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    Wyświetlanie 1-9 z 9
    Tytuł:
    Correlation between Microstructure/Fracture Surfaces and Material Properties
    Autorzy:
    Bidulský, R.
    Bidulská, J.
    Actis Grande, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1418955.pdf
    Data publikacji:
    2012-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.20.Ev
    81.40.-z
    62.20.mm
    62.25.Mn
    Opis:
    The present paper deals with the evaluation of the effect of different vacuum heat treatments on the microstructure and fracture surfaces of a low alloyed sintered Fe-[1.5Cr-0.2Mo]-0.6C steel, in correlation with the mechanical and plastic properties achieved. The heat treatment consists of the sintering process in vacuum furnace at 1393 K for 1800 s, followed by different cooling conditions and an integrated final tempering at 473 K for 3600 s. The average cooling rates, calculated in the range of 1393 K to 673 K, were 0.1, 0.235, 3, and 6 K/s, respectively. Vacuum heat treatment is supporting the bainitic-martensitic microstructure, the higher the faster cooling rate applied. This provides a marked increase in strength coupled to a decrease in ductility. The decrease of the impact energy after heat treatment is justified by the microstructural changes, especially if a part of bainite is converted to brittle martensite. Samples with bainitic microstructure presented higher impact energies than those with martensitic microstructure. This is fully confirmed by the fracture surface analysis at higher magnification, revealing three main micromechanisms of fracture: brittle, ductile and quasi-cleavage.
    Źródło:
    Acta Physica Polonica A; 2012, 122, 3; 548-552
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Analysis of the Fracture Surfaces of New Development Insulated Iron Powder Compounds
    Autorzy:
    Bidulský, R.
    Bidulská, J.
    Kvačkaj, T.
    Actis Grande, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1201089.pdf
    Data publikacji:
    2014-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.-y
    81.20.Ev
    81.40.Np
    Opis:
    Goal of the present paper is the analysis of the fracture surfaces of an Insulated Iron Powder Compound (IIPC) with different additions of aluminium alloy (0.25, 0.5 and 0.75 wt.%), in order to improve the mechanical properties, evaluated as the transverse rupture strength (TRS) with sufficient magnetic properties (mainly represented by the iron loss and coercivity force). Investigation of microstructure and porosity development concluded that improvements in bending strength and impact values require the reduction of surface oxides during the heat treatment, in order to get a proper load bearing area between the adjacent particles.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 1; 154-155
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Porosity Evaluation during ECAP in Aluminium PM Alloy
    Autorzy:
    Bidulská, J.
    Kvačkaj, T.
    Bidulský, R.
    Actis Grande, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1418956.pdf
    Data publikacji:
    2012-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.07.Bc
    81.20.Ev
    81.40.-z
    Opis:
    The main aim of this paper is to show porosity evolution during application of various processing conditions including pressing, sintering and equal channel angular pressure. An aluminium based powder (Al-Mg-Si-Cu-Fe) was used as investigated material. After applying different pressing pressures (400 and 600 MPa), specimens were dewaxed in a ventilated furnace at 400C for 60 min. Sintering was carried out in a vacuum furnace at 610C for 30 min. The specimens were processed by single equal channel angular pressure pass. A significant disadvantage of powder metallurgy processing methods is the presence of porosity. Pores act as crack initiators and, due to their presence, the distribution of stress is inhomogeneous across the cross-section and leads to reduction of the effective load bearing area. The equal channel angular pressure process, causing stress distribution in deformed specimens, made the powder particles to squeeze together to such an extent that the initially interconnected pores transform to small isolated pores. The proposed safety diagram includes the combined effect of stress and strain behaviour during equal channel angular pressure. The "safety line" eliminates and quantifies the effect of large pores as a potential fracture initiation sites with respect to the mechanical viewpoint.
    Źródło:
    Acta Physica Polonica A; 2012, 122, 3; 553-556
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigation of Fracture Surfaces of Soft Magnetic Materials
    Autorzy:
    Bidulská, J.
    Kvačkaj, T.
    Bidulský, R.
    Actis Grande, M.
    Ferraris, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/1533971.pdf
    Data publikacji:
    2010-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.-y
    81.20.Ev
    81.40.Np
    Opis:
    The present paper focused on the analysis of the fracture surfaces of a new development insulated iron powder compound with the addition of the aluminium alloy in order to improve the mechanical properties. Results show that in the pressed state, mainly pores act as crack initiators and due to their presence the distribution of stress is inhomogeneous across the cross-section and leads to the reduction of the effective load bearing area. Investigation of fracture surfaces concluded that improvements in bonding during the pressing process and heat treatment can be helpful in the development of soft magnetic materials to give a suitable combination between pressing pressure, annealing temperature and time as well as magnetic properties.
    Źródło:
    Acta Physica Polonica A; 2010, 118, 5; 800-801
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Effects of Chemical Composition on Soft Magnetic Materials Behaviour
    Autorzy:
    Bidulský, R.
    Actis Grande, M.
    Ferraris, L.
    Ferraris, P.
    Bidulská, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1533981.pdf
    Data publikacji:
    2010-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.-y
    81.20.Ev
    81.40.Rs
    Opis:
    The main aim of the presented work was to study the effects of chemical composition on the magnetic properties (in terms of B-H characteristics) of an insulated iron powder compound with various addition of the aluminium alloy (0, 5 and 10 wt%). The magnetic properties of the powder were significantly influenced by density and "sintering" effects. The addition of aluminium alloy maintaining suitable values of coercive force, remanence and core losses; this makes the modified insulated iron powder compound a promising soft magnetic material in several applications.
    Źródło:
    Acta Physica Polonica A; 2010, 118, 5; 802-803
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microdeformation Processes in Soft Magnetic Compounds
    Autorzy:
    Bidulský, R.
    Bidulská, J.
    Petroušek, P.
    Fedoriková, A.
    Dudrová, E.
    Actis Grande, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1032942.pdf
    Data publikacji:
    2017-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.-y
    81.20.Ev
    81.40.Np
    Opis:
    Porosity can be defined in different ways. The most frequently used definition is the total porosity, which is the total volume fraction of empty space in the specimen. The presence of pores strongly affects the fracture mode. Besides the evaluation of geometry and quality of connections, fractographic analysis enables a quantification of the important microstructural characteristics of the plane porosity. This quantity allows to quantify the existing relations between microstructure and properties. The fractographic evaluation of the distribution of microdeformation processes in the volume of experimental material demonstrates the influence of porosity on the concentration of deformation flows into the microvolume of connections. Plain porosity contributes to the recognition of critical microstructural defects and therefore, to enable evaluating the relationship between the processing parameters, microstructural constituents, and pores. In the fractography evaluation, the analysis of the quality of interparticle bonding using determination of elementary types of fracture facets allows to interpret the mechanical and plastic properties of investigated materials.
    Źródło:
    Acta Physica Polonica A; 2017, 131, 5; 1367-1370
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of ECAP-Back Pressure on the Porosity Distribution
    Autorzy:
    Bidulská, J.
    Kvačkaj, T.
    Kočiško, R.
    Bidulský, R.
    Actis Grande, M.
    Donič, T.
    Martikán, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1538174.pdf
    Data publikacji:
    2010-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.05.Bx
    81.20.Ev
    81.40.-z
    81.70.Fy
    Opis:
    The main aim of this paper is to show how back pressure equal channel angular pressing (ECAP-BP) influences the porosity distribution in powder metallurgy (PM) aluminium alloys. When back pressure is applied, the accumulation of damage in deformed samples decreases due to the fact that the shear strain takes place under predominantly compressive stresses. Consequently, ECAP-BP influences the porosity distribution in terms of the severe shear deformation involved. According to the obtained results, interesting applications for this new progressive method in physical and metallurgical research fields are shown.
    Źródło:
    Acta Physica Polonica A; 2010, 117, 5; 864-868
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Interparticle Neck Connections in Innovative Insulated Iron Powder Compounds
    Autorzy:
    Bidulský, R.
    Bidulská, J.
    de Oro, R.
    Hryha, E.
    Maccarini, M.
    Forno, I.
    Actis Grande, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/1402111.pdf
    Data publikacji:
    2015-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.-y
    81.20.Ev
    81.40.Np
    Opis:
    Goal of the present paper is the analysis of the interparticle neck connections in a system made of insulated iron powder compounds with different additions of an Al-Mg-Si-Cu alloy (0.25, 0.5 and 0.75 wt%). The introduction of the aluminium alloy powder has been made in order to improve the mechanical properties, evaluated as the transverse rupture strength, without decreasing the magnetic properties (evaluated in terms of iron loss and coercivity force). The fracture analysis of investigated systems puts into evidence the breaking of interparticle neck connections. Heat treatment (at the temperature of 500°C) contributes to the early stages of interparticle neck developments. The chosen aluminium alloy presents a sort of pre-sintering behaviour at 500°C, with the possibility of mass-transport processes around the insulated iron powder compounds. The air heat treatment applied aims at providing an increase in the mechanical behaviour of the material, with a final good rigidity after the cooling process. Fracture surfaces and transverse rupture strength values show that, at 500 MPa, the strength and the area related to the inter-particle necks can be correlated to the occasional broken insulated point-to-point surfaces that hinder the development of inter-particles necks.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 4; 647-650
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of Microstructural and Mechanical Properties after Cold Rolling of an Electro-Sinter-Forged Cu-Sn Alloy
    Autorzy:
    Gobber, F. S.
    Bidulská, J.
    Fais, A.
    Franchini, F.
    Bidulský, R.
    Kvačkaj, T.
    Actis Grande, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/352541.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Electro-Sinter-Forging
    powder metallurgy
    CuSn15
    rolling
    Opis:
    Traditional press and sinter processes have gained in the last decades more and more importance in the manufacturing of high volume and precise mechanical components especially in the field of iron based powders. In recent years, the reductions of processing times and temperatures were spotted as critical targets to increase productivity and reduce energy consumption. Electric current assisted sintering (ECAS) technologies have always been seen as an alternative to traditional furnace based sintering techniques and have been the target of different researches with the specific purpose of reducing both operational times and costs. The aim of the present study is to investigate the effect of an innovative process called Electro Sinter Forging (ESF) applied to CuSn15 powders. Thanks to a very short processing time (less than 1 second to densify loose powders), this process is able to retain a very small grain size, thus enhancing mechanical properties of the processed materials. Furthermore, to the authors knowledge, cold – rolled electro – sinter – forged alloys has never been investigated before. First of all, bars were electro – sinter – forged and subsequently characterized in the as sinter – forged condition. The observation of microstructure evidenced an extremely fine microstructure and a reduced degree of porosity. Afterwards, bars were cold rolled after different reduction ratios; macrostructural integrity of the rolled bars was assessed before evaluating the effects of cold rolling on the sinter – forged microstructure.
    Źródło:
    Archives of Metallurgy and Materials; 2020, 65, 2; 787-792
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-9 z 9

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