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Tytuł:
Zastosowanie obrazowania autofluorescencyjnego w diagnostyce chorób jelita grubego ‒ aktualny stan wiedzy
The usefulness of autofluorescense imaging in the diagnosis of colorectal diseases ‒ current state of knowledge
Autorzy:
Strzelczyk, N.
Kwiatek, S.
Latos, W.
Sieroń, A.
Stanek, A.
Powiązania:
https://bibliotekanauki.pl/articles/261397.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Wydział Podstawowych Problemów Techniki. Katedra Inżynierii Biomedycznej
Tematy:
obrazowanie autofluorescencyjne
wskaźnik wykrywania gruczolaków
rak jelita grubego
wrzodziejące zapalenie jelita grubego
chłoniak jelita grubego
autofluorescence imaging
adenoma detection rate
colorectal cancer
colitis ulcerosa
colorectal lymphoma
Opis:
Kolonoskopia światła białego jest złotym standardem w diagnostyce chorób jelita grubego, jednak wciąż poszukiwane są metody, które umożliwią szybsze i bardziej precyzyjne stawianie rozpoznań. Jedną z tych metod jest obrazowanie autofluorescencyjne. Wykorzystuje ono zjawisko wzbudzania przez światło endogennie występujących w tkankach fluoroforów. Tkanki nowotworowe i zmienione zapalnie wykazują odmienną autofluorescencję niż tkanki zdrowe, co pozwala na ich różnicowanie. Istnieje wiele prac wykazujących korzyści z zastosowania autofluorescencji w diagnostyce chorób jelita grubego. Zwiększa ona współczynnik wykrywania polipów, umożliwia ocenę charakteru histopatologicznego zmiany w trakcie kolonoskopii, zwiększa dokładność oceny stopnia nasilenia wrzodziejącego zapalenia jelita grubego oraz ułatwia wykrywanie ognisk neoplazji u pacjentów z nieswoistymi zapaleniami jelit, a także zwiększa wykrywalność zmian o charakterze chłoniaka. Obrazowanie autofluorescencyjne przyczynia się do szybkiego i precyzyjnego postawienia rozpoznania oraz wcześniejszego włączenia odpowiedniego leczenia.
White light colonoscopy is the gold standard in the diagnostics of colorectal diseases, however new methods that will allowed faster and more precise diagnosis are still sought. One of these methods is autofluorescence imaging. It uses the phenomenon of light excitation of endogenous fluorophores in tissues. Autofluorescence of normal tissue differs from that characteristic of inflamed or neoplastic tissues, which allows their differentiation. There are many studies showing the benefits of autofluorescence imaging in the diagnosis of colon diseases. It improves polyp detection rate, makes it possible to assess histopathological severity of the lesion during colonoscopy, improves the evaluation of ulcerative colitis severity, facilitates the detection of colorectal neoplasia in patients with inflammatory bowel disease, and improves the detection of lymphoma lesions. Autofluorescence imaging contributes to the fast and precise diagnosis and the early initiation of appropriate treatment.
Źródło:
Acta Bio-Optica et Informatica Medica. Inżynieria Biomedyczna; 2018, 24, 1; 40-48
1234-5563
Pojawia się w:
Acta Bio-Optica et Informatica Medica. Inżynieria Biomedyczna
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
X-Ray Absorption Near Edge Structure and Mössbauer Spectroscopy in Study of Iron Valence States in Tissues
Autorzy:
Dziedzic-Kocurek, K.
Banaś, A.
Kwiatek, W. M.
Stanek, J.
Powiązania:
https://bibliotekanauki.pl/articles/2044673.pdf
Data publikacji:
2006-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.18.Fs
61.10.Ht
Opis:
X-ray absorption near edge structure Fe K-edge spectra and $\text{}^{57}$Fe Mössbauer spectra of selected standard compounds were recorded at room temperature. Valence and spin states of Fe in these samples known from Mössbauer spectroscopy were correlated with the shapes of X-ray absorption near edge structure spectra in search of possible application of X-ray absorption near edge structure spectroscopy as analytical tool determining local electronic states of iron in tissues. As an example, the X-ray absorption near edge structure spectra of healthy and cancerous tissues of prostate are shown, suggesting Fe$\text{}^{3+}$ in cancerous tissues.
Źródło:
Acta Physica Polonica A; 2006, 109, 3; 341-345
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Study of Human Osteoblast-Like MG 63 Cells Proliferation on Resorbable Polymer-Based Nanocomposites Modified with Ceramic and Carbon Nanoparticles
Autorzy:
Wiecheć, A.
Stodolak-Zych, E.
Frączek-Szczypta, A.
Błażewicz, M.
Kwiatek, W.
Powiązania:
https://bibliotekanauki.pl/articles/1490257.pdf
Data publikacji:
2012-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
82.35.Np
87.17.Ee
Opis:
Polymer-based nanocomposites containing biocompatible and bioactive nanocomponents seem to be excellent materials that could be used in many biomedical applications. The aim of this study was biological evaluation of resorbable polymer-based nanocomposites (PLA, PCL) and their modifications with ceramic nanoparticles (silica - $SiO_2$, montmorillonite - MMT) or carbon nanotubes. The nanocomposites were seeded with the human osteoblast-like MG 63 cells. After 1, 3 and 7 days of incubation, Trypan blue exclusion test was used to determine the viability and number of cells. The cell population density depending on incubation time and cell population doubling time was calculated. The cell proliferation abilities on the all applied nanocomposites and on control material (polystyrene cell culture plate) were also compared. The number of cells growing on the nanocomposite surfaces increased with the incubation time. The cell viability was not decreased for all applied materials during the entire study (97-100%). The ceramic nanoparticles and carbon nanotubes modified the bone cell growth and proliferation rate. Results of this study confirm that all types of the nanocomposites are appropriate to the growing and proliferation of human osteoblast-like cells.
Źródło:
Acta Physica Polonica A; 2012, 121, 2; 546-550
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synchrotron Radiation Induced X-Ray Emission - SRIXE
Autorzy:
Kwiatek, W.
Powiązania:
https://bibliotekanauki.pl/articles/1920883.pdf
Data publikacji:
1992-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.En
87.15.Mi
Opis:
The synchrotron radiation induced X-ray emission (SRIXE) technique was found very useful and sensitive for determination of trace elements content and distribution in different types of materials. Due to properties of synchrotron radiation the SRIXE technique became very unique and powerful for trace elements analysis. This paper describes the phenomena related to production of characteristic X-rays and principles of the method. The properties of SRIXE such as minimum detectable limit, spatial resolution, radiation damage, and depth sensitivity are also discussed. Selected applications are given to emphasize the usefulness of the technique.
Źródło:
Acta Physica Polonica A; 1992, 82, 2; 263-271
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Study of Selected Biomaterials Using Vibrational Spectroscopy
Autorzy:
Paluszkiewicz, C.
Kwiatek, W.
Długoń, E.
Wesełucha-Birczyńska, A.
Piccinini, M.
Powiązania:
https://bibliotekanauki.pl/articles/1809387.pdf
Data publikacji:
2009-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.64.km
87.64.kp
87.64.Ee
87.85.jf
Opis:
Vibrational spectroscopy has been extensively used for in vitro and in vivo investigations of degradation mechanism and kinetics of different biomedical materials as well as it has been used to characterize the crystalline and amorphous domains in bio-mineralization process. Infrared and Raman spectroscopy methods are valuable tools in the biomaterials engineering allowing to study processes occurring during their preparation. In vitro tests, where the materials are immersed in simulated body fluids and/or artificial saliva, were used to evaluate the biocompatibility of biomaterials. This kind of tests are a wide range of repeatable and reproducible methods, which are regulated by international standards for commercial use and scientific development of new materials and products. The aim of this work was to examine phase composition of materials applied in dentistry. The bioactivity of such biomaterials was studied by immersing the samples in synthetic body fluid and artificial saliva. The changes were determined by the Fourier transform infrared and Raman microspectroscopy as well as scanning electron microscopy. It was found that results obtained by vibrational spectroscopy show the differences between the studied samples. Chemical reactions occurring during incubation of cements in artificial saliva as well as in synthetic body fluid result in formation of phosphates which deposit on the cement surface.
Źródło:
Acta Physica Polonica A; 2009, 115, 2; 533-536
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sulphur XANES Analysis of Cultured Human Prostate Cancer Cells
Autorzy:
Kwiatek, W.
Podgórczyk, M.
Paluszkiewicz, Cz.
Balerna, A.
Kisiel, A.
Powiązania:
https://bibliotekanauki.pl/articles/1812260.pdf
Data publikacji:
2008-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.64.kd
87.19.xj
Opis:
Prostate cancer is one of the most commonly diagnosed cancers in men throughout the world. It is believed that changes to the structure of protein binding sites, altering its metabolism, may play an important role in carcinogenesis. Sulphur, often present in binding sites, can influence such changes through its chemical speciation. Hence there is a need for precise investigation of coordination environment of sulphur. X-ray absorption near edge structure spectroscopy offers such possibility. Cell culture samples offer histologically well defined areas of good homogeneity, suitable for successful and reliable X-ray absorption near edge structure analysis. This paper presents sulphur speciation data collected from three different human prostate cancer cell lines (PC-3, LNCaP and DU-145). Sulphur X-ray absorption near edge structure analysis was performed on K-edge structure. The spectra of cells were compared with those of cancerous tissue and with organic substances as well as inorganic compounds.
Źródło:
Acta Physica Polonica A; 2008, 114, 2; 463-470
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Rozkład wybranych metali ciężkich w osadach dennych Zbiornika Dobczyckiego
Distribution of heavy metals in sediments of Dobczyce reservoir
Autorzy:
Reczynski, W.
Kwiatek, W.M.
Kubica, B.
Golas, J.
Jakubowska, M.
Niewiara, E.
Dutkiewicz, E.
Stobinski, M.
Skiba, M.
Powiązania:
https://bibliotekanauki.pl/articles/15167.pdf
Data publikacji:
2006
Wydawca:
Uniwersytet Warmińsko-Mazurski w Olsztynie / Polskie Towarzystwo Magnezologiczne im. Prof. Juliana Aleksandrowicza
Tematy:
zbiornik Dobczyce
osady denne
metale ciezkie
pojemnosc sorpcyjna
stezenie pierwiastkow
arsen
kadm
chrom
miedz
Opis:
Osady denne stanowią istotny składnik środowiska wodnego, akumulując składniki mineralne, w tym metale ciężkie. Zbiornik Dobczycki, będąc rezerwuarem wody pitnej dla aglomeracji krakowskiej, spełnia bardzo ważną funkcję gospodarczą. W badaniach osadów dennych Zbiornika Dobczyckiego wykonano analizę wierzchniej ich warstwy w 17 punktach pomiarowych. Pozwoliło to na opisanie dystrybucji metali w czaszy zbiornika oraz ocenę czynników warunkujących tę dystrybucję. Analizę wykonano dwoma metodami: metodą atomowej spektrometrii absorpcyjnej oraz metodą PIXE. Stwierdzono, z wykorzystaniem narzędzi statystycznych, że ze względu na stężenie metali, punkty poboru próbek można podzielić na dwie grupy: leżące poza dawnym nurtem rzeki Raby (niższe stężenia metali ciężkich) oraz usytuowane w dawnym nurcie rzeki (wyższe stężenia). Odpowiada to zmieniającym się właściwościom sorpcyjnym osadów, zależnym m.in. od uziarnienia, składu chemicznego i mineralnego oraz zawartości materii organicznej. Zastosowanie metody PIXE umożliwiło wykonanie wielopierwiastkowej analizy składu bez wstępnej procedury przygotowania próbek, z wystarczającą czułością oznaczeń, lecz mniejszą precyzją niż metoda ASA. Metody te mogą być komplementarne z punktu widzenia potrzeb analiz środowiskowych.
Sediments constitute important part of water systems, accumulating mineral compounds, such as heavy metals. Dobczyce Reservoir, being the main drinking water source for the city of Krakow, is important from the economical point of view. In the present research, analysis of elemental composition of sediment samples (upper 10 cm layer) in 17 sampling points was performed. It enabled us to analyse distribution of analysis of elements in Dobczyce Reservoir and to assess what factors influenced that distribution. The analysis was carried out by means of two instrumental methods, namely PIXE and ASA. Based on the statistical analysis of the results, it was found that all the sampling points could be divided into two groups – one situated out of the Raba river current (characterized by lower concentration of elements) and the other along the river current (higher concentration of elements). Such a division results from the differences in chemical and mineralogical composition of sediments as well as from their organic matter content and physical properties. The use of PIXE method makes it possible to analyze sediments in a multielemental mode without sample pretreatment, obtaining satisfactory sensitivity but less precision than with the use of AAS method. Both methods could be considered as complementary in environmental analysis.
Źródło:
Journal of Elementology; 2006, 11, 3
1644-2296
Pojawia się w:
Journal of Elementology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preliminary Study on Chemical Speciation of Sulphur in Cancerous Tissues
Autorzy:
Kwiatek, W. M.
Banaś, A.
Banaś, K.
Kisiel, A.
Cinque, G.
Falkenberg, G.
Powiązania:
https://bibliotekanauki.pl/articles/2044744.pdf
Data publikacji:
2006-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.64.Gb
Opis:
Sulphur is vital for almost all living organisms by participating in a wide variety of metabolic processes. Nevertheless its biochemistry is only partially understood, due to it a few tools such as X-ray absorption near edge structure may be used to determine its chemical speciation in biological system. In this paper we focused on analysis of composition and elemental distribution in tissue structures of biological samples. We examined cancerous and non-cancerous prostate tissues. Experiments were carried out on the L-beam line at the HASYLAB, DESY (Hamburg, Germany) and DAΦNE-Light Facility at the Laboratori Nationali di Frascati (Frascati, Italy). Synchrotron radiation induced X-ray emission measurements reveal the significant differences in concentration of sulphur between cancerous and non-cancerous tissues. X-ray absorption near edge structure spectra show two main types of sulphur that are represented by X-ray peaks at 2476 eV and 2484 eV. This suggests that different sulphur components are present in the measured samples.
Źródło:
Acta Physica Polonica A; 2006, 109, 3; 383-387
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preliminary Investigations of Elemental Content, Microporosity, and Specific Surface Area of Porous Rocks Using PIXE and X-ray Microtomography Techniques
Autorzy:
Bielecki, J.
Bożek, S.
Dutkiewicz, E.
Hajduk, R.
Jarzyna, J.
Lekki, J.
Pieprzyca, T.
Stachura, Z.
Szklarz, Z.
Kwiatek, W.
Powiązania:
https://bibliotekanauki.pl/articles/1490118.pdf
Data publikacji:
2012-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.70.Tx
91.65.-n
47.56.+r
Opis:
Determination of physical properties of porous geological materials is of great importance for oil industry. The knowledge of rocks properties is usually obtained from porosity studies such as pore size distribution, specific surface area determination, and hydrodynamic permeability calculations. This study describes determination of elemental composition and measurements of the particular physical properties of geological samples (porous sandstone rocks) by means of the nuclear and X-ray microprobes at the Institute of Nuclear Physics, Polish Academy of Sciences in Kraków, Poland. The special emphasis has been put on the computed microtomography method. Measurements have been carried out in close cooperation with Department of Geophysics, FGGEP AGH in Kraków, Poland. Chemical composition of the Rotliegend sandstone rock samples (few millimeters diameter), extracted from a borehole at 2679.6 m, 2741.4 m and 2742.4 m depth have been investigated using the 2.2 MeV proton beam (proton induced X-ray emission technique). Next, measurements of the porosity and the specific surface area of the pore space have been carried out using the X-ray microtomography technique. Basing on microtomographic data obtained with the high spatial resolution, simulations of the fluid dynamic in the void space of porous media have been carried out. Lattice Boltzmann method in the 3DQ19 geometrical model has been used in order to predict the hydraulic permeability of the media. In order to avoid viscosity-permeability dependence the multiple-relaxation-time model with half-way bounce back boundary conditions has been used. Computing power-consuming processing has been performed with the use of modern grid infrastructure.
Źródło:
Acta Physica Polonica A; 2012, 121, 2; 474-479
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Monitoring port regulations and traffic violations on the Szczecin-Swinoujscie fairway
Autorzy:
Uchacz, W.
Kwiatek, T.
Powiązania:
https://bibliotekanauki.pl/articles/320960.pdf
Data publikacji:
2000
Wydawca:
Polskie Forum Nawigacyjne
Tematy:
porty
żegluga
port
port regulations
Opis:
In this paper a method of utilising expert system technology for monitoring violations of chosen port regulations on the Szczecin-Swinoujście fairway is presented. The new algorithm developed by authors has been implemented into the program NEXPERT OBJECT. Information contained in this article may be useful while dealing with problems of decision support in VTS systems.
Źródło:
Annual of Navigation; 2000, 2; 143-157
1640-8632
Pojawia się w:
Annual of Navigation
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Trace Element Concentration in Diabetic Rats Tissues
Autorzy:
Kowalska, J.
Krośniak, M.
Gryboś, R.
Kwiatek, W.
Powiązania:
https://bibliotekanauki.pl/articles/1809705.pdf
Data publikacji:
2009-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
29.30.Ep
78.70.En
87.19.X-
Opis:
Diabetes is one of the most frequent diseases in developing countries and thus there is a significant interest in diabetes related studies. It was found that vanadium compounds have glucose-lowering properties in diabetes and therefore it is very important to estimate the vanadium dose in diabetes treatment. On the other hand, the proper estimation of vanadium concentration is important due to side effects that occur in vanadium supplementation. In this study the influence of V(IV) and V(V) compounds with different ligands on the concentration of K, Ca, Mn, Fe, Cu, and Zn in selected rat's tissues was investigated by means of proton induced X-ray emission technique. As a result of the measurements it was found that the concentration of vanadium depends on the organ. The highest value was determined in spleen while the lowest in pancreas. It was also found that the concentration of other elements depends on the presence of vanadium and its concentration. The most meaningful influence of vanadium presence was on iron concentration in spleen, on copper and zinc in kidney, and on manganese in pancreas.
Źródło:
Acta Physica Polonica A; 2009, 115, 2; 556-560
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Sediments Causing Damage to Water Meters in a Large Drinking Water Distribution System
Autorzy:
Kopeć, M.
Roman, M.
Kąc, M.
Budziak, A.
Paluszkiewicz, C.
Zarzycki, A.
Kąc, S.
Dutkiewicz, E.
Cichoń, T.
Bochnia, T.
Kwiatek, W.
Powiązania:
https://bibliotekanauki.pl/articles/1030652.pdf
Data publikacji:
2018-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
89.60.-k
78.70.En
61.05.cp
82.80.-d
82.80.Gk
Opis:
Preliminary studies on the sediments collected from water meters of Krakow water supply system were performed in the cooperation with the Municipal Water Supply and Sewage. Creation and deposition of sediments on the measuring devices installed in the water supply system is a serious technological and economical problem for water companies, defectively operating for this reason water meters must be replaced. It is evident that knowledge of the chemical and phase composition of sediments is an important step towards resolving the problem of impurities in water supply systems. Four different samples of sediments, coming from water meters, were investigated using the proton-induced X-ray emission, the X-ray diffraction, the Fourier transform infrared and Raman spectroscopy. The X-ray methods revealed presence of amorphous and fine-crystalline phases as well as high content of iron-based compounds. As a crystalline phase, the most frequently appeared: goethite, lepidocrocite, iron oxides (hematite, maghemite, magnetite), calcium carbonate, and quartz. In one of the samples, the nanocrystalline phase was found and identified as hydrous iron oxyhydroxide ferrihydrite. Vibrational spectroscopy methods confirmed the composition of crystalline phases as well as enabled to estimate the abundance of amorphous phase in samples.
Źródło:
Acta Physica Polonica A; 2018, 133, 2; 296-301
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Infrared Spectroscopy in Molecular Study of the Piezoelectric Effect in Pigs Shin Bone
Autorzy:
Lipiec, E.
Kowalska, J.
Wiecheć, A.
Zieliński, P.
Kwiatek, W.
Iwaniec, M.
Powiązania:
https://bibliotekanauki.pl/articles/1490248.pdf
Data publikacji:
2012-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.30.Jw
07.57.Ty
77.65.-j
87.50.ct
Opis:
Despite growing number of literature demonstrating the piezoelectric effect in bones at macro level there's still a lack of papers describing this effect at molecular level. In order to examine this effect more specifically, a study has been conducted to show the possibility of using infrared spectroscopy on samples contained in the electric field. This is the first known research on applying infrared spectroscopy to study the influence of electric field and compressive stress on bones' structure represented by the molecular IR spectrum. The samples used in this experiment as a model were prepared in pellet form, made from powdered pig's shin bone mixed with KBr (mass ratio of about 1:100). The spectra were obtained in transmission mode. Three different types of experiments were performed at each sample, which were subjected to: (a) fixed electric field (E < 40 kV/m), (b) variable electric field (0-40 kV/m), (c) compressive stress (P < 100 MPa). The obtained data have shown that the electric field and compressive stress on sample modified infrared spectra of the bone. Qualitative as well as quantitative changes in the spectral range between 900 $cm^{-1}$ and 1200 $cm^{-1}$ and the band at 562 $cm^{-1}$ ($PO_4^{3-}$ asymmetric and symmetric stretching, respectively) were observed. The relative area obtained by decomposition of the $PO_4^{3-}$ band reaches an extreme value in the external compressive stress (10 MPa), that occur under physiological conditions. Based on presented data, it was proved that the applied factors (electric field, compressive stress) can change the oscillation energy and the number of molecule's degrees of freedom.
Źródło:
Acta Physica Polonica A; 2012, 121, 2; 539-542
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Identification of Corrosion Products on Fe and Cu Metals using Spectroscopic Methods
Autorzy:
Święch, D.
Paluszkiewicz, C.
Piergies, N.
Pięta, E.
Lelek-Borkowska, U.
Kwiatek, W.
Powiązania:
https://bibliotekanauki.pl/articles/1030643.pdf
Data publikacji:
2018-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
33.20.Ea
82.80.Gk
42.55.Ye
Opis:
In this study, the Fourier-transform infrared absorption and the Raman spectroscopies for analysis of corrosion products formed on the Fe and Cu metal surfaces after deposition in the chloride containing solution, were used. The obtained spectral patterns show that main constituent species of the corrosion products for Fe metal sample is lepidocrocite, while in the case of Cu surface there is formed mainly paratacamite. The obtained results confirm that application of vibrational spectroscopic methods is precise tool for identification and analysis of the corrosion products.
Źródło:
Acta Physica Polonica A; 2018, 133, 2; 286-288
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
FTIR Study of Multifunctional Coatings
Autorzy:
Paluszkiewicz, C.
Długoń, E.
Kwiatek, W.
Powiązania:
https://bibliotekanauki.pl/articles/1490258.pdf
Data publikacji:
2012-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
82.80.Gk
81.15.Pq
68.37.Yz
82.80.Dx
78.30.Er
Opis:
Nanoparticles of hydroxyapatite (HAp) or tricalcium phosphates (TCP) connected with fibrous phase create biomimetic system between the natural fibrous and ceramic materials building a bone. Chemical bonding between the implant and host tissue takes place through the phosphate layer, which is created on the bioactive implant surface when in contact with the body fluids environment. The Fourier transform infrared spectroscopy can yield microstructural information on the segment level complementary to the morphological information acquired from X-ray scattering as well as electron microscopy. The Fourier transform infrared method is applied to study thin films on different substrates. Moreover, the Fourier transform infrared microscope technique allows to obtain surface and cross-section maps in reflection and transmission modes. This leads to visualization of chemical imaging between substrates and films. In this work, the coatings with different addition of nanohydroxyapatite were deposited by electrodeposition method on titanium and Ti6Al4V alloys. Additionally, sublayers, such as $TiO_2$, were used to increase hydroxyapatite coating adhesion. The selection of suspension composition, depositing time and layer heat treatment conditions have the conclusive influence on the films parameters. All these experimental parameters were monitored during the sample preparation procedure. Changes in phase composition of biomaterials were determined by the Fourier transform infrared reflection technique based on focal plane array detection system. It has been found that results obtained by the Fourier transform infrared spectroscopy show the differences between the studied samples as well as that optimum time of HAp deposition was 90 s.
Źródło:
Acta Physica Polonica A; 2012, 121, 2; 551-554
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 27

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