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Tytuł:
Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
Autorzy:
Son, S. H.
Park, S. C.
Kim, J. H.
Kim, Y. H.
Lee, M. S.
Ahn, J.-W.
Powiązania:
https://bibliotekanauki.pl/articles/352665.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrorefining
tin
electronic waste
recycling
high purity
elektrorafinacja
cyna
odpady elektroniczne
recykling
Opis:
The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure, morphology, and band gap of Ti-V-O mixed oxides processed by coprecipitation and calcination
Autorzy:
Park, M.
Lim, Y.
Sung, Y.
Kwak, D.
Lee, J.
Powiązania:
https://bibliotekanauki.pl/articles/1061893.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Hd
Opis:
Mixed oxides of Ti-V-O were co-precipitated by wet process using TiCl₄ and VOCl₃ as starting materials. As-precipitated gels were calcinated at 800°C for 4 hours in oxygen atmosphere. Effects of vanadium content on the structural evolution, morphology, and band gap of Ti-V-O oxides were investigated. Calcination has produced mixtures of TiO₂/VO₂/V₂O₅ oxides and has allowed formation of Ti_{1-x}V_{x}O₂. Lattice parameters of rutile TiO₂ were precisely measured to investigate vanadium substitution into single rutile phase of Ti_{1-x}V_{x}O₂ with varying vanadium content. As vanadium addition was increased, particles were coarsening rapidly during calcination. Band gap of the Ti-V-O oxides was measured using ultraviolet visible light spectrometer. A decrease of band gap down to 1.7 eV with the addition of maximum of 10 at.% of vanadium was measured, which is due to the formation of single phase of Ti_{1-x}V_{x}O₂ as well as the formation of metallic VO₂ or V₂O₅ particles.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 875-877
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sintering and Microstructures of SUS 316L Powder Produced by 3D Printing Process
Autorzy:
Kim, W. J.
Nguyen, H.-H.
Kim, H. Y.
Nguyen, M.-T.
Park, H. S.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/356018.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
3D printing
selective laser sintering
SUS 316L
flake powder
Opis:
Selective laser sintering (SLS) is a type of laminating sintering technique, using CO2 laser with (metal, polymer, and ceramic) powders. In this result, the flake SUS 316L was used to achieve a high porous product, and compare to spherical type. After SLS, the porosity of flake-type sample with 34% was quite higher than that of the spherical-type one that had only 11%. The surface roughness of the flake SLS sample were also investigated in both inner and surface parts. The results show that the deviation of the roughness of the surface part is about 64.40μm, while that of the internal one was about 117.65μm, which presents the containing of high porosity in the uneven surfaces. With the process using spherical powder, the sample was quite dense, however, some initial particles still remained as a result of less energy received at the beneath of the processing layer.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1215-1218
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pharmacokinetics and pharmacodynamics (PK/PD) of irbesartan in Beagle dogs after oral administration at two dose rates
Autorzy:
Carlucci, L.
Song, K.H.
Yun, H.I.
Park, H.J.
Seo, K.W.
Giorgi, M.
Powiązania:
https://bibliotekanauki.pl/articles/31017.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Opis:
Irbesartan (Irb) is an angiotensin II type 1 receptor antagonist widely used in humans to treat hypertension. Age-related diseases such as hypertension are increasingly being diagnosed in dogs and there is the need for new drugs. The PK/PD of Irb was tested in Beagle dogs. Ten healthy Beagles were orally administered two dose rates (2 and 5 mg/kg), according to a cross over study design. Blood collections for PK analysis and systolic blood pressure (SBP), heart and respiratory rate, mucous membranes colour, capillary refill time and temperature evaluations were performed at scheduled intervals. The drug plasma concentration was dose dependent. The dogs administered 5 mg/kg showed a significant reduction in SBP, while in those receiving 2 mg/kg, this parameter was minimally affected. A counter clockwise hysteresis showed no direct correlation between SBP and plasma concentrations. The minimum effective concentration was theorized to be within the range 550-800 ng/mL. Although further studies are necessary, 5 mg/kg seems to be the more appropriate dose to obtain a hypotensive effect in Beagle dogs.
Źródło:
Polish Journal of Veterinary Sciences; 2013, 16, 3
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oligonol prevented the relapse of dextran sulfate sodium-ulcerative colitis through enhancing Nrf2-mediated antioxidative defense mechanism
Autorzy:
Kim, K.-J.
Park, J.-M.
Lee, J.-S.
Kim, Y.S.
Kangwan, N.
Han, Y.-M.
Kang, E.A.
An, J.M.
Park, Y.K.
Hahm, K.-B.
Powiązania:
https://bibliotekanauki.pl/articles/69501.pdf
Data publikacji:
2018
Wydawca:
Polskie Towarzystwo Fizjologiczne
Tematy:
ulcerative colitis
inflammatory bowel disease
oxidative stress
oligonol
polyphenol
adaptive response
quinone oxidoreductase
relapse
nuclear factor-kappaB
tumour necrosis factor-alpha
Źródło:
Journal of Physiology and Pharmacology; 2018, 69, 3
0867-5910
Pojawia się w:
Journal of Physiology and Pharmacology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetic Response of Mn(III)F(salen) at Low Temperatures
Autorzy:
Park, J.
Risset, O.
Shiddiq, M.
Peprah, M.
Knowles, E.
Andrus, M.
Beedle, C.
Ehlers, G.
Podlesnyak, A.
Čižmár, E.
Nagler, S.
Hill, S.
Talham, D.
Meisel, M.
Powiązania:
https://bibliotekanauki.pl/articles/1368508.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ee
78.70.Nx
76.30.-v
75.10.Jm
Opis:
The low temperature magnetic response of Mn(III)F(salen), salen = $H_{14}C_{16}N_{2}O_{2}$, an S=2 linear-chain system, has been studied. Using a single crystal with the field applied perpendicular to the chain direction, torque magnetometry, down to 20 mK and up to 18 T, revealed a feature at 3.8 T when T ≤ 400 mK. ESR ( ≈200 GHz) studies, using single crystals at 4 K and in 5 T, have not detected any signal. In 10 mT, the temperature dependence of the susceptibility of powder-like samples can be reasonably fit when J/$k_{B}$=50 K and g=2. In addition, these data are unchanged for P ≤1.0 GPa. Using a randomly-oriented, powder-like, deuterated (12 of 14 H replaced by D) sample of 2.2 g at 270 mK, neutron scattering data, acquired with the Cold Neutron Chopper Spectrometer at the Spallation Neutron Source, show several well defined excitations that may be from the zero-field energy levels of antiferromagnetic S=2 spins with g=2, J/$k_{B}$=50 K, D/$k_{B}$=2.8 K, and E/$k_{B}$=0.5 K.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 228-229
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Frustrated zig-zag spin chains formed by hydrogen bonds in [Cu(H₂O)(OH)(tmen)]₂[Pd(CN)₄]·2H₂O
Autorzy:
Čižmár, E.
Orendáčová, A.
Orendáč, M.
Kuchár, J.
Feher, A.
Park, J.
Meisel, M.
Powiązania:
https://bibliotekanauki.pl/articles/1054768.pdf
Data publikacji:
2017-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.30.Et
76.30.-v
75.40.-s
Opis:
The magnetic properties of the novel dimeric compound [Cu(H₂O)(OH)(tmen)]₂[Pd(CN)₄]·2H₂O (tmen=N,N,N',N'-tetramethylethylenediamine) with modulated crystal structure were studied in the temperature range from 95 mK to 300 K. Magnetic measurements revealed a presence of weak antiferromagnetic exchange coupling in the compound. The temperature dependence of specific heat is characterized by the presence of a Schottky-like maximum at 0.47 K and a λ-anomaly at 0.28 K, indicating the formation of long-range order in the system. The comparison of the experimental data with theoretical predictions revealed the presence of antiferromagnetic intradimer exchange coupling J/k_{B}= -1.2 K and interdimer coupling of a similar strength mediated via hydrogen bonds between dimeric units forming a frustrated magnetic zig-zag chain structure.
Źródło:
Acta Physica Polonica A; 2017, 131, 4; 940-942
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation And Stabilization Of Silver Nanoparticles In Ethanol By Phosphinic Acid
Redukcja i stabilizacja nanocząstek srebra w etanolu przez kwas fosforowy
Autorzy:
Kim, J.-K.
Shim, H.-M.
Park, M. J.
Koo, K.-K.
Powiązania:
https://bibliotekanauki.pl/articles/356073.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silver
nanoparticle
kinetic analysis
phosphinic acid
reduction
srebro
nanocząstki
analiza kinetyczna
kwas fosforowy
redukcja
Opis:
Although phosphinic acid (H3PO2) has a powerful reduction potential, the reduction of silver ions by phosphinic acid salt has not yet been reported. In this work, colloidal silver has successfully synthesized by reducing silver ions in ethanol with phosphinic acid as a reducing agent. The effects of [AgNO3]/[H3PO2] ratios and reaction temperature were considered. Spherical silver nanoparticles with cubic structure were successfully prepared and their diameters were measured to be 8.5±0.9 nm − 11.3±0.2 nm. Half-life analysis showed that the reduction of silver ions proceeded with the reaction order of 1.30 on concentration of phosphinic acid and activation energy of 120.7 kJ/mol.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1293-1296
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of High-Strength Gray Cast Iron Using Permanent Magnet Scrap
Autorzy:
Park, S.-Y.
Kim, J. H.
Seo, S. J.
On, J. S.
Lim, K. M.
Powiązania:
https://bibliotekanauki.pl/articles/352204.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gray cast iron
rare earth element
Nd-Fe-B magnet scrap
graphite formation
microstructure
Opis:
In this study, we have developed the manufacturing technology for high strength gray cast irons by using the spent permanent magnet scraps. The cast specimen inoculated by using a spent magnet scraps showed the excellent tensile strength up to 306MPa. This tensile strength value is 50MPa higher than that of the specimen cast without inoculation, and is similar to that of the specimen inoculated by using the expensive misch-metal. These superior mechanical properties are attributed to complex sulfides created during solidification that promote the formation and growth of Type-A graphite. It is therefore concluded that spent magnets scrap can provide an efficient and cost-effective inoculation agent for the fabrication of high-performance gray cast iron.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1113-1117
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and performance of fly ash granule filter for trapping gaseous cesium
Autorzy:
Park, J. J.
Shin, J. M.
Yang, J. H.
Park, G. I.
Powiązania:
https://bibliotekanauki.pl/articles/147633.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
fabrication
gaseous cesium
granule filters
performance test
pyroprocessing
trapping
Opis:
Although a disk-type fly ash filter has shown a good performance in trapping gaseous cesium, it has difficulty in charging filters into a filter container and discharging waste filters containing radioactive cesium from a container by remote action. To solve the difficulty of the disk-type fly ash filter, five types of granule filters, including a ball type, tube type, and sponge-structure type have been made. Among them, the best filter type was chosen through simple crucible tests. The five types of granule filters packed into containers were loaded into five alumina crucibles of 50 cc. Five grams of CsNO3 was used as a gaseous cesium source. They were then placed in a muffle furnace and heated to 900°C and maintained for 2 hours. After the experiment, the weights of the cesium trapped filters were measured. Among the five types of granule filters, the sponge-structure type granule filter was the best, which has the highest trapping capacity of cesium. Its capacity is 0.42 g-Cs/g-filter. The chosen sponge-structure type granule filters and disk-type filters have been tested using a two-zone tube furnace. Cs volatilization and Cs trapping zones were maintained at 900 and 1000°C, respectively. Sixteen grams of CsNO3 was used as a gaseous cesium source. The cesium trapping profile of the sponge-structure type granule filters was almost similar to that of the disk-type fly ash filters. For both cases, cesium was successfully trapped within the third filter.
Źródło:
Nukleonika; 2015, 60, No. 3, part 2; 565-570
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Characterization of CoCrFeNiMn High Entropy Alloy Powder Processed by Gas Atomization
Autorzy:
Park, T. G.
Lee, S. H.
Lee, B.
Cho, H. M.
Choi, W. J.
Kim, B. S.
Shin, K. S.
Kim, T.-S.
Powiązania:
https://bibliotekanauki.pl/articles/353649.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high entropy alloy
gas atomization
spark plasma sintering
CoCrFeNiMn
Opis:
In this study, precisely controlled large scale gas atomization process was applied to produce spherical and uniform shaped high entropy alloy powder. The gas atomization process was carried out to fabricate CoCrFeNiMn alloy, which was studied for high ductility and mechanical properties at low temperatures. It was confirmed that the mass scale, single phase, equiatomic, and high purity spherical high entropy alloy powder was produced by gas atomization process. The powder was sintered by spark plasma sintering process with various sintering conditions, and mechanical properties were characterized. Through this research, we have developed a mass production process of high quality and spherical high entropy alloy powder, and it is expected to expand applications of this high entropy alloy into fields such as powder injection molding and 3D printing for complex shaped components.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1055-1059
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evolution Of Precipitate Morphology During Extrusion In Mg ZK60A Alloy
Ewolucja morfologii wydzieleń podczas wytłaczania stopu Mg ZK60A
Autorzy:
Park, J.
Jung, K. H.
Lee, G. A.
Kawasaki, M.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/356233.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnesium alloy
ZK60A
precipitation
extrusion
stopy magnezu
wydzielenia
wytłaczanie
Opis:
In this study, a continuously casted ZK60A magnesium alloy (Mg-Zn-Zr) was extruded in two different extrusion ratios, 6:1 and 10:1. The evolution of precipitates was investigated on the two extruded materials and compared with that of as-casted material. The microstructural analysis was performed by electron backscatter diffraction and transmission electron microscopy, and the compositional information was obtained using energy-dispersive X-ray spectroscopy. Several distinct morphologies of precipitates were observed, such as dot, rod, and disk shaped. The formation mechanisms of those precipitates were discussed with respect to the heat and strain during the extrusion process.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1423-1426
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Ti Powder Addition On The Fabrication Of TiO2 Nanopowders
Wpływ dodatku nanoproszku Ti na zagęszczanie i spiekanie nanoproszków TiO2
Autorzy:
Raihanuzzaman, R. M.
Park, H. Y.
Ghomashchi, R.
Kwon, T. H.
Son, H.-T.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/353186.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2 nanopowder
magnetic pulsed compaction
densification
sintering
nanoproszek Ti
magnetyczne zagęszczanie impulsowe
zagęszczanie
spiekanie
Opis:
Sintered samples of Ti added TiO2 nanopowders were fabricated by combined application of magnetic pulsed compaction (MPC) and sintering. The effect of Ti nano powder on density, shrinkage and hardness of the samples were investigated as part of the study. The optimum processing conditions were found to be around 0.5 GPa MPC pressure and 1450°C sintering temperature, illustrating maximum density, hardness and minimum shrinkage. High pressure compaction using MPC was found to enhance density with increasing MPC pressure up to 0.9 GPa, and significantly reduce the total shrinkage (about 16% in this case) in the sintered bulks compared to other general processes (about 18%). While sintered samples blended with micro Ti showed presence of microstructural cracks, the samples with 1-2% nano Ti had less or no cracks on them. Overall, the inclusion of nano Ti indicated improvement in mechanical properties of TiO2 nanopowders sintered preforms as opposed to micro Ti-added TiO2.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1473-1477
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on Microstructure and Impact Toughness of Ti-6Al-4V Manufactured by Selective Laser Melting Process
Autorzy:
Lee, K.-A.
Kim, Y.-K.
Yu, J.-H.
Park, S.-H.
Kim, M.-C.
Powiązania:
https://bibliotekanauki.pl/articles/354570.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
selective laser melting
Ti-6Al-4V
microstructure
impact toughness
heat treatment
Opis:
This study manufactured Ti-6Al-4V alloy using one of the powder bed fusion 3D-printing processes, selective laser melting, and investigated the effect of heat treatment (650°C/3hrs) on microstructure and impact toughness of the material. Initial microstructural observation identified prior-β grain along the building direction before and after heat treatment. In addition, the material formed a fully martensite structure before heat treatment, and after heat treatment, α and β phase were formed simultaneously. Charpy impact tests were conducted. The average impact energy measured as 6.0 J before heat treatment, and after heat treatment, the average impact energy increased by approximately 20% to 7.3 J. Fracture surface observation after the impact test showed that both alloys had brittle characteristics on macro levels, but showed ductile fracture characteristics and dimples at micro levels.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1341-1346
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development of Hydrophobic Surgical Forceps using Powder Injection Molding and Surface Treatment
Autorzy:
Park, D. Y.
Park, B. R.
Gal, C. W.
Lin, D.
Han, J. S.
Jeong, M.-S.
Bollina, R.
Hwang, W.
Park, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/352093.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powder injection molding
hydrophobic
debinding
sintering
surface treatment
Opis:
Hydrophobic surgical forceps of end-effectors for laparoscopic operations or minimally invasive surgery were developed through powder injection molding (PIM) and surface treatment. Processing conditions for mixing, debinding, and sintering were investigated to produce defect-free components. An optimum solid loading was determined by torque rheometry experiments. The optimized processing conditions for debinding and sintering were designed through the measurement of weight loss and shrinkage behavior by thermogravimetric analysis and dilatometry experiments. After producing the surgical forceps based on the optimized processing conditions via PIM, surface treatment was carried out to generate the hydrophobic structure on the surface.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 473-480
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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