Informacja

Drogi użytkowniku, aplikacja do prawidłowego działania wymaga obsługi JavaScript. Proszę włącz obsługę JavaScript w Twojej przeglądarce.

English (EN)·Polski (PL)·Yкраїнський (UK)
Przejdź do strony domowej biblioteki Centralna Biblioteka Wojskowa Link otwiera się w nowym oknie Logo biblioteki Prolib Integro - strona głównaCentralna Biblioteka Wojskowa

Wyszukujesz frazę "Fe powder" wg kryterium: Wszystkie pola

  Lista filtrów
Wyrównaj
    Wyświetlanie 1-45 z 45
    Tytuł:
    Densification and Magnetic Properties of Fe Powder Compacts According to Heat-Treatment Conditions
    Autorzy:
    Yoo, Hyo-Sang
    Kim, Yong-Ho
    Kim, Cheol-Woo
    Son, Hyeon-Taek
    Powiązania:
    https://bibliotekanauki.pl/articles/2203721.pdf
    Data publikacji:
    2023
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Fe powder
    heat-treatment
    microstructure
    density
    Opis:
    In this study, the effects of heat-treatment conditions of Fe powder compacts on densification, microstructure, strength and magnetic properties were investigated. The prepared Fe powder was compressed in a mold of diameter 20 mm at a pressure of 800 MPa for 30 sec. This Fe powder compact was heat-treated under different atmospheres (air and 90% Ar + 10% H2 and heat-treatment temperatures (300 and 700℃). The Fe powder compacts heat-treated in an Ar+H2 mixed gas atmosphere showed a denser microstructure and higher density than the Fe powder compacts heat-treated in an air atmosphere. Oxygen content in the heat-treatment conditions played a significant role in the improvement of the densification and magnetic properties.
    Źródło:
    Archives of Metallurgy and Materials; 2023, 68, 1; 47--50
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of Mechanical Alloying Parameters on Phase Formation in Al-Cu-Fe Powder
    Autorzy:
    Mitka, M.
    Lityńska-Dobrzyńska, L.
    Góral, A.
    Maziarz, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/1375540.pdf
    Data publikacji:
    2014-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.20.Ev
    61.44.Br
    61.05.cp
    68.37.Hk
    Opis:
    In the present study the effect of mechanical alloying parameters on phase formation in $Al_{62}Cu_{25.5}Fe_{12.5}$ (at.%) alloy was investigated. Mixtures of Al, Cu and Fe powder with different particles size were ball milled in Fritsch 5 Pulverisette planetary mill using tungsten carbide vials and balls. The milling was performed with the rotation speed 250 and 300 rpm up to 40 h. Stearic acid or hexane were used as process control agent (PCA). The microstructure of the powders prepared with different milling parameters was investigated using X-ray diffraction and scanning electron microscopy. It was found that increase of the rotation speed as well as decrease of particle size of initial Al powder particles accelerates the formation of homogeneous microstructure of the powder. The mixture of icosahedral quasicrystal and β-Al(Cu, Fe) cubic phase has been obtained for the powders milled at 300 rpm up to 20 h. Prolonged milling time results in transformation to single ordered β phase.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 4; 984-987
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Magnetic Properties of Sintered Fe₅₀Co₅₀ Powder Cores
    Autorzy:
    Olekšáková, D.
    Kollár, P.
    Füzer, J.
    Onderko, F.
    Dobák, S.
    Viňáš, J.
    Fáberová, M.
    Bureš, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/1032708.pdf
    Data publikacji:
    2017-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Vv
    85.70.-w
    75.50.Bb
    Opis:
    We investigated coercivity, total losses and complex permeability of sintered Fe-Co powder cores to detect magnetization processes performing in ac magnetic field. The Fe-Co solid solution alloy powders with 50:50 wt% ratio were prepared by 1, 15, and 20 h alloyed mixture of pure chemical elements in planetary ball mill. The resulting powder was subsequently sintered into a disk form. The compaction was performed at a pressure of 800 MPa for 5 min at temperatures of 400°C, 500°C and 600°C in vacuum oxidation protective atmosphere, with pressure of 5×10¯³ Pa. The best magnetic properties exhibit sample prepared from 1 h alloyed powder, compacted at 600°C.
    Źródło:
    Acta Physica Polonica A; 2017, 131, 4; 807-809
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Consolidation of Nanocrystalline Nd-Fe-B Powder by Hydrostatic Extrusion at High Temperature
    Autorzy:
    Gizynski, T.
    Kaszuwara, W.
    Kulczyk, M.
    Leonowicz, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1030247.pdf
    Data publikacji:
    2017-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Ww
    Opis:
    Hydrostatic extrusion is a modern method of shaping material microstructure and properties. Hydrostatic extrusion can also be successfully used for consolidation of hard magnetic powders. The effect of extrusion temperature, within the range of 700-800°C, on the magnetic properties of the bulk, final product was studied. A commercial MQU-F42 powder, dedicated to hot pressing, was placed in copper capsules and initially cold compacted up to 60% of the theoretical density. Subsequently, the billet was heated in an oven to temperatures 700 and 800°C, respectively and subjected to hydrostatic extrusion. The extruded product had a form of a copper rod, with the Nd-Fe-B core, having 96% of theoretical density (true strain 1.85 after extrusion at 800°C). The extrusion process led to deterioration of the coercivity, for which coarsening of the Nd₂Fe₁₄B grains was blamed. In order to prove this hypothesis, the starting powder was annealed in a temperature range of 550-900°C for various times. The crystallite size, measured after annealing by the X-ray diffraction method, showed that with extension of time and elevation of the temperature the crystallite size increases, however the dominating parameter is the temperature. Correlation of the crystallite size with temperature indicates that when the crystallites are larger than 80 nm the magnetic properties dramatically decrease. Additionally, after HE at 800°C micrometric size Nd-rich phase appear in the microstructure. The Nd is squeezed from the grain boundary of the Nd₂Fe₁₄B phase leading to non-isolated grains, which also contributes to the deterioration of the coercivity.
    Źródło:
    Acta Physica Polonica A; 2017, 131, 5; 1260-1263
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Properties of Magnets Obtained by Hydrostatic Extrusion of Nd-Fe-B Powder
    Autorzy:
    Gizynski, T.
    Kaszuwara, W.
    Pawlik, P.
    Kulczyk, M.
    Leonowicz, M.
    Michalski, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/1387955.pdf
    Data publikacji:
    2015-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Ww
    Opis:
    Nd-Fe-B MQ powder was initially densified in a copper capsule to reach about 60% of the theoretical density. Subsequently, three various processes of hydrostatic extrusion were conducted at room temperature. The values of true strain, obtained during the all three stages, were 1.38, 0.89, 0.94, respectively. The investigation performed showed that the coercivity of the material decreases as the strain increases. Decrease of the remanence was observed only for the highest strains. Size of the particles was strongly reduced during the extrusion processes. X-ray diffraction did not show changes in the phase structure of the material. The Mössbauer study, of the sample extruded within all the three stages, showed existence of the Nd₂Fe₁₄B phase and 16% of other phase. Analysis of magnetization versus temperature confirmed that the additional phase was ferromagnetic.
    Źródło:
    Acta Physica Polonica A; 2015, 127, 2; 626-628
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Imaging of Magnetic Domains and Domain Walls in Spherical Fe-Si Powder Using Magnetic Force Microscopy
    Autorzy:
    Strečková, M.
    Baťková, M.
    Baťko, I.
    Hadraba, H.
    Bureš, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/1367241.pdf
    Data publikacji:
    2014-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Bb
    75.60.Ch
    75.70.Kw
    Opis:
    The commercial Fe-Si powder, produced by Högänes Corporation, represents promising soft magnetic material for technological applications. The powder consists of spherical particles with diameter up to 150 μm. Internal microstructure of the powder is formed by grains of diameter of about 30 μm. Each separate grain has a random orientation of the easy magnetization axis and is sufficiently large to split into several magnetic domains. A comparative study of the atomic force microscopy (AFM) topography and the corresponding magnetic force microscopy (MFM) images was employed in order to examine the correlation between the grain size, boundaries of grains and characterization of the magnetic domains, which gives us an important knowledge about possible behavior of particles under the influence of the external magnetic field and further utilization of the spherical Fe-Si particles in electrotechnical industry. The grain size and the crystallographic orientation of grains were analyzed by the electron backscattering diffraction (EBSD) technique.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 1; 92-93
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Carbon Co-Deposition During Gas Reduction of Water-Atomized Fe-Cr-Mo Powder
    Autorzy:
    Ali, B.
    Choi, S. H.
    Seo, S. J.
    Maeng, D. Y.
    Lee, C. G.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/352709.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    water atomization
    Fe-based powder
    oxide reduction
    powder metallurgy
    sinter-hardening alloys
    Opis:
    The water atomization of iron powder with a composition of Fe-3Cr-0.5Mo (wt.%) at 1600°C and 150 bar creates an oxide layer, which in this study was reduced using a mixture of methane (CH4) and argon (Ar) gas. The lowest oxygen content was achieved with a 100 cc/min flow rate of CH4, but this also resulted in a co-deposition of carbon due to the cracking of CH4. This carbon can be used directly to create high-quality, sinter hardenable steel, thereby eliminating the need for an additional mixing step prior to sintering. An exponential relationship was found to exist between the CH4 gas flow rate and carbon content of the powder, meaning that its composition can be easily controlled to suit a variety of different applications.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1119-1124
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Effect of Transition Metals on Quasicrystalline Phase Formation in Mechanically Alloyed Al65Cu20Fe15 Powder
    Autorzy:
    Mitka, M.
    Kalita, D.
    Góral, A.
    Lityńska-Dobrzyńska, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/351525.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    mechanical alloying
    quasicrystal
    Al-Cu-Fe
    transition metals
    Opis:
    The effect of replacing iron with transition metals (M = Mn, Cr, Co) on the microstructure of mechanically alloyed Al65 Cu20 Fe15 quasicrystalline powder was examined by X-ray diffraction and transmission electron microscopy methods. Powders of various compositions were milled in a high-energy planetary ball mill up to 30 hours at a rotation speed 350 rpm using WC milling media. The amount of the fourth additions was constant in all powders and Fe atoms were replaced with Mn, Cr or Co in a 1:1 ratio, while the content of the Al and Cu was selected in two ways: they remained the same as in the initial ternary Al65 Cu20 Fe15 alloy or changed to obtain e/a ratio = 1.75 (optimal for icosahedral quasicrystalline phase). Quasicrystalline phase formed in the quaternary Al65 Cu20 Fe7.5 M7.5 powders, whereas in the second group of compositions only crystalline phases were identified.
    Źródło:
    Archives of Metallurgy and Materials; 2020, 65, 3; 1129-1133
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Post-Heat Treatment on Microstructure and Mechanical Properties of Cu-Fe-Co Powder Alloy Fabricated by Hot Pressing
    Autorzy:
    Çelik, E.
    Aslan, A. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/353200.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    diamond cutting tools
    Cu-Fe-Co alloy
    powder metallurgy
    hot pressing
    heat treatment
    Opis:
    In this study, the powder mixture which consists of Cu-Fe-Co was produced by using the method of hot pressing technique. In addition, effect of heat treatment process on microstructure and mechanical properties of this alloy was investigated. Following the hot pressing process applied on the samples, heat treatment was carried out at 950°C for two different dwelling times (90 and 180 minutes). Measured density values were considered as physical characteristics, while hardness and fracture strength values were considered as mechanical characteristics. It was observed that porosity rates of hot pressed samples were decreased by increasing of temperature and pressing parameters. In this study it was observed that Cu was spread in matrix and filled the micro porosities. Hardness values were determined to be decreased as a result of grain growth after heat treatment process. That 4 fold increased elongation % values which were achieved by TRS experiments were observed as well.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 1; 371-377
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and Characterization of Fe/$SiO_{2}$ Powder Composites Using Impregnation Method
    Autorzy:
    Kabátová, M.
    Füzer, J.
    Füzerová, J.
    Dudrová, E.
    Kollár, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1367476.pdf
    Data publikacji:
    2014-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.20.Ev
    77.84.Lf
    75.60.Ej
    Opis:
    Fe/$SiO_{2}$ powder composite materials based on irregularly and/or spherically shaped iron powder particles with an addition of $SiO_{2}$ nanopowder were prepared in two ways, (i) by mixing the Fe/$SiO_{2}$ powder with 1.0 wt.% of Shellac dissolved in ethanol and (ii) by vacuum/pressure impregnation of low-temperature sintered Fe/$SiO_{2}$ components with shellac dissolved in ethanol and with thermoplast SL450. $SiO_{2}$ was implemented either as nanopowder or by sol-gel coating. Vacuum/pressure impregnation (VPI) of pre-sintered samples was performed in a steel container. The influence of iron particle shape and processing conditions on the electro-insulating layer was microscopically evaluated and correlated with the values of the electrical resistivity and coercivity. It has been found that the continuity, distribution and thickness of insulating phase is strongly controlled by the shape of iron particles. Using the VPI procedure, the irregular surface of iron particles may cause discontinuities of insulating layer, while the spherical iron particles are well covered with continuous evenly distributed insulating layer.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 1; 134-135
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Application of a Ball-milled Fe-Cu-Ni Powder Mixture to Fabricate Sintered Diamond Tools
    Autorzy:
    Borowiecka-Jamrożek, J.
    Konstanty, J.
    Lachowski, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/383184.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    metallography
    mechanical properties
    sintered diamond tools
    powder mixtures
    hot pressing
    metalografia
    właściwości mechaniczne
    narzędzia diamentowe
    prasowanie na gorąco
    Opis:
    This article discusses results of an analysis of mechanical properties of a sintered material obtained from a mixture of elemental iron, copper and nickel powders ball milled for 60 hours. The powder consolidation was performed by hot pressing in a graphite mould. The hot pressing was carried out for 3 minutes at 900 °C and under a pressure of 35 MPa. The sintered specimens were tested for density, porosity, hardness and tensile strength. Their microstructures and fracture surfaces were also examined using a scanning electron microscope (SEM). The study was conducted in order to determine the suitability of the sintered material for the manufacture of metal-bonded diamond tools. It was important to assess the effects of chemical composition and microstructure of the sintered material on its mechanical properties, which were compared with those of conventional metal bond material produced from a hot-pressed SMS grade cobalt powder. Although the studied material shows slightly lower strength and ductility as compared with cobalt, its hardness and offset yield strength are sufficiently high to meet the criteria for less demanding applications.
    Źródło:
    Archives of Foundry Engineering; 2018, 18, 1; 5-8
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Adhesion of the powder flame sprayed coatings using Fe-Cr-Co-Mo powder
    Autorzy:
    Rzeźnikiewicz, A.
    Cetnarowski, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/115133.pdf
    Data publikacji:
    2018
    Wydawca:
    Stowarzyszenie Inżynierów i Techników Mechaników Polskich
    Tematy:
    natryskiwanie płomieniowo-proszkowe
    powłoka natryskiwana
    siła przyczepności
    modyfikacja powierzchni
    powder flame spraying
    spraying coating
    adhesion strength
    surface modification
    Opis:
    The aim of the research was to assess the adhesion of the powder flame sprayed coatings to the previously prepared substrate. The spraying tests were carried out using Rototec 51000 base powders which was Ni-Al-Mo alloys, then coated with an outer coating made of Rototec 19404, which is an alloy Fe-Cr-Co-Mo. The coatings were tested for adhesion in accordance with the PN-EN ISO 14916:2017 standard and also topography tests of sprayed coatings using scanning electron microscopy.
    Źródło:
    Welding Technology Review; 2018, 90, 11; 16-19
    0033-2364
    2449-7959
    Pojawia się w:
    Welding Technology Review
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characteristics Of The Porous Body Sintered By Nano-Sized Fe-Cr-Al Alloy Powder
    Charakterystyka porowatego korpusu spiekanego z nanometrycznego proszku stopu Fe-Cr-Al
    Autorzy:
    Lee, S.-I.
    Lee, S.-H.
    Gu, B.-U.
    Lee, D.-W.
    Kim, B.-K.
    Powiązania:
    https://bibliotekanauki.pl/articles/356635.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Fe-Cr-Al powder
    metallic sponges
    sintering temperature
    oxidation resistance
    proszek Fe-Cr-Al
    proszek nanometryczny
    temperatura spiekania
    odporność na utlenianie
    Opis:
    Porous metal with uniform honeycomb structure was successfully produced by sintering using Fe-Cr-Al nano powder, which was prepared by the pulsed wire evaporation (PWE) in ethanol. Its process consisted of the several steps; 1) coating on the surface of polyurethane sponge with the liquid droplets generated from the ethanol-based slurry where the Fe-Cr-Al nano powders were uniformly dispersed, 2) heat treatment of debinding to remove the polyurethane sponge and 3) sintering of the porous green body formed by Fe-Cr-Al nano powders. The strut thickness of porous Fe-Cr-Al was increased by the increase of spraying times in ESP step. Also, The shrinkages and the oxidation resistance of the sintered porous body was increased with increase of sintering temperature. The optimal sintering temperature was shown to 1450°C in views to maximize the oxidation resistance and sinterability.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1275-1279
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characteristics of Al-Fe sinters made by the powder metallurgy route
    Charakterystyka spieków Al-Fe wytworzonych metodą metalurgii proszków
    Autorzy:
    Majchrowska, M.
    Lasek, K.
    Nowak, M.
    Pałka, P.
    Sułkowski, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/264175.pdf
    Data publikacji:
    2018
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
    Tematy:
    Al/Fe sinters
    powder metallurgy
    interface
    intermetallic compounds
    microstructure
    spieki Al/Fe
    metalurgia proszków
    interfejs
    związki międzymetaliczne
    mikrostruktura
    Opis:
    The Al/Fe material was prepared by the powder metallurgy route with an additional intermediate stage which was a centrifuge of powder mixture. The application of the centrifuge stage was applied to obtain circular phase distribution of Al-rich phases in a sintered material. Iron powder with a particle size under 100 μm and aluminum powder with a particle size of about 25 μm, were used as starting materials. To determine the effect of centrifuging time on the distribution of Fe-Al particles, scanning electron microscopy (SEM, EDS) and XRD techniques were used. Microstructure observations show the influence of the centrifuging time on the distribution of Fe particles. It was observed that a longer centrifuging time caused changes in the ratio concentration of elements and allowed the growth of the intermetallic phase at the interface between solid Al and Fe particles.
    Spiekane materiały Al/Fe wytwarzano metodą metalurgii proszków z wprowadzeniem etapu pośredniego w postaci odwirowania mieszaniny proszku. Etap wirowania miał na celu uzyskanie kulistego rozkładu faz bogatych w Al w spiekanym materiale. Proszek żelaza o wielkości cząstek poniżej 100 μm i proszek aluminium o wielkości cząstek około 25 μm zastosowano jako materiały wyjściowe. W celu określenia wpływu czasu wirowania mieszanki na rozkład faz w wytworzonym materiale zastosowano techniki skaningowej mikroskopii elektronowej (SEM, EDS) i dyfraktometrii rentgenowskiej (XRD). Obserwacje mikrostruktury wykazały istotny wpływ czasu wirowania na mikrostrukturę uzyskanych spieków. Zaobserwowano, że dłuższy czas wirowania spowodował zmianę stosunku stężenia pierwiastków i pozwolił na wzrost fazy międzymetalicznej na granicy faz między stałymi cząstkami Al i Fe. Badania mikrotwardości obszarów spiekanego materiału świadczą o zwiększeniu twardości w obszarach nowo utworzonych faz międzymetalicznych.
    Źródło:
    Metallurgy and Foundry Engineering; 2018, 44, 4; 195-203
    1230-2325
    2300-8377
    Pojawia się w:
    Metallurgy and Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Manufacturing And High Temperature Oxidation Properties Of Electro-Sprayed Fe-24.5% Cr-5%Al Powder Porous Metal
    Wytwarzanie i wysokotemperaturowe utlenianie elektro-rozpylanego porowatego proszku Fe-24.5% Cr-5%Al
    Autorzy:
    Lee, K-A.
    Oh, J-S.
    Kong, Y-M.
    Kim, B-K.
    Powiązania:
    https://bibliotekanauki.pl/articles/350912.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    powder porous metal
    electro-spray process
    electric wire explosion
    Fe-24Cr-5Al
    high temperature oxidation
    porowaty proszek metalu
    elektrorozpylanie
    utlenianie wysokotemperaturowe
    Opis:
    Fe-Cr-Al based Powder porous metals were manufactured using a new electro-spray process, and the microstructures and high-temperature oxidation properties were examined. The porous materials were obtained at different sintering temperatures (1350°C, 1400°C, 1450°C, and 1500°C and with different pore sizes (500 μm, 450 μm, and 200 μm). High-temperature oxidation experiments (TGA, Thermal Gravimetry Analysis) were conducted for 24 hours at 1000°C in a 79% N2+ 21% O2, 100 mL/min. atmosphere. The Fe-Cr-Al powder porous metals manufactured through the electro-spray process showed more-excellent oxidation resistance as sintering temperature and pore size increased. In addition, the fact that the densities and surface areas of the abovementioned powder porous metals had the largest effects on the metal’s oxidation properties could be identified.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1169-1173
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructural Evolution of Sinter-Forged Fe-Cr-Mo-C Alloy Depending on Cu Addition
    Autorzy:
    Oh, Min Chul
    Kim, Moontae
    Lee, Jisung
    Ahn, Byungmin
    Powiązania:
    https://bibliotekanauki.pl/articles/355446.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Astaloy CrL
    Fe-based alloy
    pre-alloyed powder
    powder forging
    microstructure
    Opis:
    Pre-alloyed Astaloy CrLTM (Fe-1.5 wt% Cr-0.2 wt% Mo), a commercial Fe-based alloy powder for high strength powder metallurgy products, was sintered and hot forged with additions of 0.5 wt% C and 0~2 wt% Cu. To investigate the influence of various Cu contents, the microstructural evolution was characterized using density measurements, scanning electron microscope (SEM) and electron backscatter diffraction (EBSD). Transverse rupture strength (TRS) was measured for each composition and processing stage. The correlation between Cu additions and properties of sinter-forged Fe-Cr-Mo-C alloy was discussed in detail.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 2; 539-542
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Powder Size on the Microstructure and Magnetic Properties of Nd-Fe-B Magnet Alloy
    Autorzy:
    Cho, Ju-Young
    Abbas, Sardar Farhat
    Choa, Yong-Ho
    Kim, Taek-Soo
    Powiązania:
    https://bibliotekanauki.pl/articles/353634.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B
    gas atomization
    powder size
    crystal orientation
    hot deformation
    Opis:
    Rare earth Nd-Fe-B, a widely used magnet composition, was synthesized in a shape of powders using gas atomization, a rapid solidification based process. The microstructure and properties were investigated in accordance with solidification rate and densification. Detailed microstructural characterization was performed by using scanning electron microscope (SEM) and the structural properties were measured by using X-ray diffraction. Iron in the form of α-Fe phase was observed in powder of about 30 μm. It was expected that fraction of Nd2 Fe14 B phase increased rapidly with decrease in powder size, on the other hand that of α-Fe phase was decreased. Nd-rich phase diffused from grain boundary to particle boundary after hot deformation due to capillary action. The coercivity of the alloy decreased with increase in powder size. After hot deformation, Nd2 Fe14 B phase tend to align to c-axis.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 2; 623-626
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Particle Size of a Powder upon the Properties and Microstructure of Boron-modified Fe-Ni-Mo-Cu Sinters
    Autorzy:
    Karwan-Baczewska, Joanna
    Perek-Nowak, Małgorzata
    Majchrowska, Magdalena
    Rosso, Mario
    Powiązania:
    https://bibliotekanauki.pl/articles/2201983.pdf
    Data publikacji:
    2023
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
    Tematy:
    processing
    powder metallurgy
    Distaloy SA powder
    activated sintering
    particle fraction
    Opis:
    The article discusses the effect of different particle fractions of prealloyed iron powder on the microstructure, density and hardness of sintered material. Each particle fraction (apart from 160–200 µm, which is a trace fraction) was modified with boron, its contents being, respectively, 0.2 wt.%, 0.4 wt.% and 0.6 wt.%. Next, the powder mixtures were pressed under a pressure of 600 MPa, and the final compacts were subject to sintering at 1200°C for 60 min in a hydrogen atmosphere. It was observed that the higher values of density and hardness were found in samples made from finer fractions of powder. A higher homogeneity of the microstructure and the highest degree of compactness was obtained in sinters from powder of 40–56 µm particle size, with 0.4 wt.% boron. Due to the use of small particle fractions of prealloyed powder, a higher degree of compactness in sinters was obtained with lower boron content. Also indicated was which particle fraction of Fe-Ni-Mo-Cu powder should be applied to obtain density in sinters with boron addition equal to almost 100% of the relative density of the analyzed alloy. The presented studies have both scientific and technological aspects.
    Źródło:
    Journal of Casting & Materials Engineering; 2023, 7, 1; 1--8
    2543-9901
    Pojawia się w:
    Journal of Casting & Materials Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Effect of Powder Particle Biencapsulation with Ni-P Layer on Local Corrosion of Bonded Nd-(Fe,Co)-B Magnetic Material
    Bienkapsulacja cząstek proszku powłokami Ni-P jako sposób poprawy odporności wiązanych magnesów Nd-(Fe,Co)-B na korozję lokalną
    Autorzy:
    Klimecka-Tatar, D.
    Pawłowska, G.
    Sozańska, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/352049.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B bonded magnets
    biencapsulation
    local corrosion
    Ni-P layers
    magnes wiązany
    bienkapsulacja
    korozja
    powłoki Ni-P
    Opis:
    Effect of the Nd-(Fe,Co)-B powder particle biencapsulation with Ni-P layer on bonded magnetic materials corrosion behaviour has been investigated. Bonded magnets were prepared from single-phase, nanocrystalline magnetic Nd11 Fe77 Co5 B6 powder. Powder particles before consolidation were preliminary etched and then coated with bilayer (powder biencapsulation). The powder surface was coated as a first with autocatalytic applied Ni-P layer during 5, 15 and 30 minutes in Ni(II) containing bath and the second layer was thermosetting epoxy-resin. Impact of the used biencapsulation process was rated on the basis of polarization curves recorded in phosphate environment with addition of chloric ions. It has been established that the used biencapsulation method satisfactorily isolate individual particles of the powder and consequently, significantly inhibits corrosion processes of the final material, especially in passivating environment containing Cl-.
    W pracy zaprezentowano wyniki badań nad wpływem bienkapsulacji cząstek proszku powłokami Ni-P/żywica epoksy-dowan na odporność korozyjną magnesów wiązanych. Materiały magnetyczne zostały przygotowane z jednofazowego, na-nokrystalicznego proszku Nd11 Fe77 Co5 B6. Cząstki proszku przed konsolidacją były wstępnie trawione, a następnie pokryte podwójną warstwą (bienkapsulacja proszku). Powierzchnia proszku w pierwszej kolejności została poddana 5 i 30 minutowemu autokatalitycznemu nanoszeniu warstw Ni-P. Drugą warstwę stanowił materiał spoiwa, czyli żywica epoksydowa. Dokonano oceny wpływu zastosowanej metody bienkapsulacji na odporność na korozję lokalną na podstawie krzywych polaryzacji zarejestrowanych w środowisku fosforanowym (0,5M, pH = 3) z dodatkiem jonów chlorowy. Stwierdzono, że zastosowane metody bienkapsulacji zadowalająco izolują pojedyncze cząstki proszku, a co za tym idzie, hamują proces korozji materiału końcowego, zwłaszcza w środowisku pasywującym zawierającym Cl- .
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 1; 153-157
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structure and Properties of Fe-Ni-Al-Si Alloys Produced by Powder Metallurgy
    Autorzy:
    Novák, P.
    Mejzlíková, L.
    Hošek, V.
    Martínek, M.
    Marek, I.
    Michalcová, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1418514.pdf
    Data publikacji:
    2012-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.66.Dk
    62.20.Qp
    Opis:
    Reactive sintering powder metallurgy is a simple alternative to conventional melting and powder metallurgy processes. During this process, pressed powder mixture of pure metals or other precursors is transformed into bulk intermediary phases by thermally activated in situ reaction. This process was previously tested on Fe-Al and Fe-Al-Si alloys. Positive effect of silicon on the reactive sintering behaviour was determined, leading to the development of novel carbon-free high-silicon FeAl20Si20 alloy (given in wt%). In this work, the effect of nickel on the pressureless reactive sintering of Fe-Al-Si pressed powder mixtures was studied. To explain the nickel influence, differential thermal analysis was utilized. Microstructure, phase composition and porosity of the FeAl20Si20Nix (x = 0, 5, 10, 20 wt%) alloys was described. Hardness, wear resistance, high-temperature oxidation resistance and thermal stability were evaluated as functions of nickel content. Results showed that porosity decreases with growing nickel content down to less than 3 vol.%. Oxidation rate of these alloys is more than 10 times lower than that of original FeAl20Si20 alloy. Thermal stability and abrasive wear resistance of these alloys is also superior to Fe-Al and Fe-Al-Si materials.
    Źródło:
    Acta Physica Polonica A; 2012, 122, 3; 524-527
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Mechanical Activation on the in situ Formation of TiB2 Particulates in the Powder Mixture of TiH2 and FeB
    Autorzy:
    Huynh, X.-K.
    Kim, B.-W.
    Kim, J. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/355844.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    mechanical activation
    in situ formation
    TiB2 particulate
    Fe-matrix
    specific ball-milling energy
    Opis:
    The in situ formation of TiB2 particulates via an interface reaction between Ti and FeB powders was studied. The effects of mechanical activation by high-energy milling on the decomposition of TiH2 and the interface reactions between Ti and FeB powders to form TiB2 were investigated. Powder mixtures were fabricated using planetary ball-milling under various milling conditions. The specific ball-milling energy was calculated from the measured electrical power consumption during milling process. High specific milling energy (152.6 kJ/g) resulted in a size reduction and homogeneous dispersion of constituent powders. This resulted in a decrease in the decomposition temperature of TiH2 and an increase in the formation reaction of TiB2 particulates in the Fe matrix, resulting in a homogeneous microstructure of nanoscale TiB2 evenly distributed within the Fe matrix. In contrast, the powder mixture milled with low specific milling energy (36.5 kJ/g) showed an inhomogeneous microstructure composed of relatively large Fe-Fe2 B particles surrounded by a thin layer of Fe-TiB2 within a finely dispersed Fe-TiB2 matrix region.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1393-1398
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Effect of Adding Iron Powder From Plasma Cutting on the Microstructure, Mechanical Properties of the Composite Based on Aluminum Powder Matrix Made Using Powder Metallurgy
    Autorzy:
    Wędrychowicz, M.
    Bydałek, A. W.
    Migas, P.
    Skrzekut, T.
    Noga, P.
    Madej, P.
    Kałasznikow, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/2049543.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Fe composite
    iron powder
    plasma cutting
    aluminum matrix composites
    powder metallurgy
    mechanical properties
    Opis:
    The paper presents the results of research on the effect of added iron powder from plasma cutting on the mechanical properties and structure of a composite rod based on aluminum powder. The iron powder came from plasma cutting of steel elements and was handed over by the enterprise “AK Anatol” from Żary. One of the ways to dispose of it is to use it as a filler in aluminum composite rods. Research shows that Fe can be distributed in aluminum evenly, and increase in mechanical properties is achieved at the expense of only a slight increase in density. The proposed system does not reduce the amount of waste produced by plasma cutting but finds a use for some of it. The sintering point of the powder required a strongly reducing atmosphere (Po2 < 10-50 atm) which seems virtually unachievable under laboratory conditions. The reinforcing mechanism is related to the fragmentation of the matrix aggregate particles and the uniform distribution of Fe particles in the aluminum matrix.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 1; 273-279
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The influence of Iron and Aluminium Powder Pressing on the Course of Shrinkage and Properties of the Fe40Al Phase Obtained by Reaction Sintering
    Autorzy:
    Berendt-Marchel, M.
    Siemiaszko, Dariusz
    Powiązania:
    https://bibliotekanauki.pl/articles/2048785.pdf
    Data publikacji:
    2022
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    intermetallic
    powder metallurgy
    reaction sintering
    mechanical properties
    Opis:
    The effect of the compaction rate on the structure, microstructure and properties of Fe-Al sinters obtained during the SHS reaction is presented in this paper. It was found that increasing the uniaxial pressing pressure led to the increase of the contact area between iron and aluminium particles, which improved the conduction and lowered heat losses during the self-propagating high-temperature synthesis (SHS) reaction and thus result with a sintered material with an improved phase homogeneity. On the other hand, an increase in the pressing pressure causes air be trapped in the pores and later on reacts with iron and aluminium to form oxides. In this work, the shrinkage course was analysed at six different pressing pressures: 50, 100, 150, 200, 300 and 400 MPa. The green compacts were then subjected to the PAIS process (pressure-assisted induction sintering) at a temperature of 1000°C under a load of 100 kN for 5 min. Such prepared samples were subjected to density, porosity, and microhardness (HV0.1) measurements. X-ray diffraction phase analysis and SEM observations were performed together with EDS chemical composition measurements. For studied chemical composition of the samples and sample geometry, 200 MPa compacting pressure was found to be optimal in order to obtain the best sample homogeneity.
    Źródło:
    Archives of Metallurgy and Materials; 2022, 67, 1; 121-126
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of wear mechanisms in sintered Fe-1.5 Wt % Cu alloys
    Charakterystyka mechanizmów zużycia spiekanych stopów Fe-1.5Cu
    Autorzy:
    Mazahery, A.
    Shabani, M. O.
    Powiązania:
    https://bibliotekanauki.pl/articles/354551.pdf
    Data publikacji:
    2012
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    właściwości tribologiczne
    proszki spiekane
    porowatość
    tribological properties
    powder processing
    porosity
    Opis:
    In this research, increasing amount of ultimate tensile strength and hardness in sintered Fe-1.5 Wt % Cu alloys is observed with increasing the density. The influence of different applied pressure of 300, 450, 600 and 750 MPa on porosity and wear behavior has been also studied. Cross-section micrographs of worn surfaces show that the pores are closed by plastic deformation or oxides and metallic particles after the wear test. According to the wear test results, specimens with 14 vol. % porosity are more wear resistant than the specimens with low porosity values of 11 vol. %. Thus, oxidation wear and surface plastic deformation are the main wear mechanisms identified in this investigation. Abrasion wear was also characterized as the result of abrasive debris agglomeration and the asperities of the pins.
    Obserwowano wzrost wytrzymałości na rozciąganie i twardości spiekanych stopów Fe-1.5Cu (% wag) wraz ze wzrostem ich gęstości. Badano także wpływ różnych wartości ciśnienia 300, 450, 600 i 750 MPa na porowatość i zużycie stopów. Mikrofotografie przekrojów zużytych powierzchni pokazują, że po teście zużycia pory są zamknięte wskutek odkształcenia plastycznego lub przez tlenki i cząstki metaliczne. Według wyników badań zużycia próbki o porowatości 14% są bardziej odporne na zużycie niż próbki o niższej porowatości 11%. Utlenianie i odkształcenie plastyczne powierzchni to główne mechanizmy zużycia zidentyfikowane w tej pracy. Stwierdzono także, że ścieranie jest wynikiem aglomeracji ściernych drobin i nierówności pinów.
    Źródło:
    Archives of Metallurgy and Materials; 2012, 57, 1; 93-103
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Odporne na zużycie powłoki eutektyczne układu Fe-Mn-C-B-Si-Ni-Cr otrzymane metodą napawania z wykorzystaniem drutów proszkowych
    Wear resistance of eutectic coating of system Fe-Mn-C-B-Si-Ni-Cr obtained by welding method with use wire powder
    Autorzy:
    Pashechko, M.
    Kindraczuk, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/395262.pdf
    Data publikacji:
    2010
    Wydawca:
    Stowarzyszenie Inżynierów i Techników Mechaników Polskich
    Tematy:
    powłoki eutektyczne
    druty proszkowe
    napawanie
    eutectic coating
    wire powder
    welding method
    Opis:
    W artykule omówiono właściwości tribologiczne powłoki eutektycznej na bazie układu Fe-Mn-C-B-Si-Ni-Cr otrzymanej metodą napawania łukowego w osłonie gazowej GMA z użyciem drutu proszkowego. Badanie przeprowadzono dla próbek z powłoką eutektyczną w układzie trzpień-tarcza podczas ruchu ślizgowego na sucho dla prędkości 0,4 m/s przy przyłożonych obciążeniach 3, 7 i 10 MPa. Materiał przeciwpróbki stal C 45. Po tarciu strukturę i rozkład atomów na powierzchni powłoki eutektycznej badano z użyciem skaningowego mikroskopu elektronowego SEM. Na podstawie uzyskanych wyników badań zaproponowano mechanizm zużycia opracowanych materiałów kompozytowych eutektycznych. W procesie tarcia występuje segregacja atomów C, B i Si na powierzchniu tarcia, spowodowana termodyfuzją, aktywizowana cyklicznym rozgrzewaniem powierzchni tarcia. Wskutek tribosyntezy powstają fazy nanokrystaliczne, które powodują zwiększenie odporności na zużycie kompozytów eutektycznych. Mechanizm tarcia jest utleniający.
    Wear resistance of eutectic coating of system Fe-Mn-C-B-Si-Ni-Cr obtained by welding method with use wire powder was studied. The coating were obtained by gas metal arc welding GMA with use of wire powder. Pin-on-disk dry sliding wear tests at sliding speeds 0,4 m/s and under loads 3, 7, 10 MPa were conducted for pin specimens with eutectic coatings. Material of counter-sample was steel C 45. After friction structure and distribution of atoms in the eutectic coatings due to wear was studied by scanning electron microscopy (SEM). Segregation of the C, B and Si caused of the thermal diffusion, activated by of the friction heating of the friction surface. Tribosyntese arise as a result of nanocrystalline phase, which increase the wear resistance of composites eutectic. The mechanism of friction is oxidizing
    Źródło:
    Postępy Nauki i Techniki; 2010, 5; 156-161
    2080-4075
    Pojawia się w:
    Postępy Nauki i Techniki
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of Fe-TiB2 Nanocomposites by Spark-Plasma Sintering of a (FeB, TiH2) Powder Mixture
    Autorzy:
    Huynh, X.-K.
    Kim, B.-W.
    Kim, J.-S.
    Powiązania:
    https://bibliotekanauki.pl/articles/351368.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Fe-TiB2 nanocomposite
    mechanical activation
    spark plasma sintering
    self-propagating high-temperature synthesis reaction
    Opis:
    Fe-40wt% TiB2 nanocomposites were fabricated by mechanical activation and spark-plasma sintering of a powder mixture of iron boride (FeB) and titanium hydride (TiH2). The powder mixture of (FeB, TiH2) was prepared by high-energy ball milling in a planetary ball mill at 700 rpm for 3 h followed by spark-plasma sintering (SPS) at various conditions. Analysis of the change in relative sintered density and densification rate during sintering showed that a self-propagating high-temperature synthesis reaction occurs to form TiB2 from FeB and Ti. A sintered body with relative density higher than 98% was obtained after sintering at 1150°C for 5 and 15 min. The microstructural observation of sintered compacts with the use of FE-SEM and TEM revealed that ultrafine particulates with approximately 5 nm were evenly distributed in an Fe-matrix. A hardness value of 83 HRC was obtained, which is equivalent to that of conventional WC-20 Co systems.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 2; 1043-1047
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Modification of the Surface of the Iron Powder as an Ingredient of the High Calorific Mixture
    Autorzy:
    Czajka, B.
    Wachowski, L.
    Łapiński, A.
    Rzodkiewicz, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/358561.pdf
    Data publikacji:
    2008
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    iron powder
    Fe-KClO4 mixture
    Raman spectroscopy (RS)
    ellipsometry
    thermo-programmed reduction (TPR)
    thermogravimetric analysis
    TG/DTA
    Opis:
    Textural properties of iron powders obtained by reduction of iron(II) compounds and by electrolysis were determined. Their specific surfaces were 0.38 and 0.43 m2g-1 respectively, and the prevailing grain sizes amounted to 10 and 43 ?m respectively. Total content of the determined metallic impurities was 0.055 wt.% in the preparation obtained by the electrolysis while in the preparation obtained by reduction it was 0.025 wt.%. It was proved that in initial samples the α-Fe2O3 phase occurred in the outer oxide layer present on the surface of Fe grains, and below this phase a layer of magnetite was found, the thickness of which was considerably greater in iron obtained by electrolysis. Measurements of selected properties showed that modification of the iron powder surface carried out by reduction with dihydrogen led to decreasing the linear rate of burning of the high calorific mixture Fe/KClO4 but it did not affect its calorific value. Moreover, it was found that modification of the iron powder surface resulted in lowering the temperature of ignition of the analysed mixture and decreasing the quantity of the released oxygen generated by decomposition of the oxidant, which did not react with the iron powder.
    Źródło:
    Central European Journal of Energetic Materials; 2008, 5, 3-4; 87-102
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Determination of Ignition Sensitivity of Selected Heat Powders
    Autorzy:
    Czajka, B.
    Styczyński, S.
    Tabat, S.
    Szal, D.
    Wachowski, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/357966.pdf
    Data publikacji:
    2011
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    heat powder
    ignition sensitivity
    Fe-KClO4
    EDS test
    Opis:
    Ignition sensitivity is one of the factors defning the characteristics of high calorifc mixture with low emission of gaseous product. It was found that Zr-BaCrO4 mixture is sensitive to ignition by electric spark energy of 0.82 J, whereas activation of Fe-KClO4 mixture depends on the iron powder employed and the composition of its surface oxide layers. Energy required for the activation of high calorifc mixture in form of powder designated as FeK, FeR or FeE is equal to 0.08, 0.59 and 1.1 J, while in the form of pellet 6.92, 10.2 and 14.1 J. Activation of Fe-KClO4 mixture with a strip of heat paper as well as with the electric spark has revealed that the mixture containing iron powder obtained by atomization method (FeA) is not active.
    Źródło:
    Central European Journal of Energetic Materials; 2011, 8, 1; 3-13
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Wpływ procesu azotowania gazowego na strukturę i twardość metalowych materiałów spiekanych na bazie Fe
    The influence of gas nitriding process on the structure and hardness of sintered metal Fe-based materials
    Autorzy:
    Wendland, J.
    Borowski, J.
    Małdziński, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/211462.pdf
    Data publikacji:
    2011
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Obróbki Plastycznej
    Tematy:
    metalurgia proszków
    azotowanie gazowe
    powder metallurgy
    gas nitriding
    Opis:
    W pracy przedstawiono wyniki badań materiału spiekanego na bazie proszku Astaloy Mo poddanego procesowi azotowania gazowego przy trzech stanach jego gęstości. Obróbkę cieplno-chemiczną prowadzono przy 5 kombinacjach czasu azotowania i potencjału azotowego. Badania obejmowały obserwacje struktury i pomiar mikrotwardości przed i po procesie azotowania. Wykazano, że dyfuzja azotu nastąpiła na wskroś próbek.
    The results of examination of sintered materials in three states of density based on Astaloy Mo powder after gas nitriding are presented in this paper. Thermo-chemical treatment was conducted in 5 combinations of nitriding time and nitrogen potential. The tests consisted of structure observation and microhardness measurements before and after nitriding. It was shown that the diffusion of nitrogen occurred right through the samples
    Źródło:
    Obróbka Plastyczna Metali; 2011, 22, 2; 75-82
    0867-2628
    Pojawia się w:
    Obróbka Plastyczna Metali
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure and Magnetic Properties of NdFeB Sintered Magnets Diffusion-Treated with Cu/Al Mixed Dyco Alloy-Powder
    Autorzy:
    Lee, M.-W.
    Bae, K.-H.
    Lee, S.-R.
    Kim, H.-J.
    Jang, T.-S.
    Powiązania:
    https://bibliotekanauki.pl/articles/353351.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B sintered magnets
    grain boundary diffusion process
    low melting point element
    DyCo alloy-powder diffusion
    Opis:
    We investigated the microstructural and magnetic property changes of DyCo, Cu + DyCo, and Al + DyCo diffusion-treated NdFeB sintered magnets. The coercivity of all diffusion treated magnet was increased at 880ºC of 1st post annealing(PA), by 6.1 kOe in Cu and 7.0 kOe in Al mixed DyCo coated magnets, whereas this increment was found to be relatively low (3.9 kOe) in the magnet coated with DyCo only. The diffusivity and diffusion depth of Dy were increased in those magnets which were treated with Cu or Al mixed DyCo, mainly due to comparatively easy diffusion path provided by Cu and Al because of their solubility with Ndrich grain boundary phase. The formation of Cu/Al-rich grain boundary phase might have enhanced the diffusivity of Dy-atoms. Moreover, relatively a large number of Dy atoms reached into the magnet and mostly segregated at the interface of Nd2 Fe14 B and grain boundary phases covering Nd2 Fe14 B grains so that the core-shell type structures were developed. The formation of highly anisotropic (Nd, Dy)2Fe14B phase layer, which acted as the shell in the core-shell type structure so as to prevent the reverse domain movement, was the cause of enhancing the coercivity of diffusion treated NdFeB magnets. Segregation of cobalt in Nd-rich TJP followed by the formation of Co-rich phase was beneficial for the coercivity enhancement, resulting in the stabilization of the metastable c-Nd2O3 phase.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1263-1266
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fe-Al based composite reinforced with ultra-fine Al2O3 oxides for high temperature applications
    Autorzy:
    Kopec, Mateusz
    Jóźwiak, Stanisław
    Kowalewski, Zbigniew
    Powiązania:
    https://bibliotekanauki.pl/articles/2055052.pdf
    Data publikacji:
    2021
    Wydawca:
    Polskie Towarzystwo Mechaniki Teoretycznej i Stosowanej
    Tematy:
    cermet composites
    reaction synthesis
    powder method
    electron microscopy
    Opis:
    In this paper, an Fe-Al based composite reinforced with ultra-fine Al2O3 oxides was obtained through sintering of aluminium, iron and mullite ceramic powders using self-propagated high temperature synthesis (SHS). The powder mixture with a 50%wt. content of the ceramic reinforcement was cold pressed and subsequently subjected to the sintering process in vacuum at 1200◦C for 25 minutes under external loading of 25 kN. The complex microstructure of the Fe-Al matrix reinforced with ultra-fine Al2O3 oxides was found to be desired in high temperature applications since only 3% of the relative weight gain was observed after 100 hours of annealing at 900◦C.
    Źródło:
    Journal of Theoretical and Applied Mechanics; 2021, 59, 3; 509--513
    1429-2955
    Pojawia się w:
    Journal of Theoretical and Applied Mechanics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Wpływ wielkości frakcji proszku amorficznego Fe60Co10Y8W1B20 na właściwości magnetyczne i mechaniczne kompozytu w osnowie polimerowej
    The influence of powder fraction on magnetic and mechanical properties of a resin bonded composite made from amorphous metallic Fe60Co10Y8W1B20 powder
    Autorzy:
    Pietrusiewicz, P.
    Nabiałek, M.
    Dośpiał, M.
    Bukowska, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/946147.pdf
    Data publikacji:
    2014
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Inżynierii Materiałów Polimerowych i Barwników
    Tematy:
    kompozyt z osnową polimerową
    kompozyt amorficzny
    materiał amorficzny
    materiał nanokrystaliczny
    materiał magnetyczny
    szkło metaliczne
    proszek amorficzny
    właściwości magnetyczne
    właściwości mechaniczne
    polymer matrix composite
    amorphous composite
    amorphous material
    nanocrystalline material
    magnetic material
    metallic glass
    amorphous powder
    magnetic properties
    mechanical properties
    Opis:
    W pracy badano wpływ wielkości frakcji amorficznego proszku wiązanego polimerem na właściwości magnetycznie miękkie i mechaniczne. Proszek został otrzymany poprzez niskoenergetyczne mielenie amorficznej płytki wytworzonej metodą wtłaczania ciekłego stopu do miedzianej formy. Na podstawie badań dyfrakcji promieni rentgenowskich stwierdzono, że kompozyty miały strukturę amorficzną. Wykorzystując magnetometr wibracyjny zmierzono statyczne pętle histerezy magnetycznej, na podstawie których wyznaczono parametry takie jak: magnetyzacja nasycenia (μoMs.) oraz pole koercji (Hc). Zmierzono mikrotwardość wykorzystując metodę Vickersa. Na podstawie przeprowadzonych badań stwierdzono, że wielkość amorficznych cząstek istotnie wpływa na zmianę parametrów magnetycznych jak i mechanicznych badanych kompozytów. Dodatkowo stwierdzono, że osnowa polimerowa izolująca amorficzne cząstki wpłynęła na pogorszenie parametrów magnetycznie miękkich w porównaniu do masywnych płytek.
    In the paper investigates the effect of the volume fraction of amorphous powders on the soft magnetic and mechanical properties. The powder was obtained by low-energy milling of amorphous plates produced by the injection of a liquid alloy into a copper mold. On the basis of X-ray diffraction, it was found that the composites had an amorphous structure. Using the vibrating sample magnetometer, the static hysteresis loops were measured, on which basis the basic magnetic parameters such as saturation magnetization (μoMs) and the coercive field (Hc) were determined. Microhardness was measured using the Vickers method. From the examinations, it was found that the size of the amorphous particles significantly influences the change of magnetic and mechanical parameters of the studied composites. Additionally it was found that the polymeric matrix insulating the amorphous particles affected the deterioration of soft magnetic parameters in comparison to the massive plates.
    Źródło:
    Przetwórstwo Tworzyw; 2014, [R.] 20, nr 1 (157), 1 (157); 76-81
    1429-0472
    Pojawia się w:
    Przetwórstwo Tworzyw
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Zastosowanie krajowego renianu amonu do wytwarzania spieków ciężkich W-Re-Ni-Fe przeznaczonych na rdzenie pocisków przeciwpancernych
    Application of Domestic Ammonium Perrhenate for Production of W-Re-Ni-Fe Heavy Alloys Intended for Armour-Piercing Kinetic Energy Penetrators
    Autorzy:
    Majewski, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/403837.pdf
    Data publikacji:
    2013
    Wydawca:
    Wojskowa Akademia Techniczna im. Jarosława Dąbrowskiego
    Tematy:
    metalurgia proszków
    rdzenie pocisków przeciwpancernych
    wolfram
    ren
    powder metallurgy
    kinetic energy penetrators
    tungsten
    rhenium
    Opis:
    W artykule przedstawiono wybrane wyniki eksperymentów związanych z możliwościami wykorzystania krajowego renianu(VII) amonu (NH₄ReO₄) produkcji Instytutu Metali Nieżelaznych w Gliwicach do otrzymywania spieków ciężkich W-Re-Ni-Fe. Omówione zostały zjawiska występujące w spiekach na osnowie wolframu zawierających dodatek renu, związane z tzw. "efektem renu", które powodują polepszenie niektórych właściwości tych materiałów. Opisano proces technologiczny wytwarzania badanych spieków, na który składają się m.in. prasowanie izostatyczne na zimno i 2-etapowe spiekanie. Zaprezentowano wyniki badań mikrostruktury, a także wybranych właściwości mechanicznych materiałów wytworzonych z użyciem krajowego renianu amonu i dokonano ich porównania ze spiekami wykonanymi z użyciem importowanego renianu, a także z klasycznym spiekiem W-Ni-Fe. Opisano również przykładowe rezultaty badań balistyki końcowej rdzeni pocisków podkalibrowych wykonanych z badanych materiałów z użyciem krajowego renianu amonu. Badania te przeprowadzono z wykorzystaniem specjalnego stanowiska badawczego do strzelania pociskami podkalibrowymi. Przedstawiono wyniki badań przebijalności, także efekty "samoostrzenia" rdzeni, które zaobserwowano w przypadku niektórych spieków.
    Experiments results connected to possibilities of use of the domestic ammonium perrhenate (NH₄ReO₄) produced by the Institute of Non-Ferrous Metals in Gliwice for obtaining W-Re-Ni-Fe heavy alloys were presented in the paper. Characteristic phenomena occurring in the sinters on the base of tungsten containing addition of rhenium (connected with so-called "rhenium effect") were explained. This effect causes improvement of selected properties of these materials. Production process of investigated sinters was described. This process contains, among others, cold isostatic pressing and 2-staged sintering. Selected results of microstructure investigation and mechanical properties of obtained materials produced with addition of domestic ammonium perrhenate were presented. They were compared with properties of sinters produced with addition of imported ammonium perrhenate and also with classical heavy alloys (W-Ni-Fe). Moreover the selected results of final ballistics of kinetic energy penetrators made of investigated materials with addition of domestic ammonium perrhenate were described. These experiments were conducted with using of special ballistic stand for shell shooting. Results of penetration and also "selfsharpening effects" observed in some cases were described in the paper.
    Źródło:
    Problemy Mechatroniki : uzbrojenie, lotnictwo, inżynieria bezpieczeństwa; 2013, 4, 2 (12); 53-67
    2081-5891
    Pojawia się w:
    Problemy Mechatroniki : uzbrojenie, lotnictwo, inżynieria bezpieczeństwa
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Analysis of Densification Process and Structure of PM Al-Mg-Si-Cu-Fe and Al-Zn-Mg-Cu-Sn Alloys
    Analiza procesu zagęszczania i struktury spiekanych stopów Al-Mg-Si-Cu-Fe i Al-Zn-Mg-Cu-Sn
    Autorzy:
    Bidulský, R
    Bidulská, J.
    Actis Grande, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/355248.pdf
    Data publikacji:
    2014
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    powder metallurgy
    aluminium alloy
    compressibility
    microstructure
    metalurgia proszków
    stop aluminium
    ściśliwość
    mikrostruktura
    Opis:
    The paper is focused on the role of the pressing pressure on the densification behaviour of PM aluminium alloys. Commercially aluminium based powders Al-Mg-Si-Cu-Fe and Al-Zn-Mg-Cu-Sn were used as materials to be investigated. The apparent density of the powder mixes was determined according to MPIF St. 04. A set of cylinder test specimen 55x10x10 mm3 was uniaxially pressed in a floating hardened steel die. Compaction pressures ranged from 50 MPa up to 700 MPa. Considering the densification of metal powders in uniaxial compaction, quantification of aluminium compaction behaviour was performed. The compressibility behaviour was evaluated, considering the effect on specimens, as well as on their microstructure. The development of compressibility values with pressing pressure enables to characterize the effect of particles geometry and matrix plasticity on the compaction process.
    Przedmiotem pracy jest wpływ ciśnienia prasowania na zagęszczanie proszków stopów aluminium. Materiałem badanym były komercyjne proszki aluminium Al-Mg-Si-Cu-Fe I Al-Zn-Mg-Cu-Sn. Gęstość pozorna mieszanek proszków określono według MPIF St.04. Cylindryczne próbki 55x10x10 mm3 ściskane były jednokierunkowo w samonastawnej matrycy z hartowanej stali. Nacisk wahał się od 50 MPa do 700 MPa. Biorąc pod uwagę zagęszczenie proszków metali w trakcie prasowania jednoosiowego, przeprowadzono kwantyfikacje zagęszczania aluminium. Oceniono zachowanie ściśliwości biorąc pod uwagę wpływ na próbki, jak również na ich mikrostrukturę. Zestawienie wartości ściśliwości z ciśnieniem prasowania pozwala scharakteryzować wpływ geometrii cząstek i plastyczności matrycy na proces prasowania.
    Źródło:
    Archives of Metallurgy and Materials; 2014, 59, 1; 17-23
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study on Crystal Structure and Magnetic Properties of Ba4Co2Fe36O60 by Sol-Gel Method
    Autorzy:
    Jeong, K.-P.
    Yang, S.-W.
    Kim, J.-G.
    Powiązania:
    https://bibliotekanauki.pl/articles/351655.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    U-type ferrite
    sol-gel method
    nano-powder
    Opis:
    U-type ferrite typified by Ba4Co2Fe36O60 is used as a RAM (Radar Absorbing Materials) in the X-band (8-12 GHz). Ba4Co2Fe36O60 is known to have a complex crystal structure, which makes it difficult to obtain single phase and have low reproducibility. Previously known U-type ferrites have been fabricated based on a ceramic process that mixing (by a ball mill), calcining, grinding, binder mixing, drying, sieving, pressing and sintering. In contrast, the process of preparing the powder by the sol-gel method and its heat-treating is advantageous in that it can reduce the process steps and the required time. In addition, the precise stoichiometric control by the sol-gel method can effectively evaluate the effect of added or substituted elements. In this study investigates the crystal structure of Ba4Co2Fe36O60 synthesized by the sol-gel method and the morphology of U-type ferrite nano-powders according to various heat treatment conditions. Analysis of the crystal structure is used for XRD. Morphology and size are observed by SEM. In addition, VSM is performed to confirm the change of magnetic properties according to various heat treatment conditions.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1449-1452
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Iron-bearing phases affecting the colour of upper Neogene clayey sediments from Dymaczewo Stare, west-central Poland
    Autorzy:
    Klęsk, Jakub
    Błachowski, Artur
    Diduszko, Ryszard
    Kruszewski, Łukasz
    Widera, Marek
    Powiązania:
    https://bibliotekanauki.pl/articles/2204349.pdf
    Data publikacji:
    2022
    Wydawca:
    Uniwersytet im. Adama Mickiewicza w Poznaniu
    Tematy:
    mineral composition
    powder X-ray diffraction
    PXRD
    iron minerals
    57Fe Mössbauer spectroscopy
    57Fe- MS
    Poznań clays
    Mio-Pliocene
    skład mineralny
    proszkowa dyfrakcja rentgenowska
    minerały żelaza
    spektroskopia Mössbauera
    iły poznańskie
    Opis:
    The present paper investigates the colour dependence of mineral compositions in clay-rich sedimentary strata, mainly clayey silts, the emphasis being on iron-bearing minerals (rather than clay minerals) by using powder X-ray diffraction (PXRD) and 57Fe Mössbauer spectroscopy (57Fe-MS). The PXRD-based phase analysis has demonstrated the variable compositions of samples, consisting of, inter alia, quartz, calcite or gypsum, and admixtures of potassium feldspars and plagioclase. Hematite + goethite (sample D1, dark red), goethite (sample D2, pinkish brown), poorly crystalline goethite (sample D3, orange) and jarosite (sample D4, yellow) have been distinguished. A very low jarosite content was detected in sample D5 (light grey); this did not affect its colour. The potential yellow/brown shades in sample D6 (dark grey), coming from trace amounts of jarosite, are masked by macroscopically visible organic matter. In the case of the two last-named samples (D5 and D6), with trace amounts of Fe-bearing minerals, it is most likely that the organic matter was effective in influencing the light and dark grey colour of the sediment, respectively.
    Źródło:
    Geologos; 2022, 28, 2; 129--139
    1426-8981
    2080-6574
    Pojawia się w:
    Geologos
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    AC Magnetic Field Effect on the Complex Permeability Spectra of Soft Magnetic $Fe_{73}Cu_{1}Nb_{3}Si_{16}B_{7}$ Powder Cores
    Autorzy:
    Füzer, J.
    Dobák, S.
    Füzerová, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1367086.pdf
    Data publikacji:
    2014-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Bb
    07.55.-w
    85.70.-w
    Opis:
    In this work, two soft magnetic $Fe_{73}Cu_{1}Nb_{3}Si_{16}B_{7}$ powder core samples were investigated. Samples were prepared by milling of amorphous $Fe_{73}Cu_{1}Nb_{3}Si_{16}B_{7}$ ribbon at different temperature conditions: sample R, by milling at room temperature and sample L, by cryomilling at temperature of liquid nitrogen. Influence of applied exciting AC magnetic field with various amplitudes on the complex permeability spectra was studied. Obtained results are explained by the dynamics and relaxation phenomenon of domain walls under the influence of AC magnetic field.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 1; 88-89
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of closed-die hot compaction parameters on selected properties of PM Al-Si-Fe-Cu materials
    Wpływ parametrów zagęszczania na gorąco na wybrane właściwości tworzyw otrzymanych z proszku stopu Al-Si-Fe-Cu
    Autorzy:
    Wojtaszek, M.
    Dudek, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/264041.pdf
    Data publikacji:
    2010
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
    Tematy:
    proszek stopu aluminium
    zagęszczanie na gorąco w matrycach zamkniętych
    gęstość
    właściwości
    mikrostruktura
    aluminium alloy powder
    closed-die hot compaction
    density
    properties
    microstructure
    Opis:
    The work presents the results of investigations of the materials obtained by closed-die hot compaction of A117Si5Fe3Cu1.1Mg0.6Zr alloy powder. The influence of temperature and punch unit pressure on the shape of samples, as well as on relative density, selected mechanical properties and microstructure of obtained products, was estimated. The beneficial parameters of hot compaction were determined.
    Przedstawiono wyniki badań materiałów otrzymanych w procesie zagęszczania na gorąco w matrycach zamkniętych proszku stopu Al17Si5Fe3Cu1,1Mg0,6Zr. Ocenie poddano wpływ temperatury i nacisku jednostkowego stempla na kształt próbek a także na gęstość, wybrane właściwości mechaniczne oraz na stan mikrostruktury tworzyw. Wyznaczono korzystne, w przyjętych do badań warunkach procesu zagęszczania oraz w badanym zakresie, parametry formowania.
    Źródło:
    Metallurgy and Foundry Engineering; 2010, 36, 2; 91-96
    1230-2325
    2300-8377
    Pojawia się w:
    Metallurgy and Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal Behaviour of PrCo_{1-x}Fe_xO₃ Probed by X-ray Synchrotron Powder Diffraction and Impedance Spectroscopy Measurements
    Autorzy:
    Pekinchak, O.
    Sugak, D.
    Ubizskii, S.
    Suhak, Yu.
    Fritze, H.
    Vasylechko, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/1029711.pdf
    Data publikacji:
    2018-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.66.Fn
    61.05.cp
    65.40.De
    72.60.+g
    Opis:
    Crystal structure and transport properties of the mixed praseodymium cobaltites-ferrites PrCo_{1-x}Fe_xO₃ have been studied in the temperature range of 298-1173 K by a combination of in situ X-ray synchrotron powder diffraction and temperature dependent impedance spectroscopy measurements. In situ high temperature powder diffraction examination of PrCo_{1-x}Fe_xO₃ series revealed considerable anomalies in the lattice expansion which are especially pronounced for the cobalt-rich specimens. These anomalies, which are reflected in a sigmoidal dependence of the unit cell dimensions and in the considerable increase of the thermal expansion coefficients, are obviously associated with transitions of Co^{3+} ions from low spin to the higher spin states and the coupled metal-insulator transitions, occurring in in rare earth cobaltites at the elevated temperatures. Indeed, the temperature-dependent impedance measurements clearly prove the change of conductivity type from dielectric to the metallic behaviour in the mixed cobaltite-ferrites PrCo_{1-x}Fe_xO₃ at the elevated temperatures.
    Źródło:
    Acta Physica Polonica A; 2018, 133, 4; 798-801
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of DyMn Alloy-Powder Addition On Microstructure And Magnetic Properties Of NdFeB Sintered Magnets
    Wpływ dodatku proszku DyMn na mikrostrukturę i właściwości magnetyczne spiekanych magnesów NdFeB
    Autorzy:
    Lee, M.-W.
    Dhakal, D. R.
    Kim, T. H.
    Lee, S. R.
    Kim, H. J.
    Jang, T. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/357010.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B sintered magnets
    DyMn-alloy powder
    coercivity
    low melting point element
    magnesy spiekane
    proszek DyMn
    koercja
    elementy o niskiej temperaturze topnienia
    Opis:
    Micostructural change and corresponding effect on coercivity of a NdFeB sintered magnet mixed with small amount of DyMn powder was investigated. In the sintered magnet mixed with the DyMn alloy-powder Dy-rich shell was formed at outer layer of the main grains, while Mn was mostly concentrated at Nd-rich triple junction phase (TJP), lowering melting temperature of the Nd-rich phase that eventually improved the microstructural characteristics of the gain boundary phase. The coercivity of a magnet increased more than 3.5 kOe by the mixing of the DyMn alloy-powder.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1407-1409
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    New Wear Resistant Iron-Base Matrix Materials For The Fabrication Of Sintered Diamond Tools
    Nowe, odporne na zużycie ścierne materiały na bazie żelaza przeznaczone do produkcji spieków narzędziowych metaliczno-diamentowych
    Autorzy:
    Konstanty, J.
    Romański, A.
    Baczek, E.
    Tyrala, D.
    Powiązania:
    https://bibliotekanauki.pl/articles/355118.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    ball milling
    sintered diamond tools
    matrix powder
    Fe-Ni-Cu-Sn-C
    Fe-Mn-Cu-Sn-C
    hot pressing
    mielenie kulowe
    spieki narzędziowe metaliczno-diamentowe
    materiały spiekowe
    prasowanie na gorąco
    Opis:
    The possibility of the use of inexpensive iron-base powders in the production of sintered diamond tools is again explored. Ball-milled Fe-Ni-Cu-Sn-C and Fe-Mn-Cu-Sn-C powders were consolidated to a virtually pore-free condition by hot pressing at 900°C. The resultant materials are characterised by a combination of high Knoop hardness, 260-440 and yield strength, 780-1350 MPa, and resistance to abrasion. These properties can be significantly modified by changing the milling time.
    W artykule zamieszczono wyniki badań nad możliwością zastosowania tanich proszków na bazie żelaza do produkcji spiekanych narzędzi metaliczno-diamentowych. Mielone proszki Fe-Ni-Cu-Sn-C i Fe-Mn-Cu-Sn-C poddano prasowaniu na gorąco w temperaturze 900°C. Otrzymane spieki posiadają gęstość zbliżoną do teoretycznej, wysoką twardość (260-400 HK0.5), granicę plastyczności (780-1350 MPa) oraz dużą odporność na zużycie ścierne. Wymienione własności są w dużym stopniu uzależnione od czasu mielenia proszków wyjściowych.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2A; 633-637
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of Rapidly Solidified $Al_{65}Cu_{20}Fe_{15}$ Alloy in Form of Powder or Ribbon
    Autorzy:
    Lityńska-Dobrzyńska, L.
    Dutkiewicz, J.
    Stan-Głowińska, K.
    Dembinski, L.
    Coddet, C.
    Ochin, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1373231.pdf
    Data publikacji:
    2014-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.30.-t
    61.44.Br
    61.05.cp
    61.05.jm
    Opis:
    The $Al_{65}Cu_{20}Fe_{15}$ alloy has been prepared by conventional casting to the mould and by melt spinning or atomisation techniques. The melt spun ribbon was in the form of fragmented, brittle flakes, atomized powder has spherical shape with average size 17.2 μm. It was found that icosahedral I-phase was the main phase in all types of prepared samples. In the conventionally cast alloy the following phases have been identified additionally: $λ-Al_{13}Fe_4$, τ-AlCu(Fe) and $η_2-AlCu$. In the melt-spun ribbon the formation of $η_2$ is avoided, while in the atomised powder the I-phase coexists with small amount of copper rich τ-phase. In the cast ingot the I-phase form as a product of peritectic reaction λ + L, while in the ribbon and in the powder quasicrystal solidified from the undercooled melt as primary phase and next metastable cubic τ-AlCu(Fe) was formed at the interdendritic areas. Single I-phase grains of the sizes about 1 μm are observed in the ribbon close to the wheel side.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 2; 512-515
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The influence of strain rate on microstructure and mechanical behavior of P/M feal
    Wpływ prędkości odkształcenia na strukturę i charakter plastycznego płynięcia stopu FeAl otrzymanego metodą metalurgii proszków
    Autorzy:
    Śleboda, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/950798.pdf
    Data publikacji:
    2008
    Wydawca:
    Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
    Tematy:
    stopy Fe-Al
    struktura
    odkształcenie plastyczne
    prędkość odkształcenia
    metalurgia proszków
    FeAl alloys
    microstructural evolution
    mechanical behavior
    strain rate
    powder metallurgy
    Opis:
    As part of a broader study of the thermomechanical processing of P/M FeAl alloys, this research is focused on the influence of processing strain rate on the microstructural evolution and mechanical behavior of the processed materials. For the purposes of this study, water atomized FeAl powder was consolidated by hot pressing resulting in fully dense products. The consolidated P/M samples were thermomechanically processed in compression at 800 and 900oC at strain rates of 0.1 s-1 and 10 s-1, to a true strain of 1. The influence of thermomechanical processing parameters on the material flow and microstructural development of investigated alloy was analyzed. Considerable strain rate sensitivity of investigated alloy was observed, specially with reference to microstructural development.
    W niniejszej pracy przedstawiono wybrane wyniki badań wpływu prędkości odkształcenia na rozwój mikrostruktury oraz charakter odkształcenia plastycznego stopu z grupy FeAl. W badaniach zastosowano rozpylany wodą proszek stopu. W pełni zagęszczone poprzez prasowanie na gorąco próbki z proszków poddano próbie ściskania w temperaturach 800°C oraz 900°C przy prędkościach odkształcenia równych 0.1 s(-1) oraz 10 s(-1), do wartości odkształcenia rzeczywistego równej 1. W materiałach odkształconych w temperaturze 800°C rozdrobnienie mikrostruktury nastąpiło tylko przy większej prędkości odkształcenia (10 s(-1) ), natomiast w temperaturze 900°C materiał uległ rekrystalizacji niezależnie od prędkości odkształcenia. Badania wykazały stosunkowo dużą czułość stopu na prędkość odkształcenia, szczególnie w odniesieniu do zmian strukturalnych związanych z procesami rekrystalizacji.
    Źródło:
    Metallurgy and Foundry Engineering; 2008, 34, 2; 133-138
    1230-2325
    2300-8377
    Pojawia się w:
    Metallurgy and Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Wpływ zawartości osnowy polimerowej na właściwości magnetyczne amorficznego proszku Fe60Co10Y8W1B20
    Influence of polymer content on the magnetic properties of the Fe60Co10Y8W1B20 amorphous powders
    Autorzy:
    Pietrusiewicz, P.
    Nabiałek, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/277912.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Inżynierii Materiałów Polimerowych i Barwników
    Tematy:
    materiał magnetycznie miękki
    kompozyt magnetyczny
    ferromagnetyk
    proszek amorficzny
    osnowa polimerowa
    struktura kompozytu
    struktura amorficzna
    właściwości magnetyczne
    soft magnetic material
    magnetic composite
    ferromagnetic
    amorphous powder
    polymer matrix
    composite structure
    amorphous structure
    magnetic properties
    Opis:
    W pracy przedstawiono wyniki badań kompozytów składających z ferromagnetyka Fe61Co10Y8W1B20 wykazującego miękkie właściwości magnetyczne związanego polimerem (Epidian 100) w proporcjach 2%, 3% i 4% wag. Przeprowadzono badania struktury wykorzystując dyfrakcje promieni rentgenowskich. Na podstawie tych badań wykazano że proces mielenia jak i utwardzania Epidianu w nie wpływa na strukturę badanych kompozytów powodując jej krystalizację. W kolejnym etapie przeprowadzono badania magnetyczne wykorzystując magnetometr wibracyjny (VSM). Pokazano, że można sterować właściwościami poprzez odpowiednie dobranie zawartości osnowy polimerowej.
    This paper presents results of research on the composites consisting of ferromagnetic Fe61Co10Y8W1B20 alloy exhibiting soft magnetic properties of bonded polymer (Epidian 100) in the proportion of 2%, 3% and 4% by weight. Structure study was carried out using X-ray diffraction. This research have shown that the process of grinding and Epidianu hardening does not affect the structure of the composites causing its crystallization. In a next step were studied by using a vibrating sample magnetometer (VSM). It is shown that the properties can be controlled through appropriate selection of the content of the polymer matrix.
    Źródło:
    Przetwórstwo Tworzyw; 2015, T. 21, Nr 2 (164), 2 (164); 149-151
    1429-0472
    Pojawia się w:
    Przetwórstwo Tworzyw
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The character of the structure formation of model alloys of the Fe-Cr-(Zr, Zr-B) system synthesized by powder metallurgy
    Autorzy:
    Duriagina, Z. A.
    Romanyshyn, M. R.
    Kulyk, V. V.
    Kovbasiuk, T. M.
    Trostianchyn, A. M.
    Lemishka, I. A.
    Powiązania:
    https://bibliotekanauki.pl/articles/366907.pdf
    Data publikacji:
    2020
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    model alloys
    phase diagram
    microstructure
    microhardness
    XRD analysis
    stop modelowy
    diagram fazowy
    mikrostruktura
    mikrotwardość
    analiza XRD
    Opis:
    Purpose: The purpose of the work is to synthesize and investigate the character of structure formation, phase composition and properties of model alloys Fe75Cr25, Fe70Cr25Zr5, and Fe69Cr25Zr5B1. Design/methodology/approach: Model alloys are created using traditional powder metallurgy approaches. The sintering process was carried out in an electric arc furnace with a tungsten cathode in a purified argon atmosphere under a pressure of 6·104 Pa on a water cooled copper anode. Annealing of sintered alloys was carried out at a temperature of 800°C for 3 h in an electrocorundum tube. The XRD analysis was performed on diffractometers DRON-3.0M and DRON-4.0M. Microstructure study and phase identification were performed on a REMMA-102-02 scanning electron microscope. The microhardness was measured on a PMT-3M microhardness meter. Findings: When alloying a model alloy of the Fe-Cr system with zirconium in an amount of up to 5%, it is possible to obtain a microstructure of a composite type consisting of a mechanical mixture of a basic Fe2(Cr) solid solution, solid solutions based on Laves phases and dispersive precipitates of these phases of Fe2Zr and FeCrZr compositions. In alloys of such systems or in coatings formed based on such systems, an increase in hardness and wear resistance and creep resistance at a temperature about 800°C will be reached. Research limitations/implications: The obtained results were verified during laser doping with powder mixtures of appropriate composition on stainless steels of ferrite and ferrite-martensitic classes. Practical implications: The character of the structure formation of model alloys and the determined phase transformations in the Fe-Cr, Fe-Cr-Zr, and Fe-Cr-B-Zr systems can be used to improve the chemical composition of alloying plasters during the formation of ferrite and ferrite-martensitic stainless steel coatings. Originality/value: The model alloys were synthesized and their phase composition and microstructure were studied; also, their microhardness was measured. The influence of the chemical composition of the studied materials on the character of structure formation and their properties was analysed.
    Źródło:
    Journal of Achievements in Materials and Manufacturing Engineering; 2020, 100, 2; 49-57
    1734-8412
    Pojawia się w:
    Journal of Achievements in Materials and Manufacturing Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-45 z 45

      Ta witryna wykorzystuje pliki cookies do przechowywania informacji na Twoim komputerze. Pliki cookies stosujemy w celu świadczenia usług na najwyższym poziomie, w tym w sposób dostosowany do indywidualnych potrzeb. Korzystanie z witryny bez zmiany ustawień dotyczących cookies oznacza, że będą one zamieszczane w Twoim komputerze. W każdym momencie możesz dokonać zmiany ustawień dotyczących cookies