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Tytuł:
Design Of A Bi-Functional α-Fe2O3/Zn2SiO4:Mn2+ By Layer-By-Layer Assembly Method
Projektowanie dwufunkcyjnych proszków α-Fe2O3/Zn2SiO4:Mn2+ metodą warstwa po warstwie
Autorzy:
Yu, R.
Yun, J.
Pee, J-H.
Kim, Y.
Powiązania:
https://bibliotekanauki.pl/articles/352623.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
red pigment
α-Fe2O3
Zn2SiO4:Mn2+ layer
phosphor
bi-functional
czerwony pigment
Zn2SiO4: Mn2+
fosfor
proszki dwufunkcyjne
Opis:
This work describes the design of bi-functional α-Fe2O3/Zn2SiO4:Mn2+ using a two-step coating process. We propose a combination of pigments (α-Fe2O3) and phosphor (Zn2SiO4:Mn2+ ) glaze which is assembled using a layer-by-layer method. A silica-coated α-Fe2O3 pigment was obtained by a sol-gel method and a Zn2+ precursor was then added to the silica-coated α-Fe2O3 to create a ZnO layer. Finally, the Zn2SiO4:Mn2+ layer was prepared with the addition of Mn2+ ions to serve as a phosphor precursor in the multi-coated α-Fe2O3, followed by annealing at a temperature above 1000°C. Details of the phase structure, color and optical properties of the multi-functional α-Fe2O3/Zn2SiO4:Mn2+ were characterized by transmission electron microscopy and X-ray diffraction analyses.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1165-1167
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Warm Tensile Deformation Behavior and Constitutive Equation of Supersaturated Solid-Solutionized Al-9Mg Extruded Alloy
Autorzy:
Yang, Seung Y.
Kim, Bong H.
Lee, Da B.
Choi, Kweon H.
Kim, Nam S.
Ha, Seong H.
Yoon, Young O.
Lim, Hyun K.
Kim, Shae
Kim, Young J.
Powiązania:
https://bibliotekanauki.pl/articles/2048882.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum alloy
Al-9Mg alloy
tensile test
constitutive equation
Opis:
In this paper, as a purpose to apply the supersaturated solid-solutionized Al-9Mg alloy to the structural sheet parts of automotive, tensile tests were conducted under the various conditions and a constitutive equation was derived from the tensile test results. Al-9Mg alloy was produced using a special Mg master alloy containing Al2Ca during the casting process and extruded into the sheet. In order to study the deformation behavior of Al-9Mg alloy in warm temperature forming environments, tensile tests were conducted under the temperature of 373 K-573 K and the strain rate of 0.001/s~0.1/s. in addition, by using the raw data obtained from tensile tests, a constitutive equation of the Al-9Mg alloy was derived for predicting the optimized condition of the hot stamping process. Al-9Mg alloy showed uncommon deformation behavior at the 373 K and 473 K temperature conditions. The calculated curves from the constitutive equation well-matched with the measured curves from the experiments particularly under the low temperature and high strain rate conditions.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 4; 1013-1018
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photoluminescence Studies of Aluminum Nitride Nanowires
Autorzy:
Yang, J.
Na, H.
Kim, H.
Kebede, M.
Choi, R.
Jeong, J.
Lee, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505466.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
We report the production of AlN nanowires by the thermal heating method, for exploring their photoluminescence properties. The room-temperature photoluminescence properties were investigated with different annealing environment. While broad emissions with peaks at around 2.45 and 2.95 eV were obtained from both unannealed and annealed samples, the additional 2.1 eV peak was found from the annealed samples. We have suggested the possible emission mechanisms based on the assumption that both 2.45 eV peak and 2.1 eV peak are ascribed to the nitrogen vacancies. Annealing in N_2 environment exhibited lower intensities of 2.45 eV peak and 2.1 eV peak in comparison to those in Ar environment, presumably due to the suppression of nitrogen vacancies.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 125-127
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Specific Heat of RBa$\text{}_{2}$Cu$\text{}_{3}$O$\text{}_{7-x}$ and RBaSrCu$\text{}_{3}$O$\text{}_{7-x}$ Compounds (R = Sm, Dy, Er)
Autorzy:
Tarnawski, Z.
Kim-Ngan, N.-T. H.
Wang, X. Z.
Duijn, V. H. M.
Franse, J. J. M.
Powiązania:
https://bibliotekanauki.pl/articles/1968860.pdf
Data publikacji:
1998-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
74.70.-b
75.40.-s
Opis:
The low-temperature specific-heat C(T) data of high-T$\text{}_{c}$ superconductors RBa$\text{}_{2}$Cu$\text{}_{3}$O$\text{}_{7-x}$(R123O$\text{}_{7-x}$) were reviewed. A discussion of the C(T) data obtained on single-crystalline samples of Er123O$\text{}_{7-x}$ and Sm123O$\text{}_{7-x}$ compounds in applied magnetic fields for better evaluation of the crystal-electric-field parameters is given. The C(T) measurements of Sr-substituted compounds RBaSrCu$\text{}_{3}$O$\text{}_{7}$ revealed the λ-type of peak related to the antiferromagnetic order at 1.2 K and 0.6 K respectively for Dy- and Er-compounds. The magnetic singlet ground state in these compounds is produced by weak exchange interactions of -0.05 T/μ$\text{}_{B}$ and -0.035 T/μ$\text{}_{B}$, respectively. For Nd- and Sm-compounds, only a broad anomaly around 0.6 K was observed which is well fitted with a Schottky-type anomaly with an energy splitting of 1.4 K.
Źródło:
Acta Physica Polonica A; 1998, 93, 3; 513-522
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
Autorzy:
Son, S. H.
Park, S. C.
Kim, J. H.
Kim, Y. H.
Lee, M. S.
Ahn, J.-W.
Powiązania:
https://bibliotekanauki.pl/articles/352665.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrorefining
tin
electronic waste
recycling
high purity
elektrorafinacja
cyna
odpady elektroniczne
recykling
Opis:
The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Studies on the effect of coal particle size on biodepyritization of high sulfur coal in batch bioreactor
Autorzy:
Singh, S.
Srichandan, H.
Pathak, A.
Gahan, Ch. S.
Lee, S.
Kim, D. J.
Kim, B. G.
Powiązania:
https://bibliotekanauki.pl/articles/778523.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
biodepyritization
coal
pyrite
stirred tank bioreactor
Opis:
The moderate thermophilic mix culture bacteria were used to depyritize the Illinois coal of varying particle sizes (-100 μm, 100-200 μm, +200 μm). Mineral libration analysis showed the presence of pyrite along with other minerals in coal. Microbial depyritization of coal was carried out in stirred tank batch reactors in presence of an iron-free 9K medium. The results indicate that microbial depyritization of coal using moderate thermophiles is an efficient process. Moreover, particle size of coal is an important parameter which affects the efficiency of microbial depyritization process. At the end of the experiment, a maximum of 75% pyrite and 66% of pyritic sulphur were removed from the median particle size. The XRD analysis showed the absence of pyrite mineral in the treated coal sample. A good mass balance was also obtained with net loss of mass ranging from 5-9% showing the feasibility of the process for large scale applications.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 1; 97-102
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Recovery Of Electrodic Powder From Spent Nickel-Metal Hydride Batteries (NiMH)
Odzyskiwanie proszku elektrodowego ze zużytych akumulatorów niklowo-wodorkowych (NiMH)
Autorzy:
Shin, S. M.
Shin, D. J.
Jung, G. J.
Kim, Y. H.
Wang, J. P.
Powiązania:
https://bibliotekanauki.pl/articles/356110.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nickel-metal hybride (NiMH)
electrodic powder
nickel
rare earth elements (REE)
thermal treatment
akumulator niklowo-wodorkowy
proszek elektrodowy
nikiel
pierwiastki ziem rzadkich
obróbka termiczna
Opis:
This study was focused on recycling process newly proposed to recover electrodic powder enriched in nickel (Ni) and rare earth elements (La and Ce) from spent nickel-metal hydride batteries (NiMH). In addition, this new process was designed to prevent explosion of batteries during thermal treatment under inert atmosphere. Spent nickel metal hydride batteries were heated over range of 300°C to 600°C for 2 hours and each component was completely separated inside reactor after experiment. Electrodic powder was successfully recovered from bulk components containing several pieces of metals through sieving operation. The electrodic powder obtained was examined by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDX) and image of the powder was taken by scanning electron microscopy (SEM). It was finally found that nickel and rare earth elements were mainly recovered to about 45 wt.% and 12 wt.% in electrodic powder, respectively.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1139-1143
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation of Tungsten/Ammonium Perchlorate Composites and Their Reaction Kinetics
Autorzy:
Shim, H.-M.
Lee, E.-A.
Kim, J.-K.
Kim, H.-S.
Koo, K.-K.
Powiązania:
https://bibliotekanauki.pl/articles/358373.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
ammonium perchlorate
composite
thermal decomposition
Opis:
The reaction kinetics of tungsten nanoparticles/ammonium perchlorate (W/AP) composites, produced by a spray drying technique, were analyzed and compared with those of neat AP particles and aluminum nanoparticles/AP (Al/AP) composites. The W was found to raise the onset temperature of the thermal decomposition of AP by increasing the activation energy, whereas Al conversely lowered the onset temperature of AP due to the decreased activation energy. From the master plots of kinetic models with the experimental data, the Prout-Tompkins model and the 1-D diffusion controlled model were found to describe the low-temperature decomposition (LTD) and high-temperature decomposition (HTD), respectively, giving remarkable agreement with experimental curves for all heating rates. The presence of W was found to increase the HTD zone width compared with that of neat AP particles and Al/AP composites. Analysis of the average activation energy and pre-exponential factor showed that W increases the energy barrier and the frequency of occurrence of the reaction compared with that of neat AP particles at the LTD state, whereas W decreases both of them at the HTD state. The effect of Al was also shown to be similar to that of W, but the magnitudes of the variation in activation energy and the pre-exponential factor were relatively small.
Źródło:
Central European Journal of Energetic Materials; 2015, 12, 4; 703-722
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Carbon Nanotubes On The Properties Of Spark Plasma Sintered ZrO2/CNT Composites
Wpływ nanorurek węglowych na właściwości spiekanych metodą sps kompozytów ZrO2/CNT
Autorzy:
Shim, D. H.
Jung, S. S.
Kim, H. S.
Cho, H.
Kim, J. K.
Kim, T. G.
Yoon, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/351266.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
CNT
ZrO2
composite
SPS
kompozyty
Opis:
Zirconia matrix ZrO2/CNT composite materials reinforced with multiwall carbon nanotubes were fabricated using a spark plasma sintering technique. The effects of the amount of CNTs addition, sintering temperature and sintering pressure on the properties of the resulting ZrO2/CNT composites were examined. 0 to 9 vol. % CNTs were dispersed in zirconia powder, and the resulting mixture was sintered. The electrical conductivity, hardness, flexural strength, and density were measured to characterize the composites. The friction and wear properties of the composites were also tested. The flexural strength and friction coefficient of the composites were improved with up to 6 vol.% of CNT addition and the flexural strength showed a close relationship with the relative density of the composite. The electrical conductivity increased with increasing proportion of the CNTs, but the efficiency was reduced at more than 6 vol.% CNTs.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1315-1318
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Milling Time Parameter on the Microstructure and the Thermoelectric Properties of n-Type Bi2Te2.7Se0.3 Alloys
Autorzy:
Sharief, P.
Madavali, B.
Koo, J. M.
Kim, H. J.
Hong, S.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/354418.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
milling time
microstructure
thermoelectric properties
ZT
Opis:
Nanostructured thermoelectric materials receiving great attention for its high thermoelectric performance. In this research, nanostructured n-type Bi2 Te2.7 Se0.3 alloys have prepared using high energy ball milling and followed by spark plasma sintering. Also, we have varied ball milling time to investigate milling time parameter on the thermoelectric properties of n-type Bi2 Te2.7 Se0.3 powder. The powders were discrete at 10 min milling and later particles tend to agglomerate at higher milling time due to cold welding. The bulk fracture surface display multi-scale grains where small grains intersperse in between large grains. The maximum Seebeck coefficient value was obtained at 20-min milling time due to their lower carrier density. The κ values were decreased with increasing milling time due to the decreasing trend observed in their κL values. The highest ZT of 0.7 at 350 K was observed for 30-min milling time which was ascribed to its lower thermal conductivity. The Vickers hardness values also greatly improved due to their fine microstructure.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 585-590
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of SiC Particles On Sinterability Of Al-Zn-Mg-Cu P/M Alloy
Wpływ cząstek SiC na spiekalność proszku stopowego Al-Zn-Mg-Cu
Autorzy:
Rudianto, H.
Jang, G. J.
Yang, S. S.
Kim, Y. J.
Dlouhy, I.
Powiązania:
https://bibliotekanauki.pl/articles/351304.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metal matrix composites
powder metallurgy
sintering
heat treatment
kompozyty metalowe
metalurgia proszków
spiekanie
obróbka cieplna
Opis:
Premix Al-5.5Zn-2.5Mg-0.5Cu alloy powder was analyzed as matrix in this research. Gas atomized powder Al-9Si with 20% volume fraction of SiC particles was used as reinforcement and added into the alloy with varied concentration. Mix powders were compacted by dual action press with compaction pressure of 700 MPa. High volume fraction of SiC particles gave lower green density due to resistance of SiC particles to plastic deformation during compaction process and resulted voids between particles and this might reduce sinterability of this mix powder. Sintering was carried out under ultra high purity nitrogen gas from 565°-580°C for 1 hour. High content of premix Al-5.5Zn-2.5Mg-0.5Cu alloy powder gave better sintering density and reached up to 98% relative. Void between particles, oxide layer on aluminum powder and lower wettability between matrix and reinforcement particles lead to uncompleted liquid phase sintering, and resulted on lower sintering density and mechanical properties on powder with high content of SiC particles. Mix powder with wt90% of Alumix 431D and wt10% of Al-9Si-vf20SiC powder gave higher tensile strength compare to another mix powder for 270 MPa. From chemical compositions, sintering precipitates might form after sintering such as MgZn2, CuAl2 and Mg2Si. X-ray diffraction, DSC-TGA, and SEM were used to characterize these materials.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1383-1385
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Low-velocity impact characteristics of composite plates with shape memory alloy wires
Niskoprędkościowe charakterystyki uderzeniowe płyt kompozytowych zawierających włókna ze stopów z pamięcią kształtu
Autorzy:
Rim, M.-S.
Kim, E.-H.
Lee, I.
Choi, I.-H.
Ahn, S.-M.
Koo, K.-N.
Bae, J.-S.
Roh, J.-H.
Powiązania:
https://bibliotekanauki.pl/articles/279293.pdf
Data publikacji:
2011
Wydawca:
Polskie Towarzystwo Mechaniki Teoretycznej i Stosowanej
Tematy:
shape memory alloy
SMAHC
composite
low-velocity impact
impact resistance
Opis:
To investigate impact characteristics of shape memory alloy hybrid com- posites (SMAHC), several experiments were performed. Tensile tests of shape memory alloy (SMA) wires were carried out to investigate thermomechanical properties, and low-velocity impact tests of SMAHC plates and conventional composite plates without SMAs at the critical energy level. low-velocity impact tests of several types of composite plates, including composite plates with embedded SMAs/Fe/Al wires and conventional composite plates, were also done. Results of these experiments show that embedding SMAs in a composite plate can improve the impact resistance. Lastly, low-velocity impact tests of SMAHC plates with SMA wires embedded at different positions through the thickness were performed in an effort to improve the impact resistance. Embedding SMA wires at a lower position in the composite plates was the most effective for improving the impact resistance.
Do analizy charakterystyk uderzeniowych hybrydowych kompozytów SMAHC zwierających włókna SMA ze stopów wykazujących efekt pamięci kształtu przeprowadzono szereg badań eksperymentalnych. Przeprowadzono próby na rozciąganie włókien SMA w celu zbadania ich właściwości termomechanicznych oraz niskoprędkościowe testy uderzeniowe płyt SMAHC oraz konwencjonalnych płyt laminowanych przy energii krytycznej. Wykonano także testy dla płyt kompozytowych zawierających włókna SMA/Fe/Al. Rezultaty doświadczeń pokazały, że wbudowanie w strukturę laminatu włókien SMA może zwiększyć odporność kompozytu na obciążenie uderzeniowe. Opisano również badania eksperymentalne płyt SMAHC z włóknami SMA wbudowanymi na różnej głębokości. Wykazano, że najlepsze parametry posiadają kompozyty z włóknami umieszczonymi możliwie daleko od uderzanej powierzchni.
Źródło:
Journal of Theoretical and Applied Mechanics; 2011, 49, 3; 841-857
1429-2955
Pojawia się w:
Journal of Theoretical and Applied Mechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Extraction Factor Of Pure Ammonium Paratungstate From Tungsten Scraps
Współczynnik ekstrakcji czystego parawolframianu amonu z odpadów wolframowych
Autorzy:
Pee, J-H.
Kim, G. H.
Lee, H. Y.
Kim, Y. J.
Powiązania:
https://bibliotekanauki.pl/articles/356567.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
raw material
recycling
ammonium paratungstate
tungsten scraps
extraction
surowce
recykling
parawolfrawian amonu
odpady wolframowe
ekstrakcja
Opis:
Typical oxidation process of tungsten scraps was modified by the rotary kiln with oxygen burner to increase the oxidation rate of tungsten scraps. Also to accelerate the solubility of solid oxidized products, the hydrothermal reflux method was adapted. By heating tungsten scraps in rotary kiln with oxygen burner at around 900° for 2hrs, the scraps was oxidized completely. Then oxidized products (WO3 and CoWO4) was fully dissolved in the solution of NaOH by hydrothermal reflux method at 150° for 2hrs. The dissolution rate of oxidized products was increased with increasing the reaction temperature and concentration of NaOH. And then CaWO4 and H2WO4 could be generated from the aqueous sodium tungstate solution. Ammonium paratungstate (APT) also could be produced from tungstic acid using by aqueous ammonium solution. The morphologies (cubic and plate types) of APT was controlled by the stirring process of purified solution of ammonium paratungstate.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1403-1405
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Extraction Factor Of Tungsten Sources From Tungsten Scraps By Zinc Decomposition Process
Współczynnik ekstrakcji związków wolframu z odpadów wolframowych w procesie rozkładu cynku
Autorzy:
Pee, J-H.
Kim, G. H.
Lee, H. Y.
Kim, Y. J.
Powiązania:
https://bibliotekanauki.pl/articles/354774.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
raw material
recycling
zinc decomposition process
tungsten carbide
tungstic acid
surowce
recykling
proces rozkładu cynku
węglik wolframu
kwas wolframowy
Opis:
Decomposition promoting factors and extraction process of tungsten carbide and tungstic acid powders in the zinc decomposition process of tungsten scraps which are composed mostly of tungsten carbide and cobalt were evaluated. Zinc volatility was suppressed by the enclosed graphite crucible and zinc volatilization pressure was produced in the reaction graphite crucible inside an electric furnace for ZDP (Zinc Decomposition Process). Decomposition reaction was done for 2hours at 650°, which 100% decomposed the tungsten scraps that were over 30 mm thick. Decomposed scraps were pulverized under 75μm and were composed of tungsten carbide and cobalt identified by the XRD (X-ray Diffraction). To produce the WC(Tungsten Carbide) powder directly from decomposed scraps, pulverized powders were reacted with hydrochloric acid to remove the cobalt binder. Also to produce the tungstic acid, pulverized powders were reacted with aqua regia to remove the cobalt binder and oxidize the tungsten carbide. Tungsten carbide and tungstic acid powders were identified by XRD and chemical composition analysis.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1311-1314
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Characterization of CoCrFeNiMn High Entropy Alloy Powder Processed by Gas Atomization
Autorzy:
Park, T. G.
Lee, S. H.
Lee, B.
Cho, H. M.
Choi, W. J.
Kim, B. S.
Shin, K. S.
Kim, T.-S.
Powiązania:
https://bibliotekanauki.pl/articles/353649.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high entropy alloy
gas atomization
spark plasma sintering
CoCrFeNiMn
Opis:
In this study, precisely controlled large scale gas atomization process was applied to produce spherical and uniform shaped high entropy alloy powder. The gas atomization process was carried out to fabricate CoCrFeNiMn alloy, which was studied for high ductility and mechanical properties at low temperatures. It was confirmed that the mass scale, single phase, equiatomic, and high purity spherical high entropy alloy powder was produced by gas atomization process. The powder was sintered by spark plasma sintering process with various sintering conditions, and mechanical properties were characterized. Through this research, we have developed a mass production process of high quality and spherical high entropy alloy powder, and it is expected to expand applications of this high entropy alloy into fields such as powder injection molding and 3D printing for complex shaped components.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1055-1059
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 97

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