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    Wyświetlanie 1-8 z 8
    Tytuł:
    Production of high quality magnesium chloride from recycled waste magnesite powder
    Autorzy:
    Erdogan, N.
    Yersel, E.
    Celebi, C.
    Kavakli, N.
    Batar, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/110185.pdf
    Data publikacji:
    2013
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    waste magnesite powder
    leaching hydrochloride acid
    magnesium chloride
    MgCl2
    Opis:
    This study investigates the production of high-quality MgCl2 from recycled waste magnesite powder with an average particle size of d50 0.079 mm using the HCl acid leaching method. The experimental parameters were, leaching temperature, leaching time, amount of the acid, liquid-to-solid ratio, scale-up factor, acid concentration, particle size and mixing speed. The experiments were performed under reproducible conditions. The results showed that optimum leaching parameters were: temperature of 70 °C, 180 min leaching time, 130 cm3 acid consumption, 3.6 cm3/g liquid-to-solid ratio, scale-up factor of 1, 10.17 M acid concentration, 0.079 mm average particle size and a mixing speed 60 rpm. Under these optimum conditions, the leaching yield was 96.72%. The produced MgCl2 solution contained 0.04% SiO2, 0.36% CaO, 0% Fe2O3, 0% Al2O3, 46.73% MgCl2, 52.87% L.O.I. and 99.60% MgCl2+L.O.I. (= MgCl2·6H2O). These results indicated that high-quality magnesium chloride can be produced from waste magnesite powder.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2013, 49, 2; 557-566
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of UHWPE-TiO₂ Composites Produced by Gelation/Crystallization Method
    Autorzy:
    Celebi Efe, G.
    Bindal, C.
    Ucisik, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031264.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Qk
    81.05.Lg
    Opis:
    In this study, ultra-high molecular weight polyethylene (UHMWPE) - TiO₂ composites reinforced with TiO₂ particles with weight ratios of 0.5, 1 and 2% were produced by gelation/crystallization method in decalin+antioxidant solution of UHMWPE at 150°C, for 40 min by using magnetic stirrer. The gel mixture was cooled in an aluminum tray embedded in iced water under ambient conditions and dried in an oven at 130°C for 90 min to remove any residual trace of decalin. Distribution and elemental analyses of TiO₂ particles in polymer matrix was examined by SEM-EDS. Crystallization behavior was investigated by differential scanning calorimetry (DSC). Based on the results, TiO₂ particles in the UHMWPE have accelerated the crystallization, acting as nucleating agents, with increment from 56% for UHMWPE to 63.5% for UHMWPE-2 wt% TiO₂. The present bond types in composites were analyzed by Raman spectroscopy and the results are in good agreement with literature. Uniaxial tensile tests were performed to determine Young's modulus of UHMWPE-TiO₂ composites. It was found that Young's modulus of UHMWPE was increased from 52 MPa to 800 MPa with the addition of TiO₂ particles.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 767-769
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Pack Siliconizing of Ti6Al4V Alloy
    Autorzy:
    Celebi Efe, G.
    İpek, M.
    Bindal, C.
    Zeytin, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031464.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.65.Lp
    81.65.-b
    Opis:
    In this study, it was aimed to produce titanium silicide layer on Ti6Al4V by a simple, cheap and efficient method of pack siliconizing. Siliconizing was performed in a pack containing a mixture composed of SiO₂ powder as siliconizing source, pure Al powder as a reducer for siliconizing, NH₄Cl as an activator and Al₂O₃ powder as filler, at 1000°C for 8, 10 and 12 hours in open atmospheric furnace. Optical microscope and SEM-EDS studies indicate that the morphology of silicide layers has smooth, dense and layered nature. The presence of phases, confirmed by XRD analyses, reveals that the silicide layers formed at 1000°C are composed of TiSi₂, Ti₃Si₅, TiN, TiO₂ and SiO₂ compounds. Silicide layer thickness was increased with increasing process time and ranged from 7.5 to 9.0 μm. Hardness of silicide layers, measured by Vickers indentation, is over 2100 HV.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 760-762
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Gas Nitriding Behaviour of 34CrAlNi7 Nitriding Steel
    Autorzy:
    Altinsoy, I.
    Onder, K.
    Celebi Efe, F.
    Bindal, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1219733.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.65.Lp
    Opis:
    In this study, gas nitriding behavior of 34CrAlNi7-10 steel was investigated. Single stage processes were carried out at 500°C, 520C and 540C for 10, 20, 30 h, respectively. Nitrogen activity on surface was controlled by the nitriding potential $K_{N}$ which is known as thermodynamical control parameter for controlled gas nitriding process. The presence of nitrides formed on surface of test material was determined by X-ray diffraction analysis technique. The morphology of nitrided layer was studied by optical microscope. The microhardness of surface of nitrided sample in $HV_1$ was observed between 975 and 1132. Choosing the right nitriding potentials for each temperature, which give the same nitrogen concentration and activity on surface by using the Lehrer diagram, showed that all the samples had almost the same surface roughness of $R_{a}$ = 0.28-0.32 μm after gas nitriding cycles. The measurements showed that the white layer thickness varies between 4.38 μm and 28.80 μm and the growth of the layer was strongly affected by process time and temperature. Diffusion depths as Nht (HV) for each experiment were determined and compared.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 414-416
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Double Stage Nitriding on 34CrAlNi7-10 Nitriding Steel
    Autorzy:
    Altinsoy, İ.
    Çelebı Efe, G.
    Yener, T.
    Önder, K.
    Bindal, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1031228.pdf
    Data publikacji:
    2017-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.BX
    81.65.LP
    81.70.BT
    Opis:
    In this study, effect of double stage gas nitriding of 34CrAlNi7-10 steel was analyzed. Nitriding processes were carried out in two stages. in the first stage, samples were nitridied at 500°C for 10 h and then in second stage nitriding process was continued at 530 and 550°C for 20 h. During both stages, the nitrogen activity on surface was controlled by the nitriding potential, which is a thermodynamical control parameter for controlled gas nitriding process. The nitriding potential was kept constant, at value of 10, during the first stage and was varied in the range of 3.2-0.2, for both nitriding temperatures, in the second stage. The presence of nitrides, formed on the surface of test materials was determined by XRD analysis technique. The morphology of nitrided layer was studied by optical microscopy. The microhardness of the surfaces of nitrided samples in HV1 was between 955 and 1029. The measurements have shown that the thickness of the compound layer (white layer) has varied between 6.85-23.90 μm and that the growth of the white layer and microhardness gradient were strongly affected by the nitriding potential and the temperature. Diffusion depths as Nht(HV) for Vickers Hardness were determined and compared.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 3; 663-666
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects of SiC Particle Size on Properties of Cu-SiC Metal Matrix Composites
    Autorzy:
    Celebi Efe, G.
    Altinsoy, I.
    Ipek, M.
    Zeytin, S.
    Bindal, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1491445.pdf
    Data publikacji:
    2012-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Ni
    81.20.Ev
    Opis:
    This paper was focused on the effects of particle size and distribution on some properties of the SiC particle reinforced Cu composites. Copper powder produced by cementation method was reinforced with SiC particles having 1 and 30 μm particle size and sintered at 700°C. Scanning electron microscopy studies showed that SiC particles were dispersed in copper matrix homogeneously. The presence of Cu and SiC components in composites were verified by X-ray diffraction analysis technique. The relative densities of Cu-SiC composites determined by Archimedes' principle are ranged from 96.2% to 90.9% for SiC with 1 μm particle size, 97.0% to 95.0% for SiC with 30 μm particle size. Measured hardness of sintered compacts varied from 130 to 155 HVN for SiC having 1 μm particle size, 188 to 229 HVN for SiC having 30 μm particle size. Maximum electrical conductivity of test materials was obtained as 80.0% IACS (international annealed copper standard) for SiC with 1 μm particle size and 83.0% IACS for SiC with 30 μm particle size.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 1; 251-253
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparing of Commercial and Cemented Cu-SiC Composites
    Autorzy:
    Celebi Efe, G.
    Altinsoy, I.
    Yener, T.
    Ipek, M.
    Zeytin, S.
    Bindal, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1287723.pdf
    Data publikacji:
    2014-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.05.Je
    81.05.Ni
    Opis:
    SiC with 30 μm particle size reinforced copper composites have been fabricated by powder metallurgy method and sintered at 700C for 2 h in open atmosphere. Copper powder was produced by cementation method and obtained as commercial for comparing. Cemented and commercial copper powders were reinforced with SiC having 30 μm particle size at ratios of 0, 1, 2, 3, and 5 wt% for improving mechanical properties of copper without decreasing the electrical conductivity. The presence of Cu and SiC which are dominant components in the sintered composites were confirmed by X-ray diffraction analyses technique. Scanning electron microscope showed that SiC particles are distributed homogeneously in the copper matrix. The relative densities of Cu and Cu-SiC composites sintered at 700C are ranged from 98.0% to 96.2% for commercial Cu-SiC composites, 97.55 to 95.0% for cemented Cu-SiC composites, microhardness of composites ranged from 133 to 277 HV for commercial Cu-SiC composites and 127 to 229 HV for cemented Cu-SiC composites, and the electrical conductivity of composites changed between 95.6%IACS and 77.2%IACS for commercial Cu-SiC composites, 91.7%IACS and 69%IACS for cemented Cu-SiC composites. It was observed that there is a good agreement between cemented Cu-SiC and commercial Cu-SiC composites.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 2; 417-419
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    An Evaluation of Cu-B₄C Composites Manufactured by Powder Metallurgy
    Autorzy:
    Yener, T.
    Altinsoy, I.
    Yener, S.
    Celebi Efe, G.
    Ozbek, I.
    Bindal, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1401279.pdf
    Data publikacji:
    2015-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Ni
    81.20.Ev
    72.80.Tm
    Opis:
    In this study, the influences of B₄C ratios on some mechanical and physical properties such as relative density, microhardness and electrical properties of cold pressed Cu-B₄C composites were investigated. Curve fitting is applied for the estimation of electrical conductivity. Commercial copper powders with 40 μm particle size were reinforced with B₄C, with particle size of 40 μm, at ratios of 1, 2, 3 wt.%, for improving mechanical properties of copper used as electrical conductor. Cu-B₄C composites have been fabricated by powder sintering process at a temperature of 900°C for 2 h. The presence of Cu and B₄C, which are dominant components in the sintered composites, were confirmed by X-ray diffraction analysis technique and SEM-EDS. Scanning electron microscope (SEM-EDS) has shown that B₄C particles are distributed homogenously in the copper matrix. The relative densities of Cu and Cu-B₄C composites, sintered at 900°C, ranged from 95.7 to 91.6%. Microhardness of composites ranged from 84.5 to 94.6 HB. It was observed that cold pressed Cu-1 wt.% B₄C composites revealed promising physical properties. Results of electrical conductivity measurement of Cu-B₄C composite material are compared to the results of the model and the overall accuracy level above 96% is obtained.
    Źródło:
    Acta Physica Polonica A; 2015, 127, 4; 1045-1047
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-8 z 8

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