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Wyświetlanie 1-12 z 12
Tytuł:
Correlation between Microstructure/Fracture Surfaces and Material Properties
Autorzy:
Bidulský, R.
Bidulská, J.
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/1418955.pdf
Data publikacji:
2012-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
81.20.Ev
81.40.-z
62.20.mm
62.25.Mn
Opis:
The present paper deals with the evaluation of the effect of different vacuum heat treatments on the microstructure and fracture surfaces of a low alloyed sintered Fe-[1.5Cr-0.2Mo]-0.6C steel, in correlation with the mechanical and plastic properties achieved. The heat treatment consists of the sintering process in vacuum furnace at 1393 K for 1800 s, followed by different cooling conditions and an integrated final tempering at 473 K for 3600 s. The average cooling rates, calculated in the range of 1393 K to 673 K, were 0.1, 0.235, 3, and 6 K/s, respectively. Vacuum heat treatment is supporting the bainitic-martensitic microstructure, the higher the faster cooling rate applied. This provides a marked increase in strength coupled to a decrease in ductility. The decrease of the impact energy after heat treatment is justified by the microstructural changes, especially if a part of bainite is converted to brittle martensite. Samples with bainitic microstructure presented higher impact energies than those with martensitic microstructure. This is fully confirmed by the fracture surface analysis at higher magnification, revealing three main micromechanisms of fracture: brittle, ductile and quasi-cleavage.
Źródło:
Acta Physica Polonica A; 2012, 122, 3; 548-552
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Role of microstructure discontinuities in the soft magnetic composites with aluminium alloy addition
Rola niejednorodności mikrostruktury w magnetycznie miękkich kompozytach z dodatkiem stopu aluminium
Autorzy:
Bidulský, R
Bidulská, J.
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/351805.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
soft magnetic composites
insulated iron powder compound
aluminium alloy
coercivity
specific losses
magnetycznie miękkie kompozyty
materiał IIPC
stop aluminium
straty
Opis:
The paper focuses on the effect of both the aluminium alloy addition and microstructural inhomogeneties on the magnetic behaviour of soft magnetic materials tested at low frequencies. The IIPC material (base on the commercial Somaloy 1P powder) has been blended with different amounts of commercially aluminium alloy Alumix 321 (0, 5 and 10 wt %). Specimens with a different green density were obtained by pressing at a pressure in the range from 400 to 800 MPa. Different thermal treatments (in air or nitrogen at the maximum temperature of 500ºC for 30 min) were carried out on the evaluated systems. The microstructure investigation revealed that for materials with high aluminium alloy contents, pores are located nearby or around the aluminium alloy particles. The heat treatment regime resulted in a coarse-grained structure with a small number of inclusions within the grains and at the grain boundaries. The comparison of the results indicated that the magnetic properties were considerably dependent on the microstructural inhomogeneities.
Przedmiotem pracy jest wpływ dodatku stopu aluminium oraz niejednorodności mikrostruktury na właściwości magnetyczne magnetycznie miękkich materiałów badanych przy niskich częstotliwościach. Materiał IIPC (na bazie komercyjnego proszku Somaloy 1P) został zmieszany z różnymi ilościami komercyjnego stopu aluminium ALUMIX 321 (0, 5 i 10% wag.). Próbki o różnych gęstościach nasypowych prasowano stosując ciśnienie w zakresie od 400 do 800 MPa. Zastosowano różne obróbki cieplne (w powietrzu i azocie) ustalając maksymalną temperaturę 500ºC. Badania mikrostruktury pokazały, że dla materiałów o wysokiej zawartości stopu aluminium, pory sa w pobliżu lub otaczają cząstki stopu aluminium. W wyniku obróbki cieplnej tworzy się gruboziarnista struktura z minimalną liczbą wtraceń wewnątrz ziaren i na ich granicach. Porównanie wyników pokazuje, ąe właściwości magnetyczne zaleza w znacznym stopniu od niejednorodności mikrostruktury.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 2; 365-370
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of Densification Process and Structure of PM Al-Mg-Si-Cu-Fe and Al-Zn-Mg-Cu-Sn Alloys
Analiza procesu zagęszczania i struktury spiekanych stopów Al-Mg-Si-Cu-Fe i Al-Zn-Mg-Cu-Sn
Autorzy:
Bidulský, R
Bidulská, J.
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/355248.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powder metallurgy
aluminium alloy
compressibility
microstructure
metalurgia proszków
stop aluminium
ściśliwość
mikrostruktura
Opis:
The paper is focused on the role of the pressing pressure on the densification behaviour of PM aluminium alloys. Commercially aluminium based powders Al-Mg-Si-Cu-Fe and Al-Zn-Mg-Cu-Sn were used as materials to be investigated. The apparent density of the powder mixes was determined according to MPIF St. 04. A set of cylinder test specimen 55x10x10 mm3 was uniaxially pressed in a floating hardened steel die. Compaction pressures ranged from 50 MPa up to 700 MPa. Considering the densification of metal powders in uniaxial compaction, quantification of aluminium compaction behaviour was performed. The compressibility behaviour was evaluated, considering the effect on specimens, as well as on their microstructure. The development of compressibility values with pressing pressure enables to characterize the effect of particles geometry and matrix plasticity on the compaction process.
Przedmiotem pracy jest wpływ ciśnienia prasowania na zagęszczanie proszków stopów aluminium. Materiałem badanym były komercyjne proszki aluminium Al-Mg-Si-Cu-Fe I Al-Zn-Mg-Cu-Sn. Gęstość pozorna mieszanek proszków określono według MPIF St.04. Cylindryczne próbki 55x10x10 mm3 ściskane były jednokierunkowo w samonastawnej matrycy z hartowanej stali. Nacisk wahał się od 50 MPa do 700 MPa. Biorąc pod uwagę zagęszczenie proszków metali w trakcie prasowania jednoosiowego, przeprowadzono kwantyfikacje zagęszczania aluminium. Oceniono zachowanie ściśliwości biorąc pod uwagę wpływ na próbki, jak również na ich mikrostrukturę. Zestawienie wartości ściśliwości z ciśnieniem prasowania pozwala scharakteryzować wpływ geometrii cząstek i plastyczności matrycy na proces prasowania.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 1; 17-23
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Porosity Evaluation during ECAP in Aluminium PM Alloy
Autorzy:
Bidulská, J.
Kvačkaj, T.
Bidulský, R.
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/1418956.pdf
Data publikacji:
2012-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
81.07.Bc
81.20.Ev
81.40.-z
Opis:
The main aim of this paper is to show porosity evolution during application of various processing conditions including pressing, sintering and equal channel angular pressure. An aluminium based powder (Al-Mg-Si-Cu-Fe) was used as investigated material. After applying different pressing pressures (400 and 600 MPa), specimens were dewaxed in a ventilated furnace at 400C for 60 min. Sintering was carried out in a vacuum furnace at 610C for 30 min. The specimens were processed by single equal channel angular pressure pass. A significant disadvantage of powder metallurgy processing methods is the presence of porosity. Pores act as crack initiators and, due to their presence, the distribution of stress is inhomogeneous across the cross-section and leads to reduction of the effective load bearing area. The equal channel angular pressure process, causing stress distribution in deformed specimens, made the powder particles to squeeze together to such an extent that the initially interconnected pores transform to small isolated pores. The proposed safety diagram includes the combined effect of stress and strain behaviour during equal channel angular pressure. The "safety line" eliminates and quantifies the effect of large pores as a potential fracture initiation sites with respect to the mechanical viewpoint.
Źródło:
Acta Physica Polonica A; 2012, 122, 3; 553-556
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of the Fracture Surfaces of New Development Insulated Iron Powder Compounds
Autorzy:
Bidulský, R.
Bidulská, J.
Kvačkaj, T.
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/1201089.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.-y
81.20.Ev
81.40.Np
Opis:
Goal of the present paper is the analysis of the fracture surfaces of an Insulated Iron Powder Compound (IIPC) with different additions of aluminium alloy (0.25, 0.5 and 0.75 wt.%), in order to improve the mechanical properties, evaluated as the transverse rupture strength (TRS) with sufficient magnetic properties (mainly represented by the iron loss and coercivity force). Investigation of microstructure and porosity development concluded that improvements in bending strength and impact values require the reduction of surface oxides during the heat treatment, in order to get a proper load bearing area between the adjacent particles.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 154-155
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effects of Chemical Composition on Soft Magnetic Materials Behaviour
Autorzy:
Bidulský, R.
Actis Grande, M.
Ferraris, L.
Ferraris, P.
Bidulská, J.
Powiązania:
https://bibliotekanauki.pl/articles/1533981.pdf
Data publikacji:
2010-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.-y
81.20.Ev
81.40.Rs
Opis:
The main aim of the presented work was to study the effects of chemical composition on the magnetic properties (in terms of B-H characteristics) of an insulated iron powder compound with various addition of the aluminium alloy (0, 5 and 10 wt%). The magnetic properties of the powder were significantly influenced by density and "sintering" effects. The addition of aluminium alloy maintaining suitable values of coercive force, remanence and core losses; this makes the modified insulated iron powder compound a promising soft magnetic material in several applications.
Źródło:
Acta Physica Polonica A; 2010, 118, 5; 802-803
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Fracture Surfaces of Soft Magnetic Materials
Autorzy:
Bidulská, J.
Kvačkaj, T.
Bidulský, R.
Actis Grande, M.
Ferraris, L.
Powiązania:
https://bibliotekanauki.pl/articles/1533971.pdf
Data publikacji:
2010-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.-y
81.20.Ev
81.40.Np
Opis:
The present paper focused on the analysis of the fracture surfaces of a new development insulated iron powder compound with the addition of the aluminium alloy in order to improve the mechanical properties. Results show that in the pressed state, mainly pores act as crack initiators and due to their presence the distribution of stress is inhomogeneous across the cross-section and leads to the reduction of the effective load bearing area. Investigation of fracture surfaces concluded that improvements in bonding during the pressing process and heat treatment can be helpful in the development of soft magnetic materials to give a suitable combination between pressing pressure, annealing temperature and time as well as magnetic properties.
Źródło:
Acta Physica Polonica A; 2010, 118, 5; 800-801
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Identification of the critical pore sizes in sintered and ecaped aluminium 6XXX alloy
Przewidywanie powstawania porowatości podczas wyciskania w kanale kątowym stopu aluminium otrzymanego metodą proszkową
Autorzy:
Bidulská, J.
Kvačkaj, T.
Pokorný, I.
Bidulský, R
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/353976.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium alloy
ECAP
porosity
critical pore sizes
microstructure
fracture
stop aluminium
wyciskanie w kanale kątowym
porowatość
mikrostruktura
pękanie
Opis:
The main aim of this paper is to investigate, by means of comparison of experimental studies and mathematical models, the evolution of porosity as consequence of pressing, sintering and ECAPping an aluminium based powder (6xxx). After applying the compacting pressure, specimens were dewaxed in a ventilated furnace at 400º for 60 min. Sintering was carried out in a vacuum furnace at 610ºC for 30 min. The specimens were then ECAPed for 1 pass. The 2-dimensional quantitative image analysis was carried out by means of SEM and OM for the evaluation of the aforementioned characteristics. Results show the effect of processing parameters on the fracture/microstructure behaviour of the studied aluminium PM alloy. Quantitative image analysis, as well as fractographic interpretation and microstructure identification of weak sites in the studied aluminium PM alloy, provide a reliable and reproducible statistical procedure for the identification of the critical pore sizes.
Głównym celem pracy jest badanie zmian porowatości podczas prasowania, spiekania i wyciskania przez kanał katowy proszku na bazie aluminium (Ai-Mg-Si-Cu-Fe) za pomocą eksperymentu i symulacji numerycznych. Po przyłożeniu ciśnienia podczas zagęszczania usuwano lepiszcze z próbek w piecu w temperaturze 400ºC przez 60 minut. Spiekanie prowadzono w piecu próżniowym w temperaturze 610ºC przez 30 min. Próbki następnie były wyciskane przez kanał kątowy w jednym przejściu. Dwuwymiarowa ilościową analizę obrazu przeprowadzono za pomocą skaningowej mikroskopii elektronowej i mikroskopii optycznej w celu oceny wyżej wymienionych właściwości. Wyniki opisują wpływ parametrów procesu na pękanie/ mikrostrukturę badanego proszku stopu aluminium. Ilościowa analiza obrazu, jak równiez mikrostruktury w badanym stopie proszku aluminium zapewniają wiarygodne i statystycznie powtarzalne procedury dla identyfikacji miejsc inicjacji pękania.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 2; 371-375
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microdeformation Processes in Soft Magnetic Compounds
Autorzy:
Bidulský, R.
Bidulská, J.
Petroušek, P.
Fedoriková, A.
Dudrová, E.
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/1032942.pdf
Data publikacji:
2017-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.-y
81.20.Ev
81.40.Np
Opis:
Porosity can be defined in different ways. The most frequently used definition is the total porosity, which is the total volume fraction of empty space in the specimen. The presence of pores strongly affects the fracture mode. Besides the evaluation of geometry and quality of connections, fractographic analysis enables a quantification of the important microstructural characteristics of the plane porosity. This quantity allows to quantify the existing relations between microstructure and properties. The fractographic evaluation of the distribution of microdeformation processes in the volume of experimental material demonstrates the influence of porosity on the concentration of deformation flows into the microvolume of connections. Plain porosity contributes to the recognition of critical microstructural defects and therefore, to enable evaluating the relationship between the processing parameters, microstructural constituents, and pores. In the fractography evaluation, the analysis of the quality of interparticle bonding using determination of elementary types of fracture facets allows to interpret the mechanical and plastic properties of investigated materials.
Źródło:
Acta Physica Polonica A; 2017, 131, 5; 1367-1370
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of ECAP-Back Pressure on the Porosity Distribution
Autorzy:
Bidulská, J.
Kvačkaj, T.
Kočiško, R.
Bidulský, R.
Actis Grande, M.
Donič, T.
Martikán, M.
Powiązania:
https://bibliotekanauki.pl/articles/1538174.pdf
Data publikacji:
2010-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Bx
81.20.Ev
81.40.-z
81.70.Fy
Opis:
The main aim of this paper is to show how back pressure equal channel angular pressing (ECAP-BP) influences the porosity distribution in powder metallurgy (PM) aluminium alloys. When back pressure is applied, the accumulation of damage in deformed samples decreases due to the fact that the shear strain takes place under predominantly compressive stresses. Consequently, ECAP-BP influences the porosity distribution in terms of the severe shear deformation involved. According to the obtained results, interesting applications for this new progressive method in physical and metallurgical research fields are shown.
Źródło:
Acta Physica Polonica A; 2010, 117, 5; 864-868
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Interparticle Neck Connections in Innovative Insulated Iron Powder Compounds
Autorzy:
Bidulský, R.
Bidulská, J.
de Oro, R.
Hryha, E.
Maccarini, M.
Forno, I.
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/1402111.pdf
Data publikacji:
2015-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.-y
81.20.Ev
81.40.Np
Opis:
Goal of the present paper is the analysis of the interparticle neck connections in a system made of insulated iron powder compounds with different additions of an Al-Mg-Si-Cu alloy (0.25, 0.5 and 0.75 wt%). The introduction of the aluminium alloy powder has been made in order to improve the mechanical properties, evaluated as the transverse rupture strength, without decreasing the magnetic properties (evaluated in terms of iron loss and coercivity force). The fracture analysis of investigated systems puts into evidence the breaking of interparticle neck connections. Heat treatment (at the temperature of 500°C) contributes to the early stages of interparticle neck developments. The chosen aluminium alloy presents a sort of pre-sintering behaviour at 500°C, with the possibility of mass-transport processes around the insulated iron powder compounds. The air heat treatment applied aims at providing an increase in the mechanical behaviour of the material, with a final good rigidity after the cooling process. Fracture surfaces and transverse rupture strength values show that, at 500 MPa, the strength and the area related to the inter-particle necks can be correlated to the occasional broken insulated point-to-point surfaces that hinder the development of inter-particles necks.
Źródło:
Acta Physica Polonica A; 2015, 128, 4; 647-650
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of Microstructural and Mechanical Properties after Cold Rolling of an Electro-Sinter-Forged Cu-Sn Alloy
Autorzy:
Gobber, F. S.
Bidulská, J.
Fais, A.
Franchini, F.
Bidulský, R.
Kvačkaj, T.
Actis Grande, M.
Powiązania:
https://bibliotekanauki.pl/articles/352541.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Electro-Sinter-Forging
powder metallurgy
CuSn15
rolling
Opis:
Traditional press and sinter processes have gained in the last decades more and more importance in the manufacturing of high volume and precise mechanical components especially in the field of iron based powders. In recent years, the reductions of processing times and temperatures were spotted as critical targets to increase productivity and reduce energy consumption. Electric current assisted sintering (ECAS) technologies have always been seen as an alternative to traditional furnace based sintering techniques and have been the target of different researches with the specific purpose of reducing both operational times and costs. The aim of the present study is to investigate the effect of an innovative process called Electro Sinter Forging (ESF) applied to CuSn15 powders. Thanks to a very short processing time (less than 1 second to densify loose powders), this process is able to retain a very small grain size, thus enhancing mechanical properties of the processed materials. Furthermore, to the authors knowledge, cold – rolled electro – sinter – forged alloys has never been investigated before. First of all, bars were electro – sinter – forged and subsequently characterized in the as sinter – forged condition. The observation of microstructure evidenced an extremely fine microstructure and a reduced degree of porosity. Afterwards, bars were cold rolled after different reduction ratios; macrostructural integrity of the rolled bars was assessed before evaluating the effects of cold rolling on the sinter – forged microstructure.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 787-792
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-12 z 12

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