.-H.
Park, J.-Y.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352142.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silicon carbide
aerosol deposition
coating
high temperature oxidation
Opis:
This study investigated the high temperature oxidation property of SiC coated layer fabricated by aerosol deposition process. SiC coated layer could be successfully manufactured by using pure SiC powders and aerosol deposition on the Zr based alloy in an optimal process condition. The thickness of manufactured SiC coated layer was measured about 5 μm, and coating layer represented high density structure. SiC coated layer consisted of α-SiC and β-SiC phases, the same as the initial powder. The initial powder was shown to have been crushed to the extent and was deposited in the form of extremely fine particles. To examine the high temperature oxidation properties, oxidized weight gain was obtained for one hour at 1000°C by using TGA. The SiC coated layer showed superior oxidation resistance property than that of Zr alloy (substrate). The high temperature oxidation mechanism of SiC coated layer on Zr alloy was suggested. And then, the application of aerosol deposited SiC coated layer was also discussed.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1347-1351
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High-temperature Oxidation Behavior and Kinetics of Forged 12Cr-MoVW Steel
Autorzy:
Kim, Y. H.
Oak, J.-J.
Bae, K.-C.
Lee, W-J.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/351450.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ferritic/martensitic stainless steels
forging
oxidation kinetics
oxide layer
Opis:
The oxidation kinetics of forged 12Cr-MoVW steel was investigated in an air (N2+O2) atmosphere at 873-1073 K (Δ50 K) using thermogravimetric analysis. The oxidized samples were characterized using X-ray diffraction, and the surface and cross-sectional morphologies were examined using scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy. The forged 12Cr-MoVW steel samples exhibited parabolic behavior and a low oxidation rate compared with their as-cast counterparts. A protective oxide layer was uniformly formed at relatively low temperature (≤973 K) for the forged samples, which thus exhibited better oxidation resistance than the as-cast ones. These oxides are considered solid-solution compounds such as (Fe, Cr)2O3.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1099-1104
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
Autorzy:
Lee, H.-E.
Kim, Y. S.
Park, J. K.
Oh, S.-T.
Powiązania:
https://bibliotekanauki.pl/articles/355552.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high energy ball milling
Ni-base ODS superalloy
particle and crystalline size
microstructure
Opis:
Microstructure evolution of Ni-based oxide dispersion-strengthened alloy powders with milling time is investigated. The elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % were ball-milled by using horizontal rotary ball milling with the change of milling velocity. Microstructure observation revealed that large aggregates were formed in the early stages of ball milling, and further milling to 5 h decreased particle size. The average crystalline size, estimated by the peak broadening of XRD, decreased from 28 nm to 15 nm with increasing milling time from 1 h to 5 h. SEM and EPMA analysis showed that the main elements of Ni and Cr were homogeneously distributed inside the powders after ball milling of 5 h.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1253-1255
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Range resolution improvement of range-gated vision system in backscattering hazy environments
Autorzy:
Park, S.-K.
Choi, I.-Y.
Baik, S.-H.
Jeong, K.-M.
Powiązania:
https://bibliotekanauki.pl/articles/174523.pdf
Data publikacji:
2017
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
range-gated vision system
range image
windowed center-of-mass
cross-correlation
Gaussian window
Opis:
A range-gated vision system simultaneously provides two-dimensional and range images because its light intensity contains the reflectance as well as depth information. The range-resolution of the system is usually inversely proportional to the induced backscattering noise. In this paper, a range imaging technique is proposed to precisely measure range information from highly backscattering foggy environments. A windowed center-of-mass position extracted from the peak area of a cross-correlation signal of two signals, a Gaussian window signal in reduced size and a range-gated signal according to distance, is adopted as the range depth. The proposed measuring technique provides more robust and more precise range information than conventional measuring techniques for hazy targets by virtue of the reduction of backscattering bias noise usually induced by airborne particles. The experimental results and the signal processing procedures to acquire precise range information from hazy targets are described in this paper.
Źródło:
Optica Applicata; 2017, 47, 4; 533-543
0078-5466
1899-7015
Pojawia się w:
Optica Applicata
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sintering and Microstructures of SUS 316L Powder Produced by 3D Printing Process
Autorzy:
Kim, W. J.
Nguyen, H.-H.
Kim, H. Y.
Nguyen, M.-T.
Park, H. S.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/356018.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
3D printing
selective laser sintering
SUS 316L
flake powder
Opis:
Selective laser sintering (SLS) is a type of laminating sintering technique, using CO2 laser with (metal, polymer, and ceramic) powders. In this result, the flake SUS 316L was used to achieve a high porous product, and compare to spherical type. After SLS, the porosity of flake-type sample with 34% was quite higher than that of the spherical-type one that had only 11%. The surface roughness of the flake SLS sample were also investigated in both inner and surface parts. The results show that the deviation of the roughness of the surface part is about 64.40μm, while that of the internal one was about 117.65μm, which presents the containing of high porosity in the uneven surfaces. With the process using spherical powder, the sample was quite dense, however, some initial particles still remained as a result of less energy received at the beneath of the processing layer.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1215-1218
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 27

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