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Tytuł:
STEM-EDX and FIB-SEM Tomography of ALLVAC 718Plus Superalloy
Autorzy:
Kruk, A.
Cempura, G.
Lech, S.
Czyrska-Filemonowicz, A.
Powiązania:
https://bibliotekanauki.pl/articles/354670.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TEM
SEM
STEM-EDX tomography
FIB-SEM tomography
Allvac 718Plus
Opis:
Allvac 718Plus (718Plus) is a high strength, corrosion resistant nickel- based superalloy used for application in power generation, aeronautics and aerospace industry. The 718Plus microstructure consists of a γ matrix with γ’-Ni3(Al,Ti) and some δ- Ni3Nb phases as well as lamellar particles (η-Ni3Ti, η*-Ni6AlNb or Ni6(Al,Ti)Nb) precipitated at the grain boundaries. The primary strengthening mechanism for this alloy is a precipitation hardening, therefore size and distribution of precipitates are critical for the performance of the alloy. The aim of this study was to characterize precipitates in the 718Plus superalloy using Scanning Transmission Electron Microscope combined with Energy Dispersive X-ray Spectroscopy (STEM-EDX) and Focused Ion Beam Scanning Electron Microscope (FIB-SEM). The STEM-EDX and FIB-SEM tomography techniques were used for 3D imaging and metrology of the precipitates. Transmission electron microscopy and EDX spectroscopy were used to reveal details of the 718Plus microstructure and allow determine chemical composition of the phases. The study showed that electron tomography techniques permit to obtain complementary information about microstructural features (precipitates size, shape and their 3D distribution) in the reconstructed volume with comparison to conventional particle analysis methods, e.g. quantitative TEM and SEM metallography.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 535-542
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pollen morphology of some species of the genus Sansevieria petagna (Asparagaceae)
Autorzy:
Klimko, Małgorzata
Nowińska, Renata
Wilkin, Paul
Wiland-Szymańska, Justyna
Powiązania:
https://bibliotekanauki.pl/articles/952105.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
pollen variability
micromorphology
taxonomy
sem
Opis:
Pollen grains of 15 species of the genus Sansevieria were examined using light and scanning electron microscopy. The pollen grains were single, but dyads were also found. The basic shape of the pollen grains (with chemical treatment) was subprolate, prolate and prolate-spheroidal and the pollen grains were large (> 50 mm). The pollen grains observed in SEM were prolate-spheroidal, subprolate, prolate and perprolate. The aperture occupied nearly the entire distal hemisphere. The surface of non-apertural areas was microreticulate, psilate–perforate, fossulate and verrucate. The surface of the apertural area was psilate-perforate-verrucate, microreticulate-verrucategemmate and psilate-perforate. The tectum was homogeneous, with perforations. Our results suggest that some species cannot be separated based on pollen grain morphology, but only may be categorized into their groups. The present study investigated pollen grain morphology in eleven species for the first time in terms of pollen micromorphology and provided some important new data.
Źródło:
Acta Biologica Cracoviensia. Series Botanica; 2017, 59, 2
0001-5296
Pojawia się w:
Acta Biologica Cracoviensia. Series Botanica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of CuO and V2O5 Effect on IR Spectra of Polycrystalline Bismuth Niobate
Autorzy:
Kuźniarska-Biernacka, I.
Lisińska-Czekaj, A.
Czekaj, D.
Powiązania:
https://bibliotekanauki.pl/articles/352587.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
BiNbO4
ceramics
SEM
FTIR spectroscopy
Opis:
Bismuth niobate (BiNbO4) ceramics were fabricated by mixed oxide method and sintered by presureless sintering method. BiNbO4 ceramics doped with V2 O5 additive in amount 0.125 wt%, 0.250 wt% and 1 wt% of was sintered at T = 910°C whereas BiNbO4 ceramics doped with 2 wt% of CuO additive was sintered at T = 890°C and T = 910°C. It was found that V2 O5 additive improved morphology of the ceramic samples. However, the chemical composition of BiNbO4 ceramics in relation to bismuth oxide and niobium oxide manifested a tendency of lack of Bi2 O3 component. Absorption bands for the BiNbO4 compound were identified. FTIR band positions associated with NbO6 octahedra suggested that the crystal structure changes after V2 O5 incorporation.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 817-821
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nano-Scale Structure Investigation of Vapour Deposited AlCrSiN Coating Using Transmission Electron Microscope Techniques
Autorzy:
Lukaszkowicz, K.
Labisz, K.
Basiaga, M.
Jonda, E.
Powiązania:
https://bibliotekanauki.pl/articles/352381.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
AlCrSiN coating
PVD
HRTEM
SEM
nanoscale
Opis:
The investigations concerned the structural analysis of the AlCrSiN coating deposited by arc Physical Vapour Deposition method on the X40CrMoV5-1 hot work tool steel substrate. The deposition process was carried out on a device equipped with a technique of lateral, rotating cathodes. The nano/microstructure, phase identification and chemical state of the coating were analysed by high-resolution transmission electron microscopy. It was found that the investigated coatings have nanostructured nature consisting of fine crystallites. The fractographic tests were made using the scanning electron microscope and allow to state, that the coating was deposited uniformly and tightly adhere to the substrate material. In the work is presented the nature of a transition zone between the produced AlCrSiN coating and substrate material.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 837-842
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Morphology and Structure of ZnO Thin Films Deposited by ALD Method
Autorzy:
Boryło, P.
Matus, K.
Lukaszkowicz, K.
Gołombek, K.
Powiązania:
https://bibliotekanauki.pl/articles/352603.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ALD
ZnO
SEM
TEM
UV/VIS
Opis:
This paper presents research results of zinc oxide thin films deposited on a glass substrate with use of ALD method. Our researches focused on analyzing of the influence of ALD deposition process temperature on the morphology and transparency of thin layers. The morphology was examined using both scanning and transmission electron microscopes. Transparency study was performed by UV-VIS spectroscopy. For our experiments, two sets of the coating have been prepared, differing in temperature and number of cycle used during the preparation process. The first set was deposited in 100 cycles, second one in 500 cycles. Each set of tested coating contained samples prepared at different temperatures.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 129-133
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure, Chemical and Phase Composition of Clad Layers of Inconel 625 and Inconel 686
Autorzy:
Solecka, M.
Kopia, A.
Petrzak, P.
Radziszewska, A.
Powiązania:
https://bibliotekanauki.pl/articles/351519.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Inconel 625
Inconel 686
SEM
EDS
TEM
Opis:
The article presents the investigation results of microstructural, chemical composition changes after clad layers of Inconel 625 and Inconel 686 alloys weld overlaid on boiler tubes. The boiler tubes made of 16Mo3 steel were cladded in the Boiler Factory SEFAKO S.A. using CMT technique. The microstructure and chemical composition of coatings were analysed using light microscopy, scanning and transmission electron microscopy. The value of the partition coefficient k was determined for Inconel 625 and Inconel 686 clad layers. The value was calculated by dividing the average content (% wt.) of Ni, Cr, Mo, Fe, Nb and W.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 513-518
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Probing EFL Teachers’ Job Motivation in the Light of Intra-individual Level Predictors
Autorzy:
Ghanizadeh, Afsaneh
Royaei, Nahid
Powiązania:
https://bibliotekanauki.pl/articles/2127872.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
EFL instructors
SEM
Burnout
Motivation
Self-efficacy
Opis:
The present study aims to scrutinize teacher motivation in relation to two individual level predictors, namely, self-efficacy and burnout among English as a foreign language (EFL) teachers. To this end, 142 English as a foreign language (EFL) teachers were selected from various English language institutes of Mashhad and Tehran, two cities in Iran. They were requested to complete three questionnaires: the Maslach Burnout Inventory, the Teachers’ Sense of Efficacy Scale, and the Work Tasks Motivation Scale for Teachers. The findings obtained via SEM revealed that the proposed model had a good fit with the empirical data. In particular, it was found that job motivation contributed significantly to burnout depletion. It was also revealed that self-efficacy positively predicted job motivation, and burnout negatively influenced self-efficacy. However, self-efficacy surpassed motivation in predicting EFL instructors’ burnout. Results were discussed from both theoretical standpoints as well as previous empirical findings. Finally, implications were presented.
Źródło:
Polish Psychological Bulletin; 2018, 49, 3; 375-382
0079-2993
Pojawia się w:
Polish Psychological Bulletin
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Degradation of Creep Resistant Ni - alloy During Aging at Elevated Temperature Part II: Structure Investigations
Autorzy:
Kaczorowski, M.
Skoczylas, P.
Krzyńska, A.
Powiązania:
https://bibliotekanauki.pl/articles/381511.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni-base superalloy
structure investigations
SEM observation
TEM observation
nadstop niklu
badanie struktury
obserwacja SEM
obserwacja TEM
Opis:
The results of structure observations of Ni base superalloy subjected to long-term influence of high pressure hydrogen atmosphere at 750K and 850K are presented. The structure investigation were carried out using conventional light-, scanning- (SEM) and transmission electron microscopy (TEM). The results presented here are supplementary to the mechanical studies given in part I of this investigations. The results of study concerning mechanical properties degradation and structure observations show that the differences in mechanical properties of alloy subjected different temperature are caused by more advanced processes of structure degradation during long-term aging at 850K, compare to that at 750K. Higher service temperature leads to formation of large precipitates of δ phase. The nucleation and growth of needle- and/or plate-like, relative large delta precipitates proceed probably at expense strengthening γ" phases. Moreover, it can't be excluded that the least stable γ" phase is replaced with more stable γ' precipitates. TEM observations have disclosed differences in dislocation structure of alloy aged at 750K and 850K. The dislocation observed in alloy subjected to 750K are were seldom observed only, while in that serviced at high stress and 850K dislocation array and dislocation cell structure was typical.
Źródło:
Archives of Foundry Engineering; 2015, 15, 4; 45-50
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characteristics of Ledeburite in EDS Analyses of Directionally Solidified Eutectic White Cast Iron
Autorzy:
Trepczyńska-Łent, Małgorzata
Seyda, J.
Powiązania:
https://bibliotekanauki.pl/articles/2203938.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
microsegregation
SEM-EDS analysis
ledeburite
cementite
white cast iron
mikrosegregacja
analiza SEM-EDS
ledeburyt
cementyt
żeliwo białe
Opis:
The paper addresses the microsegregation of Mn, Mo, Cr, W, V, Si, Al, Cu and P in the white cast iron. Eutectic alloy with the content of 4.25% C was studied. The white cast iron was directionally solidified in the vacuum Bridgman-type furnace at a constant pulling rate v=83 μm/s and v=167 μm/s and at a constant temperature gradient G = 33.5 K/mm. The microstructural research was conducted using light and scanning electron microscopy. The microsegregation of elements in ledeburite was evaluated by EDS measurements. Content of elements in ledeburitic cementite and ledeburitic pearlite was determined. The tendency of elements to microsegregation was found dependent on the solidification rate. Microsegregation of elements between pearlite and cementite structural constituents has been specified. The effect of solidification rate on the type and intensity of microsegregation in directionally solidified eutectic white cast iron was observed. A different type of microsegregation was observed in the components of ledeburite in cementite and pearlite.
Źródło:
Archives of Foundry Engineering; 2022, 22, 4; 65--71
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Obtaining and Analyzing the Al2O3-ZrO2 Ceramic Layers on Metallic Substrate
Autorzy:
Lutcanu, Marian
Coteață, Margareta
Bernevig, Mihai Adrian
Nechifor, Cristina-Delia
Cazacu, Marius Mihai
Paraschiv, Petronela
Istrate, Bogdan
Bădărău, Gheorghe
Sandu, Ioan Gabriel
Cimpoeșu, Nicanor
Powiązania:
https://bibliotekanauki.pl/articles/2106593.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ceramic layer
atmospheric plasma spraying
SEM
EDS
Opis:
In this case ceramic layers from Metco ZrO2 and Al2O3 powders mixture (25/75; 50/50 and 75/25) were obtained through atmospheric plasma spraying (APS) after five passes on low carbon steel substrate. The sample surfaces mechanically grinded (160-2400) before and after ceramic layer deposition. Powder’s mixtures and the surface of ceramic thin layers were analyzed through: scanning electron microscopy (SEM). In order to understand the effect of surface wettability of the ceramic layers, before and after grinding the surface, three different liquids were used. Experimental results confirm the modification of the steel substrate surface characteristic from hydrophilic to hydrophobic when the ceramic layer was deposited. Surface free energy of hydration increases for all the samples with zirconia percentage addition before polishing process.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 2; 479--485
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Calcium Ions on the Structure and Properties of LaMnO3
Autorzy:
Bara, M.
Dzik, J.
Feliksik, K.
Kozielski, L.
Wodecka-Duś, B.
Goryczka, T.
Zarycka, A.
Adamczyk-Habrajska, M.
Powiązania:
https://bibliotekanauki.pl/articles/353112.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
LCMO
ceramics
manganites
X-ray diffraction
SEM
Opis:
La0,7 Ca0,3 MnO3 polycrystalline were synthesized from La2 O3 , CaO and MnO2 powder mixture using a solid state reaction technique. The compound powders were obtained through the free sintering method at different temperatures and sintering times in order to study the influence of technological conditions on Ca doped La manganites. The most important physical features as structure, microstructure and morphology were described after X-ray diffraction investigation. Photographs of the specimen fractures were taken with SEM (scanning electron microscope) and they revealed high porosity of the tested material and great tendency for its grains to create agglomerates. Influence of doping and technological conditions on lattice parameters were studied by means of Rietvield analysis. The XRD measurements reveal that La0,7 Ca0,3 MnO3 has orthorhombic symmetry with Pnma space group.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 3; 1189-1195
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The influence of micro cracks appearing during concreting of road viaducts and their impact on a frost-thaw resistance
Wpływ mikrozarysowań pojawiających się podczas betonowania wiaduktów drogowych na ich cechę mrozoodporności
Autorzy:
Jasiczak, J.
Powiązania:
https://bibliotekanauki.pl/articles/1849723.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
wiadukt betonowy
mrozoodporność betonu
mikrozarysowanie
analiza SEM
analiza XRD
concrete viaduct
concrete frost resistance
microcrack
SEM analysis
EDS analysis
Opis:
In the latest period hundreds of concrete viaducts were built in Poland within a short time range. The cases of destruction of concrete road viaducts described by the author in the article concern in the construction of such structures in various parts of our country, such as central regions of Poland, Warmia-Masuria, south – east - a total of about 30 objects. The occurring phenomenon is related to the micro cracks of the cement matrix which are not visible on the surface of the elements and become visible only after the cyclic freezing process as a result of the standard F150 frost resistance test, the so-called the standard method according to Annex N to the PN-B-06265:2018 standard. The destruction took an unprecedented course and aroused much discussion in the scientific community. This article summarizes this discussion and indicates the root cause of the destruction.
W ostatnich latach w krótkim przedziale czasu wybudowano w Polsce setki betonowych wiaduktów drogowych. Ich charakterystyczną cechą było zastosowanie wysokiej klasy betonu zawierającego cement CEM I 42,5 (podpory i przyczółki) oraz CEM I 52,5 (przęsła). Budowano często w zimie, w okresie obniżonych temperatur powietrza. Pomimo pozytywnych wcześniejszych testów laboratoryjnych beton przygotowany w warunkach budowy często nie osiągał zakładanej cechy mrozoodporności po 150 cyklach zamrażania-rozmrażania w zakresie temperatur od - 18°C do + 18°C. Procesowi towarzyszyły nietypowe zjawiska. Większy niż normatywny spadek wytrzymałości betonu następował przy jednoczesnej dużej szczelności. Brak było odprysków powierzchniowych typowych dla betonu o niskiej mrozoodporności, krzywizny krawędzi itp. Natomiast na powierzchni próbki wokół dużych ziaren kruszywa pojawia się charakterystyczna siatka mikrorys wypełnionych białymi wyciekami nieznanych związków chemicznych. Związki te zostały dokładnie przebadane za pomocą analizy SEM. Wcześniej podobny przypadek wystąpił w Polsce tylko raz, w 2002 roku . Światowa literatura przedstawia wiele przypadków związanych z zarysowaniami matrycy cementowej w wyniku na przykład opóźnionego ettringitu, także w mostach, ale analizowany w artykule przypadek jest inny, spowodowany „wrodzonymi” mikrozarysowaniami powstałymi już na etapie betonowania konstrukcji i późniejszej destrukcji podczas cyklicznego zamrażania w wyniku zjawiska opisanego w literaturze jako efekt erlina/mathera.
Źródło:
Archives of Civil Engineering; 2020, 66, 4; 221-236
1230-2945
Pojawia się w:
Archives of Civil Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Contribution of electron tomography to development of innovative materials for clean energy systems and aeronautics
Wkład tomografii elektronowej do rozwoju innowacyjnych materiałów dla niskoemisyjnych systemów energetycznych i lotnictwa
Autorzy:
Kruk, A.
Czyrska-Filemonowicz, A.
Powiązania:
https://bibliotekanauki.pl/articles/352236.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TEM
STEM-HAADF
EFTEM
FIB-SEM
tomography
tomografia
Opis:
The development of innovative materials for clean energy systems and aeronautics requires use of modern research methods to characterize the structure on the level from micro- to nanoscale. Modern two-dimensional imaging techniques recently available in electron microscopes allow use of tomographic methods to characterize the structure of materials. Application of modern three dimensional imaging techniques such as electron tomography allows accurate qualitative and quantitative measurement of the structure elements in the micro- and nanoscale. The electron tomography studies have been carried out for three-dimensional visualization and metrology of different materials for clean energy systems and aeronautics. Electron tomography results provided quantitative data about shape, size and distribution of the particles, complementary to those obtained by means of quantitative TEM metallography.
Rozwój innowacyjnych materiałów dla niskoemisyjnych systemów energetycznych i lotnictwa wymaga zastosowania nowoczesnych metod badawczych w celu scharakteryzowania struktury na poziomie od mikro- do nanoskali. Nowoczesne dwuwymiarowe techniki obrazowania od niedawna dostępne w mikroskopach elektronowych, umożliwiają zastosowanie metod tomograficznych do scharakteryzowania struktury materiałów. Zastosowanie nowoczesnych technik trójwymiarowego obrazowania, takich jak tomografia elektronowa umożliwia dokładny jakościowy i ilościowy pomiar elementów mikrostruktury w mikro- i nanoskali. Badania metodami tomografii elektronowej przeprowadzone zostały w celu trójwymiarowej wizualizacji i metrologii elementów mikrostruktury róznych materiałów konstrukcyjnych dla systemów niskoemisyjnej energetyki i lotnictwa. Badania metodami tomografii elektronowej dostarczaja danych ilościowych dotyczacych kształtów, wielkości i rozkładu przestrzennego cząstek i są one uzupełnieniem do danych uzyskiwanych za pomocą metod ilościowej analizy metalograficznej przy wykorzystaniu transmisyjnej mikroskopii elektronowej.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 2; 387-392
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Functional and Fractal Properties of Fe-Al Coatings After Gas Detonation Spraying (GDS)
Autorzy:
Chrostek, T.
Rychlik, K.
Bramowicz, M.
Senderowski, C.
Powiązania:
https://bibliotekanauki.pl/articles/355023.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-Al
intermetallic alloys
GDS
SEM
fractal analysis
Opis:
The paper presents the results and provides an analyse of the geometric structure of Fe-Al protective coatings, gas-treated under specified GDS conditions. The analysis of the surface topography was conducted on the basis of the results obtained from the SEM data. Topographic images were converted to three-dimensional maps, scaling the registered amplitude coordinates of specific gray levels to the relative range of 0÷1. This allowed us to assess the degree of surface development by determining the fractal dimension. At the same time, the generated three-dimensional spectra of the autocorrelation function enabled the researchers to determine the autocorrelation length (Sal) and the degree of anisotropy (Str) of the surfaces, in accordance with ISO 25178. Furthermore, the reconstructed three-dimensional images of the topography allowed us to evaluate the functional properties of the studied surfaces based on the Abbott-Firestone curve (A-F), also known as the bearing area curve. The ordinate describing the height of the profile was replaced by the percentage of surface amplitude in this method, so in effect the shares of the height of the three-dimensional topographic map profiles of various load-bearing properties were determined. In this way, both the relative height of peaks, core and recesses as well as their percentages were subsequently established.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 1993-1999
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Composite Coatings of Chromium and Nanodiamond Particles on Steel
Autorzy:
Gidikova, N.
Sulowski, M.
Petkov, V.
Valov, R.
Cempura, G.
Powiązania:
https://bibliotekanauki.pl/articles/356289.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
composite chromium coating
nanodiamond particles
SEM-EDS analysis
Opis:
Chrome plating is used to improve the properties of metal surfaces like hardness, corrosion resistance and wear resistance in machine building. To further improve these properties, an electrodeposited chromium coating on steel, modified with nanodiamond particles is proposed. The nanodiamond particles (average size 4 nm measured by TEM) are produced by detonation synthesis (NDDS). The composite coating (Cr+NDDS) has an increased thickness, about two times greater microhardness and finer micro-structure compared to that of unmodified chromium coating obtained under the same galvanization conditions. In the microstructure of specimen obtained from chrome electrolyte with concentration of NDDS 25 g/l or more, “minisections” with chromium shell were found. They were identified by metallographic microscope and X-ray analyser on etched section of chromium plated sample. The object of further research is the dependence of the presence of NDDS in the composite coating from the nanodiamond particles concentration in the chroming electrolyte.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 4; 2421-2424
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 76

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