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Tytuł:
Carbon Co-Deposition During Gas Reduction of Water-Atomized Fe-Cr-Mo Powder
Autorzy:
Ali, B.
Choi, S. H.
Seo, S. J.
Maeng, D. Y.
Lee, C. G.
Kim, T. S.
Park, K. T.
Powiązania:
https://bibliotekanauki.pl/articles/352709.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
water atomization
Fe-based powder
oxide reduction
powder metallurgy
sinter-hardening alloys
Opis:
The water atomization of iron powder with a composition of Fe-3Cr-0.5Mo (wt.%) at 1600°C and 150 bar creates an oxide layer, which in this study was reduced using a mixture of methane (CH4) and argon (Ar) gas. The lowest oxygen content was achieved with a 100 cc/min flow rate of CH4, but this also resulted in a co-deposition of carbon due to the cracking of CH4. This carbon can be used directly to create high-quality, sinter hardenable steel, thereby eliminating the need for an additional mixing step prior to sintering. An exponential relationship was found to exist between the CH4 gas flow rate and carbon content of the powder, meaning that its composition can be easily controlled to suit a variety of different applications.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1119-1124
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Fe Content on the Microstructure and Mechanical Properties of Ti-Al-Mo-V-Cr-Fe Alloys
Autorzy:
Bae, K.-C.
Oak, J.-J.
Kim, Y. H.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/351896.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti alloy
near-β titanium alloy
aircraft applications
structural material
landing gear
Opis:
To investigate the effect of Fe content on the correlation between the microstructure and mechanical properties in near-b titanium alloys, the Ti-5Al-5Mo-5V-1Cr-xFe alloy system has been characterized in this study. As the Fe content increased, the number of nucleation sites and the volume fraction of the α phase decreased. We observed a significant difference in the shape and size of the α phase in the matrix before and after Fe addition. In addition, these morphological deformations were accompanied by a change in the shape of the α phase, which became increasingly discontinuous, and changed into globular-type α phase in the matrix. These phenomena affected the microstructure and mechanical properties of Ti alloys. Specimen #2 exhibited a high ultimate tensile strength (1071 MPa), which decreased with further addition of Fe.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1105-1108
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation and Surface Modification of Mechanical Alloyed Ti-25.0 at.% Al Powder Mixture by Using an Electro-Discharge Technique
Autorzy:
Chang, S. Y.
Jang, H. S.
Yoon, Y. H.
Kim, Y. H.
Kim, J. Y.
Lee, Y. K.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/354212.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintering
mechanical alloying
powder consolidation
intermetallic compounds
titanium aluminides
Opis:
Electrical discharges using a capacitance of 450 μF at 0.5, 1.0, and 1.5 kJ input energies were applied in a N2 atmosphere to obtain the mechanical alloyed Ti3Al powder without applying any external pressure. A solid bulk of nanostructured Ti3Al was obtained as short as 160 μsec by the Electrical discharge. At the same time, the surface has been modified into the form of Ti and Al nitrides due to the diffusion process of nitrogen to the surface. The input energy was found to be the most important parameter to affect the formation of a solid core and surface chemistry of the compact.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1293-1297
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation Mechanism of Ti5Si3 Compact Obtained by Electro-Discharge-Sintering Directly from Physically Blended Ti-37.5 At.% Si Powder Mixture
Autorzy:
Chang, S. Y.
Cheon, Y. W.
Yoon, Y. H.
Kim, Y. H.
Kim, J. Y.
Lee, Y. K.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/353022.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintering
mechanical alloying
powder consolidation
intermetallic compounds
titanium silicide
Opis:
Characteristics of electro-discharge-sintering of the Ti-37.5at.% Si powder mixture was investigated as a function of the input energy, capacitance, and discharge time without applying any external pressure. A solid bulk of Ti5Si3 was obtained only after in less than 129 μsec by the EDS process. During a discharge, the heat is generated to liquefy and alloy the particles, and which enhances the pinch pressure can condensate them without allowing a formation of pores. Three step processes for the self-consolidation mechanism during EDS are proposed; (a) a physical breakdown of oxide film on elemental as-received powder particles, (b) alloying and densifying the consolidation of powder particles by the pinch pressure, and (c) diffusion of impurities into the consolidated surface.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1299-1302
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of a Spherical Titanium Powder by Combined Combustion Synthesis and DC Plasma Treatment
Autorzy:
Choi, S. H.
Ali, B.
Hyun, S. K.
Sim, J. J.
Choi, W. J.
Joo, W.
Lim, J. H.
Lee, Y. J.
Kim, T. S.
Park, K. T.
Powiązania:
https://bibliotekanauki.pl/articles/356067.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
combustion synthesis
DC plasma treatment
titanium powder
3D printing process
combustion parameters
Opis:
Combustion synthesis is capable of producing many types of refractory and ceramic materials, as well as metals, with a relatively lower cost and shorter time frame than other solid state synthetic techniques. TiO2 with Mg as reductant were dry mixed and hand compacted into a 60 mm diameter mold and then combusted under an Ar atmosphere. Depending on the reaction parameters (Mg concentration 2 ≤ α ≤ 4), the thermocouples registered temperatures between 1160°C and 1710°C . 3 mol of Mg gave the optimum results with combustion temperature (Tc) and combustion velocity (Uc) values of 1372°C and 0.26 cm/s respectively. Furthermore, this ratio also had the lowest oxygen concentration in this study (0.8 wt%). After combustion, DC plasma treatment was carried out to spheroidize the Ti powder for use in 3D printing. The characterization of the final product was performed using X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, and N/O analysis.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1057-1062
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Combined Effect of Zr and Si on Isothermal Oxidation of Ti
Autorzy:
Ha, S.-H.
Kim, B.-H.
Yoon, Y.-O.
Lim, H.-K.
Kim, S. K.
Powiązania:
https://bibliotekanauki.pl/articles/353260.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti
Zr
Si
silicide
oxidation
Opis:
In this study, the combined effect of Zr and Si on isothermal oxidation of Ti for 25 and 50h at 820°C, which is the temperature related to exhaust valves operation, was investigated. Si addition into Ti-5mass%Zr alloy led to a distribution of silicide Ti5Si3 phase formed by a eutectic reaction. The Ti sample containing only Zr showed more retarded oxidation rate than Ti-6Al-4V, the most prevalent Ti alloy, at the same condition. However, while a simultaneous addition of Zr and Si resulted in greater increase of oxidation resistance. The oxide layer formed after the addition of Zr and Si comprised TiO2, ZrO2, and SiO2.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1493-1495
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High Temperature Oxidation Property of SiC Coating Layer Fabricated by Aerosol Deposition Process
Autorzy:
Ham, G.-S.
Kim, S.-H.
Park, J.-Y.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352142.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silicon carbide
aerosol deposition
coating
high temperature oxidation
Opis:
This study investigated the high temperature oxidation property of SiC coated layer fabricated by aerosol deposition process. SiC coated layer could be successfully manufactured by using pure SiC powders and aerosol deposition on the Zr based alloy in an optimal process condition. The thickness of manufactured SiC coated layer was measured about 5 μm, and coating layer represented high density structure. SiC coated layer consisted of α-SiC and β-SiC phases, the same as the initial powder. The initial powder was shown to have been crushed to the extent and was deposited in the form of extremely fine particles. To examine the high temperature oxidation properties, oxidized weight gain was obtained for one hour at 1000°C by using TGA. The SiC coated layer showed superior oxidation resistance property than that of Zr alloy (substrate). The high temperature oxidation mechanism of SiC coated layer on Zr alloy was suggested. And then, the application of aerosol deposited SiC coated layer was also discussed.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1347-1351
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication Of Porous Ti By Thermal Decomposition And Sintering Of PMMA/TiH2 Powder Compact
Wytwarzanie porowatego tytanu przez rozkład termiczny i spiekanie wyprasek PMMA/TiH2
Autorzy:
Jeon, K. Ch.
Kim, Y. D.
Suk, M.-J.
Oh, S.-T.
Powiązania:
https://bibliotekanauki.pl/articles/352341.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
porous Ti
PMMA powders
thermal decomposition of TiH2
pore structure
porowaty tytan
PMMA
rozkład termiczny
struktura porów
Opis:
Porous Ti with controlled pore structure was fabricated by thermal decomposition and sintering process using TiH2 powders and Polymethylmethacrylates (PMMA) beads as pore forming agent. The beads sizes of 8 and 50 μm were used as a template for fabricating the porous Ti. The TiH2 powder compacts with 20 and 70 vol% PMMA were prepared by uniaxial pressing and sintered for 2 h at 1100°C. TGA analysis revealed that the PMMA and TiH2 were thermally decomposed at about 400°C forming pores and at about 600°C into metallic Ti phase. The porosity increased with increase in the amount of PMMA addition. Also, the microstructure observation showed that the pore size and shape were strongly dependent on the PMMA shapes.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1375-1377
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of Cu-Based SiC Composites by Spark Plasma Sintering of Cu-Nitrate Coated SiC Powders
Autorzy:
Jeong, Y.-K.
Kim, Y. S.
Oh, S.-T.
Powiązania:
https://bibliotekanauki.pl/articles/354995.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Cu-SiC composite
Cu-nitrate
spark plasma sintering
microstructure
Opis:
An optimum route to fabricate the Cu-based SiC composites with homogeneous microstructure was investigated. Three methods for developing the densified composites with sound interface between Cu and SiC were compared on the basis of the resulting microstructures. Starting with three powder mixtures of elemental Cu and SiC, elemental Cu and PCS coated SiC or PCS and Cunitrate coated SiC was used to obtain Cu-based SiC composites. SEM analysis revealed that the composite fabricated by spark plasma sintering using elemental SiC and Cu powder mixture showed inhomogeneous microstructure. Conversely, dense microstructure with sound interface was observed in the sintered composites using powder mixture of pre-coated PCS and Cu-nitrate onto SiC. The relationship between powder processing and microstructure was discussed based on the role of coating layer for the wettability.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1407-1410
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis and Optimization of Micro Speaker-Box Using a Passive Radiator in Portable Device
Autorzy:
Jiang, Y.-W.
Kwon, J.-H.
Kim, H.-K.
Hwang, S.-M.
Powiązania:
https://bibliotekanauki.pl/articles/176530.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
passive radiator
speaker box
SPL improvement
Sound Pressure Level
Opis:
With the rapid development of multimedia devices such as smart phones and tablet PCs, microspeakers have been recently increasingly used for audio equipment. Improving the acoustic performance of a microspeaker is always a main concern, especially in the low frequency range. To avoid sound cancelation, a microspeaker unit is usually inserted into a speaker box. A passive radiator is also used in speaker boxes to improve the sound performance in the loudspeaker system. However, passive radiators have not been applied into microspeaker system. In this study, a speaker box with a passive radiator was analyzed and optimized to achieve a higher Sound Pressure Level (SPL) in a microspeaker system. The Finite Element Method (FEM), two-degree-of-freedom (DOF) vibration theory, and a plane circular piston sound source were used to study the electromagnetic, vibration, and acoustic characteristics, respectively. Optimization was conducted by changing the mass, stiffness, and size of the passive radiator. Based on the optimized parameters, a new sample was manufactured. The experiment results show that the SPL of the optimized speaker box with a passive radiator is improved by 5 dB at 200 Hz compared with the one without a radiator. The analysis results also matched the experiment results.
Źródło:
Archives of Acoustics; 2017, 42, 4; 753-760
0137-5075
Pojawia się w:
Archives of Acoustics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxidation Behavior of Steel with Cr Content and Water Flow Rate
Autorzy:
Kim, D.-J.
Kim, K. M.
Shin, J. H.
Cheong, Y. M.
Lee, E. H.
Lee, G. G.
Kim, S. W.
Kim, H. P.
Choi, M. J.
Lim, Y. S.
Hwang, S. S.
Powiązania:
https://bibliotekanauki.pl/articles/351548.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
steel
flow accelerated corrosion
Cr content
flow rate
surface oxides
Opis:
Fast water flow facilitates ferrous ion transport leading to flow accelerated corrosion (FAC) of carbon steel and the possibility of a large accident through a failure of a secondary pipe in a nuclear power plant. Ion transport is directly linked to oxide properties such as the thickness, chemical composition and porosity. This work deals with a precise observation of the cross section of the corroded specimen focusing on an oxide passivity and its thickness using SEM (scanning electron microscope) and TEM (transmission electron microscope) as well as an apparent weight loss and a surface observation for the specimens corroded using a rotating cylindrical electrode autoclave system in pure water of pH 7 at 150°C having dissolved oxygen below 1 ppb within a flow rate range of 0 to 10 m/s. The Cr content in steel was changed from 0.02 to 2.4 wt%. Increasing the Cr content in the alloy, the FAC rate and oxide thickness decreased. The oxide porosity tends to decrease with the Cr content and immersion time owing to the development of Cr containing oxide. The oxidation behavior is not changed with the immersion time.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1383-1387
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Study On The Metal Carbide Composite Diffusion Bonding For Mechanical Seal
Badanie łączenia dyfuzyjnego kompozytu metal węglik na mechaniczne uszczelnienie
Autorzy:
Kim, D.-K.
Shon, I.-J.
Song, J.
Ryu, W.-J.
Shin, H.-Ch.
Kwon, E.-Y.
Shin, H.
Kang, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/356399.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
diffusion bonding
nanostructures
mechanical seal
hard metal
mechanical properties
łączenie
nanostruktura
uszczelnienie mechaniczne
twardy metal
właściwości mechaniczne
Opis:
Mechanical Seal use highly efficient alternative water having a great quantity of an aqueous solution and has an advantage no corrosion brine. Metal Carbide composites have been investigated as potential materials for high temperature structural applications and for application in the processing industry. The existing Mechanical seal material is a highly expensive carbide alloy, and it is difficult to take a price advantage. Therefore the study of replacing body area with inexpensive steel material excluding O-ring and contact area which demands high characteristics is needed. The development of WC-Ni base carbide alloy optimal bonding composition technique was accomplished in this study. To check out the influence of bonding temperature and time, bonding characteristics of sintering temperature was experimented. The bonding statuses of this test specimen were excellent. The hardness of specimen and bonding rate were measured using ultrasound equipment. In this work, Powder of WC (involved VC, Cr), Co and Mo2C mixed by attrition milling for 24hours. Nanostructured WC-27.6wt.%Ni-1.5wt.%Si-0.11wt.%VC-1.1wt.%B4C composite were fabricated at 1190°C by high temperature vacuum furnace. To check out the influence of bonding temperature and time, bonding characteristics of sintering temperature was experimented. Its relative density was about 99.7%. The mechanical properties (hardness and fracture toughness) were 87.2 HRA and 4.2 M·Pam1/2, respectively. The bonding status of this test specimen was excellent and the thickness of bonding layer was 20 ~30§ at 1050 and 1060°C bonding temperature.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1479-1483
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Treatment And Modification Of Graphene Using Organosilane And Its Thermal Stability
Obróbka powierzchniowa i modyfikacja grafenu przy użyciu organosilanu i jego stabilność termiczna
Autorzy:
Kim, D.-S.
Dhand, V.
Rhee, K.-Y.
Park, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/354056.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
graphite
thermal properties
Raman spectroscopy
surface treatment
3-APTES
grafit
właściwości termiczne
spektroskopia Ramana
obróbka powierzchniowa
Opis:
In this study, graphene was functionalized via acid oxidation in the presence of a mixture of concentrated sulfuric acid and nitric acid. The oxidized graphene was silanized using the coupling agent, 3-aminopropyltriethoxsilane, resulting in functionalized graphene. The oxidized graphene and functionalized graphene were characterized by X-Ray diffraction, Fourier transform infrared spectroscopy, High-resolution micro Raman spectroscopy, thermogravimetric analysis, and atomic force microscopy to confirm the presence of functional moieties on the graphene surface. Thermal studies also demonstrate that the functionalized material is thermally stable up to higher temperatures.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1387-1391
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł

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