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Wyświetlanie 1-10 z 37
Tytuł:
Synthesis and Characterization of Si Oxide Coated Nano Ceria by Hydrolysis, and Hydrothermal Treatment at Low Temperature
Autorzy:
Kong, M.
Kim, H. W.
Powiązania:
https://bibliotekanauki.pl/articles/354290.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nano-particle
water glass
hydro-reaction
coating method
Opis:
The purpose of this work was to the application of Si oxide coatings. This study deals with the preparation of ceria (CeO2) nanoparticles coating with SiO2 by water glass and hydrolysis reaction. First, the low temperature hydro-reactions were carried out at 30~100°C. Second, Silicon oxide-coated Nano compounds were obtained by the catalyzing synthesis. CeO2 Nano-powders have been successfully synthesized by means of the hydrothermal method, in a low temperature range of 100~200°C. In order to investigate the structure and morphology of the Nano-powders, scanning electron microscopy (SEM) and X-ray diffraction (XRD) were employed. The XRD results revealed the amorphous nature of silica nanoparticles. To analyze the quantity and properties of the compounds coated with Si oxide, transmission electron microscopy (TEM) in conjunction with electron dispersive spectroscopy was used. Finally, it is suggested that the simple growth process is more favorable mechanism than the solution/aggregation process.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1125-1129
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sintering and Microstructures of SUS 316L Powder Produced by 3D Printing Process
Autorzy:
Kim, W. J.
Nguyen, H.-H.
Kim, H. Y.
Nguyen, M.-T.
Park, H. S.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/356018.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
3D printing
selective laser sintering
SUS 316L
flake powder
Opis:
Selective laser sintering (SLS) is a type of laminating sintering technique, using CO2 laser with (metal, polymer, and ceramic) powders. In this result, the flake SUS 316L was used to achieve a high porous product, and compare to spherical type. After SLS, the porosity of flake-type sample with 34% was quite higher than that of the spherical-type one that had only 11%. The surface roughness of the flake SLS sample were also investigated in both inner and surface parts. The results show that the deviation of the roughness of the surface part is about 64.40μm, while that of the internal one was about 117.65μm, which presents the containing of high porosity in the uneven surfaces. With the process using spherical powder, the sample was quite dense, however, some initial particles still remained as a result of less energy received at the beneath of the processing layer.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1215-1218
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of Nickel Powders by Reduction of Nickel Hydroxide Using the Taylor Fluid Flow
Autorzy:
Park, I.-J.
Kim, D.-W.
Kim, G.-H.
Chae, H.-J.
Jung, H.-C.
Powiązania:
https://bibliotekanauki.pl/articles/355021.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni(OH)2
nickel
Taylor fluid flow
fine powder
Opis:
In this study, Ni(OH)2 was synthesized by the continuous reaction by the Taylor fluid flow and compared with those prepared from the conventional batch type reaction. The nickel powders were synthesized by reduction of Ni(OH)2 in an aqueous solution with hydrazine hydrate acting as the reductant. And then the characteristics of the nickel powder according to the synthesis method were compared. The average particle size of the synthesized Ni(OH)2 using Taylor reactor was generally decreased about 1.5~2.5 times more than the batch reaction. The nickel powders prepared by the batch reaction highly agglomerated with non-uniform particles. In the Taylor reaction, the agglomeration of particles was broken and uniform nickel powder was produced.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1443-1447
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Similarity of chromosome structure among Populus tremula var. davidiana, Populus alba and their hybrids revealed by FISH karyotype analysis
Autorzy:
Kim, Y.G.
Kwon, S.H.
Kang, H.I.
Yoem, D.B.
Kim, K.W.
Kim, H.H.
Kang, K.S.
Powiązania:
https://bibliotekanauki.pl/articles/2077655.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Instytut Dendrologii PAN
Tematy:
Karyotype analysis
Fluorescence in situ hybridization
Ribosomal DNA site
Poplar
Cytogenetics
Opis:
The genus Populus is one of the important tree species in Korean peninsula and many other coun- tries in the world. It represents the model species of forest genomics because it grows fast and reproduces rapidly. In this reason, their genetic characteristics have been well studied and the whole genome has been sequenced completely in some species. However, cytogenetic study of the genus Populus has been limited. In the present study, karyotypes of Korean aspen (P. tremula var. davidiana), Silver poplar (P. alba) and their two hybrids, Suwon aspen (P. tremula var. glandulosa) and Hyun aspen (P. alba × P. tremula var. glandulsa) were analyzed by means of the fluorescence in situ hybridization (FISH). Root samples were collected from mature trees in the demonstration forest, located at Suwon, Kyonggi province in South Korea. The fresh root cells were examined by DAPI (4’,6-diamidino-2-phenylindole) staining and FISH using 45S rDNA and 5S rDNA probes. As the results, the chromosome compositions of all species were the same as 2n = 38. The karyotype formulas of Korean aspen, Silver poplar, Suwon aspen and Hyun aspen were 28m + 6sm + 4st (2sat), 26m + 10sm (2sat) + 2st, 26m + 12sm (2sat) and 28m + 10sm (2sat), respectively. The four species had one pair of 45S rDNA site and one pair of 5S rDNA site in common with FISH karyotypes. The similarity of FISH karyotypes among four species indicated close genetic relationship and coexistence of their interspecific hybrids. This research will provide genetic information on cytogenetic research of Populus and genetic mapping that can be applied to the breeding program of Populus in the near future.
Źródło:
Dendrobiology; 2020, 83; 68-74
1641-1307
Pojawia się w:
Dendrobiology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxygen Emissions from Single-Crystalline Fe$\text{}_{3}$O$\text{}_{4}$ Surfaces Induced by Low-Energy Ion Bombardments
Autorzy:
Kim-Ngan, N.-T. H.
Soszka, W.
Powiązania:
https://bibliotekanauki.pl/articles/2046830.pdf
Data publikacji:
2006-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
68.35.-p
61.18.Bn
Opis:
Negative-charged ion energy spectra of the Fe$\text{}_{3}$O$\text{}_{4}$ (001) and (111) surface revealed large peaks attributed to the O$\text{}^{-}$ recoils from a binary collision. Under Ar$\text{}^{+}$ ion bombardments such an emission was largely affected by the screening effect of the Fe ions. A distinguished peak related to the O$\text{}^{+}$ recoil ions was observed under Ne$\text{}^{+}$ ion bombardments, while such a peak was merged into the high background in the case of Ar$\text{}^{+}$ ion ones. A weak effect from the Verwey transition was found on oxygen emissions. For the (111) surface a small peak characteristic of the O$\text{}^{+}$ recoils from double collisions appeared in the energy spectra around 140-170 K and a minimum was observed in both R$\text{}^{+}$(T) and R$\text{}^{-}$(T) curves under 6 keV Ne$\text{}^{+}$ ion beam.
Źródło:
Acta Physica Polonica A; 2006, 109, 6; 715-721
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spontaneous Formation of Titanium Nitride on the Surface of a Ti Rod Induced by Electro-Discharge-Heat-Treatment in an N2 Atmosphere
Autorzy:
Lee, W. H.
Yoon, Y. H.
Kim, Y. H.
Lee, Y. K.
Kim, J. Y.
Chang, S. Y.
Powiązania:
https://bibliotekanauki.pl/articles/352477.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
surface modification
diffusion
heat treatment
XPS
Opis:
A single pulse of 2.0 to 3.5 kJ of input energy from a 450 mF capacitor was applied to a commercially pure Ti rod in a N2 atmosphere. The surface of the Ti rod transformed from TiO2 into titanium nitride in times as short as 159 msec, providing a bimodal morphology of the cross-section. A much higher value of hardness that was observed at the edge of the cross-section was attributed to nitrogen-induced solid-solution hardening that occurred during the electrical discharge process. The activation energy (Ea) for the diffusion process was estimated to be approximately 86.9 kJ/mol. Results show that the electrical discharge process is a possible potential method for the nitriding of Ti; advantages include a short processing time and control of the nitrided layer without dimensional changes.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1281-1285
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
Autorzy:
Son, S. H.
Park, S. C.
Kim, J. H.
Kim, Y. H.
Lee, M. S.
Ahn, J.-W.
Powiązania:
https://bibliotekanauki.pl/articles/352665.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrorefining
tin
electronic waste
recycling
high purity
elektrorafinacja
cyna
odpady elektroniczne
recykling
Opis:
The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation Mechanism of Ti5Si3 Compact Obtained by Electro-Discharge-Sintering Directly from Physically Blended Ti-37.5 At.% Si Powder Mixture
Autorzy:
Chang, S. Y.
Cheon, Y. W.
Yoon, Y. H.
Kim, Y. H.
Kim, J. Y.
Lee, Y. K.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/353022.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintering
mechanical alloying
powder consolidation
intermetallic compounds
titanium silicide
Opis:
Characteristics of electro-discharge-sintering of the Ti-37.5at.% Si powder mixture was investigated as a function of the input energy, capacitance, and discharge time without applying any external pressure. A solid bulk of Ti5Si3 was obtained only after in less than 129 μsec by the EDS process. During a discharge, the heat is generated to liquefy and alloy the particles, and which enhances the pinch pressure can condensate them without allowing a formation of pores. Three step processes for the self-consolidation mechanism during EDS are proposed; (a) a physical breakdown of oxide film on elemental as-received powder particles, (b) alloying and densifying the consolidation of powder particles by the pinch pressure, and (c) diffusion of impurities into the consolidated surface.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1299-1302
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of AZ31/CNT Surface Nano-composite by Double-pass Friction Stir Processing
Autorzy:
Kim, J. Y.
Hwang, J.-W.
Kim, H. Y.
Lee, S. M.
Jung, W.-S.
Byeon, J.-W.
Powiązania:
https://bibliotekanauki.pl/articles/355624.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
surface modification
Double-pass Friction Stir Processing
AZ31
composite
CNT
Opis:
Double-pass Friction Stir Processing (FSP) was applied to fabricate an AZ31/CNT nano-composite for surface hardening of lightweight structural components. The effects of double-pass FSP as well as groove depth (i.e., volume fraction of CNT) on the CNT distribution, dynamically recrystallized grain size, and resulting microhardness were studied. Double-pass FSP was performed for the CNT-filled plate-type specimen with different groove depths of 2, 3, and 4 mm. By applying double-pass FSP, the average size of CNT clusters decreased, implying a more homogeneous distribution. Compared with the FSPed specimen without CNT, grain size was refined from 19 μm to 3 μm and microhardness increased from 52 Hv to 83 Hv (i.e., 71% increase).
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1039-1042
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Scanning Tunneling Spectra and Low Energy Ion Scattering Studies of the Verwey Transition in MBE Fe$\text{}_{3}$O$\text{}_{4}$ (100) Thin Film
Autorzy:
Kim-Ngan, N.-T. H.
Soszka, W.
Hietschold, M.
Powiązania:
https://bibliotekanauki.pl/articles/2024029.pdf
Data publikacji:
2001-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.16.Ch
61.18.Bn
71.30.+h
Opis:
The (100) surface of magnetite Fe$\text{}_{3}$O$\text{}_{4}$ thin film was studied by a UHV low-temperature scanning tunneling microscope and by an ion scattering spectroscopy. The tunneling spectra revealed a widening of the gap with decreasing temperature, which may be related to the metal-insulator phase transition in this material. A strong effect of this phase transition on ion scattering from such a surface was observed. The temperature dependence of the scattered ion yield, R$\text{}^{+}$(T), revealed two minima at around 100 K and at 125 K under Ne$\text{}^{+}$ bombardment with the primary energy up to 6 keV. The disappearance of the high-temperature minimum at a bombarding energy of 6.5 keV gave a further evidence for the ion velocity dependence of the character of the R$\text{}^{+}$(T) curve, which has been first observed for a MBE Fe$\text{}_{3}$O$\text{}_{4}$ (111) film surface.
Źródło:
Acta Physica Polonica A; 2001, 99, 2; 267-276
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-10 z 37

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