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Wyświetlanie 1-15 z 44
Tytuł:
Synthesis and Characterization of Si Oxide Coated Nano Ceria by Hydrolysis, and Hydrothermal Treatment at Low Temperature
Autorzy:
Kong, M.
Kim, H. W.
Powiązania:
https://bibliotekanauki.pl/articles/354290.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nano-particle
water glass
hydro-reaction
coating method
Opis:
The purpose of this work was to the application of Si oxide coatings. This study deals with the preparation of ceria (CeO2) nanoparticles coating with SiO2 by water glass and hydrolysis reaction. First, the low temperature hydro-reactions were carried out at 30~100°C. Second, Silicon oxide-coated Nano compounds were obtained by the catalyzing synthesis. CeO2 Nano-powders have been successfully synthesized by means of the hydrothermal method, in a low temperature range of 100~200°C. In order to investigate the structure and morphology of the Nano-powders, scanning electron microscopy (SEM) and X-ray diffraction (XRD) were employed. The XRD results revealed the amorphous nature of silica nanoparticles. To analyze the quantity and properties of the compounds coated with Si oxide, transmission electron microscopy (TEM) in conjunction with electron dispersive spectroscopy was used. Finally, it is suggested that the simple growth process is more favorable mechanism than the solution/aggregation process.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1125-1129
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of The Desorption-Recombination Temperature On The Microstructure And Magnetic Properties Of HDDR Processed Nd-Fe-B Powders
Wpływ temperatury desorpcji-rekombinacji na mikrostrukturę i właściwości magnetyczne proszków Nd-Fe-B przetwarzanych metodą HDDR
Autorzy:
Lee, J.-G.
Cha, H.-R.
Liu, S.
Yu, J.-H.
Baek, Y.-K.
Kwon, H.-W.
Powiązania:
https://bibliotekanauki.pl/articles/353723.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd-Fe-B
HDDR
permanent magnet
grain boundary
metoda HDDR
magnes trwały
granica ziarna
Opis:
The effect of the desorption-recombination temperature on the microstructure and magnetic properties of hydrogenation-disproportionation-desorption-recombination (HDDR) processed Nd-Fe-B powders was studied. The NdxB6.4Ga0.3Nb20.2Febal (x=12.5-13.5, at.%) casting alloys were pulverized after homogenizing annealing, and then subjected to HDDR treatment. During the HDDR process, desorption-recombination (DR) reaction was induced at two different temperature, 810°C and 820°C. The higher Nd content resulted in enhanced coercivity of the HDDR powder, and which was attributed to the thicker and more uniform Nd-rich phase along grain boundaries. But this uniform Nd-rich phase induced faster grain growth. The remanence of the powder DR-treated at 820°C is higher than that DR-treated at 810°C. In addition, it was also confirmed that higher DR temperature is much more effective to improve squareness.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1499-1501
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Removal of Cadmium using Alkaline-Treated Activated Carbon from Leucaena Leucocephala Biomass
Autorzy:
Ibrahim, W. M. H. W.
Sulaiman, Nurul Syuhada
Amini, Mohd Hazim Mohammad
Kadir, W. R. A.
Mohamed, Mazlan
Ramle, Sitti Fatimah Mhd
Bilgin, Ugur
Rahman, Wan
Powiązania:
https://bibliotekanauki.pl/articles/2125550.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
activated carbon
cadmium
Leucaena leucocephala
adsorption
Opis:
Water contamination that caused by heavy metals is a very common phenomenon in the industrial age. One of the popular way to treat metal contaminated water is by adsorption process using activated carbon as the adsorbent. This paper works on producing activated carbon by chemical means with impregnation ratios of NaOH:char (w/w) was predetermined at 1:1 (ACT1-1), 2:1 (ACT2-1) and 3:1 (ACT3-1) under activation temperature of 700°C. Considering the Leucaena leucocephala is a wildly, easy and fast grown species, with the availability throught the year, it was chosen to be used as the precursor. The properties of these activated carbons and its potential for cadmium removal from aqueus solution was analyzed. It was found that the highest surface area was recorded at 662.76 m²/g. Four parameters were studied which are contact time, the effect of pH, initial concentration of adsorbate and temperature. The equilibrium time was achieved in 40 min treatment at initial concentrations of 30 mg/l. The adsorbent exhibited good sorption potential for cadmium at pH 8.0 and equilibrium temperature of 30℃. Based on the results, this study had proved that activated carbon from Leucaena leucocephala biomass have the good potential to be used for removal of cadmium from wastewater.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 3; 1033--1036
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Comparison Of Mercury Distribution Between The Types Of Spent Fluorescent Lamp
Porównanie dystrybucji rtęci pomiędzy rodzajami zużytych świetlówek
Autorzy:
Rhee, S. W.
Park, H. S.
Choi, H. H.
Powiązania:
https://bibliotekanauki.pl/articles/356384.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
spent fluorescent lamp
types
phosphor powder
mercury distribution
świetlówki
luminofory
dystrybucja rtęci
Opis:
Spent fluorescent lamps(SFLs) such as linear type lamp, compact type lamp and U-type lamp are used to estimate mercury distribution in the components of lamps. Determination of mercury concentration in the components of spent fluorescent lamp is performed by the DMA method. Mercury concentration in the components of spent fluorescent lamp can be varied with the manufactures of lamp. Mercury portion in phosphor powder and glass from any types of spent fluorescent lamp is estimated to be higher than 99% by the analysis of mercury distribution. Through mercury distribution in the components for SFLs, the mercury concentration in phosphor powder is much higher than that in other components regardless of the type of lamp. Hence, it is desirable that phosphor powder of spent fluorescent lamps should be controlled separately and safely.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1297-1299
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of crystal plasticity model for simulation of polycrystalline aluminum sample behavior during plain strain compression test
Zastosowanie modelu plastyczności kryształu do symulacji zachowania umocnieniowego polikrystalicznej próbki aluminiowej w płaskim stanie odkształcenia
Autorzy:
Wajda, W.
Madej, Ł.
Paul, H.
Powiązania:
https://bibliotekanauki.pl/articles/355331.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
crystal plasticity
texture
microstructure
digital material representation
plastyczność kryształu
tekstura
mikrostruktura
cyfrowa reprezentacja materiału
Opis:
Capabilities of crystal plasticity finite element (CPFE) model in application to modeling polycrystalline aluminum sample behavior during plain strain compression test are discussed within the present work. To simplify analysis of material behavior during plain strain compression the aluminum specimen is composed of only three grains, both in experiment and numerical simulation. To reconstruct appropriate grains morphology a digital material representation (DMR) technique is used. The predicted/calculated values of loads and pole figures are compared with the experimental data. Calculated results remain in good agreement with experimental data what highlight predictive capabilities of the proposed approach in modeling material behavior under loading conditions. The conclusions regarding model capabilities and possible improvements during further work are also drawn in the paper.
W artykule przedstawiono możliwości opisu zachowania umocnieniowego, polikrystalicznej próbki aluminiowej ściskanej w płaskim stanie odkształcenia, z wykorzystaniem modelu plastyczności kryształu i Metody Elementów Skończonych. Ściskana próbka składała się z trzech ziaren, co ułatwiło analizę jej zachowania umocnieniowego oraz weryfikacje wyników numerycznych. Zastosowanie modelu plastyczności kryształów do symulacji zachowania odkształceniowego próbek polikrystalicznych wymaga odwzorowania rzeczywistej (mikro)struktury próbki, do czego wykorzystano koncepcje Cyfrowej Reprezentacji Materiału (DMR - ang. Digital Material Representation). Metoda DMR umożliwia rekonstrukcje morfologii oraz określenie początkowej orientacji ziaren w symulacji. Wyniki obliczeń w postaci figur biegunowych oraz naprężenia w funkcji odkształcenia zostały porównane z wynikami doświadczalnymi. Obliczone wyniki wykazują dobra zgodność z doświadczeniem. W artykule omówiono wyniki porównania oraz przedstawiono wnioski głównie dotyczące kierunku udoskonalenia modelu w dalszej pracy.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 2; 493-496
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The nitrogen content effect on carbonitride coagulation in 40Cr8 steel with micro-additions V and V + Al
Wpływ zawartości azotu na koagulację węglikoazotków w stali 40Cr8 z mikrododatkami V i V + Al
Autorzy:
Głowacz, E.
Adrian, H
Osuch, W.
Powiązania:
https://bibliotekanauki.pl/articles/352501.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
coagulation
carbonitrides
HSLA steels
koagulacja
węglikoazotki
stal HSLA
Opis:
The work examines the effect of nitrogen and micro-additions V and V+Al on the austenite grain size and the coagulation of carbonitride precipitates in 40Cr8 steel. The analyzed materials underwent heat treatment consisting in holding the material at 1200ºC for 1h, which was next exposed to furnace cooling down to 820ºC and maintained at this temperature for 20hrs, and subsequently quenched in water. With the application of electron microscopy, the microstructure and the formed carbonitride precipitates were examined. The SigmaScanPro software was used to perform the quantitative metallographic analysis of the precipitates. The study demonstrated that increase in the content of nitrogen inhibits the coagulation rate of carbonitrides, whereas aluminium favours the tendency for coagulation and efficiently inhibits the austenite grain growth.
W pracy badano wpływ azotu i mikrododatków V, V+Al na wielkość ziarna austenitu oraz koagulacje wydzieleń węglikoazotku w stali 40Cr8. Próbki z badanych wytopów poddano obróbce cieplnej polegającej na wygrzewaniu przy temperaturze 1200ºC przez czas 1h, następnym chłodzeniem z piecem do temperatury 820ºC i wytrzymaniu przy tej temperaturze przez czas 20h oraz chłodzeniu w wodzie. Przy wykorzystaniu mikroskopii elektronowej badano mikrostrukturę oraz powstałe wydzielenia węglikoazotku. Za pomocą programu SigmaScan Pro przeprowadzono ilościową analizę metalograficzną wydzieleń. Badania wykazały, że wzrost zawartości azotu hamuje szybkość koagulacji węglikoazotku, podczas gdy aluminium sprzyja skłonności do koagulacji i skutecznie hamuje rozrost ziarn austenitu.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 2; 607-611
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effects Of Environmental Factors On The Dispersion Behavior Of Iron Oxide In Aqueous Solutions With Poly Acrylic Acid
Wpływ parametrów charakteryzujących wodne roztwory poli(kwasu akrylowego) na dyspersję tlenku żelaza
Autorzy:
Lee, E.-H.
Kim, K.-M.
Maeng, W.-Y.
Hur, D.-H.
Powiązania:
https://bibliotekanauki.pl/articles/354513.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
polyacrylic acid
dispersion stability
magnetite
nanoparticles
suspension
poli(kwas akrylowy)
stabilność dyspersji
magnetyt
nanocząstki
zawiesina
Opis:
After preparing aqueous suspensions from magnetite particles with a poly-acrylic acid, we investigated the effects of several experimental parameters. We characterized the stability of the suspensions using visual inspection, sedimentation, adsorption, and thermal stability of the dispersant. The dispersion stability is affected by the solution pH, the concentrations of magnetite particles, the molecular weight, the concentration of the dispersants, and the temperature. The stability of the suspensions increased as the concentration of the dispersant and the temperature increased. In terms of the molecular weights of the dispersant, the suspensions with dispersant of low-molecular weight (1800) were more stable than those of high-molecular weight (250000) at room temperature. However, at high temperature the suspensions with high-molecular weight showed stability. The adsorption efficiency of the dispersant was very low. The dispersant of high-molecular weight showed a higher thermal integrity than that of low-molecular weight. From this work, we obtained the optimum conditions for stable aqueous suspensions of magnetite particles.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1561-1564
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Solvent Extraction of Co, Ni and Mn from NCM Sulfate Leaching Solution of Li(NCM)O2 Secondary Battery Scraps
Autorzy:
Hong, H. S.
Kim, D. W.
Choi, H. L.
Ryu, S.-S.
Powiązania:
https://bibliotekanauki.pl/articles/355577.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
waste recycling
NCM-system lithium ion battery
reduction
leaching
Opis:
As a part of the study on recycling Li(NCM)O2 lithium-ion battery scraps, solvent extraction experiments were performed using different extraction agents such as PC88A, Cyanex272 and D2EHPA to separate Co, Ni and Mn from the leaching solution. When the ratio of Mn to Ni was about 0.4 in the leaching solution, the separation factor for Co and Mn was found to be less than 10 so that the separation of Co and Ni was insufficient. When solvent extraction was done using the solution with the lower Mn/Ni ratio of 0.05 where Mn was removed by potassium permanganate and chlorine dioxide, more than 99% of Mn could be extracted through five courses of extraction using 30vol% D2EHPA while the extraction rates of Co and Ni were around 17% and 11%, respectively. In the case that Mn was removed from the solution, the extraction rate of Co was higher than 99% whereas less than 7% Ni was extracted using Cyanex272 suggesting that Co and Ni elements were effectively separated.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1011-1014
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sintering and Microstructures of SUS 316L Powder Produced by 3D Printing Process
Autorzy:
Kim, W. J.
Nguyen, H.-H.
Kim, H. Y.
Nguyen, M.-T.
Park, H. S.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/356018.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
3D printing
selective laser sintering
SUS 316L
flake powder
Opis:
Selective laser sintering (SLS) is a type of laminating sintering technique, using CO2 laser with (metal, polymer, and ceramic) powders. In this result, the flake SUS 316L was used to achieve a high porous product, and compare to spherical type. After SLS, the porosity of flake-type sample with 34% was quite higher than that of the spherical-type one that had only 11%. The surface roughness of the flake SLS sample were also investigated in both inner and surface parts. The results show that the deviation of the roughness of the surface part is about 64.40μm, while that of the internal one was about 117.65μm, which presents the containing of high porosity in the uneven surfaces. With the process using spherical powder, the sample was quite dense, however, some initial particles still remained as a result of less energy received at the beneath of the processing layer.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1215-1218
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The B-Li System. Calorimetric and Theoretical Studies
Układ B-Li. Badania kalorymetryczne i teoretyczne
Autorzy:
Dębski, A.
Braga, M. H.
Gąsior, W.
Powiązania:
https://bibliotekanauki.pl/articles/354959.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
phase diagrams
thermodynamic and thermochemical properties
ab initio calculations
calorimetry
diagram fazowy
właściwości termodynamiczne
właściwości termochemiczne
badania kalorymetryczne
Opis:
The standard enthalpy of formation of the B78Li22 alloy was measured with the use of the water reaction calorimetric method at 25 °C (298 K). An X-ray diffraction study of the prepared sample was conducted. The obtained diffraction pattern was different from the patterns for the B3Li and B14Li3 phases. The standard enthalpy of formation obtained for the B78Li22 alloy was -39.0 ± 0.7 kJ/mole of atoms. This value corresponds well with the formation enthalpies of the phases from the boron-lithium system. Theoretical calculations of the standard enthalpy of formation were conducted for the B78Li22 alloy and the phases from B-Li system, which were investigated earlier. A discussion of the deviations observed between both sets of data (experimental and calculated) was performed. Additionally, DTA studies were performed for 14 alloys of the concentrations from 40 to 100 at. % of Li.
Standardowa entalpia tworzenia stopu B78Li22 została zmierzona metodą kalorymetrii reakcyjnej wodnej. Próbka stopu po wyżarzaniu była poddana badaniom strukturalnym metodą dyfrakcji promieniowania rentgenowskiego. Uzyskany dyfraktogram jest inny od dyfraktogramów dla faz B3Li ora B14Li3. Zmierzona standardowa entalpia tworzenia stopu B78Li22 wyniosła -39.0 ± 0.7 kJ/mol atomów. Wartość ta dobrze koreluje z entalpią tworzenia faz z układu bor-lit. Przeprowadzone zostały również obliczenia teoretyczne standardowej entalpii tworzenia dla stopu B78Li22 oraz faz z układu B-Li, wcześniej badanych. Zaobserwowane rozbieżności między teoretycznymi i eksperymentalnymi wartościami entalpii tworzenia zostały przedyskutowane. Ponadto, wykonano pomiary DTA dla 14 stopów o stężeniach od 40 do 100 % at. Li.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 4; 2513-2520
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of Nickel Powders by Reduction of Nickel Hydroxide Using the Taylor Fluid Flow
Autorzy:
Park, I.-J.
Kim, D.-W.
Kim, G.-H.
Chae, H.-J.
Jung, H.-C.
Powiązania:
https://bibliotekanauki.pl/articles/355021.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni(OH)2
nickel
Taylor fluid flow
fine powder
Opis:
In this study, Ni(OH)2 was synthesized by the continuous reaction by the Taylor fluid flow and compared with those prepared from the conventional batch type reaction. The nickel powders were synthesized by reduction of Ni(OH)2 in an aqueous solution with hydrazine hydrate acting as the reductant. And then the characteristics of the nickel powder according to the synthesis method were compared. The average particle size of the synthesized Ni(OH)2 using Taylor reactor was generally decreased about 1.5~2.5 times more than the batch reaction. The nickel powders prepared by the batch reaction highly agglomerated with non-uniform particles. In the Taylor reaction, the agglomeration of particles was broken and uniform nickel powder was produced.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1443-1447
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Relationship Between Bake Hardening, Snoek-Köster and Dislocation-Enhanced Snoek Peaks in Coarse Grained Low Carbon Steel
Autorzy:
Lin, W.
Zhao, S.
Zhang, H.
Jin, X.
Powiązania:
https://bibliotekanauki.pl/articles/353663.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
low carbon steel
ultra-low carbon bake-hardening (ULC-BH) steel
bake hardening (BH)
Snoek peak
dislocation-enhanced Snoek peak
Snoek-Köster peak
internal friction
Opis:
In the present work, specimens prepared from coarse grained low carbon steel with different prestrains were baked and then, their bake hardening (BH) property and internal friction were determined. TEM was used to characterize the dislocation structure in BH treated samples. The measurements of internal friction in prestrained samples and baked samples were carried out using a multifunctional internal friction apparatus. The results indicate that, in coarse grained low carbon steel, the bake hardening properties (BH values) were negative, which were increased by increasing the prestrain from 2 to 5%, and then were decreased by increasing the prestrain from 5 to 10%. In the specimen with prestrain 5%, the BH value reached the maximum value and the height of Snoek-Köster peak was observed to be the maximum alike. With increasing the prestrain, both of the BH value and Snoek-Köster peak heights are similarly varied. It is concluded that Snoek-Köster and dislocation-enhanced Snoek peaks, caused by the interactions between interstitial solute carbon atoms and dislocations, can be used in further development of the bake hardening steels.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 3; 1723-1732
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation Mechanism of Ti5Si3 Compact Obtained by Electro-Discharge-Sintering Directly from Physically Blended Ti-37.5 At.% Si Powder Mixture
Autorzy:
Chang, S. Y.
Cheon, Y. W.
Yoon, Y. H.
Kim, Y. H.
Kim, J. Y.
Lee, Y. K.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/353022.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintering
mechanical alloying
powder consolidation
intermetallic compounds
titanium silicide
Opis:
Characteristics of electro-discharge-sintering of the Ti-37.5at.% Si powder mixture was investigated as a function of the input energy, capacitance, and discharge time without applying any external pressure. A solid bulk of Ti5Si3 was obtained only after in less than 129 μsec by the EDS process. During a discharge, the heat is generated to liquefy and alloy the particles, and which enhances the pinch pressure can condensate them without allowing a formation of pores. Three step processes for the self-consolidation mechanism during EDS are proposed; (a) a physical breakdown of oxide film on elemental as-received powder particles, (b) alloying and densifying the consolidation of powder particles by the pinch pressure, and (c) diffusion of impurities into the consolidated surface.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1299-1302
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxide Formation In Metal Injection Molding Of 316L Stainless Steel
Tworzenie tlenków podczas wtryskiwania proszku stali nierdzewnej 316L
Autorzy:
Jang, J. M.
Lee, W.
Ko, S.-H.
Han, C.
Choi, H.
Powiązania:
https://bibliotekanauki.pl/articles/351352.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powder injection molding
sintering
316L stainless steel
sintering atmosphere
micro parts
wtryskiwanie proszku
spiekanie
stal nierdzewna 316L
mikro-część
Opis:
The effects of sintering condition and powder size on the microstructure of MIMed parts were investigated using water-atomized 316L stainless steel powder. The 316L stainless steel feedstock was injected into micro mold with micro features of various shapes and dimensions. The green parts were debound and pre-sintered at 800°C in hydrogen atmosphere and then sintered at 1300°C and 1350°C in argon atmosphere of 5torr and 760torr, respectively. The oxide particles were formed and distributed homogeneously inside the sample except for the outermost region regardless of sintering condition and powder size. The width of layer without oxide particles are increased with decrease of sintering atmosphere pressure and powder size. The fine oxides act as the obstacle on grain growth and the high sintering temperature causes severe grain growth in micro features due to larger amount of heat gain than that in macro ones.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1281-1285
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Double Step Sintering Behavior Of 316L Nanoparticle Dispersed Micro-Sphere Powder
Dwuetapowe spiekanie mikrosferycznych nanocząstek proszku 316L
Autorzy:
Jeon, B.
Sohn, S. H.
Lee, W.
Han, C.
Kim, Y. D.
Choi, H.
Powiązania:
https://bibliotekanauki.pl/articles/355221.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
316L stainless steel
nanoparticle dispersed micro-sphere
pulse wire explosion
sintering
stal nierdzewna 316L
spiekanie dwuetapowe
mikrosferyczne nanocząstki
Opis:
316L stainless steel is a well-established engineering material and lots of components are fabricated by either ingot metallurgy or powder metallurgy. From the viewpoints of material properties and process versatility, powder metallurgy has been widely applied in industries. Generally, stainless steel powders are prepared by atomization processes and powder characteristics, compaction ability, and sinterability are quite different according to the powder preparation process. In the present study, a nanoparticle dispersed micro-sphere powder is synthesized by pulse wire explosion of 316L stainless steel wire in order to facilitate compaction ability and sintering ability. Nanoparticles which are deposited on the surface of micro-powder are advantageous for a rigid die compaction while spherical micro-powder is not to be compacted. Additionally, double step sintering behavior is observed for the powder in the dilatometry of cylindrical compact body. Earlier shrinkage peak comes from the sintering of nanoparticle and later one results from the micro-powder sintering. Microstructure as well as phase composition of the sintered body is investigated.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1155-1158
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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