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Wyświetlanie 1-15 z 39
Tytuł:
Valorization of Cobalt from Waste LIB Cathode through Cobalt Oxalate and Cobalt Oxide Synthesis by Leaching-Solvent Extract-Precipitation Stripping
Autorzy:
Swain, B.
Lee, J.-C.
Lee, C.-G.
Powiązania:
https://bibliotekanauki.pl/articles/352333.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
valorization of cobalt
cobalt oxide powder
rod-shaped cobalt oxalate
precipitation stripping
Opis:
An ecoefficient, economical and sustainable valorization process for the synthesis of Co3O4 from waste lithium-ion battery (LIB) by leaching-solvent extract-scrubbing-precipitation stripping route has been developed. Through an optimization, the waste LIB cathode was leached using 2000 mole/m3 of H2SO4 and 5 Vol. % of the H2O2 at a pulp density of 100 kg/m3 under leaching time 60 minutes and temperature 75°C. From the separated leach liquor, cobalt was purified by saponified Cyanex 272. From cobalt, loaded Cyanex 272 impurities were scrubbed and the CoC2O4·2H2O was recovered through precipitation stripping. Finally, the precipitate was calcined to synthesize Co3O4, which is a precursor for LIB cathode materials manufacturing. From TGA-DTA, followed by XRD analysis it was confirmed that at 200°C the CoC2O4·2H2O can be converted to anhydrous CoC2O4 and at 350°C the anhydrous can be converted to Co3O4 and at 1100°C the Co3O4 can be converted to CoO. Through reported route waste LIB can back to LIB manufacturing process through a versatile and flexible industrial approach.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1037-1042
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Efficient online handwritten Chinese character recognition system using a two-dimensional functional relationship model
Autorzy:
Chang, Y. F.
Lee, J. C.
Mohd Rijal, O.
Syed Abu Bakar, S. A. R.
Powiązania:
https://bibliotekanauki.pl/articles/908140.pdf
Data publikacji:
2010
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
2D
współczynnik determinacji
rozpoznawanie
pismo odręczne
pismo chińskie
falka Haara
model relacyjny
2D functional classifier
coefficient of determination
handwritten Chinese character recognition
Haar wavelet
multidimensional functional relationship model
Opis:
This paper presents novel feature extraction and classification methods for online handwritten Chinese character recognition (HCCR). The X-graph and Y-graph transformation is proposed for deriving a feature, which shows useful properties such as invariance to different writing styles. Central to the proposed method is the idea of capturing the geometrical and topological information from the trajectory of the handwritten character using the X-graph and the Y-graph. For feature size reduction, the Haar wavelet transformation was applied on the graphs. For classification, the coefficient of determination [...] from the two-dimensional unreplicated linear functional relationship model is proposed as a similarity measure. The proposed methods show strong discrimination power when handling problems related to size, position and slant variation, stroke shape deformation, close resemblance of characters, and non-normalization. The proposed recognition system is applied to a database with 3000 frequently used Chinese characters, yielding a high recognition rate of 97.4% with reduced processing time of 75.31%, 73.05%, 58.27% and 40.69% when compared with recognition systems using the city block distance with deviation (CBDD), the minimum distance (MD), the compound Mahalanobis function (CMF) and the modified quadratic discriminant function (MQDF), respectively. High precision rates were also achieved.
Źródło:
International Journal of Applied Mathematics and Computer Science; 2010, 20, 4; 727-738
1641-876X
2083-8492
Pojawia się w:
International Journal of Applied Mathematics and Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Biological Evaluation of Anodized Biodegradable Magnesium-Calcium Alloys
Autorzy:
Kim, J.
Lee, J.
Lee, K.
Park, S.
Lim, H.
Park, C.
Bae, J.
Yun, K.
Powiązania:
https://bibliotekanauki.pl/articles/1398763.pdf
Data publikacji:
2016-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
87.85.jj
87.85.J-
Opis:
The objective of this study was to evaluate the biocompatibility of studied binary magnesium-calcium (Mg-Ca) alloys for biodegradable intraosseous implants. Mg is necessary for health and is a non-toxic biodegradable material that decomposes naturally in the body. Nevertheless, Mg has been implicated in problems including diminished physical properties and corrosion resistance when degradation is too rapid prior to bone healing. This study has explored the effect of Ca on the corrosion resistance and biological evaluation after anodizing treatment with different contents of Ca alloy. Binary Mg-0.5Ca, Mg-1Ca and Mg-5Ca alloys were prepared by the casting method under an argon atmosphere and cut into disc-shaped pieces. Pure Mg alloy was used as the control. Anodic oxidation was performed for 15 minutes at a voltage of 120 V using an electrolyte solution containing Ca gluconate, sodium hexametaphosphate, and sodium hydroxide at room temperature. Corrosion resistance was analyzed using a corrosion tester. After a hydrogen evolution test, the surface pattern and phase changes were observed on a scanning electron microscop (SEM) and energy dispersive spectroscop (EDS). Microscopic evaluation of the adhesion and cell biological functions of Mg was conducted by observing the response of human fetal osteoblastic 1.19 cells with regard to changes in surface film properties, depending on the amount of Ca. Our results support the view that in Mg-xCa alloys (x=0.5, 1, 5 wt.%) treated using anodic oxidation, the increasing Ca content controls the rate of decomposition and improves corrosion resistance.
Źródło:
Acta Physica Polonica A; 2016, 129, 4; 728-735
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Rapid Synthesis of Gold Nano-Particles Using Pulse Waved Potential in a Non-Aqueous Electrolyte
Autorzy:
Jang, J. G.
Lee, J.-O.
Lee, C. K.
Powiązania:
https://bibliotekanauki.pl/articles/352529.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gold
nanoparticle
nonaqueous electrolyte
pulse wave
catalyst
Opis:
Rapid synthesis of gold nanoparticles (AuNPs) by pulsed electrodeposition was investigated in the non-aqueous electrolyte, 1-ethyl-3-methyl-imidazoliumbis(trifluoro- methanesulfonyl)imide ([EMIM]TFSI) with gold trichloride (AuCl3). To aid the dissolution of AuCl3, 1-ethyl-3-methyl-imidazolium chloride ([EMIM]Cl) was used as a supporting electrolyte in [EMIM]TFSI. Cyclicvoltammetry experiments revealed a cathodic reaction corresponding to the reduction of gold at −0.4 V vs. Pt-QRE. To confirmthe electrodeposition process, potentiostatic electrodeposition of gold in the non-aqueous electrolyte was conducted at −0.4 V for 1 h at room temperature. To synthesize AuNPs, pulsed electrodeposition was conducted with controlled duty factor, pulse duration, and overpotential. The composition, particle-size distribution, and morphology of the AuNPs were confirmed by field-emission scanning electron microscopy (FE-SEM), energy-dispersive spectroscopy (EDS), and transmission electron microscopy (TEM). The electrodeposited AuNPs were uniformly distributed on the platinum electrode surface without any impurities arising from the non-aqueous electrolyte. The size distribution of AuNPs could be also controlled by the electrodeposition conditions.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1389-1392
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
AC Microcalorimetry of Superconducting $MgCNi_3$ Single Crystals
Autorzy:
Kačmarčík, J.
Pribulová, Z.
Samuely, P.
Marcenat, C.
Klein, T.
Jang, D.
Lee, H.
Lee, S.
Powiązania:
https://bibliotekanauki.pl/articles/1813689.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
74.70.Ad
74.25.Bt
Opis:
The low-temperature specific heat of single-crystal samples of superconducting $MgCNi_3$ with typical dimensions 200 μm were measured for the first time. A computer controlled ac microcalorimeter using an optical fiber and an infrared light-emitting diode as the heat source was used down to 2 K at magnetic fields up to 8 T. The specific heat data suggest a moderate coupling in $MgCNi_3$.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 363-366
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Study on the Optimal Design of Air Pockets in an Air Bearing Applied Tilting Index Table
Autorzy:
Lee, M.-J
Lee, C.-M
Powiązania:
https://bibliotekanauki.pl/articles/971152.pdf
Data publikacji:
2009
Wydawca:
Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
Tematy:
optimal design
tilting index table
air bearing
air pocket
Opis:
The tilting index table has attached to CNC machining center with 3axes, it can be improvement of its performance and its machining efficiency. The tilting index table is a key unit in order to manufacture some non-rotational and 3-dimensional parts, using the conventional machining center. The tilting index table is directly connected to a processing object. Regarding the increase in the deflection of the table, it directly affects processing objects and increases errors and that makes impossible to obtain desired processing precision. Thus, this study performed the shape optimization of air pockets in order to minimize the deflection presented in the existing table. In the numerical optimizing method for implementing optimal design, the general full factorial design and response surface method in the design of experiments were used. A finite element analysis was used for computational experiments in which the finite element analysis was performed by using the ANSYS Workbench, which is a type of commercial FEM tool. In addition, the analysis of the results was performed by using the commercial program, Minitab 15. The results show that the optimum design results is better than those of the initial design.
Źródło:
Journal of Machine Engineering; 2009, 9, 2; 114-123
1895-7595
2391-8071
Pojawia się w:
Journal of Machine Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Allometric scaling of marbofloxacin pharmacokinetics: a retrospective analysis
Autorzy:
Yohannes, S.
Hossain, M.A.
Kim, J.Y.
Lee, S.J.
Kwak, D.M.
Suh, J.W.
Park, S.C.
Powiązania:
https://bibliotekanauki.pl/articles/31939.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Opis:
The association between physiologically dependent pharmacokinetic parameters (CLB, T1/2β, Vdss) of marbofloxacin and body weight was studied in eight animal species based on allometric equation Y = aWb, where ‘Y’ is the pharmacokinetic parameter, ‘W’ is body weight, ‘a’ is allometric coefficient (intercept) and ‘b’ is the exponent that describes relation between pharmacokinetic parameter and body weight. The body clearance of marbofloxacin has shown significant (P<0.0001) relation with size (Bwt) in various animal species. However, half-life and volume of distribution were not in association with body weight. Although half-life and volume of distribution were not in a good correlation with body weight, statistically significant association between the body clearance and body weight suggests validity of allometric scaling for predicting pharmacokinetic parameters of marbofloxacin in animal species that have not been studied yet. However further study considering large sample size and other parameters influencing pharmacokinetics of marbofloxacin is recommended.
Źródło:
Polish Journal of Veterinary Sciences; 2014, 17, 1
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Photoluminescence Studies of Aluminum Nitride Nanowires
Autorzy:
Yang, J.
Na, H.
Kim, H.
Kebede, M.
Choi, R.
Jeong, J.
Lee, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505466.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
We report the production of AlN nanowires by the thermal heating method, for exploring their photoluminescence properties. The room-temperature photoluminescence properties were investigated with different annealing environment. While broad emissions with peaks at around 2.45 and 2.95 eV were obtained from both unannealed and annealed samples, the additional 2.1 eV peak was found from the annealed samples. We have suggested the possible emission mechanisms based on the assumption that both 2.45 eV peak and 2.1 eV peak are ascribed to the nitrogen vacancies. Annealing in N_2 environment exhibited lower intensities of 2.45 eV peak and 2.1 eV peak in comparison to those in Ar environment, presumably due to the suppression of nitrogen vacancies.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 125-127
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
System Identification from Multiple-Trial Data Corrupted by Non-Repeating Periodic Disturbances
Autorzy:
Phan, M. Q.
Longman, R. W.
Lee, S. C.
Lee, J. W.
Powiązania:
https://bibliotekanauki.pl/articles/908209.pdf
Data publikacji:
2003
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
automatyka
robotyka
system identification
disturbance identification
iterative learning control
repetitive control
interaction matrix
Opis:
Iterative learning and repetitive control aim to eliminate the effect of unwanted disturbances over repeated trials or cycles. The disturbance-free system model, if known, can be used in a model-based iterative learning or repetitive control system to eliminate the unwanted disturbances. In the case of periodic disturbances, although the unknown disturbance frequencies may be the same from trial to trial, the disturbance amplitudes, phases, and biases do not necessarily repeat. Furthermore, the system may not return to the same initial state at the end of each trial before starting the next trial. In spite of these constraints, this paper shows how to identify the system disturbance-free dynamics from disturbance-corrupted input-output data collected over multiple trials without having to measure the disturbances directly. The system disturbance-free model can then be used to identify the disturbances as well, for use in learning or repetitive control. This paper represents the first extension of the interaction matrix approach to the multiple-trial environment of iterative learning control.
Źródło:
International Journal of Applied Mathematics and Computer Science; 2003, 13, 2; 185-192
1641-876X
2083-8492
Pojawia się w:
International Journal of Applied Mathematics and Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, Structure, Photoluminescence, and Raman Spectrum of Indium Oxide Nanowires
Autorzy:
Kim, H.
Na, H.
Yang, J.
Lee,, C.
Powiązania:
https://bibliotekanauki.pl/articles/1505485.pdf
Data publikacji:
2011-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.07.-b
78.55.-m
Opis:
Production of indium oxide $(In_2O_3)$ whiskers at a very low temperature of 650°C was reported. The synthetic route was comprised of a thermal heating process of a mixture of In and Mg powders. We have investigated the structural properties of the as-synthesized nanowires by using X-ray diffraction and scanning electron microscopy. The product consisted of one-dimensional nanowires, with a crystalline cubic structure of $In_2O_3$. The photoluminescence measurement with the Gaussian fitting exhibited visible light emission bands centered at 2.1 eV and 2.8 eV. The peaks of the Raman spectrum were indexed to the modes being associated with cubic $In_2O_3$.
Źródło:
Acta Physica Polonica A; 2011, 119, 2; 143-145
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development of Carbon Nanotube Based Reflection Type X-ray Source
Autorzy:
Choi, H.
Kim, J.
Lee, C.
Powiązania:
https://bibliotekanauki.pl/articles/1807922.pdf
Data publikacji:
2009-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.47.Lx
75.47.Gk
73.50.Fq
Opis:
X-ray imaging technology is a useful and leading medical diagnostic tool for health care professionals to diagnose disease in human body. Carbon nanotube based X-ray source, which we have developed in this study, could be also useful and supply integrated diagnostic X-ray imaging tool in diagnosis. Conventionally, thermionic type of tungsten filament X-ray tube is widely employed in the field of biomedical and industrial application fields. However, intrinsic problems, such as poor emission efficiency, low imaging resolution, and high electrical energy consumption etc., may cause the limitation of using the X-ray tube. To fulfill the current market requirement, specifically for medical diagnostic field, we have developed rather a portable and compact carbon nanotube based X-ray device in which microfocus high imaging resolution can be feasible.
Źródło:
Acta Physica Polonica A; 2009, 115, 6; 1078-1080
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 39

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