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Wyświetlanie 1-15 z 81
Tytuł:
Synthesis and in vitro antimicrobial evaluation of some new chalcones containing vinyl ester group and substituted alkyl chain
Autorzy:
Sharma, Vinay S.
Patel, R. B.
Powiązania:
https://bibliotekanauki.pl/articles/1191249.pdf
Data publikacji:
2016
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Antibacterial
Antifungal
Chalcone
Vinyl ester
Opis:
A novel series of chalconyl vinyl ester based derivatives were designed and synthesized. The newly synthesized compounds were studied for efficacy against several bacteria (E.Coli, P.Aeruginosa, S.Aureus, S.Pyogenus) and fungi (C.Albicans, A.Niger, Clavatus) using the broth dilution technique. Chalcones were prepared by treatment of 4-iodo acetophenone with 4-hydroxy benzaldehyde by Claisen-Schimidt condensation reaction. Various chalconyl vinyl ester derivatives (C1-C8) were prepared by reaction of chalcone with 4-n-alkoxy cinnamic acids derivatives. Compound C8 shows the best bioactive desired antibacterial analogue with less MIC value against different tested strains. All the final synthesized compounds were characterized by IR, 1H NMR, and elemental analysis.
Źródło:
World Scientific News; 2016, 54; 240-251
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Plasticization of PVC via click reaction of a monooctyl phthalate derivative
Autorzy:
Jia, P.
Wang, R.
Hu, L.
Zhang, M.
Zhou, Y.
Powiązania:
https://bibliotekanauki.pl/articles/779324.pdf
Data publikacji:
2017
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
poly(vinyl chloride)
plasticization
migration
TGA
Opis:
Modified PVC (M-PVC) material with suppressed migration and low glass transition temperature was prepared via click reaction of a monooctyl phthalate derivative. Chemical structure and composition of M-PVC were characterized by FT-IR, 1H NMR and element analysis. Thermal stability, glass transition temperature and migration stability of M-PVC were studied with TGA, DSC and migration tests, respectively. The study showed that M-PVC exhibited poor thermal stability, and low glass transition temperature of 66.0°C. No migration was found in distilled water, 10% (v/v) ethanol, 30% (w/v)acetic acid and petroleum ether. The PVC material is expected to preparing PVC products in the areas with high migration resistance requirement.
Źródło:
Polish Journal of Chemical Technology; 2017, 19, 3; 16-19
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Selected physical properties of extruded composites type of porous PVC-metal
Autorzy:
Tor-Świątek, A.
Powiązania:
https://bibliotekanauki.pl/articles/102054.pdf
Data publikacji:
2014
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
poly(vinyl chloride)
extrusion
fillers
metallic powders
Opis:
The article presents studies of selected physical and mechanical properties of hybrid materials type of polymer-metal. In the frame of this work modification of PVC with the iron and copper powder in amount of 0, 1.5 and 3% and blowing agent in amount of 0, 0.5, 1% was done. Extrudates in a form of pipe were tested to determine density, porosity, maximum tensile stress, stress at break, modulus of elasticity and elongation with break. The samples were also observed in a microscope. The studies have shown significant influence of the added components on the properties tested.
Źródło:
Advances in Science and Technology. Research Journal; 2014, 8, 23; 14-18
2299-8624
Pojawia się w:
Advances in Science and Technology. Research Journal
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of a novel environmental friendly plasticizer based on tung oil fatty acid for poly (vinyl chloride) blends
Autorzy:
Tong, H.
Hai, J.
Powiązania:
https://bibliotekanauki.pl/articles/778643.pdf
Data publikacji:
2018
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
Synthesis
plasticizer
migration resistance
poly (vinyl chloride)
Opis:
A novel environmental friendly plasticizer (TPE) derived from tung oil fatty acid with long fatty acid chain and high degree of branching was synthesized. Chemical structure of the obtained TPE was characterized with Fourier transform infrared spectroscopy (FT-IR) and  1H NMR. TPE was used to prepare plasticized PVC blends as main plasticizer. Thermal stability, mechanical properties and migration resistance of poly (vinyl chloride) plasticized with TPE were investigated. The results showed that torque data of plasticized PVC blends reached 12.4 N·m when the mass of the TPE was 50 wt.%. TPE improved the thermal stability of PVC blends obviously than dioctyl phthalate (DOP). The leaching tests showed that PVC plasticized with TPE were with higher migration resistance than that of DOP. The excellent thermal stability and high migration resistance of PVC blends showed high application value for TPE.
Źródło:
Polish Journal of Chemical Technology; 2018, 20, 2; 92-97
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The plasticizing effect of properties of manganous chloride and glycerin on poly(vinyl alcohol)
Autorzy:
Jia, P.
Zhang, M.
Bo, C.
Hu, L.
Zhou, Y.
Powiązania:
https://bibliotekanauki.pl/articles/778667.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
poly(vinyl alcohol)
glycerin
manganous chloride
blend
film
Opis:
Poly(vinyl alcohol) films were prepared with manganous chloride (MnCl2 · 4H2O) and glycerin as complex plasticizer. The micro morphology of pure PVA film and complex plasticizer plasticized PVA films was observed by scanning electron microscope (SEM). The interaction between complex plasticizer and PVA molecules was investigated by Fourier transform infrared spectroscopy (FT-IR). The influence of complex plasticizer on crystalline, thermal and mechanical properties of PVA films was studied by X-ray diffraction (XRD), differential scanning calorimetry (DSC), thermogravimetric analysis (TG), and tensile testing, respectively. The results showed that the complex plasticizer of MnCl2 · 4H2O/glycerin could interacted with PVA molecular and then effectively destroy the crystals of PVA. PVA films plasticized with complex plasticizer of MnCl2 · 4H2O/glycerin became soft and ductile, with lower tensile strength and higher elongation at break compared with PVA films. This is an important cause of plasticization of the complex plasticizer of MnCl2 · 4H2O/glycerin on PVA films.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 2; 29-33
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A role of free silanol groups of nanosilica surface in interaction with poly(vinyl pyrrolidone)
Autorzy:
Voronina, Olga
Malysheva, Maria
Nosach, Liudmyla
Voronin, Eugeny
Gun’ko, Vladimir
Charmas, Barbara
Skubiszewska-Zięba, Jadwiga
Powiązania:
https://bibliotekanauki.pl/articles/764136.pdf
Data publikacji:
2017
Wydawca:
Uniwersytet Marii Curie-Skłodowskiej. Wydawnictwo Uniwersytetu Marii Curie-Skłodowskiej
Tematy:
Nanosilica, Silanol groups, Hydrophobization, Hexamethyldisilazane, Poly(vinyl pyrrolidone) adsorption
Opis:
In this work, a role of the number of free silanol groups at a nanosilica surface (specific surface area SBET = 250 m2/g, initial amount of silanols αОН = 0.60-0.62 mmol/g) was analyzed in interaction with poly(vinyl pyrrolidone) (PVP) vs. the degree (QTMS) of silica hydrophobization by hexamethyldisilazane at 100 oC. The value of QTMS was 0.07, 0.42, 0.67, 0.81, 0.82, and 1.0. Adsorption of PVP onto a nanosilica surface was carried out from a water and water-ethanol (1:1) solutions of the polymer. It was shown that free silanol groups play a crucial role in the adsorption of poly(vinyl pyrrolidone). The value of the maximal adsorption (monolayer capacity) on completely hydrophobic nanosilica surface is approximately by 6.5 times lower than that for unmodified nanosilica
Źródło:
Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia; 2017, 72, 2
2083-358X
Pojawia się w:
Annales Universitatis Mariae Curie-Skłodowska, sectio AA – Chemia
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Design, preparation and properties of novel flame retardant thermosetting vinyl ester copolymers based on castor oil and industrial dipentene
Autorzy:
Mao, W.
Li, S.
Li, M.
Huang, K.
Xia, J.
Powiązania:
https://bibliotekanauki.pl/articles/777956.pdf
Data publikacji:
2017
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
castor oil
vinyl ester resin
copolymers
flammability
thermal properties
Opis:
A novel bio-based flame-retardant thermosetting vinyl ester resin monomer was synthesized from castor oil. The chemical structures of the monomer was characterized by FTIR and 1H-NMR. In order to improve its rigidity and expand its application in the field of bio-based materials, it was mixed with certain proportions of another reactive bio-based VER monomer, which had rigid and strong polar groups, and then a series of copolymers were prepared with thermal curing method. Then their tensile property, hardness, morphology of fractured surface, flame retardant property, DMA and thermostability were all investigated. The results indicated that the copolymers had relatively high tensile strength of 11.2 MPa, and the limiting oxygen index is above 23% in all prepared copolymers. DMA demonstrates that the glass transition temperature of the cured resins is up to 56.1°C. Thermogravimetric analysis shows that the copolymers have excellent thermal stability.
Źródło:
Polish Journal of Chemical Technology; 2017, 19, 3; 1-8
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Studies on Viscoelastic, Thermal and Morphological Properties of Vinyl Ester - Mixed Diluents System
Autorzy:
Ranjan, J. K.
Raghu Raja Pandiyan, K.
Goswami, S.
Powiązania:
https://bibliotekanauki.pl/articles/354420.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
vinyl ester resin
dynamic mechanical analysis
TGA
DSC
morphology
Opis:
Vinyl ester resin networks formed by using mixture of diluents were prepared. Methyl methacrylate (MMA) diluent was mixed in various proportions with vinyl ester resin which was already premixed with styrene diluent (45 wt. %). Weight ratios e.g. 80:20, 70:30 and 60:40 of VE resin: MMA diluents were studied. Viscoelastic properties of the cross-linked resin were studied by dynamic mechanical analyzer in terms of storage modulus and tanδ. Thermal analysis was performed using non-isothermal mode of Differential scanning calorimetry. The samples with mixed diluents, showed higher modulus, and glass transition temperature in comparison to that of the pure vinyl ester-styrene resin cross-linked in presence of styrene only. The difference in thermal stability between vinyl ester-styrene and vinyl ester-MMA-styrene was checked. Vinyl Ester – 20 wt. % MMA-Styrene samples have the best thermal property among all other prepared samples. Multiphase morphology was formed for the thermoset crosslinked with mixed diluents in contrast to that formed with single diluent. With increase in MMA content in the resin dispersed domain size increased.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 3; 1845-1850
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Physico-chemical properties of chitosan composites with synthetic polymers and inorganic additives
Autorzy:
Lewandowska, Katarzyna
Powiązania:
https://bibliotekanauki.pl/articles/1034867.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
Tematy:
AFM
chitosan
poly(vinyl alcohol)
polyvinylpyrrolidone composites
rheological properties
Opis:
In the present study the results of rheological measurements and atomic force microscopy (AFM) of polymer composites with montmorillonite (MMT) are presented. Chitosan is blended with synthetic polymers and inorganic additives in acetic acid solution and this solution is cast to prepare the mixture film. Flow measurements were made on a Bohlin Visco 88 rotary viscometer in the temperature range 25ºC-40ºC. The apparent shear viscosity and rheological parameters of the unmodified components and their composites were determined and discussed. Polymer films were examined using a Scanning Probe Microscopy SPM production Veeco. The obtained results suggest that the modification of several properties of polymer composites is a consequence of the interaction between the polymeric components and inorganic additives.
Źródło:
Progress on Chemistry and Application of Chitin and its Derivatives; 2015, 20; 162-169
1896-5644
Pojawia się w:
Progress on Chemistry and Application of Chitin and its Derivatives
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface properties of chitosan composites with poly(vinyl alcohol) and hydroxyapatite
Autorzy:
Lewandowska, Katarzyna
Powiązania:
https://bibliotekanauki.pl/articles/1035048.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
Tematy:
AFM
chitosan
composites
hydroxyapatite
poly(vinyl alcohol)
surface properties
Opis:
Surface properties of composites containing chitosan (Ch), poly(vinyl alcohol) (PVA) with hydroxyapatite (HAP) were investigated by contact angle measurements and atomic force microscopy (AFM). Thin films of Ch/HAP and Ch/PVA/HAP composites have been formed by casting methods from acetic acid solutions. Measurements of the contact angle for diiodomethane (D), and glycerol (G) on the surface of chitosan films, Ch/HAP and chitosan/PVA/HAP films were made and surface free energy was calculated. It was found that chitosan/HAP or Ch/PVA/HAP blend surface is enriched in high surface energy component i.e. chitosan. The study of composites by AFM showed a completely different morphology when compared with unmodified components. The roughness of composites increase after the addition of hydroxyapatite. This may indicates a strong interaction between the polymeric components and inorganic additive.
Źródło:
Progress on Chemistry and Application of Chitin and its Derivatives; 2015, 20; 177-182
1896-5644
Pojawia się w:
Progress on Chemistry and Application of Chitin and its Derivatives
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Viscometric studies of microcrystalline chitosan/poly(vinyl alcohol) mixtures
Autorzy:
Lewandowska, Katarzyna
Powiązania:
https://bibliotekanauki.pl/articles/1035416.pdf
Data publikacji:
2011
Wydawca:
Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
Tematy:
microcrystalline chitosan
poly(vinyl alcohol)
polymer blends
viscometric study
Opis:
In the present paper, the results of viscosity measurements in dilute solutions of microcrystalline chitosan (MCCh) with poly(vinyl alcohol) (PVA) of different degrees of hydrolysis are presented. Microcrystalline chitosan is blended with poly(vinyl alcohol) in aqueous 0.1 MCH3COOH/0.2 M NaCl. Viscosity measurements of dilute polymer solution were carried out in an Ubbelohde capillary viscometer. The final result depends on (I) the thermodynamic goodness of the solvent, on (II) the applied extrapolation method used for determination of the interaction parameters, on (III) the assumed miscibility criteria, on (IV) the degree of hydrolysis of PVA, and on (V) the blend composition.
Źródło:
Progress on Chemistry and Application of Chitin and its Derivatives; 2011, 16; 43-48
1896-5644
Pojawia się w:
Progress on Chemistry and Application of Chitin and its Derivatives
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Poli(alkohol winylowy) - biodegradowalne tworzywo winylowe
Poly(vinyl alcohol) - biodegradable vinyl material
Autorzy:
Pająk, J.
Ziemski, M.
Nowak, B.
Powiązania:
https://bibliotekanauki.pl/articles/1287265.pdf
Data publikacji:
2010
Wydawca:
Stowarzyszenie Inżynierów i Techników Przemysłu Chemicznego. Zakład Wydawniczy CHEMPRESS-SITPChem
Tematy:
poli(alkohol winylowy)
zastosowanie
biodegradacja
poli(vinyl alcohol)
application
biodegradation
Opis:
W artykule scharakteryzowano biodegradowalny polimer poli(alkohol winylowy) (PVA). Przedstawiono zastosowanie PVA w różnych dziedzinach przemysłu, farmacji i medycyny. Zaprezentowano mechanizmy biodegradacji poli(alkoholu winylowego) i efektywność tego procesu w różnych warunkach środowiska.
In this article biodegradable polymer poly (vinyl alcohol) (PVA) was characterized as well as its application in the various fields of industry, pharmacy and medicine. The mechanisms of the biodegradation of poly (vinyl alcohol) and the effectiveness of this process in different environmental conditions were presented.
Źródło:
Chemik; 2010, 64, 7-8; 523-530
0009-2886
Pojawia się w:
Chemik
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Correlation of chromosome damage and promoter methylation status of the DNA repair genes MGMT and hMLH1 in Chinese vinyl chloride monomer (VCM)-exposed workers
Autorzy:
Wu, Fen
Liu, Jing
Qiu, Yu-Lan
Wang, Wei
Zhu, Shou-Min
Sun, Pin
Miao, Wen-Bin
Li, Yong-Liang
Brandt-Rauf, Paul W.
Xia, Zhao-Lin
Powiązania:
https://bibliotekanauki.pl/articles/2179802.pdf
Data publikacji:
2013-03-01
Wydawca:
Instytut Medycyny Pracy im. prof. dra Jerzego Nofera w Łodzi
Tematy:
vinyl chloride monomer
chromosome damage
MGMT
hMLH1
DNA methylation
Opis:
Objective: To explore the association of the methylation status of MGMT and hMLH1 with chromosome damage induced by vinyl chloride monomer (VCM). Materials and Methods: Methylation of MGMT and hMLH1 was measured in 101 VCM-exposed workers by methylation-specifi c PCR. Chromosome damage in peripheral blood lymphocytes was measured by the cytokinesis-block micronucleus assay. The subjects were divided into chromosome damaged and non-damaged groups based on the normal reference value of micronuclei frequencies determined for two control groups. Results: MGMT promoter methylation was detectable in 5 out of 49 chromosome damaged subjects, but not in the chromosome non-damaged subjects; there was a signifi cant difference in MGMT methylation between the two groups (p < 0.05). Conclusions: We detected aberrant promoter methylation of MGMT in a small number of chromosome damaged VCM-exposed workers, but not in the chromosome non-damaged subjects. This preliminary observation warrants further investigation in a larger study.
Źródło:
International Journal of Occupational Medicine and Environmental Health; 2013, 26, 1; 173-182
1232-1087
1896-494X
Pojawia się w:
International Journal of Occupational Medicine and Environmental Health
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Nanofillers on the Mechanical Properties of Vinyl Ester Resin Used as a Carbon Fiber Reinforced Polymer Matrix
Autorzy:
Kubit, Andrzej
Bucior, Magdalena
Kluz, Rafał
Ochałek, Krzysztof
Burnat, Katarzyna
Powiązania:
https://bibliotekanauki.pl/articles/2201802.pdf
Data publikacji:
2022
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
composites
nanofillers
vinyl ester resin
nano-reinforced polymers
reinforced polymer
Opis:
This article presents the results of research aimed at determining the influence of selected nanofillers of vinyl ester resin on the mechanical properties of the cured resin. The influence of the resin with nanofillers as a matrix on the properties of the unidirectional CFRP composite was also investigated. Graphite, silicon oxide and titanium dioxide nanopowders were used as resin nanofillers. Each of the fillers was considered in two different contents, i.e. 1 wt.% and 2 wt.%. The variants with such nanofillers content were compared with the unfilled reference variant. The uniaxial tensile strength tests of the resin samples were carried out, showing the possibility of increasing the strength by 19.35% for the variant 1 wt.% of silica nanopowder content. For CFRP composites, the possibility of increasing the strength in the three-point bending test by 25.57% due to the use of a matrix reinforced with graphite nanopowder with a content of 1 wt.% was demonstrated. Based on the analysis of fracture surfaces performed using SEM microscopy, it was shown that the fillers used lead to a significant improvement in the adhesion of the matrix to the composite fibers.
Źródło:
Advances in Science and Technology. Research Journal; 2022, 16, 4; 10--21
2299-8624
Pojawia się w:
Advances in Science and Technology. Research Journal
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermal and atomic force microscopy (afm) studies of microcrystalline chitosan/poly(vinyl alcohol) mixtures
Autorzy:
Lewandowska, Katarzyna
Powiązania:
https://bibliotekanauki.pl/articles/1035498.pdf
Data publikacji:
2010
Wydawca:
Sieć Badawcza Łukasiewicz - Polskie Towarzystwo Chitynowe
Tematy:
AFM
microcrystalline chitosan
poly(vinyl alcohol)
polymer blends
thermal analysis
Opis:
In the present paper, the results of thermal analysis (DSC and TGA) and atomic force microscopy studies of microcrystalline chitosan (MCCh) with poly(vinyl alcohol) (PVA) are presented. Microcrystalline chitosan is blended with poly(vinyl alcohol) in acetic acid solution and this solution is cast to prepare the blend film. From thermal curves the thermal transitions: Tg, Tm and characteristic temperatures of decomposition: Tdi, Tmax have been determined and compared. The influence of the degree of PVA hydrolysis on the thermal properties of blend systems has been discussed. The surface properties of the MCCh and PVA films and their blends have been studied by tapping-mode atomic force microscopy (AFM). The changes of topography images were considered by determining the root mean square (RMS) deviation in the image data. The obtained results suggested that in solid MCCh/PVA mixtures the components are poorly miscible.
Źródło:
Progress on Chemistry and Application of Chitin and its Derivatives; 2010, 15; 11-16
1896-5644
Pojawia się w:
Progress on Chemistry and Application of Chitin and its Derivatives
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 81

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