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Wyświetlanie 1-15 z 160
Tytuł:
Structural Characterization of Some Table Salt Samples by XRD, ICP, FTIR and XRF Techniques
Autorzy:
Yalçin, Ş.
Mutlu, İ.
Powiązania:
https://bibliotekanauki.pl/articles/1490744.pdf
Data publikacji:
2012-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
Opis:
In this study, we have investigated structure and impurities of six different salts which have a great importance in our everyday life, namely source salt, Himalayan salt, rock salt, sea salt, lake salt and reduced sodium salt (minsalt) by means of different analytical methods, namely X-ray powder diffraction, scanning electron microscope-energy dispersive X-ray spectroscopy, inductive coupling plasma optic emission spectroscopy, X-ray fluorescence spectrometer and the Fourier transform infrared spectroscopy. With the light of obtained results, suitability and performance of the different analytical methods were discussed in some details.
Źródło:
Acta Physica Polonica A; 2012, 121, 1; 50-52
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Isobaric Thermal Expansion and Isothermal Compression of Powdered NiFe Based Alloys Studied by In-Situ EDXRD
Autorzy:
Olekšáková, D.
Füzer, J.
Kollár, P.
Bednarčík, J.
Lathe, C.
Powiązania:
https://bibliotekanauki.pl/articles/1200812.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.50.Bb
61.05.cp
Opis:
The aim of the present work was to study the isothermal compression and isobaric thermal expansion behaviour of ball-milled NiFe (81 wt.% of Ni) and NiFeMo (79 wt.% of Ni, 16 wt.% of Fe) alloy and follow its phase evolution when exposed to high pressure and temperature. In-situ pressure-temperature energy dispersive X-ray (EDXRD) diffraction experiments were performed at the MAX80 instrument (beamline F2.1). The compressibility of NiFe alloy at 400 °C was evaluated for pressure values of up to 3.5 GPa. The EDXRD spectra revealed the presence of cubic FeNi_{3} phase as determined from the shift of (111), (200) and (220) reflection lines in corresponding EDXRD spectra.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 128-129
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The quantitative dependence of reducibility on mineralogical composition in iron ore sinters (blast furnace sinters)
Autorzy:
Krztoń, H.
Stecko, J.
Kania, Z.
Powiązania:
https://bibliotekanauki.pl/articles/1058082.pdf
Data publikacji:
2016-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
89.20.Bb
Opis:
Reducibility is a parameter which describes the ability of oxygen, combined with iron, to be removed from iron ore sinters by a reducing gas used in a blast furnace, and is often characterized by a Fe²⁺ content in a sinter. In sinters, iron at Fe²⁺ valence can occur in various types of minerals, which differ in values of reducibility. The set of sinters with the reducibility from 0.63%/min to 1.49%/min, prepared in the different laboratory conditions, were examined in terms of their mineral composition. The quantitative dependences between the fractions of the individual mineral constituents of the sinters and the values of reducibility were sought. The increase of the reducibility was correlated with a decrease of the content of magnetite and a rise of the fraction of hematite.
Źródło:
Acta Physica Polonica A; 2016, 130, 4; 1147-1150
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thin layers XRD study technique on an example of cobalt tetrafluoro phthalocyanine
Autorzy:
Sukhikh, A.
Basova, T.
Gromilov, S.
Powiązania:
https://bibliotekanauki.pl/articles/1075647.pdf
Data publikacji:
2016-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
68.55.Nq
Opis:
Thin layers X-ray diffraction study technique utilizing single-crystal X-ray diffractometer equipped with microfocus X-ray tube is described. It is shown that the layers of the tetra-fluorinated cobalt phthalocyanine (CoPcF₄), deposited by thermal evaporation in vacuum on a polished surface of the substrate (glass, quartz), have a highly oriented polycrystalline structure. All the crystallites have the (00l) plane oriented along the surface of the substrate. CoPcF₄ X-ray diffraction pattern indexing was conducted and unit cell parameters were determined. It is shown that crystal phase of both polycrystalline powder and thin layers of CoPcF₄ are isostructural to that of α -CoPc.
Źródło:
Acta Physica Polonica A; 2016, 130, 4; 889-891
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Growth and Characterization of Wide-Gap $Cd_{1-x}Zn_{x}Se$ Ternary Alloys by Using Electron Beam Evaporation Technique
Autorzy:
Suthagar, J.
Rajesh, S.
Perumal, K.
Balasubramaniam, T.
Suthan Kissinger, N.
Powiązania:
https://bibliotekanauki.pl/articles/1538742.pdf
Data publikacji:
2010-03
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
71.55.Gs
61.05.cp
Opis:
$Cd_{1-x}Zn_{x}Se$ films with different zinc content were deposited by electron beam evaporation technique onto glass substrates for the application of solid-state photovoltaic devices. The structural, surface morphological and optical properties of $Cd_{1-x}Zn_{x}Se$ films have been studied in the present work. The host material, $Cd_{1-x}Zn_{x}Se$, has been prepared by the physical vapor deposition method of electron beam evaporation technique under the pressure of 1 × $10^{-5}$ mbar. The X-ray diffractogram indicates that these alloy films are polycrystalline in nature, of hexagonal structure with strong preferential orientation of the crystallites along (002) direction. Linear variation of lattice constant with composition (x) is observed. Surface roughness measured by atomic force microscopy is used to estimate the interface roughness. The optical properties show that the band gap $(E_{g})$ values vary from 2.08 to 2.64 eV as zinc content varies from 0.2 to 0.8. The surface morphological studies show the very small, fine and hardly distinguishable grains smeared all over the surface. The material properties would be altered and excellently controlled by adiusting the system composition x.
Źródło:
Acta Physica Polonica A; 2010, 117, 3; 506-511
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Angular Distribution of N-Doped Carbon Nanotubes in Alumina Membrane Channels: A High-Energy X-ray Diffraction Study
Autorzy:
Hawelek, L.
Brodka, A.
Dore, J.
Honkimäki, V.
Kyotani, T.
Yang, Q.
Burian, A.
Powiązania:
https://bibliotekanauki.pl/articles/1538877.pdf
Data publikacji:
2010-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
61.48.De
Opis:
An alignment study of multi-wall N-doped carbon nanotubes prepared by a template pyrolytic carbon deposition method inside channels of an alumina membrane has been performed using high-energy X-ray diffraction on the ID15B beamline at the European Synchrotron Radiation Facility (ESRF, Grenoble). The two-dimensional diffraction pattern of the deposited carbon nanotubes, recorded directly, within the alumina membrane, using an image plate detector, exhibits two non-continuous arcs corresponding to the 002 graphitic reflection. The following values of the angle between the axis of the carbon nanotubes lying along the membrane channels and the incident beam were taken for five positions: 0°, 30°, 45°, 60° and 90°. The anisotropic scattering distribution of the two-dimensional patterns indicates an orientational alignment of the nanotubes. The one-dimensional intensity patterns obtained by scanning around the circumference of the (0 0 2) ring have allowed an estimation of the angular distribution of the nanotubes axes.
Źródło:
Acta Physica Polonica A; 2010, 117, 2; 302-306
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Cu Negative Ion Implantation on Physical Properties of $Zn_{1-x}Mn_xTe$ Films
Autorzy:
Pogrebnjak, A.
Shypylenko, A.
Amekura, H.
Takeda, Y.
Opanasyuk, A.
Kurbatov, D.
Kolotova, I.
Klymov, O.
Kozak, C.
Powiązania:
https://bibliotekanauki.pl/articles/1400485.pdf
Data publikacji:
2013-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
61.72.uj
Opis:
The paper deals with the investigations of structural properties of $Zn_{1-x}Mn_xTe$ films, which were fabricated under various deposition conditions using the thermal evaporation method in a closed volume. The surface morphology of the samples was studied, the phase analysis of their structures was performed, the elemental analysis of the films and the crystal lattice constant were investigated. The texture perfection of the films before and after copper ion implantation was evaluated.
Źródło:
Acta Physica Polonica A; 2013, 123, 5; 939-942
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Isostructural Transition in RTAl Compounds at High Temperatures
Autorzy:
Prchal, J.
Javorský, P.
de Boer, F.
Moleman, A.
Powiązania:
https://bibliotekanauki.pl/articles/1813676.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.50.Ks
61.05.cp
Opis:
Based on previously discovered forbidden values of the c/a ratio, we studied anomalies in the temperature evolution of the lattice parameters (a, c) of several hexagonal RTAl compounds at high temperatures (above room temperature). The compound $ErNi_{0.45}Cu_{0.55}Al$, that seemed to be impossible to be prepared in single-phase form, reaches the single-phase state at temperatures above 493 K (220°C). On the other hand, the compound $TbNi_{0.7}Cu_{0.3}Al$ - that was expected to undergo a first-order structural phase transition at high temperatures - exhibits a second-order type transition when approaching the critical values of the c/a ratio. These results are in agreement with idea of a forbidden range of c/a values in these compounds.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 335-338
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Structure Characterisation of Micro-and Nanocrystalline Powders of Dy_{1-x}R_xFeO₃ (R = La, Pr, Nd, Sm, Gd)
Autorzy:
Pavlovska, O.
Lutsyuk, I.
Kondyr, A.
Zhydachevskyy, Ya.
Vakhula, Ya.
Pieniążek, A.
Vasylechko, L.
Powiązania:
https://bibliotekanauki.pl/articles/1029717.pdf
Data publikacji:
2018-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Fn
61.05.cp
Opis:
This work deals with the study of the phase and crystal structure behaviour of new micro- and nanocrystalline ferrites Dy_{1-x}R_xFeO₃ obtained by solid state reactions (R = La, Pr) and sol-gel citrate (R = Nd, Sm, Gd) techniques. It was established that all synthesized samples adopt orthorhombic perovskite structure isotypic with GdFeO₃. Unit cell dimensions and atomic coordinates of the mixed rare earth ferrites derived by full profile Rietveld refinement technique agree well with the data of the "pure" DyFeO₃ and RFeO₃ compounds, thus proving formation of continuous solid solutions Dy_{1-x}R_xFeO₃ in the DyFeO₃-RFeO₃ systems (R = La, Pr, Nd, Sm, Gd). Peculiarity of the Dy_{1-x}La_xFeO₃ series is the lattice parameters crossover and formation of dimensionally tetragonal structure at x ≈0.97.
Źródło:
Acta Physica Polonica A; 2018, 133, 4; 802-805
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The law of growth of nitrided layer in 31CrMoV9 steel
Autorzy:
Syla, N.
Aliaj, F.
Dalipi, B.
Powiązania:
https://bibliotekanauki.pl/articles/1068250.pdf
Data publikacji:
2016-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
81.65.Lp
Opis:
The law of growth of nitrided layers produced by gaseous nitriding of 31CrMoV9 alloy steel at different process parameters is described. 31CrMoV9 steel specimens were subjected to nitriding process in ammonia gas at three different temperatures: 510, 550 and 590°C, and for each temperature four different nitriding times were used. This way twelve specimens were produced. Nitrided specimens were investigated with optical microscopy, electron probe micro-analysis and x-ray diffraction. The nitrogen depth concentration profiles, deduced from electron probe micro-analysis, in conjunction with results of optical microscopy, were used to determine the thickness of the nitrided layers, i.e. the diffusion depth of nitrogen. From the dependence of the nitrided layer thickness on process parameters (temperature and time) it was possible to deduce the law that governs the growth of the nitrided layer for 31CrMoV9 alloy steel. Through this law, then, it is possible to predetermine the layer thickness for every real process parameter in nitriding of 31CrMoV9 steel, which is very important for technological applications.
Źródło:
Acta Physica Polonica A; 2016, 130, 1; 83-86
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystal perfection studies of single crystal superalloy turbine blades by X-ray diffraction methods
Autorzy:
Gancarczyk, K.
Albrecht, R.
Bogdanowicz, W.
Sieniawski, J.
Powiązania:
https://bibliotekanauki.pl/articles/1112679.pdf
Data publikacji:
2016-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.66.Dk
61.05.cp
Opis:
In the paper the crystal structure of single crystal CMSX-4 blade casts, applied in high pressure turbine of aircraft engines was analyzed. The longitudinal section of blade, cast at withdrawal rate of 3 mm/min was used as a sample. During the conducted research, following X-ray diffraction methods were applied: EFG Ω-scan, Auleytner X-ray topography and analysis of diffraction reflex profile ("rocking curve"). The authors determined crystal orientation in entire blade casts on the basis of set criterion concerning values of angle α - deviation of [001] direction from the direction of cast withdrawal. Conclusions concerning the crystal structure quality of the blade were drawn based on results from three different research methods. Local changes in crystal orientation on the surface of blade cast, also areas with significant structure defect degree and the presence of internal stresses were characterized.
Źródło:
Acta Physica Polonica A; 2016, 130, 4; 1088-1090
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of Ultrasonically Sprayed ZnO Films: Thermal Annealing Effect
Autorzy:
Ozutok, F.
Demirselcuk, B.
Sarica, E.
Turkyilmaz, S.
Bilgin, V.
Powiązania:
https://bibliotekanauki.pl/articles/1490746.pdf
Data publikacji:
2012-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.20.Ci
61.05.cp
Opis:
ZnO thin films were deposited on microscope glass substrates by ultrasonic spray pyrolysis technique. The effects of annealing under various temperatures on the optical and structural properties of ZnO thin films were analyzed. The as-deposited and annealed ZnO thin films were investigated by UV/VIS spectrophotometer and X-ray diffractometer. Some of the optical properties of the films such as transmittance, absorbance and band gap energy were investigated by UV/VIS spectrophotometer. The crystallinity levels of the films were investigated, the structural parameters such as diffraction angle, full-width at half maximum, lattice parameters, grain size and dislocation density were calculated and structural properties were analyzed. X-ray diffraction patterns indicated that the ZnO films had a polycrystalline hexagonal wurtzite structure.
Źródło:
Acta Physica Polonica A; 2012, 121, 1; 53-55
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Specific Heat Study of $PrNi_4Si$
Autorzy:
Procházková, K.
Daniš, S.
Svoboda, P.
Powiązania:
https://bibliotekanauki.pl/articles/1813660.pdf
Data publikacji:
2008-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
75.50.-y
Opis:
Here we present the results of pilot polycrystalline study of $PrNi_4Si$. The X-ray study did not confirm the expected $CaCu_5$-type structure. Instead of this, the orthorhombic structure with the space group Cmmm was found. The zero-field specific heat was measured in the temperature range 2-300 K. The data were analyzed using the sum of the phonon, electronic, and magnetic contributions to specific heat, respectively. The magnetic part of the specific heat can be well described using the Schottky formula for the 9 crystal-field singlet levels of the pz3 H4 ground-state multiplet of the $Pr^{3+}$ ion.
Źródło:
Acta Physica Polonica A; 2008, 113, 1; 299-302
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
On the Crystal and Magnetic Behavior οf $ScFe_{4}Al_{8}$ Single Crystal
Autorzy:
Rećko, K.
Dobrzyński, L.
Lemée-Cailleau, M.
Waliszewski, J.
Talik, E.
Suski, W.
Courtois, P.
Powiązania:
https://bibliotekanauki.pl/articles/1810469.pdf
Data publikacji:
2009-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.fm
61.05.cp
Opis:
Nuclear and magnetic properties of the $ScFe_{4}Al_{8}$ single crystal were found to exhibit unparalleled complexity of nuclear and magnetic structures. Our previous neutron measurements revealed presence of two modulation vectors, both along [ε, ε, 0], however with different critical temperatures. Recent experiments forced us to revise our knowledge of the structural ordering in the sample. So far, the crystal structure of this alloy, being of $ThMn_{12}$-type, has never been questioned.
Źródło:
Acta Physica Polonica A; 2009, 115, 1; 206-208
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Structural Stability of Soft Magnetic Fe-Co-Zr-W-B Metallic Glasses Investigated by the in-situ X-ray Diffraction
Autorzy:
Michalik, S.
Bednarcik, J.
Pawlik, P.
Matija, R.
Sovak, P.
Powiązania:
https://bibliotekanauki.pl/articles/1366893.pdf
Data publikacji:
2014-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
61.43.Dq
Opis:
The atomic structure of as-prepared $Fe_{61}Co_{(14-x)}Zr_{5}W_{x}B_{20}$ (x=1, 2 and 4) ribbon samples and their thermal stability were investigated by in-situ high-energy X-ray diffraction experiments. It was observed that higher W concentration causes the tiny shift of the main peak of the reduced atomic pair distribution function to higher values of interatomic distances and increases the coefficient of volume thermal expansion. The crystallization process occurs in two steps and is qualitatively the same for all studied specimens. Firstly the $Fe_{23}B_{6}$ phase is created and later is transformed to other types of borides together with the creation of a Fe-based phase.
Źródło:
Acta Physica Polonica A; 2014, 126, 1; 66-67
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 160

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