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Wyświetlanie 1-15 z 27
Tytuł:
Influence of Nb Addition on Magnetic Properties of the Nanocrystalline $(Nd₁₀Fe₆₇B₂₃)_{100-x}Nbₓ$ (where x = 1, 2, 4) Alloy Ribbons
Autorzy:
Szwaja, M.
Pawlik, K.
Pawlik, P.
Gębara, P.
Michalski, B.
Powiązania:
https://bibliotekanauki.pl/articles/1387907.pdf
Data publikacji:
2015-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.20.En
75.75.-c
75.75.Cd
Opis:
In the present work the magnetic properties and phase constitution of $(Nd₁₀Fe₆₇B₂₃)_{100-x}Nbₓ$ (where x = 1, 2, 4) alloys in the form of ribbons were investigated. The base alloys were prepared by arc-melting the high purity elements with pre-alloyed Fe-B under an Ar atmosphere. The ribbon samples were obtained by controlled atmosphere melt-spinning technique. In order to generate the nanocrystalline microstructure and hard magnetic properties, samples were annealed at various temperatures (from 923 K to 1023 K) for 5 min. The aim of the present work was to determine the influence of Nb admixture and annealing conditions on the phase constitution and magnetic properties.
Źródło:
Acta Physica Polonica A; 2015, 127, 2; 623-625
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Properties of Magnets Obtained by Hydrostatic Extrusion of Nd-Fe-B Powder
Autorzy:
Gizynski, T.
Kaszuwara, W.
Pawlik, P.
Kulczyk, M.
Leonowicz, M.
Michalski, B.
Powiązania:
https://bibliotekanauki.pl/articles/1387955.pdf
Data publikacji:
2015-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ww
Opis:
Nd-Fe-B MQ powder was initially densified in a copper capsule to reach about 60% of the theoretical density. Subsequently, three various processes of hydrostatic extrusion were conducted at room temperature. The values of true strain, obtained during the all three stages, were 1.38, 0.89, 0.94, respectively. The investigation performed showed that the coercivity of the material decreases as the strain increases. Decrease of the remanence was observed only for the highest strains. Size of the particles was strongly reduced during the extrusion processes. X-ray diffraction did not show changes in the phase structure of the material. The Mössbauer study, of the sample extruded within all the three stages, showed existence of the Nd₂Fe₁₄B phase and 16% of other phase. Analysis of magnetization versus temperature confirmed that the additional phase was ferromagnetic.
Źródło:
Acta Physica Polonica A; 2015, 127, 2; 626-628
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetization Reversal Processes in Nanocrystalline (Pr, Dy)-(Fe, Co)-B Bulk Alloys
Autorzy:
Przybył, A.
Pawlik, K.
Pawlik, P.
Gębara, P.
Wysłocki, J.
Powiązania:
https://bibliotekanauki.pl/articles/1387335.pdf
Data publikacji:
2015-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.20.En
75.75.-c
75.75.Cd
Opis:
The aim of this paper was to study the phase constitution, magnetic properties and magnetization reversal processes in the rapidly solidified bulk (Pr,Dy)-(Fe,Co)-B alloys doped with Zr, Ti, Mn and Ni. The 3 mm outer diameter tubes samples of the $Pr₈Dy₁Fe₆₀Co₇Ni_{(6x)}MnₓB₁₄Zr₁Ti₃$ (where x = 0, 3, 6) alloys were produced by suction-casting technique. The admixture of Zr was introduced in order to improve their glass forming abilities while Dy was substituted to enhance the magnetocrystalline anisotropy of hard magnetic phase. The effect of Ni and Mn addition on the phase constitution and magnetic properties was studied in the presented work.
Źródło:
Acta Physica Polonica A; 2015, 127, 2; 579-581
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of phase constitution and magnetic properties of the hard magnetic nanocrystalline Nd9.5Fe63.65B21.85Nb5 alloy ribbons
Autorzy:
Szwaja, M.
Pawlik, K.
Wysłocki, J. J.
Pawlik, P.
Gębara, P.
Powiązania:
https://bibliotekanauki.pl/articles/147840.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
magnetic properties NdFeB alloys
nanocrystalline ribbon
Nd2Fe14B
X-ray diffractometry
Opis:
In order to investigate the phase constitution of the nanocrystalline Nd9.5Fe63.65B21.85Nb5 alloy ribbons in the as-cast state and after short-time annealing Mossbauer study has been carried out. In as-cast state, ribbon samples were not fully amorphous but revealed soft magnetic properties. X-ray diffraction analysis showed the presence of hard magnetic Nd2Fe14B, metastable Nd2Fe23B3 and paramagnetic Nd1+epsilonFe4B4 phases in annealed samples. Mossbauer spectroscopy was used to determine the fractions of constituent phases formed during annealing of ribbons. Magnetic measurements were made with a vibrating sample magnetometer (VSM) and have shown that with increasing annealing temperature the remanence polarization Jr and maximum energy product (BH)max values were increasing.
Źródło:
Nukleonika; 2013, 58, 1; 159-163
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetic properties of the nanocrystalline Nd9.6Fe64.32Nb4B22.08 alloy ribbons
Właściwości magnetyczne nanokrystalicznych taśm stopu Nd9,6Fe64,32Nb4B22,08
Autorzy:
Szwaja, M.
Pawlik, P.
Wysłocki, J. J.
Gębara, P.
Powiązania:
https://bibliotekanauki.pl/articles/354465.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
dyfraktometria promieniowania X
właściwości magnetyczne stopu NdFeB
Nd2Fe14B
taśma nanokrystaliczna
X-ray diffractometry
magnetic properties NdFeB alloys
nanocrystalline ribbon
Opis:
Studies of magnetic properties and phase constitution of nanocrystalline Nd9.6Fe64.32Nb4B22.08 alloy ribbon samples are presented. In as-cast state, ribbon samples were fully amorphous and soft magnetic. Subsequent annealing resulted in an evolution of the phase constitution together with change of their magnetic properties. The main phase observed in the material is Nd2Fe14B hard magnetic phase.
W pracy badano własności magnetyczne oraz skład fazowy taśm wytworzonych ze stopu Nd9,6Fe64,32Nb4B22,08. Taśma w stanie po odlaniu ma amorficzną budowę i wykazuje miękkie właściwości magnetyczne. Wygrzewanie taśm powoduje zmiany składu fazowego wraz ze zmianą ich właściwości magnetycznych. Podstawową fazą obserwowaną w badanym materiale jest faza magnetycznie twarda Nd2Fe14B.
Źródło:
Archives of Metallurgy and Materials; 2012, 57, 1; 233-236
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Structural Stability of Soft Magnetic Fe-Co-Zr-W-B Metallic Glasses Investigated by the in-situ X-ray Diffraction
Autorzy:
Michalik, S.
Bednarcik, J.
Pawlik, P.
Matija, R.
Sovak, P.
Powiązania:
https://bibliotekanauki.pl/articles/1366893.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
61.43.Dq
Opis:
The atomic structure of as-prepared $Fe_{61}Co_{(14-x)}Zr_{5}W_{x}B_{20}$ (x=1, 2 and 4) ribbon samples and their thermal stability were investigated by in-situ high-energy X-ray diffraction experiments. It was observed that higher W concentration causes the tiny shift of the main peak of the reduced atomic pair distribution function to higher values of interatomic distances and increases the coefficient of volume thermal expansion. The crystallization process occurs in two steps and is qualitatively the same for all studied specimens. Firstly the $Fe_{23}B_{6}$ phase is created and later is transformed to other types of borides together with the creation of a Fe-based phase.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 66-67
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigations of the magnetization reversal processes in nanocrystalline Nd-Fe-B alloys doped by Nb
Autorzy:
Kaźmierczak, M.
Pawlik, P.
Wysłocki, J.
Wnuk, I.
Gębara, P.
Pawlik, K.
Przybył, A.
Powiązania:
https://bibliotekanauki.pl/articles/1052622.pdf
Data publikacji:
2017-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.30.Sg
75.50.Bb
Opis:
In the following article the magnetic properties and phase composition of (Nd₁₀Fe₆₇B₂₃)_{100-x}Nb_{x} (where x=5, 6, 7, 8, 9) alloys in the form of ribbons are discussed. The X-ray diffraction studies revealed the coexistence of amorphous and nanocrystalline structures consisting of Nd₂Fe₁₄B, Nd_{1+ε}Fe₄B₄ and metastable Nd₂Fe₂₃B₃ phases. The shape of M_{rev} (M_{irr}) suggests that the magnetization reversal proceeds through the nucleation of the reversal domain for the ribbon doped with 5-7 at.% of Nb and the subsequent pinning of the domain walls for ribbons doped with 8 and 9 at.% of Nb.
Źródło:
Acta Physica Polonica A; 2017, 131, 4; 789-791
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Glass forming abilities and crystallization process in amorphous Pr-Fe-Co-Zr-Nb-B alloys of various B content
Autorzy:
Pawlik, K.
Pawlik, P.
Kaszuwara, W.
Wysłocki, J.
Powiązania:
https://bibliotekanauki.pl/articles/1054842.pdf
Data publikacji:
2017-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
64.70.dg
61.05.cp
75.20.En
75.50.Vv
Opis:
The influence of boron contents on the glass forming abilities and magnetic properties of melt-spun ribbon samples produced from Pr₉Fe_{50+x}Co₁₃Zr₁Nb₄B_{23-x} (x=0, 2, 5, 8) alloys, were investigated. For all compositions, the rapidly solidified samples were fully amorphous, which was confirmed by X-ray diffractometry and the Mössbauer spectroscopy. Differential scanning calorimetry and differential thermal analysis studies revealed good glass forming abilities for all investigated specimens and allowed to determine thermal stability parameters of the amorphous phase. For all alloy ribbons, very large supercooled liquid region before crystallization ΔT_x reaching 100 K was measured. The Kissinger plots were constructed to determine the activation energies for crystallization. Annealing of specimens at temperatures ranging from 923 K to 1033 K for 5 min resulted in significant change of the phase constitution. The X-ray diffractometry studies have shown presence of hard magnetic Pr₂(Fe,Co)₁₄B and paramagnetic Pr_{1+x}Fe₄B₄ phases. Furthermore, with the increase of B contents in the alloy composition crystallization of α-Fe phase occurs at wider range of the annealing temperature. Anomaly of both thermal and magnetic properties was observed for the Pr₉Fe₅₂Co₁₃Zr₁Nb₄B₂₁ alloy ribbons.
Źródło:
Acta Physica Polonica A; 2017, 131, 4; 979-981
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Phase Composition and Magnetic Properties of the Nanocrystalline $Fe_{64.32}Pr_{9.6}B_{22.08}W_{4}$ Alloy
Autorzy:
Filipecka, K.
Pawlik, K.
Pawlik, P.
Wysłocki, J.
Gębara, P.
Przybył, A.
Powiązania:
https://bibliotekanauki.pl/articles/1367656.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ww
75.50.Kj
71.20.Eh
Opis:
The aim of the present work was to study the influence of annealing conditions on magnetic properties and the phase constitution of rapidly solidified $Fe_{64.32}Pr_{9.6}B_{22.08}W_{4}$ alloy ribbons. The base alloy was prepared by arc-melting of the high purity elements under an Ar atmosphere. Subsequently the ribbon samples were obtained by melt-spinning technique under low pressure of Ar. In order to develop nanocrystalline structure, the samples were annealed at 1003 K for 5, 10, 20 and 30 min. The room temperature magnetic properties were determined from hysteresis loops measured by VSM magnetometry in the external magnetic field up to 2 T. For comparison the influence of annealing temperature on magnetic properties was studied for the same alloy composition. The ribbons were annealed at temperatures from 929 K to 1023 K for 5 min. X-ray diffractometry was used to determine the phase composition of annealed ribbons. Heat treatment resulted in an evolution of the phase constitution, that caused changes in magnetic properties of the alloy.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 164-165
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Magnetic Properties of the Nanocrystalline Fe-Co-Zr-Ti-Pr-B Alloys
Autorzy:
Pawlik, P.
Powiązania:
https://bibliotekanauki.pl/articles/1813665.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ww
75.50.Kj
71.20.Eh
Opis:
Investigation of the $Fe_{60}Co_{13}Zr_1Ti_3Pr_9B_{14}$ alloy 1 mm diameter rods and 3 mm outer diameter tubes showed a possibility of processing nanocrystalline magnets by direct quenching. It was revealed that the low temperature annealing of the tube samples at 573 K/10 min resulted in an improvement of the intrinsic coercivity that reaches≈1260 kA/m, which was a similar value to that measured for thin ribbon annealed at 973 K/10 min. The X-ray diffraction analysis revealed that the hard magnetic $Pr_2(Fe, Co)_{14}B$ was the single crystalline phase that precipitated during rapid solidification process of the tube and rod samples and during devitrification annealing of the ribbons.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 315-318
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Measurements of Magnetocaloric Effect in $LaFe_{11.14}Co_{0.66}Si_{1.2-x}Al_{x}$ (x=0.1, 0.2, 0.3) Alloys
Autorzy:
Gębara, P.
Pawlik, P.
Michalski, B.
Wysłocki, J.
Powiązania:
https://bibliotekanauki.pl/articles/1387211.pdf
Data publikacji:
2015-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.30.Sg
75.50.Bb
Opis:
In the present work, phase constitution and thermomagnetic properties of $LaFe_{11.14}Co_{0.66}Si_{1.2-x}Al_{x}$ (where x = 0.1, 0.2, 0.3) alloys were investigated. Ingot samples were obtained by arc-melting under the low pressure of Ar atmosphere. Subsequently samples were annealed at 1323 K for 15 days. X-ray diffraction of all samples revealed coexistence of two crystalline phases dominant $La(Fe,Si)_{13}$-type and minor bcc α -Fe. Furthermore, the magnetic measurements at various temperatures allowed to study the Curie temperature, magnetic entropy changes and relative cooling power.
Źródło:
Acta Physica Polonica A; 2015, 127, 2; 576-578
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Annealing Temperature on the Phase Constitution and Magnetic Properties of the Pr₈Dy₁Fe₆₀Co₇Mn₆B₁₄Zr₁Ti₃ Alloy Ribbons
Autorzy:
Przybył, A.
Pawlik, K.
Pawlik, P.
Gębara, P.
Kaszuwara, W.
Wysłocki, J.
Filipecka, K.
Powiązania:
https://bibliotekanauki.pl/articles/1402331.pdf
Data publikacji:
2015-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.20.En
91.60.Pn
Opis:
Melt-spun ribbons were produced from the Pr₈Dy₁Fe₆₀Co₇Mn₆B₁₄Zr₁Ti₃ base alloy at the surface velocity of the cooper wheel of 30 m/s. The studies showed amorphous structure of ribbons and their soft magnetic properties. X-ray diffraction was used to determine phase constitution of all obtained samples. Annealing of ribbons caused formation of nanocomposite structure, which was a result of coexistence of hard magnetic RE₂(Fe,Co)₁₄B and soft magnetic α-Fe phases. Basic magnetic properties such as: coercivity $\text{}_{J}H_{c}$, remanence $J_{r}$ and maximum energy product $(BH)_\text{max}$ were determined from the measured hysteresis loops. The microstructure of selected specimens was observed by transmission electron microscopy technique.
Źródło:
Acta Physica Polonica A; 2015, 128, 1; 94-97
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Tungsten Addition on Phase Constitution and Magnetic Properties of the Bulk $Fe_{65}Pr_{9}B_{26-x}W_x$ Alloys
Autorzy:
Filipecka, K.
Pawlik, P.
Pawlik, K.
Gębara, P.
Przybył, A.
Pruba, M.
Powiązania:
https://bibliotekanauki.pl/articles/1402336.pdf
Data publikacji:
2015-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ww
75.50.Kj
71.20.Eh
Opis:
The effect of tungsten addition on phase constitution and magnetic properties of the bulk $Fe_{65}Pr_9B_{26-x}W_{x}$ (where x=2, 4, 6, 8) alloys was studied. The base alloys were prepared by arc-melting of the high purity elements under Ar atmosphere. Samples were produced by suction of an arc-molten alloy to a water-cooled copper mould (the suction-casting method). In order to develop nanocrystalline structure, the samples were subjected to annealing. Heat treatment resulted in an evolution of the phase constitution that caused changes in magnetic properties of the alloys. X-ray diffractometry was used to determine the phase composition of annealed samples. The analysis showed presence of hard magnetic $Pr_2Fe_{14}B$, paramagnetic $Pr_{1+x}Fe_4B_4$ and soft ferromagnetic α-Fe phases of annealed samples. The room temperature magnetic properties were determined from hysteresis loops measured by VSM magnetometer in the external magnetic field up to 2 T. The highest hard magnetic parameters were measured for the rod sample of $Fe_{65}Pr_9B_{20}W_6$ annealed at 1003 K for 5 min.
Źródło:
Acta Physica Polonica A; 2015, 128, 1; 104-106
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and magnetic properties of the as - cast Nd10Fe83Zr1B6 ribbons, studied by X-ray diffraction and Mössbauer spectroscopy
Autorzy:
Ceglarek, A.
Płusa, D.
Pawlik, P.
Gębara, P.
Powiązania:
https://bibliotekanauki.pl/articles/147920.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
hard magnetic magnets
melt-spinning technique
Mössbauer spectroscopy
nanocomposites
Opis:
The Nd10Fe83Zr1B6 alloy ribbons, prepared by melt-spinning technique, have been investigated by X-ray diffraction (XRD) and Mossbauer spectroscopy. Magnetic properties were studied by Faraday balance and vibrating sample magnetometry (VSM). The ribbon samples were produced at various surface velocities of the copper wheel from 10 m/s to 20 m/s. The XRD and Mossbauer spectra analysis have shown that the ribbons consist of the soft magnetic alfa-Fe, hard magnetic Nd2Fe14B and disordered phases. The results showed that a uniform Nd2Fe14B/alfa-Fe nanocomposite structure with fine alfa-Fe grains can be obtained at an optimum velocity of the cooper roll of 20 m/s. The samples produced in these conditions had the best magnetic properties (mi0HC= 0.84 T, mi0MR = 1.05 T, mi0MS = 1.36 T, (BH)max = 160 kJ/m3) with strong exchange coupling between the hard magnetic Nd2Fe14B and soft magnetic mi-Fe phases. The amorphous phase existing between grains causes an increase in the remanence and remanence ratio.
Źródło:
Nukleonika; 2013, 58, 1; 105-108
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetization Reversal Processes in the Nanocrystalline Fe-Co-Zr-Ti-Pr-B Magnets
Autorzy:
Pawlik, K.
Pawlik, P.
Wysłocki, J.
Kaszuwara, W.
Powiązania:
https://bibliotekanauki.pl/articles/1813515.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Ww
75.50.Kj
71.20.Eh
Opis:
Magnetization reversal processes in the magnets derived from the $Fe_{60}Co_{13}Zr_1Ti_3Pr_9B_{14}$ alloy were investigated. It was shown that the processing technique affects the magnetization reversal processes. For the nanocrystalline ribbon samples pinning of the domain walls arises at low external magnetic fields while nucleation of reversed domains occurs at higher fields. However, the nucleation fields are lower than the pinning fields for the nanocrystalline rod and tube samples produced by suction-casting technique.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 39-42
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 27

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