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Tytuł:
Ignition and Combustion Performance of the Primary Condensed-phase Combustion Products from Boron-based Fuel-rich Propellants
Autorzy:
Liu, L.-L.
He, G.-G.
Wang, Y.-H.
Hu, S.-G.
Powiązania:
https://bibliotekanauki.pl/articles/358859.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
boron-based fuel-rich propellant
primary combustion products
ignition
combustion performance
Opis:
The primary condensed-phase combustion products of a boron-based fuel-rich propellant were ignited using a high-power CO2 laser in a pressurized and windowed combustion chamber under variable pressure. The ignition and combustion performances were characterized using an ultraviolet-visible spectrometer and a high-speed camera. The experimental results showed that the combustion of the condensed-phase combustion products originate from the combustion of carbon, and boron may not take any part in the combustion process because of the formation of a thick boron oxide coating and agglomeration after the primary combustion process. Both particle size and the ingredients play an important role in the combustion reaction of the condensed-phase products. It was observed that a lower particle size and a higher boron carbide content are beneficial for the combustion reaction of the products; higher primary and secondary combustion pressures clearly improved the secondary combustion efficiency of the propellant in the combustion reaction.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 2; 448-460
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Automatic calibration system for digital-display vibrometers based on machine vision
Autorzy:
He, W.
Xu, G.
Rong, Z.
Li, G.
Liu, M.
Powiązania:
https://bibliotekanauki.pl/articles/221163.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
image recognition
calibration
vibration measurement
machine vision
automatic testing
digital-display vibrometer
Opis:
Considering the low efficiency during the process of traditional calibration for digital-display vibrometers, an automatic calibration system for vibrometers based on machine vision is developed. First, an automatic vibration control system is established on the basis of a personal computer, and the output of a vibration exciter on which a digital-display vibrometer to be calibrated is installed, is automatically adjusted to vibrate at a preset vibration level and a preset frequency. Then the display of the vibrometer is captured by a digital camera and identified by means of image recognition. According to the vibration level of the exciter measured by a laser interferometer and the recognized display of the vibrometer, the properties of the vibrometer are calculated and output by the computer. Image recognition algorithms for the display of the vibrometer with a high recognition rate are presented, and the recognition for vibrating digits and alternating digits is especially analyzed in detail. Experimental results on the built-up system show that the prposed image recognition methods are very effective and the system could liberate operators from boring and intense calibration work for digital-display vibrometers.
Źródło:
Metrology and Measurement Systems; 2014, 21, 2; 317-328
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Experimental Evidence for Jahn-Teller Transition in a Fe(II)Fe(III) Bimetallic Oxalate
Autorzy:
Tang, G.
He, Y.
Xu, F.
Zhang, Q.
Powiązania:
https://bibliotekanauki.pl/articles/1400401.pdf
Data publikacji:
2013-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Xx
76.80.+y
Opis:
Bimetallic oxalate ${[N-(n-C_4H_9)_4][FeFe(C_2O_4)_3]}_{n}$ has been investigated by the Mössbauer spectroscopy. The Mössbauer studies confirm that high-spin Fe(III) (S=5/2) and Fe(II) (S=2) ions are present in the compound. These spectra above 60 K consist of three quadrupole doublets, indicating that there are three different Fe sites in the material. The Mössbauer results reveal that spontaneous magnetization of Fe(II) sublattices increases more steeply than that of Fe(III) sublattices as the temperature decreases from $T_{C}$. Great increase of quadrupole splitting at 50 K provides compelling evidence for the predicted Jahn-Teller transition.
Źródło:
Acta Physica Polonica A; 2013, 123, 1; 118-120
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
An autonomous multi-sensor satellite system based on multi-agent blackboard model
Autonomiczny wieloczujnikowy system satelitarny oparty na wieloagentowym modelu tablicowym
Autorzy:
He, L.
Li, G.
Xing, L.
Chen, Y.
Powiązania:
https://bibliotekanauki.pl/articles/300595.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Polskie Naukowo-Techniczne Towarzystwo Eksploatacyjne PAN
Tematy:
satelita autonomiczny
model tablicowy
wieloagentowy
harmonogramowanie adaptacyjne
planowanie
autonomous satellite
blackboard model
multi-agent
adaptive scheduling
planning
Opis:
Traditional Earth observation satellite cannot work well in terms of emergencies, environmental uncertainties and scientific events discovery. Therefore, it is of significance to study the new generation of autonomous Earth observation satellite. In order to develop an autonomous satellite system with distributed and coordinated functions, this paper proposes an autonomous satellite system based on distributed multi-agent blackboard model. Multiple agents including functions of pre-processing, planning, scheduling and execution are designed. Agents share information and communicate through a blackboard which stores the task sequence, the action sequence and the satellite status. An adaptive rule-based heuristic scheduling algorithm and a forward search planning algorithm are proposed. The simulation experiments and computational results prove that the system can deal with scientific events discovery, satellite faults, cloud obscuration and emergencies without human intervention, which can greatly enhance the efficiency and reliability of Earth observation satellites. The validity of the proposed model and algorithm is proved.
Tradycyjne satelity obserwacji Ziemi nie nadają się do pracy w sytuacjach kryzysowych, warunkach niepewności środowiskowej oraz w okolicznościach związanych z odkryciami naukowymi. Dlatego też istotne znaczenie ma badanie nowej generacji autonomicznych satelitów obserwacji Ziemi. W celu opracowania autonomicznego systemu satelitarnego o rozproszonych i skoordynowanych funkcjach, w niniejszej pracy zastosowano rozproszony wieloagentowy model tablicowy. Zaprojektowano agenty, w tym funkcje wstępnego przetwarzania, planowania, harmonogramowania i wykonania. Agenty te wymieniają między sobą informacje i komunikują się za pośrednictwem tablicy (ang. blackboard), na której przechowywane są informacje dotyczące sekwencji zadań i działań oraz stanu satelity. Zaproponowano adaptacyjny, regułowy, heurystyczny algorytm harmonogramowania oraz algorytm planowania metodą wyszukiwania w przód. Przeprowadzone eksperymenty symulacyjne oraz wyniki obliczeń dowodzą, że omawiany system sprawdza się w przypadkach odkryć naukowych, awarii satelitarnych, zachmurzenia oraz w sytuacjach kryzysowych nie wymagając interwencji człowieka, co może znacznie zwiększać wydajność i niezawodność satelitów obserwacji Ziemi. W pracy wykazano trafność proponowanego modelu i algorytmów.
Źródło:
Eksploatacja i Niezawodność; 2017, 19, 3; 447-458
1507-2711
Pojawia się w:
Eksploatacja i Niezawodność
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mannose inhibition of nitrate uptake by wheat roots
Autorzy:
Li, J.-Z.
Cram, W.J.
He, G.-Y.
Powiązania:
https://bibliotekanauki.pl/articles/58372.pdf
Data publikacji:
2010
Wydawca:
Polskie Towarzystwo Botaniczne
Tematy:
mannose
inhibition
nitrate uptake
wheat
Triticum aestivum
plant root
Opis:
The effect of mannose on nitrate uptake was investigated by a new non-invasive technique. Under normal condition, nitrate uptake by wheat (Triticum aestivum L.) roots was about 1-7 µmol gfwt-1 h-1. After the addition of 10 mM mannose, net nitrate influx by wheat roots started to decrease and reached a new steady state at -40 ±50% of the control value after 73 min. After mannose supplied for 2 h, its removal caused net nitrate influx to be recovered to an original rate. Therefore, the inhibition of mannose on nitrate uptake is not due to the onset of programmed cell death because it starts too rapidly and it is reversible, however, it is probably due to Pi and consequent ATP depletion.
Źródło:
Acta Societatis Botanicorum Poloniae; 2010, 79, 2; 107-110
0001-6977
2083-9480
Pojawia się w:
Acta Societatis Botanicorum Poloniae
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ephedrine production from suspension cultures of Ephedra alata L. callus
Autorzy:
Hegazi, G.A.
Ghareb, H.E.
Gabr, M.F.
Powiązania:
https://bibliotekanauki.pl/articles/2096962.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
shake-flask culture
in vitro
alkaloid
biotic elicitor
Aspergillus niger
yeast extract
Opis:
Ephedra alata is an important Egyptian medicinal plant with enormous applications in pharmaceutical industry. Shake-flask suspension cultures of E. alata were established from internodal segment-derived callus. The suspension cultures were treated with two biotic elicitors, namely Aspergillus niger and yeast extract, to enhance the synthesis of ephedrine – the bioactive constituent of E. alata. Ephedrine was quantified using the high performance liquid chromatography technique. Ephedrine concentration was not directly related to biomass production. Aspergillus niger and yeast extract enhanced the production of ephedrine by 2.5- to 7-fold after different durations of incubation as compared to ephedrine content in the mother plant. Treatment with the fungal elicitor A. niger extract induced the maximum accumulation of ephedrine at the concentration of 1.67%; it also increased ephedrine biosynthesis by 7-fold in 24-day-old culture as compared to the ephedrine content in the mother plant and caused higher ephedrine biosynthesis than that in the control treatment without elicitors. The present protocol could be applicable for the large-scale production of ephedrine from E. alata.
Źródło:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology; 2020, 101, 1; 25-33
0860-7796
Pojawia się w:
BioTechnologia. Journal of Biotechnology Computational Biology and Bionanotechnology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Enhanced Non-linear Viscoelastic Properties of Polymer Bonded Explosives Based on Graphene and a Neutral Polymeric Bonding Agent
Autorzy:
Lin, C.
He, G.
Liu, J.
Pan, L.
Liu, S.
Powiązania:
https://bibliotekanauki.pl/articles/358748.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
polymer bonded explosives
graphene
neutral polymeric bonding agent
creep behaviour
Opis:
During their long-term storage and transport, polymer bonded explosives (PBXs) will be subjected to complex thermal physical environments with combined thermal and mechanical loads. The creep behaviour results in a change of physical and mechanical properties, which consequently influences the explosive performance. In this work, graphene and a neutral polymeric bonding agent (NPBA) were selected to improve the non-linear creep properties of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB)-based PBXs. The results were compared with the creep response of the corresponding PBXs without additives and with graphene alone. It was observed that graphene and an NPBA exhibited a positive effect, improving the creep resistance of TATB-based PBXs. The compressive and tensile strength of 0.5 wt.% graphene-filled PBXs were improved by 5.1% and 29.2%, respectively, compared to raw TATB-based PBXs without additives. The performance of the PBXs was further enhanced by the addition of 0.1 wt.% NPBA. For a given stress and temperature, the TATB-based PBXs with graphene and NPBA deformed significantly less than the PBXs filled with graphene alone.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 4; 788-805
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Adsorption behaviors of typical aromatic pollutants in biologically treated coking wastewater on powdered coal
Autorzy:
Sun, H.
Wang, Y.
Bian, Y.
He, X.
Li, G.
Powiązania:
https://bibliotekanauki.pl/articles/110777.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
aromatic pollutants
wastewater treatment
adsorption affinity
competitive adsorption
Opis:
The raw coal was utilized as adsorbent based on its remarkable adsorption ability of coal slime to organic compounds in the flotation process. This paper mainly investigates adsorption behaviors of benzpyrole (BZP), pyrrole (PR) and benzoic acid (BA) on powdered coal (PC). In the monocomponent solution, the removal efficiencies of BZP, PR and BA reached 85.23%, 55.02% and 24.84% at PC dosage of 20 g/dm3. Adsorption behaviors of three pollutants fitted perfectly to the pseudo-second order kinetics model and liquid film diffusion occupied the largest proportion in rate-limiting step according to the diffusion rates. Furthermore, the influences of pH on adsorption behaviors and competitive adsorption mechanism of three pollutants were also reported.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 496-504
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Combined Influence of Silicon Content and Oxygen Concentration on the Oxidation Process of Silicon-Containing Steels
Autorzy:
Yuan, Q.
Xu, G.
Zhou, M.
He, B.
Hu, H.
Powiązania:
https://bibliotekanauki.pl/articles/352126.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silicone content
oxygen concentration
mass gain
isothermal holding time
Opis:
The combined influence of silicon content and oxygen concentration on silicon-containing steels was investigated, via a heating route similar to that applied in the industrial reheating process, using a Simultaneous Thermal Analyzer (STA). Four different oxygen concentrations and three different isothermal holding times were designed. The results show that the effect of silicon on the mass gain depends on the oxygen concentration and the oxidation time. The mass gain of low-silicon steel is greater than that of high-silicon steel at 1260°C in the oxygen concentrations of 1.0 vol.% and 2.0 vol.%, even when the isothermal holding time is 90 minutes. However, there is a critical time point for mass gain in oxygen concentrations ≥3.0 vol.%. The mass gain of lowsilicon steel is greater before and smaller after this critical point. The critical time is deferred with decreasing oxygen concentration.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 445-450
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Controlled Synthesis and Application of Nano-energetic Materials Based on the Copper Oxide/Al System
Autorzy:
He, S.
Chen, J.
Yang, G.
Qiao, Z.
Li, J.
Powiązania:
https://bibliotekanauki.pl/articles/358254.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
nanoenergetic material
CuO/Al
laser ignition
plate-like
hollow sphere
Opis:
Nanothermite composites containing metal oxide and metal fuel are attracting attention due to their outstanding combustion characteristics. The morphology of metal oxide is important for the performance of nanothermite composites. In this paper, branch-, plate-, sphere-, and hollow sphere-like CuO nano/microstructures were synthesized via a facile hydrothermal process. The CuO/Al based nanothermites were prepared via ultrasonic mixing of the asobtained CuO products and nano-Al. The combustion behaviour of CuO/Al based nanothermites was analyzed by DSC and laser ignition. This study shows that this nanoscale mixing resulted in a large interfacial contact area and low diffusional resistance between the fuel and the oxidizer, and the reaction reflects large energy and laser ignition sensitivity.
Źródło:
Central European Journal of Energetic Materials; 2015, 12, 1; 129-144
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Energy-aware key management in mobile wireless sensor networks
Autorzy:
He, X.
Szalachowski, P.
Kotulski, Z.
Fotiou, N.
Marias, G. F.
Polyzos, G. C.
Meer de, H.
Powiązania:
https://bibliotekanauki.pl/articles/106190.pdf
Data publikacji:
2012
Wydawca:
Uniwersytet Marii Curie-Skłodowskiej. Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej
Tematy:
wireless sensor networks
Diffie-Hellman key agreement
key management
Opis:
Wireless sensor networks have received wide attention recently across the indoor and outdoor applications. On the other hand, more and more application scenarios require sensor nodes to be mobile, which imposes new technological challenges for security. Key management is the core for secure data communications among the resource-constrained sensor nodes. In this paper, based on the Group Diffie-Hellman key agreement protocols and the energy level of each node in the network, we propose Energy Aware Group Diffie-Hellman key management protocol for mobile wireless sensor networks. The simulation results show that the proposed key management protocol provide significant improvement in maximizing the lifetime of networks.
Źródło:
Annales Universitatis Mariae Curie-Skłodowska. Sectio AI, Informatica; 2012, 12, 4; 83-96
1732-1360
2083-3628
Pojawia się w:
Annales Universitatis Mariae Curie-Skłodowska. Sectio AI, Informatica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Factors Affecting the Measurement of the Percentage of Gaseous Products from Boron-based Fuel-rich Propellants
Autorzy:
Liu, L.-L.
He, G.-Q.
Wang, Y.-H.
Liu, P.-J.
Powiązania:
https://bibliotekanauki.pl/articles/358720.pdf
Data publikacji:
2014
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
fuel-rich propellant
percentage gaseous products
combustion
filter media
Opis:
Acid-washed asbestos, carbon fibre, and MgO with carbon fibre were used as the filter media in order to compare their filtering qualities in the estimation of the percentage of gaseous products (PGP) arising from the combustion of singlebase propellants, double-base propellants, and boron-based fuel-rich propellants. The comparison was based on an analysis of the experimentally registered influence of the propellant formulation, the propellant load, the maximum chamber pressure and the thickness of the MgO filter layer on the PGP from the fuel-rich propellant, and in particular on the PGP produced by combustion of boron-based fuel-rich propellant. The results showed that the experimental values of the PGP were closer to the theoretically predicted values when carbon fibre mixed with MgO powder was used as the filter medium. The PGP of boron-based fuel-rich propellant increased when the AP was in part replaced by HMX, when the AP content was increased and when boron was in part replaced by magnesium-aluminum alloy. In terms of the apparatus used in these experiments, the propellant loading density was found to have little correspondence with the PGP for boron-based fuel-rich propellant. The optimal propellant loading density for the chamber volume of 85 cm3 was found to be 2-2.5 g, in view of the reliability and safety of the experiment. It is emphasised that the thickness of the MgO filter layer is very important for the accuracy and reliability of the experiment, and that the optimum should be determined by experiment.
Źródło:
Central European Journal of Energetic Materials; 2014, 11, 1; 15-29
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Reducing the salinity impact on soilless culture of tomatoes using supplemental Ca and foliar micronutrients
Autorzy:
Saleh, S.
Liu, G.
Liu, M.
Liu, W.
Gruda, N.
He, H.
Powiązania:
https://bibliotekanauki.pl/articles/12688394.pdf
Data publikacji:
2019
Wydawca:
Uniwersytet Przyrodniczy w Lublinie. Wydawnictwo Uniwersytetu Przyrodniczego w Lublinie
Tematy:
plant cultivation
tomato
Solanum lycopersicum
soilless culture
vegetative growth
fruit quality
yield
calcium supplementation
foliar application
foliar nutrition
micronutrient
salinity impact
salt stress
physiological parameter
Opis:
Salt stress is known as one of the most severe abiotic factors limiting the plant production all over the world. In this study, three additives: (i) supplemental Ca (5 mmol L–1) to nutrient solution, (ii) foliar application of micronutrients (Fe, Mn and Zn at 60, 160 and 110 mg L–1, respectively), and (iii) combination of both of them were evaluated aiming to reduce the negative impact of salt stress on tomato plants cultivated in a soilless culture and improve the internal quality of fruits. The obtained results show that salinity reduced vegetative growth and physiological parameters, fruit yield and its components, and even more lowered fruit market classification of tomatoes. Salinity treatment reduced most of essential macro- and micronutrients in tomato fruit, whilst Na content was increased. Tomato productivity and fruit quality were ameliorated under saline conditions by increasing Ca into nutrient solution and applying a foliar application of micronutrients. A combination of both additives ranked the first to alleviate the adverse effects of salinity on tomatoes, followed by solo supplemental Ca into saline nutrient solution. On the other hand, the internal fruit quality of antioxidant compounds, such as vitamin C, lycopene, α-carotene, β-carotene and lutein as well as acidity, total soluble solid and dry matter percent, were increased under saline conditions.
Źródło:
Acta Scientiarum Polonorum. Hortorum Cultus; 2019, 18, 3; 187-200
1644-0692
Pojawia się w:
Acta Scientiarum Polonorum. Hortorum Cultus
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Differential responses of aquatic and aerobic forms of Echinochloa crus-galli (L.) Beauv. and E. colona (L.) Link. by morpho-physiological and molecular analysis
Autorzy:
Khedr, A.-H.A.
Serag, M.M.
Shaaban, H.E.
Abogadallah, G.M.
Powiązania:
https://bibliotekanauki.pl/articles/9989.pdf
Data publikacji:
2017
Wydawca:
Fundacja na Rzecz Młodych Naukowców
Tematy:
alcohol dehydrogenase
ADH zob.alcohol dehydrogenase
aquatic form
aerobic form
Echinochloa crus-galli
Echinochloa colona
habitat alteration
morphophysiological analysis
molecular analysis
phosphoenolopyruvate carboxylase
Rubisco
Opis:
Echinochloa crus-galli and E. colona are serious weeds around the world. Morphological and biochemical features of aquatic and aerobic forms of both species were investigated experimentally by transplanting the seedlings reciprocally between water-saturated and aerobic soils (70% field capacity). When the plants were grown in water-saturated soil, a significant decrease in tiller height was observed in E. crus-galli, but not in E. colona. Upon growing the plants in aerobic soil, internode length and spike dry weight increased significantly in E. crus-galli, but decreased significantly in E. colona. Growth under aerobic condition caused a significant increase in PEPC/Rubisco ratio, but a significant decrease was observed under water-saturated conditions. When E. crus-galli was transplanted in aerobic soil, several forms of peroxidase were upregulated. Contrarily, in E. colona peroxidase isoforms did not respond to habitat change. Gene expression of ADH in E. colona was constitutive at a fairly high level under native habitats then enhanced with reversing habitat that caused anoxic and mild drought conditions. Both species tend to grow faster under aerobic conditions by modifying the photosynthetic machinery and capacity of scavenging of reactive oxygen species. Furthermore, ADH appears to play a role in supporting growth under water-saturated conditions.
Źródło:
Environment, Earth and Ecology; 2017, 1, 1
2543-9774
2451-4225
Pojawia się w:
Environment, Earth and Ecology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Characterization of Four Energetic Transition Metal Complexes of 3,4-Diamino-1,2,4-triazole
Autorzy:
Yin, X.
Jin, X.
Xu, C.-X.
He, P.
Wang, K.
Zhang, J.-G.
Powiązania:
https://bibliotekanauki.pl/articles/358716.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
3,4-diamino-1,2,4-triazole
theoretic study
crystal structure
thermal stability
sensitivity
Opis:
Four complexes with the formula of [M5(DATr)12~14(H2O)6](ClO4)10 (M = Mn (1), Co (2), Ni (3), Zn (4)) about their synthesis, structures and some energetic properties (such as sensitivities tests) have been described, where the DATr here denotes 3,4-diamino-1,2,4-triazole. These four compounds are all light metallic complexes with good thermal stability. The structures of 2-4 were determined by single-crystal X-ray diffraction, and the crystal structures mainly consist of penta-nuclear units. All the structures have a common interesting property in which DATr plays a role of bi-dentate ligand. Besides, it is observed from the crystal structure of 4 that DATr can be also act as a mono-dentate ligand. Thermodynamic studies of their decomposition properties and kinetic parameters show that the four complexes have high thermal stabilities. Furthermore, tests of their impact and friction sensitivities show that complexes (2) and (3) can be potential candidates as primary explosives to replace toxic lead azide.
Źródło:
Central European Journal of Energetic Materials; 2016, 13, 2; 301-320
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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