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Wyświetlanie 1-15 z 141
Tytuł:
Graphite Nanosheet Exfoliation From Graphite Flakes Through Functionalization Using Phthalic Acid
Złuszczanie nanoarkuszy grafitu z płatków grafitu przy użyciu kwasu ftalowego
Autorzy:
Kim, J. H.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/351457.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
exfoliation
graphite nanosheet
functionalization
grafting molecule
Friedel-Crafts acylation
złuszczanie
nanoarkusz grafitu
funkcjonalizacja
kwas ftalowy
acylowanie Friedela-Craftsa
Opis:
In order to fabricate graphite nanosheets from graphite flakes, edge-functionalized graphite nanosheets were prepared by a functionalization method using phthalic acid as the molecule to be grafted. A polyphosphoric acid/P2O5 solution containing graphite and phthalic acid were heated at different temperatures for 72 h in a nitrogen atmosphere. It was confirmed by transmission electron microscopy and atomic force microscopy that the resultant phthalic acid-functionalized graphite nanosheets had a large surface area of 20.69 μm2 in average and an average thickness of 1.39 nm. It was also found by X-ray diffractometry and Fourier transform infrared spectroscopy (FT-IR) analysis that the functionalization caused the formation of C=O bonds at the edges of the graphite nanosheets. The yield from this functionalization method was found to be dependent on the reaction temperature, only when it is between 70 and 130°C, because of the dehydration of phthalic acid at higher temperatures. This was confirmed by FT-IR analysis and the observation of low thermal energies at low temperatures.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1251-1255
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Transient Liquid Phase Behavior of Sn-Coated Cu Particles and Chip Bonding using Paste Containing the Particles
Autorzy:
Hwang, J. H.
Lee, J.-H.
Powiązania:
https://bibliotekanauki.pl/articles/353042.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Sn-coated Cu
immersion plating
chip bonding
intermetallic compounds (IMC)
transient liquid phase (TLP)
sintering
Opis:
Sn-coated Cu particles were prepared as a filler material for transient liquid phase (TLP) bonding. The thickness of Sn coating was controlled by controlling the number of plating cycles. The Sn-coated Cu particles best suited for TLP bonding were fabricated by Sn plating thrice, and the particles showed a pronounced endothermic peak at 232°C. The heating of the particles for just 10 s at 250°C destroyed the initial core-shell structure and encouraged the formation of Cu-Sn intermetallic compounds. Further, die bonding was also successfully performed at 250°C under a slight bonding pressure of around 0.1 MPa using a paste containing the particles. The bonding time of 30 s facilitated the bonding of Sn-coated Cu particles to the Au surface and also increased the probability of network formation between particles.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1143-1148
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Discussions and Comments on the Paper: E. S. Dzidowski, 2013, "The Effect of Secondary Metalworking Processes on Susceptibility of Aircraft to Catastrophic Failures and Prevention Methods", Archives of Metallurgy and Materials, 58 (4), pp. 1207-1212)
Autorzy:
Wanhill, R. J. H.
Powiązania:
https://bibliotekanauki.pl/articles/352896.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aircraft
materials
cracking
prevention
workability optimization
Opis:
The paper ‘The effect of secondary metalworking processes on susceptibility of aircraft to catastrophic failures and prevention methods’ [1] emphasizes that fatigue is the main failure mode for metallic aircraft structures. This is corroborated by Figure 1 [2,3] and other sources [4-6]. (...) The discussions and comments in the following sections of the present document are directed to the foregoing statements and their validities.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 773-779
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Properties Of MgB2/Ga Composites Prepared By Mechanical Alloying
Właściwości kompozytów MgB2/Ga wytworzonych przez mechaniczne stopowanie
Autorzy:
Yoon, K.
Ahn, J.-H.
Powiązania:
https://bibliotekanauki.pl/articles/355192.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnesium diboride
superconductors
mechanical alloying
ball milling
dwuborek magnezu
nadprzewodnik
stopowanie mechaniczne
frezowanie kulowe
Opis:
In this study, we examined the effect of Ga-doping and mechanical alloying in MgB2 on microstructural and phase evolution. A comparison was made between in-situ and ex-situ processed Mg-B-Ga samples. Densification was markedly improved by ex-situ sintering of ball-milled MgB2+Ga. The Ga-doping and ball-milling prior to sintering resulted in the formation of impurity phases such as MgO, Ga5Mg2 and Ga2O3. Lattice parameter of MgB2 increased with increasing ball-milling duration as well as by Ga-doping.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1271-1274
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of Submicroscale Ag-Coated Cu Particles by Multi-Step Addition of Ag Plating Solution and Antioxidation Properties for Different Ag Shell Thicknesses
Autorzy:
Choi, E. B.
Lee, J.-H.
Powiązania:
https://bibliotekanauki.pl/articles/351202.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ag-coated Cu particle
submicrometer
Glycol-based Ag plating solution
mult-step addition
antioxidation
Opis:
For application as a low-cost conductive filler material, submicroscale Cu@Ag particles were fabricated at room temperature without any reductants by a multi-step addition method using an ethylene glycol-based Ag plating solution. Scanning electron microscopy images of the Ag-coated Cu particles demonstrated the formation of discrete Ag particles less than 100 nm in size as well as a thin Ag coating on Cu particles, during the early addition steps. However, as the thickness of the Ag coating increased, the small Ag particles agglomerated into Ag coatings with an increase in the number of Ag plating steps. Owing to the absence of additives such as surfactants, a comparison between the microstructural images and calculations indicated increased agglomeration between fabricated Ag-coated Cu particles with an increase in the number of Ag plating steps. However, thermogravimetric-differential scanning calorimetry of the agglomerated Ag-coated Cu particles after the fifth addition of the Ag plating solution demonstrated their antioxidation behavior even after 70 min in air at 150°C.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1137-1142
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects Of Process Parameters On Cu Powder Synthesis Yield And Particle Size In A Wet-Chemical Process
Wpływ parametrów procesu na wydajność syntezy proszku Cu i wielkości cząstek w procesie mokrym chemicznym
Autorzy:
Shin, Y. M.
Lee, J. H.
Powiązania:
https://bibliotekanauki.pl/articles/354168.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
wet-chemical process
micron-size Cu powder
Synthesis yield
particle size
gibbs free energy difference
proszek Cu
proces chemiczny mokry
wydajność syntezy
rozmiar cząsteczki
różnica energii swobodnej Gibbsa
Opis:
This study presents a simple wet-chemical process to prepare several micron-size Cu powders. Moreover, changes in powder synthesis yield and particle size are examined with different solvents, synthesis temperatures, and amounts of reducing agent during the synthesis. As a reducing agent and capping agent, L-ascorbic acid and polyvinyl pyrrolidone were used, respectively. The yields in distilled water or an ethylene glycol (EG)/distilled water mixture were higher than that in EG alone, and the yield increased with increasing temperature owing to a lower Δ Gred value. Increasing the L-ascorbic acid concentration also increased the yield. The Cu powder synthesized in 3 h at 90°C in distilled water with 272.8 mM of L-ascorbic acid showed the lowest average particle size of 2.52 μm, indicating mechanisms of short burst nucleation and reduced growth via the increased reduction rate of Cu ions. It is estimated that the nucleation step was nearly completed within 10 min in this system. The Cu powders synthesized in an ethylene glycol/distilled water mixture presented an average particle size of 3.76 μm and the highest yield of 87.9%.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1247-1250
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on the Microstructure and Tensile Deformation Behavior of Oxide Dispersion Strengthened Alloys Manufactured by Complex Milling Process
Autorzy:
Kim, Y.-K.
Kim, J.-H.
Gwon, J.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352535.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
oxide dispersion strengthening
microstructure
tensile deformation behavior
Opis:
This study attempted to manufacture an ODS alloy by combining multiple milling processes in mechanical alloying stage to achieve high strength and fracture elongation. The complex milling process of this study conducted planetary ball milling, cryogenic ball milling and drum ball milling in sequential order, and then the microstructure and tensile deformation behavior were investigated after additional heat treatment. The oxide particles distributed within the microstructure were fine oxide particles of 5~20 nm and coarse oxide particles of 100~200 nm, and the oxide particles were confirmed to be composed of Cr, Ti, Y and O. Results of tensile tests at room temperature measured yield strength, tensile strength and elongation as 1320 MPa, 2245 MPa and 4.2%, respectively, before heat treatment, and 1161 MPa, 2020 MPa and 5.5% after heat treatment. This results indicate that the ODS alloy of this study gained very high strengths compared to other known ODS alloys, allowing greater plastic zones.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1335-1340
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Fatigue Fracture Study on TDCB Aluminum Foam Specimen of Type Mode III Bonded with Adhesive
Autorzy:
Lee, J. H.
Cho, J. U.
Powiązania:
https://bibliotekanauki.pl/articles/356731.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum foam
fatigue fracture
fatigue analysis
load
Mode III type
specimen thickness
Opis:
This paper studies the characteristics of junction structure of closed-cell type aluminum foam, which is generally used as a shock absorber. TDCB specimens were designed for mode III type with thickness as a variable and performed a fatigue experiment on them by thickness. As the result, the load value of all specimens peaks under 0 to 25 cycles and decreases as the cycles increase. As the specimen thickens by 10 mm, the maximum load value is 1.2 times. When the thickness increases by 20 mm, the maximum value increases by 1.5 times. This study result can be utilized by investigating the mechanical characteristics of TDCB specimens for mode III type under fatigue loading conditions systematically and efficiently.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1359-1362
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study on Effects of Mold Temperature on the Injection Molded Article
Autorzy:
Han, J.-H.
Kim, Y.-C.
Powiązania:
https://bibliotekanauki.pl/articles/351919.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
injection molding
mold temperature
cooling temperature
molded article
Opis:
This is a study of the effects of temperature of injection mold on the injection molded article. By supplying water of the proper temperature in the cooling line of mold in the cooling process, the mold was the appropriate temperature, and the deformation of the injection molded article was examined according to the mold temperature. In this study, we conducted simulation analysis and experiments, and the results were analyzed. The minimum deformation of the injection molded article model obtained by supplying 50°C water in the cooling line is 0.003 mm, and the maximum deformation was 0.813 mm. Injection molded article models obtained by supplying 20°C water were found to be a minimum of 0.002 mm, with deformation of up to 0.761 mm. When comparing both conditions, the error rate of injection molded article obtained by supplying 20°C water in the mold cooling line was lower by about 0.18%.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1271-1274
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Additive Element on the Properties of Mechanically Alloyed Fe-Y2O3 Alloys
Autorzy:
Ahn, J.-H.
Kim, T. K.
Ahn, J.
Powiązania:
https://bibliotekanauki.pl/articles/356561.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
mechanical alloying
ODS alloy
nanoparticles
oxide dispersion strengthening
high-energy ball milling
Opis:
In the present work, we have examined the effect of Ti on the properties of Fe-Y2O3 alloys. The result showed that the addition of Ti was effective for improving mechanical properties. This is due to the reduction of oxides by Ti during mechanical alloying and hot-consolidation. In particular, iron oxides are effectively reduced by the addition of Ti. Compared to the pristine Fe-Y2O3 alloys, titanium-added alloys exhibited fine and uniform microstructures, resulting in at least 60% higher tensile strength.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1043-1046
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of Single Crystalline Titanium Oxide and Sodium Titanate Nanorods via Salt-Assisted Ultrasonic Spray Pyrolysis
Autorzy:
Hwangbo, Y.
Yoo, J.-H.
Lee, Y.-I.
Powiązania:
https://bibliotekanauki.pl/articles/352337.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2
nanorods
salt
Ultrasonic Spray Pyrolysis
optical properties
Opis:
The simple and continuous synthesis of single crystalline anatase titanium dioxide and sodium titanate nanorods by a saltassisted ultrasonic spray pyrolysis method is demonstrated. This method does not require expensive precursors, long reaction time, and physical templates or surfactant. In addition, its continuous nature makes it a suitable method for the large-scale preparation. Moreover, the effect of a salt concentration in a starting solution on material properties, including morphology and phase of the synthesized products was systematically investigated. The synthesized nanorods had one-dimensionality, a single crystalline and the average diameter of 12.3 nm with dual phases of titanium dioxide and sodium titanate by FE-SEM, XRD, HR-TEM as well as FFT-converted SAED pattern analysis.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1411-1414
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Compositional Dependence of Hardness of Ge-Sb-Se Glass for Molded Lens Applications
Zależność stężeniowa twardości szkła Ge-Sb-Se do zastosowań na formowane soczewki
Autorzy:
Park, J. K.
Lee, J. H.
Shin, S. Y.
Yi, J. H.
Lee, W. H.
Park, B. J.
Choi, J. H.
Kim, N. Y.
Choi, Y. G.
Powiązania:
https://bibliotekanauki.pl/articles/352228.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chalcogenide glasses
Ge-Sb-Se glass
infrared lens
molded lens
infrared camera
szkło
Ge-Sb-Se
soczewki formowane
twardość szkła
kamera termowizyjna
Opis:
Chalcogenide glass in the ternary Ge-Sb-Se system is inherently moldable, thus being considered as a strong candidate material for use in infrared-transmitting lens applications from the viewpoint of thermal and mechanical stability. In an effort to experimentally determine compositional region suitable for the molded lens applications, we evaluate its compositional dependence of hardness. Among the constituent atoms, Ge content turns out to exert a most conspicuous correlation with hardness. This phenomenological behavior is then explained in connection with the structural evolution that Ge brings about.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1205-1208
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Compressive Deformation Behavior of Thick Micro-Alloyed HSLA Steel Plates at Elevated Temperatures
Autorzy:
Lee, J.-H.
Kim, D.-O.
Lee, K.
Powiązania:
https://bibliotekanauki.pl/articles/351774.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
alloys
rolling
strain rate
compression test
HSLA steel
Opis:
The hot deformation behavior of a heavy micro-alloyed high-strength low-alloy (HSLA) steel plate was studied by performing compression tests at elevated temperatures. The hot compression tests were carried out at temperatures from 923 K to 1,223 K with strain rates of 0.002 s-1 and 1.0 s-1. A long plateau region appeared for the 0.002 s-1 strain rate, and this was found to be an effect of the balancing between softening and hardening during deformation. For the 1.0 s-1 strain rate, the flow stress gradually increased after the yield point. The temperature and the strain rate-dependent parameters, such as the strain hardening coefficient (n), strength constant (K), and activation energy (Q), obtained from the flow stress curves were applied to the power law of plastic deformation. The constitutive model for flow stress can be expressed as σ = (39.8 ln (Z) – 716.6) · ε(−0.00955ln(Z) + 0.4930) for the 1.0 s-1 strain rate and σ = (19.9ln (Z) – 592.3) · ε(−0.00212ln(Z) + 0.1540) for the 0.002 s-1 strain rate.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1191-1196
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and texture evolution during annealing of plane strain compressed Al and Al-1%Mn alloy single crystals
Ewolucja mikrostruktury i tekstury podczas wyżarzania monokryształów Al i Al-1%Mn odkształcacnych w płaskim stanie odkształcenia
Autorzy:
Miszczyk, M.
Paul, H.
Driver, J. H.
Maurice, Cl.
Powiązania:
https://bibliotekanauki.pl/articles/352673.pdf
Data publikacji:
2011
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
mikrostruktura
tekstura
płaski stan odkształcenia
rekrystalizacja
microstructure
texture
nucleation & recrystallization
plane strain compression
Opis:
The microstructure and the texture evolutions of partly recrystallized samples of pure Al and the Al-1%wt. Mn alloy have been characterized by a high resolution SEM/EBSD. The single crystals of the Goss{110}<001> and brass{110}<112> orientations, stable in the plane strain compression, were deformed in a channel-die up to 60% to develop a homogeneous structure composed of two sets of symmetrical primary microbands and then shortly annealed. It is documented that the orientations of the initial nucleus were scattered but not accidental. The disorientation axes in the orientation relationship across the recrystallization front usually coincide with one of the <112>, <221>, <102> or <111> crystallographic directions and were rather rarely close to the <110> or <001> directions. The disorientation axis of the <111>- type is only one of the few most often observed.
Przemiany tekstury w poczatkowych stadiach rekrystalizacji sa przedmiotem intensywnych badan, zwłaszcza tych które dotycza półwyrobów płaskich stosowanych w przemysle do wytwarzania opakowan droga głebokiego tłoczenia. W niniejszej pracy wykorzystano wysokorozdzielczy system SEM/EBSD do analizy tych zmian w nieswobodnie sciskanych próbkach aluminium oraz stopu Al-1%Mn. Dla przejrzystosci prowadzonej analizy, w badaniach wykorzystano próbki monokrystaliczne, o orientacjach stabilnych w płaskim stanie odkształcenia, tj. Gossf110g<001> i brassf110g<112>. Poddano je nieswobodnemu sciskaniu (powszechnie uznawanemu za modelowe przyblizenie procesu walcowania) do 40% i 60%, a nastepnie analizowano ich zachowanie w poczatkowych stadiach rekrystalizacji. W stanie po deformacji obserwowano jednorodna strukture dwu symetrycznie usytuowanych rodzin mikropasm, która w procesie rekrystalizacji sprzyjała pojawieniu sie nowych ziaren. Udokumentowano, ze orientacje poczatkowych ziaren, wyrastajacych ze struktury stanu zdeformowanego nie sa przypadkowe, i tylko scisle okreslona liczba grup orientacji moze sie pojawic w poczatkowym stadium wyzarzania. Dezorientacja obliczona poprzez migrujacy front rekrystalizacji zwiazana jest najczesciej z rotacja dookoła kierunków krystalograficznych typu <112>, <221>, <102> lub <111>, oraz rzadziej <110> lub <001>. Os dezorientacji typu <111> jest tylko jedna z kilku czesciej spotykanych.
Źródło:
Archives of Metallurgy and Materials; 2011, 56, 4; 933-938
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formation of Different Cu Nanopowders and Stability of Cu Fluids Produced by Electrical Explosion of Wire in Liquid
Autorzy:
Nguyen, M.-T.
Kim, J.-H.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/355217.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Cu nanopowder
Cu nanofluids
electrical explosion of wire
stability of nanofluids
Opis:
In this study, copper nanoparticles and nanofluids were synthesized by electrical explosion of wire (EEW) in liquid media such as water, ethanol, and acetone. The effect of the different conditions on the properties of the as-synthesized Cu powders and nanofluids were investigated. X-ray diffraction (XRD) analysis was employed to measure the phase of the as-synthesized powder. Only pure Cu phase appeared in case of acetone condition, but CuO and CuO2 phases could be observed in the others. The EEWed particle size was broadened from under 50 to 100 nm. The results showed that acetone was the best condition for achieving smaller particles, preventing the oxidation of the Cu particles and good stability of the nanofluids.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1453-1457
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 141

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