- Tytuł:
- Sonochemical-assisted magnesium borate synthesis from different boron sources
- Autorzy:
-
Yildirim, M.
Kipcak, A. S.
Derun, E. M. - Powiązania:
- https://bibliotekanauki.pl/articles/949386.pdf
- Data publikacji:
- 2017
- Wydawca:
- Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
- Tematy:
-
magnesium borate
sonochemistry
spectroscopic analysis
ultrasonification
XRD - Opis:
- In this study, sonochemical-assisted magnesium borate synthesis is studied from different boron sources. Various reaction parameters are successfully applied by a simple and green method. X-ray diffraction (XRD), Fourier transform infrared (FT-IR) and Raman spectroscopies are used to characterize the synthesized magnesium borates on the other hand surface morphologies are investigated by using scanning electron microscope (SEM). The XRD analyses showed that the products were admontite [MgO(B2O3)3 . 7(H2O)] with JCPDS (Joint Committee on Powder Diffraction Standards) no. of 01-076-0540 and mcallisterite [Mg2(B6O7(OH)6)2 . 9(H2O)] with JCPDS no. of 01-070-1902. The results that found in the spectroscopic studies were in a good agreement with characteristic magnesium borate bands in both regions of infra-red and visible. According to SEM results, obtained borates were in micro and sub-micro scales. By the use of ultrasonication, reaction yields were found between 84.2 and 97.9%. As a result, it is concluded that the sonochemical approach is a practicable synthesis method to get high effi ciency and high crystallinity in the synthesis magnesium borate compounds.
- Źródło:
-
Polish Journal of Chemical Technology; 2017, 19, 1; 81-88
1509-8117
1899-4741 - Pojawia się w:
- Polish Journal of Chemical Technology
- Dostawca treści:
- Biblioteka Nauki
Artykuł