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Wyświetlanie 1-15 z 17
Tytuł:
Dynamical analysis of stiffened plates under patch loading
Autorzy:
Srivastava, A. K. L.
Pandey, S. R.
Kumar, A.
Powiązania:
https://bibliotekanauki.pl/articles/265921.pdf
Data publikacji:
2013
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
metoda elementów skończonych
obciążenie krawędziowe
częstotliwość drgań
usztywniacz
FEM
partial edge loadings
buckling load
vibration frequency
stiffener
Opis:
The vibration characteristics of stiffened plates with cutouts subjected to in-plane partial edge loadings at one end at the plate boundaries are studied using the finite element method. Buckling loads and vibration frequencies are determined for different cutout ratios and extent of partial edge loading at one end. In the structural modelling, the plate and the stiffeners are treated as separate elements where the compatibility between these two types of elements is maintained. The main elegance of the formulation lies in the treatment of the stiffeners. The stiffeners can be placed anywhere within the plate element, and need not be placed on the nodal lines. The vibration characteristics are discussed and the results are compared with those available in the literature. Numerical results are presented for a range of cutout to plate size from 0 to 0.8.
Źródło:
International Journal of Applied Mechanics and Engineering; 2013, 18, 2; 537-553
1734-4492
2353-9003
Pojawia się w:
International Journal of Applied Mechanics and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Zero-Field Splitting Parameters of $Cr^{3+}$ in Lithium Potassium Sulphate at Orthorhombic Symmetry Site
Autorzy:
Pandey, S.
Kripal, R.
Powiązania:
https://bibliotekanauki.pl/articles/1400393.pdf
Data publikacji:
2013-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
76.30.-v
76.30.Fc
Opis:
The superposition model is used to investigate the crystal field parameters, $B_{kq}$ of $Cr^{3+}$ in lithium potassium sulphate. The zero field splitting parameters D and E are then determined using microscopic spin Hamiltonian theory and compared with the experimental values obtained by electron paramagnetic resonance. Both zero field splitting parameters D and E evaluated theoretically are in good agreement with the experimental values. The results suggest that the $Cr^{3+}$ ion occupies substitutional K^{+} site in lithium potassium sulphate.
Źródło:
Acta Physica Polonica A; 2013, 123, 1; 101-105
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Theoretical Analysis of Zero Field Splitting of $Mn^{2+}$ in Ammonium Oxalate Monohydrate
Autorzy:
Kripal, R.
Pandey, S.
Powiązania:
https://bibliotekanauki.pl/articles/1535738.pdf
Data publikacji:
2010-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
71.70.Ch
76.30.Fc
Opis:
The superposition model has been used to investigate the substitution of $Mn^{2+}$ in ammonium oxalate monohydrate. The zero field splitting parameters D and E calculated by the superposition model are compared with the experimental values $D_{exp}$ and $E_{exp}$, respectively, for $Mn^{2+}$ obtained by electron paramagnetic resonance. Both the zero field splitting parameters D and E calculated theoretically are in good agreement with the experimental values $D_{exp}$ and $E_{exp}$. The result indicates that the $Mn^{2+}$ ion substitutes for the $NH_4^{+}$ ion in ammonium oxalate monohydrate.
Źródło:
Acta Physica Polonica A; 2010, 118, 4; 629-632
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Modelling and optimization of temperature in orthopaedic drilling : An in vitro study
Autorzy:
Pandey, R. K.
Panda, S. S.
Powiązania:
https://bibliotekanauki.pl/articles/307028.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
analysis of variance
ANOVA
orthopaedic surgery
response surface methodology
Taguchi method
thermal osteonecrosis
analiza wariancji
chirurgia ortopedyczna
metoda Taguchi
Opis:
This present investigation uses the Taguchi and response surface methodology (RSM) for modelling and optimization of the temperature produced during bone drilling. The drilling of bone is a common procedure in orthopaedic surgery to produce hole for screw insertion to fixate the fracture devices and implants. A major problem which is encountered during such a procedure is the increase in temperature of the bone due to the plastic deformation of chips and the friction between the bone and the drill. The increase in temperature can result in thermal osteonecrosis which may delay healing or reduce the stability and strength of the fixation. The drilling experiments are conducted on poly-methyl-meth-acrylate (PMMA) (as a substitute for bone) using Taguchi’s L27 experimental design technique. The cutting parameters used are drill diameter, feed rate and cutting speed. The optimum cutting parameters for minimum temperature are determined by using S/N ratios and the effect of individual cutting parameters on temperature produced is evaluated using analysis of variance (ANOVA). A second-order model is established between the drilling parameters and temperature using RSM. The experimental results show that the drill diameter is the most significant drilling parameter affecting the temperature during drilling followed by cutting speed and feed, respectively. The values predicted and the values obtained from experiment are fairly close, which indicates that the developed RSM model can be effectively used to predict the temperature in orthopaedic drilling.
Źródło:
Acta of Bioengineering and Biomechanics; 2014, 16, 1; 107-116
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electro-Optical Behavior of Dye Doped Nematic Liquid Crystal
Autorzy:
Yadav, S.
Pandey, K.
Misra, A.
Manohar, R.
Powiązania:
https://bibliotekanauki.pl/articles/1505061.pdf
Data publikacji:
2011-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
64.70.M-
42.79.Kr
Opis:
We report electro-optical behavior of a dye doped nematic liquid crystal. The dye doped cells have shown some improvement in some parameters important for the display devices such as threshold voltage $(V_{th})$, splay elastic constant, rotational viscosity and response time. The suppression of screening effect improves the threshold voltage for the doped sample.
Źródło:
Acta Physica Polonica A; 2011, 119, 6; 824-828
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Leaching of Al-Based Polygrain Quasicrystalline and Related Crystalline Surfaces
Autorzy:
Yadav, T.
Mishra, S.
Pandey, S.
Singh, D.
Lowe, M.
Tamura, R.
Mukhopadhyay, N.
Srivastava, O.
McGrath, R.
Sharma, H.
Powiązania:
https://bibliotekanauki.pl/articles/1373698.pdf
Data publikacji:
2014-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.44.Br
81.16.Hc
61.66.Dk
68.37.Hk
Opis:
In the present investigation, we have studied leaching on polygrain Al-based quasicrystalline $(i-Al_{63}Cu_{25}Fe_{12})$ as well as crystalline (B2 phase; $Al_{55}Cu_{30}Fe_{15})$ alloy surfaces using a 10 mole NaOH solution. The surface was leached at varying times from 30 min to 8 h and subsequently characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and energy dispersive X-ray analysis. Leaching of the samples for 30 min generated a homogeneous layer. However further leaching for 1-8 h yielded nano-size particles on the surface. Spherical microstructure has been observed on the Al-Cu-Fe crystalline surface whereas on the quasicrystalline surface a petal-like microstructure appeared. The implications of the evolution of different microstructures in the context of structure, stability and activity are discussed. The results are compared with the microstructure of leached polygrained samples containing a mixture of different surface orientations.
Źródło:
Acta Physica Polonica A; 2014, 126, 2; 629-632
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Bioremediation of melanoidin contamination in distillery effluent using Aspergillus brasiliensis
Autorzy:
Singh, T.A.
Singh, T.
Singh, R.
Pandey, P.K.
Gaur, R.
Jamal, F.
Patel, S.K.
Bansal, S.
Powiązania:
https://bibliotekanauki.pl/articles/2097092.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
spent wash
effluent
melanoidin
bioremediation
decolorization
Opis:
The current investigation is the first report of utilization of Aspergillus brasiliensis for the decolorization of melanoidin in distillery effluent. The effluent generated from alcohol distilleries is one of the most complex wastewater with a high biological oxygen demand (BOD) and other organic, inorganic, and toxic constituents. The effluent contains melanoidin, a dark brown compound, which is difficult to remediate by using conventional technologies. The disposal of spent wash in the natural environment is hazardous and can deteriorate land and water resources. The decolorization of spent wash through physical and chemical methods remains unsuitable, and the only alternative to decolorize spent wash is biological treatment. In the current study, three fungal strains were isolated from the distillery waste and screened for their ability to decolorize melanoidin.The isolate RS2 exhibited maximum decolorization of 83% and was identified as Aspergillus brasiliensis. Its optimum growth temperature was 37EC, and the maximum efficiency was recorded after 120 h of incubation. Nutritional sources were investigated for the fungi showing the maximum decolorization of melanoidin, and starch and peptone were found to be the best carbon and nitrogen sources, respectively. At 1.5% starch concentration and 1.5% peptone concentration, the decolorization level attained was 87.45% and 88.74%, respectively. A. brasiliensis exhibited a high potential to decolorize melanoidin. The decolorization percentage was high, which makes this fungus a potential candidate for use at the industrial scale for the bioremediation of spent wash.
Źródło:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology; 2020, 101, 3; 205-213
0860-7796
Pojawia się w:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Assay of the Insensitive High Explosive FOX-7 by Non-Aqueous Titration
Autorzy:
Nandi, A. K.
Paramasivan, P.
Singh, S. K.
Mandal, A. K.
Pandey, R. K.
Powiązania:
https://bibliotekanauki.pl/articles/358156.pdf
Data publikacji:
2012
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
1,1-diamino-2,2-dinitroethene
FOX-7
non-aqueous titration
N,N-dimethylformamide
Opis:
A non-aqueous titration method was developed to assay the insensitive high explosive 1,1-diamino-2, 2-dinitroethene (FOX-7). The weak acidic nature of FOX-7 (pKa 10.6) was exploited in the assay method. The sample was dissolved in the protophilic solvent N, N-dimethylformamide and titrated against sodium methoxide solution in benzene/methanol using azo violet as indicator. FOX-7 samples obtained from regular batch operations were assayed by this method and the results were compared with that of a recrystallized sample. The method is simple, rapid and has good accuracy and precision.
Źródło:
Central European Journal of Energetic Materials; 2012, 9, 4; 343-352
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Grit Blasting and Thermal Spraying on Microstructure Evolution of P91 Weldment
Autorzy:
Thakare, J. G.
Pandey, C.
Mulik, R. S.
Mahapatra, M. M.
Narang, H. K.
Powiązania:
https://bibliotekanauki.pl/articles/947576.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
P91
HAZ
IC-HAZ
deformation zone
Opis:
In the present work, studies have been carried out on the variations in the microstructure and hardness of P91 base-metal and welded joint. This variations result from the grit blasting and thermal cycle experienced during the thermal spraying process. The microstructural effects have been analyzed in terms of the depth of the deformation zone. Scanning Electron Microscopy and Xray diffraction were used as characterization techniques. The grit blasting carried out prior to thermal spraying has resulted in the highest change in sub-surface hardness of the heat affected zone (HAZ). However, flame treatment further reduced the subsurface hardness of the heat affected zone. The depth of deformation zone was highest for inter-critical heat affected zone (IC-HAZ). The overall coating process resulted in an increase in subsurface hardness of various regions of HAZ and fusion zone (FZ). The base metal showed a 7% increase in subsurface hardness due to the overall coating process. The IC-HAZ showed maximum variation with 36% increase in subsurface hardness. The coarse grained heat affected zone (CG-HAZ) and FZ did not show any change in subsurface hardness. As a whole, the hardness and microstructure of the welded joint was observed to be more sensitive to the thermal spray coating process as compared to the base metal.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 1725-1734
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optimization of Ammonium Sulfamate Nitration for the Preparation of Ammonium Dinitramide
Autorzy:
Mandal, A. K.
Kunjir, G. M.
Singh, J.
Adhav, S. S.
Singh, S. K.
Pandey, R. K.
Bhattacharya, B.
Lakshmi Kantam, M.
Powiązania:
https://bibliotekanauki.pl/articles/358022.pdf
Data publikacji:
2014
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Opis:
The reaction kinetics for the preparation of ammonium dinitramide (ADN) is described. ADN is the ammonium salt of the dinitramide anion, and belongs to the group of inorganic oxidizers, mainly useful for energetic rocket propellant formulations, particularly for underwater applications. It is also a potential candidate to replace ammonium perchlorate (AP), in order to develop chlorine-free, green propellants. At HEMRL, ADN is prepared by the nitration of ammonium sulfamate (AS) using mixed acid, followed by hydrolysis, neutralization with ammonia (g) and rectification using solvent. The nitration of ammonium sulfamate (AS) is carried out at a subzero temperature of -40 ±1 °C. The yield of ADN is reliant on the formation of dinitramidic acid, an intermediate product formed during the hydrolysis step, and its stability is predominantly dependent upon the level of acidity and temperature of the reaction medium. Prior to these kinetics studies, process optimization of the nitration of ammonium sulfamate (AS) was performed and gave the final mole ratio of AS:HNO3:H2SO4. Since the nitration of AS is sensitive to temperature, the rate of reaction was studied at fixed temperatures with variation of time, keeping all of the other parameters, such as vessel volume, agitator speed, feed rate etc., constant. During these studies, predetermined quantities of ammonium sulfamate (AS) and mixed acid were allowed to react at a fixed temperature (-40 ±1 °C) for different reaction periods to generate the concentration profile of AS. Using this concentration profile, the reaction order and reaction rate constant were evaluated. In order to find the effect of temperature on the reaction rate and yield, experiments were conducted at other temperatures such as -30 and -50 °C. In the present studies, it was found that the optimum temperature of nitration is -40 ±1 °C and that the rate of reaction follows a pseudo second order process with rate constant 0.01113 (min-1)•(mol/L)-1. The reaction time evaluated for 55 to 60% conversion is about 70-80 minutes at -40 ±1 °C, based on this kinetics. The activation energy of AS nitration was found to be -4.6 kcal/mol, using the reaction kinetic data based on the temperature dependent rate equation derived from Arrhenius’s law.
Źródło:
Central European Journal of Energetic Materials; 2014, 11, 1; 83-97
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation and characterization of ultrafine RDX
Autorzy:
Pant, A.
Nandi, A. K.
Newale, S. P.
Gajbhiye, V. P.
Prasanth, H.
Pandey, R. K.
Powiązania:
https://bibliotekanauki.pl/articles/358126.pdf
Data publikacji:
2013
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
ultrafine RDX
drowning-out crystallization
BET surface area
SEM
mechanical and electrostatic spark sensitivity
Opis:
This paper describes the synthesis of ultrafine Hexogen (UF-RDX) of size <5μm by drowning-out crystallization. RDX was precipitated from acetone or dimethylformamide (DMF) solution by reducing the solvent power using either a miscible, non-aqueous antisolvent, n-hexane, or an aqueous antisolvent, water containing polyethylene glycol (PEG). Process parameters such as solvent/ antisolvent ratio, agitation, ultrasonication etc. were studied. UF-RDX was characterized for Brunauer-Emmett-Teller (BET) surface area, X-ray diffraction (XRD), Scanning Electron Microscope (SEM), Fourier Transform Infrared Spectroscopy (FT-IR), Differential Scanning Calorimetry (DSC) and sensitivity tests. In the case of the non-aqueous antisolvent, the precipitated RDX crystals were rod shaped of diameter <1 μm. For the aqueous antisolvent, oval shaped crystals (<5 μm) were precipitated. UF-RDX was found to be more sensitive to impact and less friction sensitive compared to production grade RDX (60-80 μm).
Źródło:
Central European Journal of Energetic Materials; 2013, 10, 3; 393-407
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Process Optimization for the Gas-Liquid Heterogeneous Reactive Crystallization Process Involved in the Preparation of the Insensitive High Explosive TATB
Autorzy:
Nandi, A. K.
Kshirsagar, A. S.
Thanigaivelan, U.
Bhattacharyya, S. C.
Mandal, A. K.
Pandey, R. K.
Bhattacharya, B.
Powiązania:
https://bibliotekanauki.pl/articles/358228.pdf
Data publikacji:
2014
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
TATB
TCTNB
amination
reaction crystallization
chloride impurity
particle size
Opis:
The thermally stable, insensitive, high explosive 1,3,5-triamino-2,4,6- trinitrobenzene (TATB) is manufactured by amination of 1,3,5-trichloro-2,4,6- trinitrobenzene (TCTNB) in toluene with NH3 gas. It is an isothermal, single-feed, semi-batch, gas-liquid heterogeneous, reaction crystallization process. The amination process is discussed by applying the chemical engineering methodology of mass transfer and reactive crystallization processes based on Two-Film Mass- Transfer (TFMT) theory. Kinetic expressions have been developed to define the chemical reactions as well as the physical phenomena (mass transfer) associated with this process. A single expression has been derived to explain the dependence of the ammonia consumption rate on various process parameters. Subsequently, the influence of various process parameters on the product quality (particle size and chloride impurity content) has been studied on the laboratory scale. Finally, the process has been established in the pilot plant, with optimized process conditions, to realize TATB of desired particle size and chloride content. The effects of feeding excess ammonia, and the presence of mercaptans/hydrogen sulphide impurities in poor quality toluene on the formation of certain undesirable by-products in TATB, are also discussed.
Źródło:
Central European Journal of Energetic Materials; 2014, 11, 1; 31-57
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation of Boric Acid by Surface Oxidation of Amorphous Boron Powder: Characterization and Quantitative Estimation
Autorzy:
Nandi, A. K.
Ghosh, M.
Newale, S. P.
Jadhav, A. J.
Prasanth, H.
Pandey, R. K.
Powiązania:
https://bibliotekanauki.pl/articles/358160.pdf
Data publikacji:
2012
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
amorphous boron powder
B2O3
boric acid
FTIR
SEM
EDX
Opis:
Amorphous Boron Powder (ABP) is used as a fuel in air breathing propulsion systems due to its high gravimetric and volumetric heat value. ABP is sensitive to air and undergoes slow oxidation during storage and handling, leading to the formation of a boric acid layer on the particle surface. This paper describes an analytical method for the estimation of boric acid in ABP. In-house samples obtained from the pilot plant of this laboratory, as well as commercial samples, were assayed for their boric acid content. The study is substantiated by characterization of the ABP samples by SEM with EDX and FTIR. The ageing characteristics of in-house boron powder was also studied.
Źródło:
Central European Journal of Energetic Materials; 2012, 9, 4; 387-398
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Assay of the Insensitive High Explosive 3-Nitro-1,2,4-triazol-5-one (NTO) by Acid-Base Titration
Autorzy:
Nandi, A. K.
Singh, S. K.
Kunjir, G. M.
Singh, J.
Mandal, A. K.
Pandey, R. K.
Powiązania:
https://bibliotekanauki.pl/articles/358351.pdf
Data publikacji:
2013
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
NTO
purity
acid-base titration
HPLC
quality control
Opis:
The insensitive high explosive 3-nitro-1,2,4-triazol-5-one (NTO) is a weak acid (pKa 3.76) due to the labile N–H bond. The weakly acidic character of this compound is exploited for its assay by aqueous acid-base titration. The NTO sample was dissolved in water and the resultant solution was titrated against 0.07 N NaOH solution using phenolphthalein as indicator. Regular batch samples were assayed by this method and the results were compared with those obtained by the HPLC method. The aqueous acid-base titration method was found to be suitable for the quality control of the product.
Źródło:
Central European Journal of Energetic Materials; 2013, 10, 1; 113-122
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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