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Wyszukujesz frazę "Lee, S. -Y." wg kryterium: Autor


Tytuł:
Fabrication of Porous Silica Fibers by Electrospinning for Sound Absorbing Materials
Autorzy:
Cho, Y.-S.
Lee, H. J.
Powiązania:
https://bibliotekanauki.pl/articles/353561.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrospinning
porous silica fiber
thermal insulator
sound absorption
Opis:
Macroporous silica fibers having spherical cavities were fabricated by electrospinning using the spinning solution prepared from the mixed dispersion of tetraethylorthosilicate (TEOS) and polystyrene nanospheres as precursor and sacrificial templates, respectively, by injection through metallic nozzle. By applying electric field, the electro-spun fibers obtained by evaporation-driven self-assembly were collected on flat substrate or rotating drum, followed by the removal of the templates by calcination. The sound absorption coefficient of the porous fibers was measured by impedance tube, and the measured value was larger than 0.9 at high frequency region of incident waves. The surface of the resulting fibers was modified using fluorine-containing silane coupling agent to produce superhydrophobic fibrous materials to prevent the infiltration of humidity.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1497-1502
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects of PVA Polymer Type and Calcination Temperature on Synthesis of Nanocrystalline Yttria Powder by Polymer Solution Route
Autorzy:
Yang, Y.-K.
Lee, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/356024.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
yttria
PVA
nanocrystalline
synthesis
nanowire
Opis:
Nano-sized yttria (Y2O3) powders were synthesized by a polymer solution route using polyvinyl alcohol (PVA) as an organic carrier. The PVA polymer affected the dispersion of yttrium ions in precursor sol. In this study, three kinds of PVA polymer (different molecular weight) were applied for synthesis of yttria powder. The PVA type as well as calcination temperature had a strongly influence on the particle morphology. Single crystal nano wire particles were observed at the temperature of polymer burn out range and the size was dependent on the PVA type. The stable, fully crystallized yttria powder was obtained through the calcination at 800°C for 1 h. The yttria powder prepared with the high weight PVA (MW: 153,000) revealed a particle size of 30 nm with a surface area of 18.8 m2/g.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1473-1476
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spontaneous Formation of Titanium Nitride on the Surface of a Ti Rod Induced by Electro-Discharge-Heat-Treatment in an N2 Atmosphere
Autorzy:
Lee, W. H.
Yoon, Y. H.
Kim, Y. H.
Lee, Y. K.
Kim, J. Y.
Chang, S. Y.
Powiązania:
https://bibliotekanauki.pl/articles/352477.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
surface modification
diffusion
heat treatment
XPS
Opis:
A single pulse of 2.0 to 3.5 kJ of input energy from a 450 mF capacitor was applied to a commercially pure Ti rod in a N2 atmosphere. The surface of the Ti rod transformed from TiO2 into titanium nitride in times as short as 159 msec, providing a bimodal morphology of the cross-section. A much higher value of hardness that was observed at the edge of the cross-section was attributed to nitrogen-induced solid-solution hardening that occurred during the electrical discharge process. The activation energy (Ea) for the diffusion process was estimated to be approximately 86.9 kJ/mol. Results show that the electrical discharge process is a possible potential method for the nitriding of Ti; advantages include a short processing time and control of the nitrided layer without dimensional changes.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1281-1285
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation and Surface Modification of Mechanical Alloyed Ti-25.0 at.% Al Powder Mixture by Using an Electro-Discharge Technique
Autorzy:
Chang, S. Y.
Jang, H. S.
Yoon, Y. H.
Kim, Y. H.
Kim, J. Y.
Lee, Y. K.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/354212.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintering
mechanical alloying
powder consolidation
intermetallic compounds
titanium aluminides
Opis:
Electrical discharges using a capacitance of 450 μF at 0.5, 1.0, and 1.5 kJ input energies were applied in a N2 atmosphere to obtain the mechanical alloyed Ti3Al powder without applying any external pressure. A solid bulk of nanostructured Ti3Al was obtained as short as 160 μsec by the Electrical discharge. At the same time, the surface has been modified into the form of Ti and Al nitrides due to the diffusion process of nitrogen to the surface. The input energy was found to be the most important parameter to affect the formation of a solid core and surface chemistry of the compact.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1293-1297
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Morphology Change Of Si Deposit In Molten Salt Electrorefining
Zmiana morfologii osadu Si podczas elektrorafinacji w stopionych solach
Autorzy:
Ryu, H. Y.
Kwon, S. C.
Han, M. H.
An, Y. S.
Lee, J. S.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/354346.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
molten salt
silicon
morphology
electrorefining
current density
sól stopiona
krzem
morfologia
elektrorafinacja
gęstość prądu
Opis:
The effects of processing parameters on the morphology change in a Si deposit recovered by means of molten salt electrorefining are evaluated using electrochemical techniques such as cyclic voltammetry and chronopotentiometry at 800°C. It was found that concentration of K2SiF6 and current density were important parameters in determining deposit size. Higher concentrations of K2SiF6 were effective in coarsening the silicon deposit and decreasing the cell potential. Silicon nanofiber was recovered at 5 wt% of K2SiF6 whereas dense particles were prepared at 30 and 50 wt% of K2SiF6. The morphology of the Si deposit was determined by the concentration of Si in the electrolyte which is related to the formation of crystal and growth of Si. The formation mechanism of the Si deposit was interpreted by using high resolution TEM as well as electrochemical properties.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1491-1497
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation Mechanism of Ti5Si3 Compact Obtained by Electro-Discharge-Sintering Directly from Physically Blended Ti-37.5 At.% Si Powder Mixture
Autorzy:
Chang, S. Y.
Cheon, Y. W.
Yoon, Y. H.
Kim, Y. H.
Kim, J. Y.
Lee, Y. K.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/353022.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintering
mechanical alloying
powder consolidation
intermetallic compounds
titanium silicide
Opis:
Characteristics of electro-discharge-sintering of the Ti-37.5at.% Si powder mixture was investigated as a function of the input energy, capacitance, and discharge time without applying any external pressure. A solid bulk of Ti5Si3 was obtained only after in less than 129 μsec by the EDS process. During a discharge, the heat is generated to liquefy and alloy the particles, and which enhances the pinch pressure can condensate them without allowing a formation of pores. Three step processes for the self-consolidation mechanism during EDS are proposed; (a) a physical breakdown of oxide film on elemental as-received powder particles, (b) alloying and densifying the consolidation of powder particles by the pinch pressure, and (c) diffusion of impurities into the consolidated surface.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1299-1302
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Heat-Treatment On Microstructure And Magnetic Properties Of Nanocrystallized Mn-Zn Ferrite Powders
Wpływ obróbki cieplnej na mikrostrukturę i właściwości magnetyczne nanokrystalicznych proszków ferrytu Mn-Zn
Autorzy:
Lee, W. H.
Hong, C. S.
Chang, S. Y.
Powiązania:
https://bibliotekanauki.pl/articles/351552.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high energy ball milling
nanosized particles
crystallite size
magnetic properties
frezowanie kulowe
nanocząstki
wielkości krystalitów
właściwości magnetyczne
Opis:
The initial ferrite powders were subjected to high energy ball milling at 300rpm for 3h, and subsequently heat-treated at 573-1273K for 1h. Based on the observation of microstructure and measurement of magnetic properties, the heat-treatment effect was investigated. The size of initial powders was approximately 70μm. After milling, the powders with approximately 230nm in size were obtained, which were composed of the nano-sized particles of approximately 15nm in size. The milled powders became larger to approximately 550nm after heat-treatment at 973K. In addition, the size of particles increased to approximately 120nm with increasing temperature up to 973K. The coercivity of initial powders was almost unchanged after milling, whereas the saturation magnetization increased. As the heat-treatment temperature increased, the saturation magnetization gradually increased and the maximum coercivity was obtained at 773K.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1347-1350
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of Mo-Si-B Intermetallic Compound Powders Under Different Heat Treatment Conditions
Autorzy:
Park, J. H.
Lee, S.
Kim, D.
Kim, Y.
Yang, S. H.
Lee, S. H.
Powiązania:
https://bibliotekanauki.pl/articles/353369.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Mo-Si-B alloys
intermetallic compounds
reitveld refinement
T2 phase
A15 phase
Opis:
In this research, we investigated the effects of reduction atmospheres on the creation of the Mo-Si-B intermetallic compounds (IMC) during the heat treatments. For outstanding anti-oxidation and elevated mechanical strength at the ultrahigh temperature, we fabricated the uniformly dispersed IMC powders such as Mo5SiB2 (T2) and Mo3Si (A15) phases using the two steps of chemical reactions. Especially, in the second procedure, we studied the influence of the atmospheres (e.g. vacuum, argon, and hydrogen) on the synthesis of IMCs during the reduction. Furthermore, the newly produced IMCs were observed by SEM, XRD, and EDS to identify the phase of the compounds. We also calculated an amount of IMCs in the reduced powders depending on the atmosphere using the Reitveld refinement method. Consequently, it is found that hydrogen atmosphere was suitable for fabrication of IMC without other IMC phases.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1509-1512
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
CO Oxidation Properties Of Selective Dissoluted Metallic Glass Composites
Utlenianie wybranych rozcieńczonych kompozytów szkieł metalicznych
Autorzy:
Kim, S. Y.
Lee, M. H.
Kim, T. S.
Kim, B. S.
Powiązania:
https://bibliotekanauki.pl/articles/355092.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
CO oxidation
metallic glasses
porous metal
catalyst materials
utlenianie
szkło metaliczne
metale porowate
materiał katalityczny
Opis:
Porous metallic materials have been widely used in many fields including aerospace, atomic energy, electro chemistry and environmental protection. Their unique structures make them very useful as lightweight structural materials, fluid filters, porous electrodes and catalyst supports. In this study, we fabricated Ni-based porous metallic glasses having uniformly dispersed micro meter pores by the sequential processes of ball-milling and chemical dissolution method. We investigated the application of our porous metal supported for Pt catalyst. The oxidation test was performed in an atmosphere of 1% CO and 3% O2. Microstructure observation was performed by using a scanning electron microscope. Oxidation properties and BET (Brunauer, Emmett, and Teller) were analyzed to understand porous structure developments. The results indicated that CO Oxidation reaction was dependent on the specific surface area.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1227-1229
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Additives on the Densification Processes and Properties of Silica-Based CMCs
Autorzy:
Ko, S.-Y.
Yong, S.-M.
Lee, S. J.
Cheong, D.-I.
Baek, S.
Powiązania:
https://bibliotekanauki.pl/articles/355134.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ceramic matrix composite
CMC
silica
densification
mechanical properties
Opis:
The effect of additives on the densification behavior and mechanical properties of pure and additive (Zr, B and Mg)-added silica ceramics were investigated for their application to the matrix phase of a silica fiber reinforced silica (SiO2 /SiO2f ) composite. The additives affected the rate of densification and crystallization (or transformation) of the amorphous silica. Among the compositions, pure silica ceramics sintered at 900°C for 1h showed the maximum flexural strength. Based on the results, SiO2 /SiO2f was fabricated by a repeated vacuum-assisted infiltration method followed by the heat treatment at 900°C for 1h. The relative density of the composite was 78.2% with a flexural strength of 22.4 MPa. Fractography revealed that the composite was damaged by strong bonding at the fiber/matrix interface and the fracture of fiber.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1485-1488
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High Temperature Oxidation Property of SiC Coating Layer Fabricated by Aerosol Deposition Process
Autorzy:
Ham, G.-S.
Kim, S.-H.
Park, J.-Y.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352142.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
silicon carbide
aerosol deposition
coating
high temperature oxidation
Opis:
This study investigated the high temperature oxidation property of SiC coated layer fabricated by aerosol deposition process. SiC coated layer could be successfully manufactured by using pure SiC powders and aerosol deposition on the Zr based alloy in an optimal process condition. The thickness of manufactured SiC coated layer was measured about 5 μm, and coating layer represented high density structure. SiC coated layer consisted of α-SiC and β-SiC phases, the same as the initial powder. The initial powder was shown to have been crushed to the extent and was deposited in the form of extremely fine particles. To examine the high temperature oxidation properties, oxidized weight gain was obtained for one hour at 1000°C by using TGA. The SiC coated layer showed superior oxidation resistance property than that of Zr alloy (substrate). The high temperature oxidation mechanism of SiC coated layer on Zr alloy was suggested. And then, the application of aerosol deposited SiC coated layer was also discussed.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1347-1351
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Compression Properties of Fe-Cr-B Alloy Manufactured using Laser Metal Deposition
Autorzy:
Joo, Y.-A.
Yoon, T.-S.
Park, S.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352075.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-Cr-B composite
laser Metal Deposition
bulk type
microstructure
compressive properties
Opis:
Fe-Cr-B alloy is a material with precipitation of boride inside Fe matrix, and it features outstanding hardness and wear resistance properties. However, Fe-Cr-B alloy is a difficult material to process, making it difficult to use as a bulk type structure material which requires delicate shapes. This study attempted to manufacture Fe-Cr-B alloy using a 3D printing process, laser metal deposition. This study also investigated the microstructure, hardness and compression properties of the manufactured alloy. Phase analysis results is confirmed that α-Fe phase as matrix and (Cr, Fe)2B phase as reinforcement phase. In the case of (Cr, Fe)2B phase, differences were observed according to the sample location. While long, coarse, unidirectional needle-type boride phases (~11 μm thickness) were observed in the center area of the sample, relatively finer boride phases (~6 μm thickness) in random directions were observed in other areas. At room temperature compression test results confirmed that the sample had a compression strength is approximately 2.1 GPa, proving that the sample is a material with extremely high strength. Observation of the compression fracture surface identified intergranular fractures in areas with needle-type boride, and transgranular fractures in areas with random borides. Based on this results, this study also reviewed the deformation behavior of LMD Fe-Cr-B alloy in relation to its microstructures.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1459-1462
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure Evolution of Ni-Based ODS Superalloy Powders During Horizontal Rotary Ball Milling
Autorzy:
Lee, H.-E.
Kim, Y. S.
Park, J. K.
Oh, S.-T.
Powiązania:
https://bibliotekanauki.pl/articles/355552.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high energy ball milling
Ni-base ODS superalloy
particle and crystalline size
microstructure
Opis:
Microstructure evolution of Ni-based oxide dispersion-strengthened alloy powders with milling time is investigated. The elemental powders having a nominal composition of Ni-15Cr-4.5Al-4W-2.5Ti-2Mo-2Ta-0.15Zr-1.1Y2O3 in wt % were ball-milled by using horizontal rotary ball milling with the change of milling velocity. Microstructure observation revealed that large aggregates were formed in the early stages of ball milling, and further milling to 5 h decreased particle size. The average crystalline size, estimated by the peak broadening of XRD, decreased from 28 nm to 15 nm with increasing milling time from 1 h to 5 h. SEM and EPMA analysis showed that the main elements of Ni and Cr were homogeneously distributed inside the powders after ball milling of 5 h.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1253-1255
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Manufacturing and Macroscopic Properties of Y2O3 Coating Layer on Ceramic (AlN) Substrate Fabricated by Aerosol Deposition
Autorzy:
Wi, D.-Y.
Ham, G.-S.
Kim, S.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/353052.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aerosol deposition
Y2O3 coating layer
AlN matrix
nano indentation
Opis:
This study attempted to manufacture an Y2O3 ceramic coating layer on a ceramic (AlN) substrate using aerosol deposition (AD) and investigated its macroscopic properties. Pure Y2O3 powder with a polygonal shape and average size of 5.0 μm was used as initial feedstock. Using aerosol deposition with suitable process conditions, an Y2O3 coating layer was successfully fabricated on aluminum nitride (AIN). The thickness of the manufactured coating layer was approximately 10 mm. The coating layer consisted of Y2O3 phase identical to that in the initial powder, and no additional oxides were identified. In regard to the roughness of the Y2O3 coating layer, the average roughness (Ra) measured 1.32 μm, indicating that the surface roughness was relatively even compared to the initial powder size (5 μm). Mechanical properties of the Y2O3 coating layer were measured using nano indentation equipment, and the indentation modulus of the Y2O3 coating layer fabricated by aerosol deposition measured 136.5 GPa. The interface of the coating layer was observed using TEM, and the deposition mechanism of the Y2O3 coating layer manufactured by aerosol deposition was also discussed.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1463-1466
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł

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