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Tytuł:
Microscopic analysis of the nanostructures impact on endothelial cells
Autorzy:
Kołodziejczyk, Agnieszka Maria
Kucińska, Magdalena
Jakubowska, Aleksandra
Siatkowska, Małgorzata
Sokołowska, Paulina
Kotarba, Sylwia
Makowski, Krzysztof
Komorowski, Piotr
Walkowiak, Bogdan
Powiązania:
https://bibliotekanauki.pl/articles/970974.pdf
Data publikacji:
2020
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
nanostructures
atomic force microscopy
transmission electron microscopy
scanning electron microscopy
cell morphology
Opis:
Nowadays nanostructures are more and more often designed as carriers for drug delivery, especially to improve the drug pharmacokinetics and pharmaco-dynamics. Numerous kinds of nanostructures are considered a good prospect for medical applications thanks to their small size, acceptable biocompatibility and toxicity. Due to the fact that nanotechnology is a new field of science, every nano-scale product must be thoroughly examined regarding its toxicity to the human body. This study provides new insights into effects of exposing endothelial cells to the selected nanostructures. Dendrimers of the fourth generation (PAMAMs), multi-walled carbon nanotubes (MWCNTs) and silver nanoparticles (SNPs) were used to evaluate nanostructures influence on endothelial cells in vitro. The nanostructures were evaluated via transmission electron microscopy and dynamic light scattering technique. The cells previously exposed to the nanostructures were observed and analyzed via the atomic force microscopy and scanning electron microscopy to obtain a quantitative evaluation of the cells morphology. The presence of multi-walled carbon nanotubes and silver nanoparticles on the cells surface was confirmed by the scanning electron microscopy. Our results confirm that the surface association and/or uptake of nanostructures by the cells resulting from physicochemical and biological processes, affect the cells morphology. Morphological changes can be induced by the membrane proteins interaction with nanomaterials, which trigger a sequence of intracel-lular biological processes.
Źródło:
Engineering of Biomaterials; 2020, 23, 154; 2-8
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Powder Grain Size and Titania Content on Mechanical and Tribological Properties of Plasma Sprayed AL2O3-TiO2 Ceramic Coatings
Autorzy:
Góral, A.
Żórawski, W.
Powiązania:
https://bibliotekanauki.pl/articles/355219.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al2O3-TiO2 coating
nanostructures
mechanical properties
wear resistance
Opis:
In this work, three ceramic composite coatings Al2O3-3TiO2 C, Al2O3-13TiO2 C, and Al2O3-13TiO2 N were plasma sprayed on steel substrates. They were deposited with two conventional powders differing the volume fraction of TiO2 and nanostructured powder. The mechanical and tribological properties of the coatings were investigated and compared. The increase in TiO2 content from 3 wt.% to 13 wt.% in the conventional feedstock improved the mechanical properties and abrasion resistance of coatings. However, the size of the used powder grains had a much stronger influence on the properties of deposited coatings than the content of the titania phase. The Al2O3-13TiO2 coating obtained from nanostructured powder revealed significantly better properties than that plasma sprayed using conventional powder, i.e. 22% higher microhardness, 19% lower friction coefficient, and over twice as good abrasive wear resistance. In turn, the Al2O3-13TiO2 conventional coating showed an increase in microhardness and abrasive wear resistance, 36% and 43%, respectively, and 6% higher coefficient of friction compared to the Al2O3-3TiO2 conventional coating.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 1; 45-53
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nanostructured targets for TNSA laser ion acceleration
Autorzy:
Torrisi, L.
Calcagno, L.
Cutroneo, M.
Badziak, J.
Rosinski, M.
Zaras-Szydlowska, A.
Torrisi, A.
Powiązania:
https://bibliotekanauki.pl/articles/146740.pdf
Data publikacji:
2016
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
target normal sheat acceleration (TNSA)
laser ion acceleration
nanostructures
surface plasmon
resonance (SPR)
Opis:
Nanostructured targets, based on hydrogenated polymers with embedded nanostructures, were prepared as thin micrometric foils for high-intensity laser irradiation in TNSA regime to produce high-ion acceleration. Experiments were performed at the PALS facility, in Prague, by using 1315 nm wavelength, 300 ps pulse duration and an intensity of 1016 W/cm2 and at the IPPLM, in Warsaw, by using 800 nm wavelength, 40 fs pulse duration, and an intensity of 1019 W/cm2. Forward plasma diagnostic mainly uses SiC detectors and ion collectors in time of fl ight (TOF) confi guration. At these intensities, ions can be accelerated at energies above 1 MeV per nucleon. In presence of Au nanoparticles, and/or under particular irradiation conditions, effects of resonant absorption can induce ion acceleration enhancement up to values of the order of 4 MeV per nucleon.
Źródło:
Nukleonika; 2016, 61, 2; 103-108
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of photoanode structure and sensitization conditions on the photovoltaic response of dye-sensitized solar cells
Autorzy:
Gnida, Paweł
Słodek, Aneta
Schab-Balcerzak, Ewa
Powiązania:
https://bibliotekanauki.pl/articles/2083481.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Stowarzyszenie Elektryków Polskich
Tematy:
dye-sensitized solar cells
N719
phenothiazine derivatives
TiO2 nanostructures
co-sensitization
co-adsorbents
Opis:
This work summarises investigations focused on the photoanode impact on the photovoltaic response of dye-sensitized solar cells. This is a comparison of the results obtained by the authors’ research team with literature data. The studies concern the effect of the chemical structure of the applied dye, TiO₂ nanostructure, co-adsorbents addition, and experimental conditions of the anode preparation. The oxide substrates were examined using a scanning electron microscope to determine the thickness and structure of the material. The TiO₂ substrates with anchored dye molecules were also tested for absorption properties in the UV-Vis light range, largely translating into current density values. Photovoltaic parameters of the fabricated devices with sandwich structure were obtained from current-voltage measurements. During tests conducted with the N719 dye, it was found that devices containing an 8.4 μm thick oxide semiconductor layer had the highest efficiency (5.99%). At the same time, studies were carried out to determine the effect of the solvent and it was found that the best results were obtained using an ACN : tert-butanol mixture (5.46%). Next, phenothiazine derivatives (PTZ-1–PTZ-6) were used to prepare the devices; among the prepared solar cells, the devices containing PTZ-2 and PTZ-3 had the highest performance (6.21 and 6.22%, respectively). Two compounds designated as Th-1 and M-1 were used to prepare devices containing a dye mixture with N719.
Źródło:
Opto-Electronics Review; 2022, 30, 1; art. no. e140739
1230-3402
Pojawia się w:
Opto-Electronics Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Chemical evaluation of the quality of nanostructures synthesized on the surface of indium phosphide
Autorzy:
Kovachov, S.S.
Bogdanov, I.T.
Pimenov, D.O.
Bondarenko, V.V.
Konovalenko, A.A.
Skurska, M.M.
Konovalenko, I.S.
Suchikova, Y.O.
Powiązania:
https://bibliotekanauki.pl/articles/2175768.pdf
Data publikacji:
2021
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
semiconductors
nanostructures
chemical criterion
indium phosphide
quality indicators
półprzewodniki
nanostruktury
kryterium chemiczne
fosforek indu
wskaźniki jakości
Opis:
Purpose: The article proposes a methodology for determining the chemical quality criterion of porous layers synthesized on the surface of semiconductors, based on taking into account the chemical parameters of the surface that can affect the properties of nanostructures. Design/methodology/approach: The chemical quality criterion was evaluated in terms of stoichiometry, stability of structures over time, uniformity of distribution over the surface, and the presence of an oxide phase. As an example, a calculation is demonstrated for the por-InP/InP structure synthesized on a mono-InP surface. The results of calculating the chemical quality criterion were evaluated using the Harrington scale to rank samples by quality level. Findings: A chemical criterion for the quality of porous layers synthesized on the surface of semiconductors has been developed. This criterion contains a set of indicators sufficient for a comprehensive assessment of the surface condition and is universal in nature. The studies carried out make it possible to reasonably approach the determination of the modes of electrochemical processing of semiconductors and open up new perspectives in the construction of a model of self-organization of a porous structure. Research limitations/implications: The chemical quality criterion does not allow evaluating the obtained nanostructures in terms of geometric parameters. Therefore, in the future, there is a need to develop a morphological quality criterion and determine a methodology for assessing a generalized quality criterion for nanostructures synthesized on the surface of semiconductors, which may include economic, environmental, technological indicators, and the like. Practical implications: Study results are expedient from a practical point of view, since they make it possible to reasonably approach the determination of the modes of electrochemical processing of semiconductors, synthesize nanostructures with predetermined properties, and create standard samples of nanomaterial composition. Originality/value: Methodology for assessing the quality of porous semiconductors by a chemical criterion has been applied for the first time in engineering science. The article will be useful to engineers, who are engaged in the synthesis of nanostructures, researchers and scientists, as well as specialists in nanometrology.
Źródło:
Archives of Materials Science and Engineering; 2021, 110, 1; 18--26
1897-2764
Pojawia się w:
Archives of Materials Science and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synteza nanocząstek złota na powierzchni koloidów krzemionkowych
Synthesis of gold nanoparticles on the surface of colloidal silica
Autorzy:
Choma, J.
Dziura, A.
Jamioła, D.
Nyga, P.
Jaroniec, M.
Powiązania:
https://bibliotekanauki.pl/articles/236878.pdf
Data publikacji:
2010
Wydawca:
Polskie Zrzeszenie Inżynierów i Techników Sanitarnych
Tematy:
nanomateriały
nanocząstki
krzemionka koloidalna
nanostruktury krzemionkowo-złote
synteza
nanomaterials
colloidal silica
silica-gold nanostructures
synthesis
Opis:
Nanomateriały, w tym nanostruktury krzemionkowo-złote, składające się z krzemionkowego rdzenia pokrytego nanocząstkami złota cieszą się w ostatnich latach dużym zainteresowaniem, z uwagi na ich wyjątkowe właściwości, które można wykorzystać w spektroskopii, katalizie, adsorpcji, analityce i inżynierii środowiska. W pracy omówiono najnowsze doniesienia związane z wykorzystaniem tych nanomateriałów w inżynierii środowiska, głównie w procesach oczyszczania wody. Przedstawiono wyniki syntezy nanostruktur krzemionkowo-złotych, która polegała na powierzchniowej modyfikacji koloidalnych cząstek krzemionki (600 nm) grupami aminopropylowymi, na których osadza się metaliczne złoto w wyniku reakcji redukcji kwasu tetrachlorozłotowego formaldehydem. Różnicując ilość zredukowanego kwasu tetrachlorozłotowego, uzyskano różne pokrycie cząstek krzemionki złotem, od małych ilości aż do kompletnego pokrycia powierzchni krzemionki. Zasadniczą techniką badawczą, którą posłużono się do wizualizacji stopnia pokrycia cząstek krzemionki złotem była skaningowa mikroskopia elektronowa (SEM). Stwierdzono, że otrzymane przy jej pomocy zdjęcia dobrze ilustrują właściwości i morfologię otrzymanych nanostruktur krzemionkowo-złotych.
The past few years have witnessed a growing interest in nanomaterials, and these include silica-gold nanostructures, consisting of siliceous cores covered with gold nanoparticles. Such interest is attributable to the unique properties of these nanostructures when used in spectroscopy, catalysis, adsorption, analysis and environmental pollution control. This work gives an account of recent reports on the application of the nanostructures in environment engineering, especially in water treatment. The main objective was to present an effective strategy for the synthesis of silica-gold nanostructures. The synthesis involves the surface modification of colloidal silica (600 nm) with aminopropyl groups, where deposition occurs of the gold being formed during the reduction of tetrachloroauric acid with formaldehyde. The degree of coverage of the colloidal silica surface with gold (which ranged from small-sized to complete) depended on the quantity of the tetrachloroauric acid used. The morphology of silica particles and the degree of surface coverage with gold nanoparticles were vizualized by scanning electron microscopy.
Źródło:
Ochrona Środowiska; 2010, 32, 3; 3-6
1230-6169
Pojawia się w:
Ochrona Środowiska
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Optoelectronic properties of Fluoride tin oxides/porous silicon/p-Silicon heterojunction
Autorzy:
Hadi, H. A.
Powiązania:
https://bibliotekanauki.pl/articles/411926.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
porous silicon
electrochemical etching
spray pyrolysis
fluoride-doped tin oxide film
nanostructures
SEM
AFM
photodetector
Opis:
In this paper, formation of a nanostructure semi transparence fluoride tin oxides (FTO) by spray pyrolysis technique on porous silicon PS layer. Porous silicon PS layer was prepared by anodization of p-type silicon wafers to fabricate of the UV- Visible Fluoride-doped tin oxide /Porous silicon /p-Si heterojunction photodetector. Optical properties of FTO thin films were measured. The optical band gap of 3.77 eV for SnO2 : F for film was deduced. From (I-V) and (C-V) measurements, the barrier ØB height for FTO/PS diode was of 0.77, and the built in voltage Vbi, which was of 0.95 V. External quantum efficiency was 55 % at 500 nm which corresponding to peak responsivity of 1.15 A/W at 1 V bias. The PS band gap in the vicinity of PS/c-Si heterojunction was 1.38 eV.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 17, 2; 142-152
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Redukcja fluorowanego grafitu (CF)n w fali spalania i charakterystyka produktów reakcji
Self-sustaining reductive defluorination of (CF)N and characterization of reaction products
Autorzy:
Cudziło, S.
Huczko, A.
Szala, M.
Bystrzejewski, M.
Powiązania:
https://bibliotekanauki.pl/articles/208415.pdf
Data publikacji:
2006
Wydawca:
Wojskowa Akademia Techniczna im. Jarosława Dąbrowskiego
Tematy:
synteza spaleniowa
rozwarstwiony grafit
nanostrukturalne węgliki i krzemki
combustion synthesis
exfoliated graphite
carbides
silicides
nanostructures
Opis:
Badano proces spalania mieszanin fluorowanego grafitu (CF)n z różnymi reduktorami: NaN₃, B, Ti, ZrTi, Si, CaSi₂, AlSi, TiSi, MoSi₂ i CrSi₂. Okazało się, że reakcje pomiędzy tymi substratami są dostatecznie szybkie i egzotermiczne, aby proces redukcyjnego defluorowania przebiegał w reżimie samopodtrzymującej się, wysokotemperaturowej syntezy. Wykonano pomiary ciepła reakcji oraz zbadano skład fazowy i mikrostrukturę skondensowanych produktów spalania. Obserwacje mikroskopowe ujawniły obecność rozwarstwionego grafitu we wszystkich próbkach. Nanometryczne struktury w formie włókien, prętów i krystalitów 3D także wykryto w większości produktów reakcji.
Mixtures of fluorinated graphite (CF)n with different reductants, such as NaN₃, B, Ti, ZrTi, Si, CaSi₂, AlSi, TiSi, MoSi₂, and CrSi₂ were investigated. Reactions between these substrates are fast and exothermic enough to proceed in a high temperature self-sustaining regime. Heat effects accompanying the reactions were measured and the solid reaction products were analyzed. SEM observation revealed the presence of exfoliated graphite in each case. Nanostructures, like nanofibers, nanorods, nanospheres and nano-sized crystals, were also present in most of the products. Phase (XRD) and elemental composition as well as porous structure (N₂ adsorption) of chosen reaction products were also determined.
Źródło:
Biuletyn Wojskowej Akademii Technicznej; 2006, 55, 4; 257-265
1234-5865
Pojawia się w:
Biuletyn Wojskowej Akademii Technicznej
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Carbon nanostructure growth: new application of magnetron discharge
Autorzy:
Breus, A.
Abashin, S.
Serdiuk, O.
Powiązania:
https://bibliotekanauki.pl/articles/2055755.pdf
Data publikacji:
2021
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
nanotechnology
plasma synthesis
carbon nanostructures
magnetron discharge
arc spots
nanotechnologia
synteza plazmowa
nanostruktury węglowe
rozpylanie magnetronowe
wyładowania
Opis:
Purpose: The application of a common magnetron discharge to the growth of carbon nanostructures is studied. The simplicity of the proposed technique can be beneficial for the development of new plasma reactors for large-scale production of carbon nanostructures. Design/methodology/approach: Graphite cathode was treated by carbon-containing powder accelerated by use of nozzle, and then aged in hydrogen. Superposition of glow and arc discharges was obtained, when putting the cathode under the negative biasing with respect to the walls of a vacuum chamber. The pulsed discharge was preserved through the whole time of treatment. This process was explained in terms of interaction of glow discharge plasma with a surface of the cathode made of non-melting material. Findings: The plasma treatment resulted in generation of the diverse nanostructures confirmed by SEM and TEM images. Spruce-like nanostructures and nanofibers are observed near the cathode edge where the plasma was less dense; a grass-like structure was grown in the area of “race-track”; net-like nanostructures are found among the nanofibers. These findings allow concluding about the possible implementation of the proposed method in industry. Research limitations/implications: The main limitation is conditioned by an explosive nature of nanostructure generation in arcs; thus, more elaborate design of the setup should be developed in order to collect the nanospecies in the following study. Practical implications: High-productivity plasma process of nanosynthesis was confirmed in this research. It can be used for possible manufacturing of field emitters, gas sensors, and supercapacitors. Originality/value: Synthesis of carbon nanostructures is conducted by use of a simple and well-known technique of magnetron sputtering deposition where a preliminary surface treatment is added to expand the production yield and diversity of the obtained nanostructures.
Źródło:
Journal of Achievements in Materials and Manufacturing Engineering; 2021, 109, 1; 17--25
1734-8412
Pojawia się w:
Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Study On The Metal Carbide Composite Diffusion Bonding For Mechanical Seal
Badanie łączenia dyfuzyjnego kompozytu metal węglik na mechaniczne uszczelnienie
Autorzy:
Kim, D.-K.
Shon, I.-J.
Song, J.
Ryu, W.-J.
Shin, H.-Ch.
Kwon, E.-Y.
Shin, H.
Kang, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/356399.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
diffusion bonding
nanostructures
mechanical seal
hard metal
mechanical properties
łączenie
nanostruktura
uszczelnienie mechaniczne
twardy metal
właściwości mechaniczne
Opis:
Mechanical Seal use highly efficient alternative water having a great quantity of an aqueous solution and has an advantage no corrosion brine. Metal Carbide composites have been investigated as potential materials for high temperature structural applications and for application in the processing industry. The existing Mechanical seal material is a highly expensive carbide alloy, and it is difficult to take a price advantage. Therefore the study of replacing body area with inexpensive steel material excluding O-ring and contact area which demands high characteristics is needed. The development of WC-Ni base carbide alloy optimal bonding composition technique was accomplished in this study. To check out the influence of bonding temperature and time, bonding characteristics of sintering temperature was experimented. The bonding statuses of this test specimen were excellent. The hardness of specimen and bonding rate were measured using ultrasound equipment. In this work, Powder of WC (involved VC, Cr), Co and Mo2C mixed by attrition milling for 24hours. Nanostructured WC-27.6wt.%Ni-1.5wt.%Si-0.11wt.%VC-1.1wt.%B4C composite were fabricated at 1190°C by high temperature vacuum furnace. To check out the influence of bonding temperature and time, bonding characteristics of sintering temperature was experimented. Its relative density was about 99.7%. The mechanical properties (hardness and fracture toughness) were 87.2 HRA and 4.2 M·Pam1/2, respectively. The bonding status of this test specimen was excellent and the thickness of bonding layer was 20 ~30§ at 1050 and 1060°C bonding temperature.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1479-1483
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Otrzymywanie nanostruktur krzemionkowo-złotych metodą redukcji kwasu tetrachlorozłotowego na modyfikowanych cząstkach krzemionkowych
Preparation of silica-gold core-shell nanostructures by reduction of tetrachloroauric acid on modified silica particles
Autorzy:
Choma, J.
Jaroniec, M.
Dziura, A.
Nyga, P.
Jamioła, D.
Powiązania:
https://bibliotekanauki.pl/articles/210907.pdf
Data publikacji:
2012
Wydawca:
Wojskowa Akademia Techniczna im. Jarosława Dąbrowskiego
Tematy:
nanostruktury krzemionkowo-złote
kwas tetrachlorozłotowy
analiza SEM
powtarzalność syntezy
core-shell nanostructures
tetrachloroauric acid
SEM analysis
synthesis reproducibility
Opis:
Nanostruktury typu "core-sell", w szczególności nanostruktury krzemionkowo-złote, składające się z krzemionkowego rdzenia pokrytego nanocząstkami złota cieszą się w ostatnich latach dużym zainteresowaniem z uwagi na ich wyjątkowe właściwości oraz potencjalne zastosowania w adsorpcji, katalizie, spektroskopii, ochronie środowiska, biotechnologii, nanotechnologii i innych dziedzinach. W tej pracy przedstawiono powtarzalność syntezy nanostruktur krzemionkowo-złotych. Wspomniane nanostruktury otrzymano poprzez depozycję nanocząstek złota powstałych w wyniku redukcji kwasu tetrachlorozłotowego za pomocą formaldehydu na modyfikowanych cząstkach krzemionki (600 nm) grupami aminopropylowymi. Tak otrzymane cząstki złota miały wymiary ok. 50 nm. Syntezę nanostruktur krzemionkowo-złotych powtarzano czterokrotnie w ciągu dłuższego czasu, aby sprawdzić powtarzalność tej procedury. Morfologię tak otrzymanych nanostruktur charakteryzowano za pomocą skaningowej elektronowej mikroskopii (SEM). Analiza SEM wykazała, że prawie całkowita powierzchnia modyfikowanych cząstek krzemionki została pokryta jednorodnie nanocząstkami złota i że powtarzalność tego procesu jest zadowalająca.
Core-shell nanostructures, including silica-gold core-shell particles, attracted a lot of attention due to their unique properties and potential applications in adsorption, catalysis, spectroscopy, environmental protection, biotechnology, nanotechnology and other areas. In this work, the reproducibility of the synthesis of core-shell silica-gold nanostructures is presented. These nanostructures were prepared by depositing gold nanoparticles via reduction of tetrachloroauric acid with formaldehyde on 600 nm silica particles modified with aminopropyl groups. The resulting gold particles have diameters of about 50 nm. Four preparations of silica-gold core-shell particles were performed at different times to check the reproducibility of this synthesis route. The morphology of the resulting nanostructures has been studied by scanning electron microscopy (SEM). The SEM analysis showed that the almost entire surface of modified silica particles have been covered uniformly with gold nanoparticles and the reproducibility of this process is satisfactory.
Źródło:
Biuletyn Wojskowej Akademii Technicznej; 2012, 61, 1; 183-198
1234-5865
Pojawia się w:
Biuletyn Wojskowej Akademii Technicznej
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cold plasma in the nanotechnology of catalysts
Autorzy:
Tyczkowski, J.
Kapica, R.
Powiązania:
https://bibliotekanauki.pl/articles/778491.pdf
Data publikacji:
2007
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
kataliza
nanostruktura
plazma zimna
CVD
tlenek kobaltu
cienka warstwa
catalysis
nanostructures
cold plasma
metal-organic chemical vapor deposition
cobalt oxides
thin films
Opis:
In the paper the preparation of catalysts with the use of cold plasmas is discussed. A special attention is focused on nanocatalysts. In general, there are three main trends in this field: (1) plasma enhanced preparation of ..classical" catalysts, (2) plasma sputtering of catalytically active compounds, especially metal and metal oxide nanoparticles, and (3) plasma-enhanced metal-organic chemical vapor deposition (PEMOCVD) of very thin metal and metal oxide films with specific nanostructure. It is shown that the cold plasma techniques are very effective methods for designing the nanocatalysts with distinct and tunable chemical activity, specificity and selectivity. Finally, our preliminary investigations concerning CoOx catalytic films fabricated by the PEMOCVD method are presented.
Źródło:
Polish Journal of Chemical Technology; 2007, 9, 1; 36-42
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Justification of the most rational method for the nanostructures synthesis on the semiconductors surface
Autorzy:
Suchikova, Y.
Vambol, S.
Vambol, V.
Mozaffari, N.
Powiązania:
https://bibliotekanauki.pl/articles/368501.pdf
Data publikacji:
2019
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
hierarchies’ analysis method
chemical etching
electrochemical etching
lithographic etching
nanostructures synthesis
metoda hierarchii analitycznej
trawienie chemiczne
wytrawianie elektrochemiczne
litografia
synteza nanostruktur
Opis:
Purpose: of this paper is to justification the most rational method for the nanostructures synthesis on the semiconductors surface, which is capable of providing high quality synthesized nanostructures at low cost and ease of the process. Design/methodology/approach: The choice of the optimal method of synthesis was carried out using the hierarchy analysis method, which is implemented by decomposing the problem into more simple parts and further processing judgments at each hierarchical level using pair comparisons. Findings: The article describes the main methods of synthesis of nanostructures, presents their advantages and disadvantages. The methods were evaluated by such criteria as: environmental friendliness, efficiency, stages number of the technological process, complexity, resources expenditure and time and effectiveness. Using the hierarchy analysis method, has been established that electrochemical etching is the most important alternative, and when choosing a nanostructures synthesis method on the semiconductors surface, this method should be preferred. Such studies are necessary for industrial serial production of nanostructures and allow reducing expenses at the realization of the problem of synthesis of qualitative samples. Research limitations/implications: In this research, the hierarchy analysis method was used only to select a rational method for synthesizing nanostructures on the semiconductors surface. However, this research needs to be developed with respect to establishing a correlation between the synthesis conditions and the nanostructures acquired properties. Practical implications: First, was been established that the optimal method for the nanostructures synthesis on the semiconductors surface is electrochemical etching, and not lithographic or chemical method. This allowed the theoretical and empirical point of view to justify the choice of the nanostructures synthesis method in the industrial production conditions. Secondly, the presented method can be applied to the synthesis method choice of other nanostructures types, which is necessary in conditions of resources exhaustion and high raw materials cost. Originality/value: In the article, for the first time, the choice of the nanostructures synthesis method on the semiconductors surface is presented using of paired comparisons of criteria and available alternatives. The article will be useful to engineers involved in the nanostructures synthesis, researchers and scientists, as well as students studying in the field of "nanotechnology".
Źródło:
Journal of Achievements in Materials and Manufacturing Engineering; 2019, 92, 1-2; 19-28
1734-8412
Pojawia się w:
Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mikrofalowe solwotermalne syntezy nanocząstek
MicrowaveSolvothermal Synthesis nanoparticles
Autorzy:
Łojkowski, W.
Ejsmont, K.
Powiązania:
https://bibliotekanauki.pl/articles/399000.pdf
Data publikacji:
2011
Wydawca:
Politechnika Białostocka. Oficyna Wydawnicza Politechniki Białostockiej
Tematy:
mikrofalowe solwotermalne syntezy
nanocząsteczki
Laboratorium Nanostruktur dla Fotoniki i Nanomedycyny
Microwave Solvothermal Synthesis (MSS)
nanoparticles
Laboratory of Nanostructures for Photonic and Nanomedicine
Opis:
The article presents the method of Microwave Solvothermal Synthesis of nanoparticles (MSS). It facilitates the generation of particles of second generation which are covered with carefully chosen molecules. It gives the possibility to use their specialized properties in various scientific areas and what is more, it takes part in the development of technologies in industry. A Laboratory of Nanostructures for Photonic and Nanomedicine, which is located in the Institute of High Pressure Physics, has also been presented. The Laboratory, has been working on the development and improvement of MSS technology since 2002. Moreover, the article presents the reactors which are owned by the Institute and which enable this synthesis as well as the example of MSS technology which allows to obtain quantum dots of zinc oxide. Furthermore, main features and advantages of this method, which confirm the belief that it is worth continuing research on its development, have been mentioned. At the end of this article two research projects which relate to the use of the MSS technology on a large scale and which serve a crucial role in amelioration of human life, have been shown.
Źródło:
Ekonomia i Zarządzanie; 2011, 3, 3; 105-115
2080-9646
Pojawia się w:
Ekonomia i Zarządzanie
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Functional model for the synthesis of nanostructures of the given quality level
Autorzy:
Suchikova, Y.O.
Kovachov, S.S.
Shishkin, G.O.
Pimenov, D.O.
Lazarenko, A.S.
Bondarenko, V.V.
Bogdanov, I.T.
Powiązania:
https://bibliotekanauki.pl/articles/2175807.pdf
Data publikacji:
2021
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
functional model
electrochemical etching
quality level
semiconductors
nanostructures
IDEF0 methodology
model funkcjonalny
trawienie elektrochemiczne
poziom jakości
półprzewodniki
nanostruktury
metodologia IDEF0
Opis:
Purpose: The aim of this paper is to develop a functional model for the synthesis of nanostructures of the given quality level, which will allow to effectively control the process of nanopatterning on the surface of semiconductors with tunable properties. Design/methodology/approach: The paper uses the IDEF0 methodology, which focuses on the functional design of the system under study and describes all the necessary processes with an accuracy sufficient for an unambiguous modelling of the system's activity. Based on this methodology, we have developed a functional model for the synthesis of nanostructures of the given quality level and tested its effectiveness through practice. Findings: The paper introduces a functional model for the synthesis of nanostructures on the surface of the given quality level semiconductors and identifies the main factors affecting the quality of nanostructures as well as the mechanisms for controlling the formation of porous layers with tunable properties. Using the example of etching single-crystal indium phosphide electrochemically in a hydrochloric acid solution, we demonstrate that the application of the suggested model provides a means of forming nanostructures with tunable properties, assessing the quality level of the nanostructures obtained and bringing the parameters in line with the reference indicators at a qualitatively new level. Research limitations/implications: Functional modelling using the IDEF0 methodology is widely used when process control is required. In this study it has been applied to control the synthesis of nanostructures of the given quality level on the surface of semiconductors. However, these studies require continuation, namely, the establishment of correlations between the technological and resource factors of synthesis and the acquired properties of nanostructures. Practical implications: This study has a significant practical effect. Firstly, it shows that functional modelling can reduce the time required to form large batches of the given quality level nanostructures. This has made it possible to substantiate the choice of the initial semiconductor parameters and nanostructure synthesis modes in industrial production from the theoretical and empirical perspective. Secondly, the presented methodology can be applied to control the synthesis of other nanostructures with desired properties and to reduce the expenses required when resources are depleted and the cost of raw materials is high. Originality/value: This paper is the first to apply the IDEF0 methodology to control the given quality nanostructure synthesis. This paper will be of value to engineers who are engaged in the synthesis of nanostructures, to researchers and scientists as well as to students studying nanotechnology.
Źródło:
Archives of Materials Science and Engineering; 2021, 107, 2; 72--84
1897-2764
Pojawia się w:
Archives of Materials Science and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 16-30 z 32

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