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    Wyświetlanie 1-39 z 39
    Tytuł:
    Valorization of Cobalt from Waste LIB Cathode through Cobalt Oxalate and Cobalt Oxide Synthesis by Leaching-Solvent Extract-Precipitation Stripping
    Autorzy:
    Swain, B.
    Lee, J.-C.
    Lee, C.-G.
    Powiązania:
    https://bibliotekanauki.pl/articles/352333.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    valorization of cobalt
    cobalt oxide powder
    rod-shaped cobalt oxalate
    precipitation stripping
    Opis:
    An ecoefficient, economical and sustainable valorization process for the synthesis of Co3O4 from waste lithium-ion battery (LIB) by leaching-solvent extract-scrubbing-precipitation stripping route has been developed. Through an optimization, the waste LIB cathode was leached using 2000 mole/m3 of H2SO4 and 5 Vol. % of the H2O2 at a pulp density of 100 kg/m3 under leaching time 60 minutes and temperature 75°C. From the separated leach liquor, cobalt was purified by saponified Cyanex 272. From cobalt, loaded Cyanex 272 impurities were scrubbed and the CoC2O4·2H2O was recovered through precipitation stripping. Finally, the precipitate was calcined to synthesize Co3O4, which is a precursor for LIB cathode materials manufacturing. From TGA-DTA, followed by XRD analysis it was confirmed that at 200°C the CoC2O4·2H2O can be converted to anhydrous CoC2O4 and at 350°C the anhydrous can be converted to Co3O4 and at 1100°C the Co3O4 can be converted to CoO. Through reported route waste LIB can back to LIB manufacturing process through a versatile and flexible industrial approach.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 2; 1037-1042
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Efficient online handwritten Chinese character recognition system using a two-dimensional functional relationship model
    Autorzy:
    Chang, Y. F.
    Lee, J. C.
    Mohd Rijal, O.
    Syed Abu Bakar, S. A. R.
    Powiązania:
    https://bibliotekanauki.pl/articles/908140.pdf
    Data publikacji:
    2010
    Wydawca:
    Uniwersytet Zielonogórski. Oficyna Wydawnicza
    Tematy:
    2D
    współczynnik determinacji
    rozpoznawanie
    pismo odręczne
    pismo chińskie
    falka Haara
    model relacyjny
    2D functional classifier
    coefficient of determination
    handwritten Chinese character recognition
    Haar wavelet
    multidimensional functional relationship model
    Opis:
    This paper presents novel feature extraction and classification methods for online handwritten Chinese character recognition (HCCR). The X-graph and Y-graph transformation is proposed for deriving a feature, which shows useful properties such as invariance to different writing styles. Central to the proposed method is the idea of capturing the geometrical and topological information from the trajectory of the handwritten character using the X-graph and the Y-graph. For feature size reduction, the Haar wavelet transformation was applied on the graphs. For classification, the coefficient of determination [...] from the two-dimensional unreplicated linear functional relationship model is proposed as a similarity measure. The proposed methods show strong discrimination power when handling problems related to size, position and slant variation, stroke shape deformation, close resemblance of characters, and non-normalization. The proposed recognition system is applied to a database with 3000 frequently used Chinese characters, yielding a high recognition rate of 97.4% with reduced processing time of 75.31%, 73.05%, 58.27% and 40.69% when compared with recognition systems using the city block distance with deviation (CBDD), the minimum distance (MD), the compound Mahalanobis function (CMF) and the modified quadratic discriminant function (MQDF), respectively. High precision rates were also achieved.
    Źródło:
    International Journal of Applied Mathematics and Computer Science; 2010, 20, 4; 727-738
    1641-876X
    2083-8492
    Pojawia się w:
    International Journal of Applied Mathematics and Computer Science
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Biological Evaluation of Anodized Biodegradable Magnesium-Calcium Alloys
    Autorzy:
    Kim, J.
    Lee, J.
    Lee, K.
    Park, S.
    Lim, H.
    Park, C.
    Bae, J.
    Yun, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398763.pdf
    Data publikacji:
    2016-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    87.85.jj
    87.85.J-
    Opis:
    The objective of this study was to evaluate the biocompatibility of studied binary magnesium-calcium (Mg-Ca) alloys for biodegradable intraosseous implants. Mg is necessary for health and is a non-toxic biodegradable material that decomposes naturally in the body. Nevertheless, Mg has been implicated in problems including diminished physical properties and corrosion resistance when degradation is too rapid prior to bone healing. This study has explored the effect of Ca on the corrosion resistance and biological evaluation after anodizing treatment with different contents of Ca alloy. Binary Mg-0.5Ca, Mg-1Ca and Mg-5Ca alloys were prepared by the casting method under an argon atmosphere and cut into disc-shaped pieces. Pure Mg alloy was used as the control. Anodic oxidation was performed for 15 minutes at a voltage of 120 V using an electrolyte solution containing Ca gluconate, sodium hexametaphosphate, and sodium hydroxide at room temperature. Corrosion resistance was analyzed using a corrosion tester. After a hydrogen evolution test, the surface pattern and phase changes were observed on a scanning electron microscop (SEM) and energy dispersive spectroscop (EDS). Microscopic evaluation of the adhesion and cell biological functions of Mg was conducted by observing the response of human fetal osteoblastic 1.19 cells with regard to changes in surface film properties, depending on the amount of Ca. Our results support the view that in Mg-xCa alloys (x=0.5, 1, 5 wt.%) treated using anodic oxidation, the increasing Ca content controls the rate of decomposition and improves corrosion resistance.
    Źródło:
    Acta Physica Polonica A; 2016, 129, 4; 728-735
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Rapid Synthesis of Gold Nano-Particles Using Pulse Waved Potential in a Non-Aqueous Electrolyte
    Autorzy:
    Jang, J. G.
    Lee, J.-O.
    Lee, C. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/352529.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    gold
    nanoparticle
    nonaqueous electrolyte
    pulse wave
    catalyst
    Opis:
    Rapid synthesis of gold nanoparticles (AuNPs) by pulsed electrodeposition was investigated in the non-aqueous electrolyte, 1-ethyl-3-methyl-imidazoliumbis(trifluoro- methanesulfonyl)imide ([EMIM]TFSI) with gold trichloride (AuCl3). To aid the dissolution of AuCl3, 1-ethyl-3-methyl-imidazolium chloride ([EMIM]Cl) was used as a supporting electrolyte in [EMIM]TFSI. Cyclicvoltammetry experiments revealed a cathodic reaction corresponding to the reduction of gold at −0.4 V vs. Pt-QRE. To confirmthe electrodeposition process, potentiostatic electrodeposition of gold in the non-aqueous electrolyte was conducted at −0.4 V for 1 h at room temperature. To synthesize AuNPs, pulsed electrodeposition was conducted with controlled duty factor, pulse duration, and overpotential. The composition, particle-size distribution, and morphology of the AuNPs were confirmed by field-emission scanning electron microscopy (FE-SEM), energy-dispersive spectroscopy (EDS), and transmission electron microscopy (TEM). The electrodeposited AuNPs were uniformly distributed on the platinum electrode surface without any impurities arising from the non-aqueous electrolyte. The size distribution of AuNPs could be also controlled by the electrodeposition conditions.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1389-1392
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    AC Microcalorimetry of Superconducting $MgCNi_3$ Single Crystals
    Autorzy:
    Kačmarčík, J.
    Pribulová, Z.
    Samuely, P.
    Marcenat, C.
    Klein, T.
    Jang, D.
    Lee, H.
    Lee, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/1813689.pdf
    Data publikacji:
    2008-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    74.70.Ad
    74.25.Bt
    Opis:
    The low-temperature specific heat of single-crystal samples of superconducting $MgCNi_3$ with typical dimensions 200 μm were measured for the first time. A computer controlled ac microcalorimeter using an optical fiber and an infrared light-emitting diode as the heat source was used down to 2 K at magnetic fields up to 8 T. The specific heat data suggest a moderate coupling in $MgCNi_3$.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 1; 363-366
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Study on the Optimal Design of Air Pockets in an Air Bearing Applied Tilting Index Table
    Autorzy:
    Lee, M.-J
    Lee, C.-M
    Powiązania:
    https://bibliotekanauki.pl/articles/971152.pdf
    Data publikacji:
    2009
    Wydawca:
    Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
    Tematy:
    optimal design
    tilting index table
    air bearing
    air pocket
    Opis:
    The tilting index table has attached to CNC machining center with 3axes, it can be improvement of its performance and its machining efficiency. The tilting index table is a key unit in order to manufacture some non-rotational and 3-dimensional parts, using the conventional machining center. The tilting index table is directly connected to a processing object. Regarding the increase in the deflection of the table, it directly affects processing objects and increases errors and that makes impossible to obtain desired processing precision. Thus, this study performed the shape optimization of air pockets in order to minimize the deflection presented in the existing table. In the numerical optimizing method for implementing optimal design, the general full factorial design and response surface method in the design of experiments were used. A finite element analysis was used for computational experiments in which the finite element analysis was performed by using the ANSYS Workbench, which is a type of commercial FEM tool. In addition, the analysis of the results was performed by using the commercial program, Minitab 15. The results show that the optimum design results is better than those of the initial design.
    Źródło:
    Journal of Machine Engineering; 2009, 9, 2; 114-123
    1895-7595
    2391-8071
    Pojawia się w:
    Journal of Machine Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Allometric scaling of marbofloxacin pharmacokinetics: a retrospective analysis
    Autorzy:
    Yohannes, S.
    Hossain, M.A.
    Kim, J.Y.
    Lee, S.J.
    Kwak, D.M.
    Suh, J.W.
    Park, S.C.
    Powiązania:
    https://bibliotekanauki.pl/articles/31939.pdf
    Data publikacji:
    2014
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Opis:
    The association between physiologically dependent pharmacokinetic parameters (CLB, T1/2β, Vdss) of marbofloxacin and body weight was studied in eight animal species based on allometric equation Y = aWb, where ‘Y’ is the pharmacokinetic parameter, ‘W’ is body weight, ‘a’ is allometric coefficient (intercept) and ‘b’ is the exponent that describes relation between pharmacokinetic parameter and body weight. The body clearance of marbofloxacin has shown significant (P<0.0001) relation with size (Bwt) in various animal species. However, half-life and volume of distribution were not in association with body weight. Although half-life and volume of distribution were not in a good correlation with body weight, statistically significant association between the body clearance and body weight suggests validity of allometric scaling for predicting pharmacokinetic parameters of marbofloxacin in animal species that have not been studied yet. However further study considering large sample size and other parameters influencing pharmacokinetics of marbofloxacin is recommended.
    Źródło:
    Polish Journal of Veterinary Sciences; 2014, 17, 1
    1505-1773
    Pojawia się w:
    Polish Journal of Veterinary Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Photoluminescence Studies of Aluminum Nitride Nanowires
    Autorzy:
    Yang, J.
    Na, H.
    Kim, H.
    Kebede, M.
    Choi, R.
    Jeong, J.
    Lee, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1505466.pdf
    Data publikacji:
    2011-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.07.-b
    78.55.-m
    Opis:
    We report the production of AlN nanowires by the thermal heating method, for exploring their photoluminescence properties. The room-temperature photoluminescence properties were investigated with different annealing environment. While broad emissions with peaks at around 2.45 and 2.95 eV were obtained from both unannealed and annealed samples, the additional 2.1 eV peak was found from the annealed samples. We have suggested the possible emission mechanisms based on the assumption that both 2.45 eV peak and 2.1 eV peak are ascribed to the nitrogen vacancies. Annealing in N_2 environment exhibited lower intensities of 2.45 eV peak and 2.1 eV peak in comparison to those in Ar environment, presumably due to the suppression of nitrogen vacancies.
    Źródło:
    Acta Physica Polonica A; 2011, 119, 2; 125-127
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    System Identification from Multiple-Trial Data Corrupted by Non-Repeating Periodic Disturbances
    Autorzy:
    Phan, M. Q.
    Longman, R. W.
    Lee, S. C.
    Lee, J. W.
    Powiązania:
    https://bibliotekanauki.pl/articles/908209.pdf
    Data publikacji:
    2003
    Wydawca:
    Uniwersytet Zielonogórski. Oficyna Wydawnicza
    Tematy:
    automatyka
    robotyka
    system identification
    disturbance identification
    iterative learning control
    repetitive control
    interaction matrix
    Opis:
    Iterative learning and repetitive control aim to eliminate the effect of unwanted disturbances over repeated trials or cycles. The disturbance-free system model, if known, can be used in a model-based iterative learning or repetitive control system to eliminate the unwanted disturbances. In the case of periodic disturbances, although the unknown disturbance frequencies may be the same from trial to trial, the disturbance amplitudes, phases, and biases do not necessarily repeat. Furthermore, the system may not return to the same initial state at the end of each trial before starting the next trial. In spite of these constraints, this paper shows how to identify the system disturbance-free dynamics from disturbance-corrupted input-output data collected over multiple trials without having to measure the disturbances directly. The system disturbance-free model can then be used to identify the disturbances as well, for use in learning or repetitive control. This paper represents the first extension of the interaction matrix approach to the multiple-trial environment of iterative learning control.
    Źródło:
    International Journal of Applied Mathematics and Computer Science; 2003, 13, 2; 185-192
    1641-876X
    2083-8492
    Pojawia się w:
    International Journal of Applied Mathematics and Computer Science
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis, Structure, Photoluminescence, and Raman Spectrum of Indium Oxide Nanowires
    Autorzy:
    Kim, H.
    Na, H.
    Yang, J.
    Lee,, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1505485.pdf
    Data publikacji:
    2011-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.07.-b
    78.55.-m
    Opis:
    Production of indium oxide $(In_2O_3)$ whiskers at a very low temperature of 650°C was reported. The synthetic route was comprised of a thermal heating process of a mixture of In and Mg powders. We have investigated the structural properties of the as-synthesized nanowires by using X-ray diffraction and scanning electron microscopy. The product consisted of one-dimensional nanowires, with a crystalline cubic structure of $In_2O_3$. The photoluminescence measurement with the Gaussian fitting exhibited visible light emission bands centered at 2.1 eV and 2.8 eV. The peaks of the Raman spectrum were indexed to the modes being associated with cubic $In_2O_3$.
    Źródło:
    Acta Physica Polonica A; 2011, 119, 2; 143-145
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
    Autorzy:
    Jo, Y. J.
    Yoon, Y. H.
    Kim, Y. H.
    Chang, S. Y.
    Kim, J. Y.
    Lee, Y. K.
    Van Tyne, C. J.
    Lee, W. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356790.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    titanium
    implant
    porous
    sintering
    X-ray photoelectron spectroscopy (XPS)
    Opis:
    A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Development of Carbon Nanotube Based Reflection Type X-ray Source
    Autorzy:
    Choi, H.
    Kim, J.
    Lee, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1807922.pdf
    Data publikacji:
    2009-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.47.Lx
    75.47.Gk
    73.50.Fq
    Opis:
    X-ray imaging technology is a useful and leading medical diagnostic tool for health care professionals to diagnose disease in human body. Carbon nanotube based X-ray source, which we have developed in this study, could be also useful and supply integrated diagnostic X-ray imaging tool in diagnosis. Conventionally, thermionic type of tungsten filament X-ray tube is widely employed in the field of biomedical and industrial application fields. However, intrinsic problems, such as poor emission efficiency, low imaging resolution, and high electrical energy consumption etc., may cause the limitation of using the X-ray tube. To fulfill the current market requirement, specifically for medical diagnostic field, we have developed rather a portable and compact carbon nanotube based X-ray device in which microfocus high imaging resolution can be feasible.
    Źródło:
    Acta Physica Polonica A; 2009, 115, 6; 1078-1080
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    High-temperature Oxidation Behavior and Kinetics of Forged 12Cr-MoVW Steel
    Autorzy:
    Kim, Y. H.
    Oak, J.-J.
    Bae, K.-C.
    Lee, W-J.
    Park, Y. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/351450.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    ferritic/martensitic stainless steels
    forging
    oxidation kinetics
    oxide layer
    Opis:
    The oxidation kinetics of forged 12Cr-MoVW steel was investigated in an air (N2+O2) atmosphere at 873-1073 K (Δ50 K) using thermogravimetric analysis. The oxidized samples were characterized using X-ray diffraction, and the surface and cross-sectional morphologies were examined using scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy. The forged 12Cr-MoVW steel samples exhibited parabolic behavior and a low oxidation rate compared with their as-cast counterparts. A protective oxide layer was uniformly formed at relatively low temperature (≤973 K) for the forged samples, which thus exhibited better oxidation resistance than the as-cast ones. These oxides are considered solid-solution compounds such as (Fe, Cr)2O3.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1099-1104
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A stepwise ISO-based TQM implementation approach using ISO 9001:2015
    Autorzy:
    Chen, C.-K.
    Anchecta, K.
    Lee, J. -D.
    Dahlgaard, J. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/407353.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Total Quality Management
    TQM
    ISO QMS
    ISO 9000
    ISO 9001:2015
    international standard
    Opis:
    The lack of an implementation roadmap always deters enterprises from choosing Total Quality Management (TQM) as its major management approach. This paper proposes a stepwise ISO-based TQM implementation approach which is based on the notion of the new threedimensional overall business excellence framework developed by Dahlgaard et al. [1]. The proposed approach consists of nine steps comprising three categories: “TQM faith building”, “TQM tools and techniques learning”, and “system development”. The steps in each of the three categories are arranged to span across the proposed nine-step approach. The ISO 9001:2015 standard is used as a case study to demonstrate the proposed approach. The ideas and benefits of the proposed approach are further discussed in relation to this illustration.
    Źródło:
    Management and Production Engineering Review; 2016, 7, 4; 65-75
    2080-8208
    2082-1344
    Pojawia się w:
    Management and Production Engineering Review
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Morphology Change Of Si Deposit In Molten Salt Electrorefining
    Zmiana morfologii osadu Si podczas elektrorafinacji w stopionych solach
    Autorzy:
    Ryu, H. Y.
    Kwon, S. C.
    Han, M. H.
    An, Y. S.
    Lee, J. S.
    Lee, J. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354346.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    molten salt
    silicon
    morphology
    electrorefining
    current density
    sól stopiona
    krzem
    morfologia
    elektrorafinacja
    gęstość prądu
    Opis:
    The effects of processing parameters on the morphology change in a Si deposit recovered by means of molten salt electrorefining are evaluated using electrochemical techniques such as cyclic voltammetry and chronopotentiometry at 800°C. It was found that concentration of K2SiF6 and current density were important parameters in determining deposit size. Higher concentrations of K2SiF6 were effective in coarsening the silicon deposit and decreasing the cell potential. Silicon nanofiber was recovered at 5 wt% of K2SiF6 whereas dense particles were prepared at 30 and 50 wt% of K2SiF6. The morphology of the Si deposit was determined by the concentration of Si in the electrolyte which is related to the formation of crystal and growth of Si. The formation mechanism of the Si deposit was interpreted by using high resolution TEM as well as electrochemical properties.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1491-1497
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Study On Dispersion Stability Of Nickel Nanoparticles Synthesized By Wire Explosion In Liquid Media
    Badanie stabilności dyspersji nanocząstek niklu wytworzonych metodą WEP w ciekłym medium
    Autorzy:
    Kim, C. K.
    Lee, G.-J.
    Lee, M. K.
    Rhee, C. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/356909.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    nickel nanofluid
    pulsed wire evaporation
    surfactant
    zeta potential
    dispersion stability
    nanocząstka niklu
    środek powierzchniowo czynny
    stabilność dyspersji
    potencjał zeta
    dyspersja
    Opis:
    In this study, nickel nanoparticles were synthesized in ethanol using portable pulsed wire evaporation, which is a one-step physical method. From transmission electron microscopy images, it was found that the Ni nanoparticles exhibited a spherical shape with an average diameter of 7.3 nm. To prevent aggregation of the nickel nanoparticles, a polymer surfactant was added into the ethanol before the synthesis of nickel nanoparticles, and adsorbed on the freshly synthesized nickel nanoparticles during the wire explosion. The dispersion stability of the prepared nickel nanofluids was investigated by zeta-potential analyzer and Turbiscan optical analyzer. As a result, the optimum concentration of polymer surfactant to be added was suggested for the maximized dispersion stability of the nickel nanofluids.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1379-1382
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization Of The Graded Microstructure In Powder Sintered Porous Titanium
    Charakterystyka gradientowej mikrostruktury porowatego tytanu spiekanego z proszku
    Autorzy:
    Oak, J.-J.
    Bang, J. I.
    Bae, K.-C.
    Kim, Y. H.
    Lee, Y. C.
    Chun, H. H.
    Park, Y. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356239.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    titanium
    powder metallurgy
    porous structure
    sintering
    biomaterial
    tytan
    metalurgia proszków
    struktura porowata
    spiekanie
    biomateriał
    Opis:
    The proposed sintering process produce porosity and functional graded microstructure in the sinterd titanium powders. Titanium powders with different micro sizes were sintered at the proposed temperature region at 1200 and 1300°C for 2h. The apatite-forming on the graded microstructure is observed by immersion test in Hanks balanced salt soluion at 37°C. Sintering condition of titanium powders is estimated by thermogravitmetry-differential thermal analysis (TG-DTA). The synthersied surface structures and apatite-forming ability were characterized by a field emission scanning electron microscopy (FE-SEM) observation and energy dispersive X-ray spectroscopy (EDS) analysis. As results, these graded microstructure of sintered porous titanium powders reveals apatite-forming ability as osseointegration by calcification in Hanks balanced salt soluion(HBSS) at 37°C.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1265-1269
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structural Properties and Mechanical Behavior of the 2 Step-Reinforced Al-Si/SiCp Metal Matrix Composite by Titanium-Fiber
    Autorzy:
    Oak, J.-J.
    Lee, Y. C.
    Park, Y. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356010.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    metal matrix composite
    sintering
    Ti fiber
    mechanical properties
    diffusion
    Opis:
    In this study, the newly designed Al-9Si/SiC particles (SiCp) + Ti-fiber (2step-reinforced Al-9Si alloy matrix) metal matrix composites (MMCs) were fabricated by hot-pressing sintering at 560°C. 2step-reinforced Al-based MMCs were characterized by thermal shrinkage, phase transition, microstructure and tensile strength. The addition of Ti-fiber reduced thermal shrinkage was caused by temperature difference in sintering process as well as enhanced assistance for tensile strength and plastic deformation at room temperature. Experimental results reveal that the 2step-reinforcment sintering by ceramic and metal has a significant effect to increase interface bonding in boundary of each component material and the improved mechanical properties were due to the influence of interfacial product by diffusion. Tensile strength and elongation at room temperature by 2step-reinforcement were improved in 19.5% and 26.2% more than those of Al-9Si/SiCp, respectively. Especially, it reveals that diffusion direction may be varied by sintering methods at low temperature in this study.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1089-1097
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The effect of patterns on image-based modelling of texture-less objects
    Autorzy:
    Hafeez, J.
    Jeon, H.-J.
    Hamacher, A.
    Kwon, S.-C.
    Lee, S.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/221814.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    structure-from-motion
    feature detection
    patterns analysis
    3D reconstruction
    surface comparison
    Opis:
    The task of generating fast and accurate three-dimensional (3D) models of objects or scenes through a sequence of non-calibrated images is an active field of research. The recent development in algorithm optimization has resulted in many automatic solutions that can provide an accurate 3D model from texture-full objects. Structure-from-motion (SfM) is an image-based method that uses discriminative point-based feature identifier, such as SIFT, to locate feature points in the images. This method faces difficulties when presented with the objects made of homogenous or texture-less surfaces. To reconstruct such surfaces a well-known technique is to apply an artificial variety by covering the surface with a random texture pattern prior to the image capturing process. In this work, we designed three series of image patterns which are tested based on the contrast and density ratio which increases from the first to the last pattern within the same series. The performance of the patterns is evaluated by reconstructing the surface of a texture-less object and comparing it with the true data. Using the best-found patterns from the experiments, a 3D model of a Moai statue is reconstructed. The experimental results demonstrate that the density and structure of a pattern highly affects the quality of the reconstruction.
    Źródło:
    Metrology and Measurement Systems; 2018, 25, 4; 755-767
    0860-8229
    Pojawia się w:
    Metrology and Measurement Systems
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    An Experimental Study on the Determination of Optimal Lubrication Conditions in a High-Speed Spindle
    Autorzy:
    Park, S.-J.
    Hwang, Y.-K
    Lee, C.-M
    Powiązania:
    https://bibliotekanauki.pl/articles/971161.pdf
    Data publikacji:
    2009
    Wydawca:
    Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
    Tematy:
    optimal lubrication condition
    oil-air lubrication
    high speed spindle
    Opis:
    The heat generation inside spindles becomes a major factor that limits the allowable maximum rotational speed in machine tools and decreases the cutting quality. It is necessary to accurately estimate the temperature distribution in spindles caused by the heat generation in bearings and its heat transfer characteristics in order to perform the high-speed and high-precision in high-speed spindles. In addition, an accurate correction process is required according to the results of the estimation through investigating the thermal deformation error. A commercial program, MINITAB, was used to establish an experiment plan that analyzes the heat generation characteristics of the spindle system according to the operation and lubrication conditions of the spindle. Also, the change in the outer ring temperature of bearings was measured according to the experimental plan. After establishing a response surface model using the results of the experiment, the estimation equation of the quadratic polynomial model was proposed for determining the optimal lubrication condition. A verification experiment was applied to verify the accuracy of the experimental equation determined by the estimated regression model and the experimental value used in the estimation of the regression model.
    Źródło:
    Journal of Machine Engineering; 2009, 9, 2; 106-113
    1895-7595
    2391-8071
    Pojawia się w:
    Journal of Machine Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigation of Localized Electric Field in the Type-II InAs/GaAsSb/GaAs Structure
    Autorzy:
    Lee, S.
    Kim, J.
    Yoon, S.
    Kim, Y.
    Honsberg, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398577.pdf
    Data publikacji:
    2016-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.66.Fd
    78.40.-q
    73.40.Lq
    73.50.Pz
    Opis:
    The effect of localized electric field (F) was investigated in the type-II InAs/GaAsSb/GaAs structures. To compare type-I to type-II, two types of samples with different Sb contents was grown by molecular beam epitaxy, whose Sb contents are 3% (type-I) and 16% (type-II), respectively. In the both samples, we performed excitation power dependent-photoreflectance at 10 K and the result showed that the period of the Franz-Keldysh oscillation, revealed above the band gap $(E_{g})$ of GaAs, was broadened in the only type-II system, which means that F was also increased because it is proportional to the period of the Franz-Keldysh oscillation while the period of the Franz-Keldysh oscillations stayed unchanged in type-I system. This phenomenon is explained by that the F was affected by the band bending effect caused by the spatially separated photo-excited carriers in the interface between GaAsSb and GaAs. The F changed linearly as a function of square root of excitation power as expected for the F. Moreover, F was calculated using fast Fourier transform method for a qualitative analysis, which is in a good agreement with the theory of triangular well approximation.
    Źródło:
    Acta Physica Polonica A; 2016, 130, 5; 1213-1216
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Surfactant Addition on Bi2Te3 Nanostructures Synthesized by Hydrothermal Method
    Autorzy:
    Dharmaiah, P.
    Lee, C. H.
    Madavali, B.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/351609.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    bismuth telluride
    hydrothermal synthesis
    spark plasma sintering
    thermoelectric materials
    X-ray diffraction
    Opis:
    In the present work, we have prepared Bi2Te3 nanostructures with different morphologies such as nano-spherical, nanoplates and nanoflakes obtained using various surfactant additions (EG, PVP, and EDTA) by a hydrothermal method. The shape of the nanoparticles can be controlled by addition of surfactants. The samples were characterized by x-ray diffraction (XRD) and scanning electron microscopy (SEM). It is found that the minority BiOCl phase disappears after maintained pH at 10 with EG as surfactant. SEM bulk microstructure reveals that the sample consists of fine and coarse grains. Temperature dependence of thermoelectric properties of the nanostructured bulk sample was investigated in the range of 300-450K. The presence of nanograins in the bulk sample exhibits a reduction of thermal conductivity and less effect on electrical conductivity. As a result, a figure of merit of the sintered bulk sample reached 0.2 at 400 K. A maximum micro Vickers hardness of 102 Hv was obtained for the nanostructured sample, which was higher than the other reported results.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1005-1010
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Recovery Of Electrodic Powder From Spent Lithium Ion Batteries (LIBs)
    Odzysk proszku elektrodowego z zużytych akumulatorów litowo-jonowych
    Autorzy:
    Shin, S. M.
    Jung, G. J.
    Lee, W-J.
    Kang, C. Y.
    Wang, J. P.
    Powiązania:
    https://bibliotekanauki.pl/articles/354084.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    lithium ion battery
    electrodic powder
    cobalt
    lithium
    thermal treatment
    bateria litowo-jonowa
    proszek elektrodowy
    kobalt
    lit
    obróbka termiczna
    Opis:
    This study was focused on recycling process newly proposed to recover electrodic powder enriched in cobalt (Co) and lithium (Li) from spent lithium ion battery. In addition, this new process was designed to prevent explosion of batteries during thermal treatment under inert atmosphere. Spent lithium ion batteries (LIBs) were heated over the range of 300°C to 600°C for 2 hours and each component was completely separated inside reactor after experiment. Electrodic powder was successfully recovered from bulk components containing several pieces of metals through sieving operation. The electrodic powder obtained was examined by X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDS), and atomic absorption spectroscopy (AA) and furthermore image of the powder was taken by scanning electron microscopy (SEM). It was finally found that cobalt and lithium were mainly recovered to about 49 wt.% and 4 wt.% in electrodic powder, respectively.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1145-1149
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure Evolution of Tungsten-Based ODS Alloys Reinforced with the γ(Ni, Fe) Phase by a Secondary Ball Milling Method
    Autorzy:
    Chen, C.
    Zeng, Y.
    Lee, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1375180.pdf
    Data publikacji:
    2014-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.20.Ev
    81.20.Wk
    81.07.Bc
    81.05.Ni
    Opis:
    In the current study, $W-5Ni-2Fe-Y_2O_3$ model alloys were produced using a high-energy planetary ball mill. The presence of the γ(Ni, Fe) phase is favored with respect to material properties in this alloy. Therefore, a secondary ball milling method was introduced to obtain a fine and uniformly distributed γ(Ni, Fe) phase. Phase development of mechanical alloyed powders was investigated by X-ray diffraction. The results show that the formation of the γ(Ni, Fe) phase was found after 18 h of a pre-milling procedure. A further secondary milling method produced a uniform microstructure with grain refinement. TEM results also show changes in the lattice parameters of the tungsten and γ(Ni, Fe) phase associated with the solid solubility limits in the alloy produced by secondary ball milling.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 4; 907-911
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Argon Plasma in a New Process for Improving the Physical and Anti-bacterial Properties of Crosslinked Cotton Cellulose with Dimethyloldihydroxyethyleneurea-Maleic Acid
    Zastosowanie plazmy niskotemperaturowej w środowisku argonu w procesie obróbki tkanin bawełnianych sieciowanych za pomocą kwasu dimetylodihydroxyetylenourylomaleinowego dla polepszenia właściwosci fizycznych oraz antybakteryjnych
    Autorzy:
    Tsou, C H
    Suen, M C
    Tsou, C Y
    Chen, J C
    Yeh, J T
    Lin, S M
    Lai, Y C
    Hwang, J Z
    Huang, S H
    Hung, W S
    Hu, C C
    Lee, K R
    Lai, J Y
    Powiązania:
    https://bibliotekanauki.pl/articles/232331.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
    Tematy:
    cotton
    plasma
    antibacterial
    crosslinking
    crosslink length
    crosslinks number per anhydroglucose
    surface distribution
    odour absorption
    bawełna
    plazma
    właściwości antybakteryjne
    sieciowanie tkanin bawełnianych
    kwas dimetylodihydroxyetylenourylomaleinowy
    odporności na zagniecenia
    pochłanianie zapachów
    żywica termoutwardzalna
    Opis:
    This study reports the findings of an argon (Ar) plasma treatment added to the traditional pad-dry-cure process between dry and cure treatments. This new process is called the "paddry-plasma-cure process". The crosslinking agent was a mixture of dimethyloldihydroxyethyleneurea (DMDHEU) and maleic acid (MA). Results show that Ar plasma treatment can increase the bonded crosslinking agent (i.e., the nitrogen content). The dry crease recovery angle (DCRA), wet crease recovery angle (WCRA), and tensile strength retention (TSR) of the pad-dry-plasma-cure finished fabrics were higher than those of traditional pad-dry-cure finished fabrics at a given nitrogen content. Additionally it was found that the number of crosslinks per anhydroglucose unit (CL/AGU) and the length of crosslinks of pad-dry-plasma-cure-finished fabrics were higher than that of traditional pad-dry-cure finished fabrics at the same resin concentration in the pad bath. DCRA, WCRA and TSR values of pad-dry-plasma-cure-finished fabrics were higher than those of pad-dry-curefinished fabrics at the same CL/AGU value. However, activation energies for the pad-dryplasma-cure process were higher than those for the pad-dry-cure process. The anti-bacterial ability and odour absorption of the pad-dry-plasma-cure and pad-dry-plasma-cure finished fabrics were higher than those for the pad-dry-cure finished fabrics. The surface distribution of crosslinking agents for the pad-dry-plasma-cure process was higher than that of the pad-dry-cure process. Thus the pad-dry-plasma-cure process is excellent for improving the physical properties, bacterial inhibition, and odour absorption of finished cotton fabrics and for decreasing their formaldehyde release.
    Artykułu odnosi się do problematyki możliwości i celowości wprowadzenia modyfikacji plazmowej w warunkach niskociśnieniowych i w środowisku argonu do konwencjonalnego procesu wykończenia przeciw mnącego z zastosowaniem reaktywnych żywic termoutwardzalnych. Badano kąt odprężenia na sucho i na mokro, i stwierdzono polepszenie właściwości odporności na zagniecenia w wyniku dodatkowego zastosowania plazmy. Badano również właściwości antybakteryjne i pochłanianie zapachów, które okazały się korzystniejsze dla dodatkowej obróbki plazmowej. W wyniku zmodyfikowanej obróbki uzyskano mniejsze wydzielanie formaldehydu z gotowej tkaniny.
    Źródło:
    Fibres & Textiles in Eastern Europe; 2015, 1 (109); 49-56
    1230-3666
    2300-7354
    Pojawia się w:
    Fibres & Textiles in Eastern Europe
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Finite element analysis of three-point bending of a T-beam structural biaxial highly oriented polymer material
    Analiza metodą elementów skończonych zginania trójpunktowego belki teowej wykonanej z wysoko zorientowanego dwuosiowo materiału polimerowego
    Autorzy:
    Wei, C.-L.
    Chang, Y.
    Lee, Y.-C.
    Lee, R.
    Luo, T.-W.
    Chen, J.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/946988.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
    Tematy:
    solid phase processing
    highly oriented polymer (HOP)
    orthotropic materials
    T-beam
    three-point bending
    finite element
    proces w fazie stałej
    wysoko zorientowany polimer
    materiały ortotropowe
    belka teowa
    zginanie trójpunktowe
    elementy skończone
    Opis:
    Polymers with biaxial aligned molecular chains are also orthotropic materials, which are characterized by high tensile strength and low shear strength in the length direction. When orthotropic materials are used as structural shapes with poor shear strength, they are likely to undergo premature failure under shear stress. Therefore, in three-point bending, the cross-section of the entire profile not only bears tensile stress and compressive stress in the length direction, but also simultaneously exhibits shear stress. This study analyzes the distribution of tensile stress, compressive stress and shear stress in the length direction of highly oriented polymers (HOP) by finite element analysis to find the most suitable length-to-height ratio for these materials when used as structural shapes. The finite element analysis software, Abaqus, is utilized to simulate HOP T-beam to analyze the load stress of a T-beam. With a fixed cross–section area, as the length of the material changes, its shear strength also changes. Accordingly, the order of occurrence of tensile failure and shear failure can be investigated. The simulation reveals that when the length-to-height ratio is between 4 : 1 and 20 : 1, a zone of stress in which tensile failure and shear failure occur can be found. This result can be exploited in the design and development of structural beam.
    Polimery o dwuosiowo zorientowanych łańcuchach makrocząsteczek są materiałami ortotropowymi, wykazującymi dużą wytrzymałość na rozciąganie oraz niewielką wytrzymałość na ścinanie w kierunku długości. Elementy konstrukcyjne wytworzone z materiału ortotropowego o małej wytrzymałości na ścinanie są podatne na przedwczesne uszkodzenie pod wpływem naprężeń ścinających. Przy zginaniu trójpunktowym w przekroju ich profilu występują zarówno naprężenia rozciągające i ściskające w kierunku podłużnym, jak i naprężenia ścinające. Metodą elementów skończonych analizowano rozkład naprężeń rozciągających, ściskających i ścinających w kierunku podłużnym wysoko zorientowanych polimerów (HOP) w celu określenia optymalnego stosunku długości do wysokości w kształtach konstrukcyjnych. Do symulacji naprężeń obciążeniowych w zginaniu trójpunktowym belki teowej wykorzystano program komputerowy Abaqus. Stwierdzono, że przy stałej powierzchni przekroju poprzecznego belki jej wytrzymałość na ścinanie zmienia się wraz ze zmianą długości. Badano również kolejność występowania uszkodzeń pod wpływem działania sił rozciągających i ścinających. Symulacja wykazała, że przy stosunku długości do wysokości w zakresie od 4 : 1 do 20 : 1 występuje strefa naprężeń, w której mogą się pojawiać uszkodzenia w wyniku rozciągania lub ścinania. Uzyskane wyniki można wykorzystać w projektowaniu i optymalizacji belek konstrukcyjnych.
    Źródło:
    Polimery; 2018, 63, 3; 219-223
    0032-2725
    Pojawia się w:
    Polimery
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    An analysis on the thermal characteristics according to the viscosity of bearing lubricant and the cooling condition for the high speed motor spindle
    Autorzy:
    Choi, D. B.
    Lee, J. J.
    Kim, S. T.
    Kwon, H. D.
    Kim, C. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/1429194.pdf
    Data publikacji:
    2008
    Wydawca:
    Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
    Tematy:
    high speed motor spindle
    thermal displacement cooling condition
    lubricant viscosity
    Opis:
    Thermal displacement of the high speed machine tools has a large influence on machining accuracy. The high speed motor spindle with many heat sources is widely used for the high speed machine tools recently. The important problem in this spindle is to reduce and minimize the thermal effects by motor and bearings. This paper presents the analysis on thermal characteristics for high speed motor spindle system with oil-air lubricated angular contact ceramic ball bearings and built-in motor. An analysis on the thermal characteristics of spindle is performed according to the cooling conditions and the viscosity of bearing lubricants by using finite element method. This results can be applied to the design and manufacturing for the high speed motor spindle.
    Źródło:
    Journal of Machine Engineering; 2008, 8, 4; 88-98
    1895-7595
    2391-8071
    Pojawia się w:
    Journal of Machine Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Trace Elements (Co, Cr) on the Microstructure and Physical Properties of Al-Si-Cu-Mg-Fe Extruded Alloy
    Autorzy:
    Ahn, S. S.
    Sharief, P.
    Lee, C. H.
    Son, H. T.
    Kim, Y. H.
    Kim, Y. C.
    Hong, S.
    Hong, S. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/352787.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Si alloy
    microstructure
    extrusion
    coefficient of thermal expansion
    trace elements
    Opis:
    Trace elements Co, Cr were added to investigate their influence on the microstructure and physical properties of Al-Si extruded alloy. The Co, Cr elements were randomly distributed in the matrix, forms intermetallic phase and their existence wereconfirmed by XRD, EDS and SEM analysis. With addition of trace elements, the microstructure was modified, Si particle size was reduced and the growth rate of β-(Al5 FeSi) phase limited. Compared to parent alloy, hardness and tensile strength were enhanced while the linear coefficient of thermal expansion (CTE) was significantly reduced by 42.4% and 16.05% with Co and Cr addition respectively. It is considered that the low CTE occurs with addition of Co was due to the formation of intermetallic compound having low coefficient of thermal expansion. The results suggested that Co acts as an effective element in improving the mechanical properties of Al-Si alloy.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 3; 857-862
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Quantitative Analysis of Cryomilled Nanocrystalline Ti-6Al-4V Alloy Powder by X-Ray Diffraction
    Autorzy:
    Oh, M.
    Yu, H. K.
    Lee, J.-H.
    Oh, M. C.
    Jung, S.-H.
    Ahn, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/356265.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    nanocrystalline
    cryomilling
    Ti alloy
    X-ray diffraction
    size-strain plot method
    Opis:
    A nanocrystalline Ti alloy powder was fabricated using cryomilling. The grain size and lattice strain evolution during cryomilling were quantitatively analyzed using X-ray diffraction (XRD) based on the Scherrer equation, Williamson-Hall (W-H) plotting method, and size-strain (S-S) method assuming uniform deformation. Other physical parameters including stress and strain have been calculated. The average crystallite size and the lattice strain evaluated from XRD analysis are in good agreement with the result of transmission electron microscopy (TEM).
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1439-1442
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
    Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
    Autorzy:
    Son, S. H.
    Park, S. C.
    Kim, J. H.
    Kim, Y. H.
    Lee, M. S.
    Ahn, J.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/352665.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    electrorefining
    tin
    electronic waste
    recycling
    high purity
    elektrorafinacja
    cyna
    odpady elektroniczne
    recykling
    Opis:
    The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Carbon Co-Deposition During Gas Reduction of Water-Atomized Fe-Cr-Mo Powder
    Autorzy:
    Ali, B.
    Choi, S. H.
    Seo, S. J.
    Maeng, D. Y.
    Lee, C. G.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/352709.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    water atomization
    Fe-based powder
    oxide reduction
    powder metallurgy
    sinter-hardening alloys
    Opis:
    The water atomization of iron powder with a composition of Fe-3Cr-0.5Mo (wt.%) at 1600°C and 150 bar creates an oxide layer, which in this study was reduced using a mixture of methane (CH4) and argon (Ar) gas. The lowest oxygen content was achieved with a 100 cc/min flow rate of CH4, but this also resulted in a co-deposition of carbon due to the cracking of CH4. This carbon can be used directly to create high-quality, sinter hardenable steel, thereby eliminating the need for an additional mixing step prior to sintering. An exponential relationship was found to exist between the CH4 gas flow rate and carbon content of the powder, meaning that its composition can be easily controlled to suit a variety of different applications.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1119-1124
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Heat Treatment on Microstructure and Impact Toughness of Ti-6Al-4V Manufactured by Selective Laser Melting Process
    Autorzy:
    Lee, K.-A.
    Kim, Y.-K.
    Yu, J.-H.
    Park, S.-H.
    Kim, M.-C.
    Powiązania:
    https://bibliotekanauki.pl/articles/354570.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    selective laser melting
    Ti-6Al-4V
    microstructure
    impact toughness
    heat treatment
    Opis:
    This study manufactured Ti-6Al-4V alloy using one of the powder bed fusion 3D-printing processes, selective laser melting, and investigated the effect of heat treatment (650°C/3hrs) on microstructure and impact toughness of the material. Initial microstructural observation identified prior-β grain along the building direction before and after heat treatment. In addition, the material formed a fully martensite structure before heat treatment, and after heat treatment, α and β phase were formed simultaneously. Charpy impact tests were conducted. The average impact energy measured as 6.0 J before heat treatment, and after heat treatment, the average impact energy increased by approximately 20% to 7.3 J. Fracture surface observation after the impact test showed that both alloys had brittle characteristics on macro levels, but showed ductile fracture characteristics and dimples at micro levels.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1341-1346
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of Different Mechanical Milling Processes On Morphology And Microstructural Changes Of Nano And Micron Al-Powders
    Wpływ różnych procesów mielenia na morfologię i mikrostrukturę nanometrycznych i mikronowych proszków Al
    Autorzy:
    Kim, H.-S.
    Madavali, B.
    Eom, T.-J.
    Kim, C.- M.
    Koo, J.-M.
    Lee, T. H.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/355715.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al alloys
    high-energy ball milling
    low energy ball milling
    plastic deformation
    stopy Al
    wysokoenergetyczne mielenie kulkowe
    mielenie energooszczędne
    odkształcenia plastyczne
    Opis:
    In this research, effect of the various mechanical milling process on morphology and microstructural changes of nano and micron Al-powders was studied. The milling of Al-powders was performed by both high energy and low energy ball milling process. The influence of milling (pulverizing) energy on the structural changes of Al-powders was studied. Al-nanoparticles were agglomerated during the MA and its size was increased with increasing milling while micron Al-powder gets flattened shape during high energy ball milling due to severe plastic deformation. Meanwhile, structural evolution during high energy ball milling of the nano powder occurred faster than that of the micron powder. A slight shift in the position of X-ray diffraction peaks was observed in nano Al-powders but it was un-altered in macro Al-powders. The variation in lattice parameters was observed only for nano Al powders during the high energy ball milling due to lattice distortion.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1235-1239
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Oxide Formation In Metal Injection Molding Of 316L Stainless Steel
    Tworzenie tlenków podczas wtryskiwania proszku stali nierdzewnej 316L
    Autorzy:
    Jang, J. M.
    Lee, W.
    Ko, S.-H.
    Han, C.
    Choi, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/351352.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    powder injection molding
    sintering
    316L stainless steel
    sintering atmosphere
    micro parts
    wtryskiwanie proszku
    spiekanie
    stal nierdzewna 316L
    mikro-część
    Opis:
    The effects of sintering condition and powder size on the microstructure of MIMed parts were investigated using water-atomized 316L stainless steel powder. The 316L stainless steel feedstock was injected into micro mold with micro features of various shapes and dimensions. The green parts were debound and pre-sintered at 800°C in hydrogen atmosphere and then sintered at 1300°C and 1350°C in argon atmosphere of 5torr and 760torr, respectively. The oxide particles were formed and distributed homogeneously inside the sample except for the outermost region regardless of sintering condition and powder size. The width of layer without oxide particles are increased with decrease of sintering atmosphere pressure and powder size. The fine oxides act as the obstacle on grain growth and the high sintering temperature causes severe grain growth in micro features due to larger amount of heat gain than that in macro ones.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1281-1285
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    High Temperature Deformation Flow Of A ZK60A Magnesium Alloy After Extrusion
    Płynięcie stopu magnezu ZK60A podczas wysokotemperaturowego odkształcenia w trakcie wytłaczania
    Autorzy:
    Kawasaki, M.
    Lee, H. J.
    Oh, M. C.
    Ahn, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/354374.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    activation energy
    extrusion
    flow mechanics
    magnesium alloy
    tensile property
    energia aktywacji
    wytłaczanie
    mechanika przepływu
    stop magnezu
    rozciąganie
    Opis:
    Flow behavior of a ZK60A magnesium alloy after continuous casting and subsequent extrusion was examined in tension at a range of strain rates of 3.0×10-6 − 1.0×10-2 s-1 at temperatures of 473-623K. The results demonstrated that the alloy exhibited a maximum elongation of ~250% at 523K when tested at an initial strain rate of 1.0×10-5 s-1 and strain rate sensitivity, m, of ~0.3-0.4 and the activation energy of ~94 kJ/mol were calculated under the testing conditions. The detailed investigation suggested that the high temperature flow of the ZK60A alloy having submicrometer grains demonstrates quasi-superplastic flow behavior controlled by a dislocation viscous glide process.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1327-1330
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Self-Consolidation Mechanism Of Porous Ti-6Al-4V Implant Prototypes Produced By Electro-Discharge-Sintering Of Spherical Ti-6Al-4V Powders
    Mechanizm autokonsolidacji prototypów porowatych implantów wytworzonych przez spiekanie sferycznych proszków Ti-6Al-4V
    Autorzy:
    Lee, W. H.
    Jo, Y. J.
    Kim, Y. H.
    Jo, Y. H.
    Seong, J. G.
    Van Tyne, C. J.
    Chang, S. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/356277.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ti-6Al-4V
    implant
    porous
    sintering
    electrodischarge
    porowatość
    spiekanie
    proszki spiekane
    Opis:
    Electro-Discharge-Sintering (EDS) was employed to fabricate Ti-6Al-4V porous implant prototypes from atomized powders (100 – 150 μm), that were subjected to discharges of 0.75 to 2.0 kJ/0.7g-powder from 150, 300, and 450 μF capacitors. Both fully porous and porous-surfaced Ti-6Al-4V compacts with various solid core sizes were self-consolidated in less than 86 – 155 μsec. It is known that EDS can simultaneously produce the pinch pressure to squeeze and deform powder particles and the heat to weld them together. The formation of a solid core in these prototypes depends on the amounts of both the pinch pressure and heat generated during a discharge. The size of the solid core and the thickness of the porous layer can be successfully controlled by manipulating the discharge conditions such as input energy and capacitance.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1185-1189
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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